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CN219091098U - A purification device for developing silane coupling agent - Google Patents

A purification device for developing silane coupling agent Download PDF

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Publication number
CN219091098U
CN219091098U CN202223281273.7U CN202223281273U CN219091098U CN 219091098 U CN219091098 U CN 219091098U CN 202223281273 U CN202223281273 U CN 202223281273U CN 219091098 U CN219091098 U CN 219091098U
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purification
coupling agent
silane coupling
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丁桂清
朱夏明
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Shandong Lingxiao New Material Co ltd
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Abstract

本实用新型涉及提纯设备技术领域,且公开了一种用于研制硅烷偶联剂提纯装置,升温箱和提纯箱,所述提纯箱活动连接于升温箱顶部内壁,提纯箱顶部外壁设置有隔热块,隔热块顶部外壁设置有冷凝管,所述提纯箱两端均设置有排气机构,且提纯箱内设置有带动排气机构运转的驱动机构。本实用新型,通过设置的排气机构和驱动机构,能够有效地提高搅拌效率,搅拌更为均匀,同时提高溶液的溶解速率,并且带动活塞板在连接管道内来回移动,对提纯箱内部进行吸气,并将气体通过出气管进行排出,从而能够进一步加快提纯速率,提高其效率,节约时间。

Figure 202223281273

The utility model relates to the technical field of purification equipment, and discloses a purification device for developing a silane coupling agent, a heating box and a purification box. block, the outer wall of the top of the heat insulation block is provided with a condensation pipe, both ends of the purification box are provided with an exhaust mechanism, and the purification box is provided with a drive mechanism to drive the operation of the exhaust mechanism. The utility model, through the provided exhaust mechanism and driving mechanism, can effectively improve the stirring efficiency, make the stirring more uniform, increase the dissolution rate of the solution at the same time, and drive the piston plate to move back and forth in the connecting pipeline to absorb the inside of the purification box. Gas, and the gas is discharged through the outlet pipe, which can further speed up the purification rate, improve its efficiency and save time.

Figure 202223281273

Description

一种用于研制硅烷偶联剂提纯装置A purification device for developing silane coupling agent

技术领域technical field

本实用新型涉及提纯设备技术领域,尤其涉及一种用于研制硅烷偶联剂提纯装置。The utility model relates to the technical field of purification equipment, in particular to a purification device for developing a silane coupling agent.

背景技术Background technique

硅烷偶联剂常用于处理二氧化硅、炭黑等无机填料,在橡胶、硅橡胶等聚合物中起活性剂、偶联剂、交联剂、补强剂的作用,作为金属表面防锈剂具有特殊功能,用硅烷偶联剂处理金属表面,有效改善其表面的耐腐性、抗氧化性以及增加其与树脂等高分子材料的粘接性,其在进行使用前需要对其进行提纯。Silane coupling agent is often used to treat inorganic fillers such as silica and carbon black, and acts as an active agent, coupling agent, crosslinking agent, and reinforcing agent in polymers such as rubber and silicone rubber, and is used as a metal surface rust inhibitor With special functions, the metal surface is treated with a silane coupling agent, which can effectively improve the corrosion resistance and oxidation resistance of the surface and increase its adhesion with polymer materials such as resins. It needs to be purified before use.

现有的提纯设备在进行使用时,仅仅依靠热量来对溶液进行蒸发,此方式在进行提纯时速率较慢,需要消耗大量时间来对其进行提纯,十分浪费时间When the existing purification equipment is in use, it only relies on heat to evaporate the solution. This method is slow in purification, and it takes a lot of time to purify it, which is a waste of time.

为此,我们提出一种用于研制硅烷偶联剂提纯装置。To this end, we propose a purification device for the development of silane coupling agent.

实用新型内容Utility model content

本实用新型主要是解决上述现有技术所存在的技术问题,提供一种用于研制硅烷偶联剂提纯装置。The utility model mainly solves the technical problems existing in the above-mentioned prior art, and provides a purification device for developing a silane coupling agent.

为了实现上述目的,本实用新型采用了如下技术方案,一种用于研制硅烷偶联剂提纯装置,包括升温箱和提纯箱,所述提纯箱活动连接于升温箱顶部内壁,提纯箱顶部外壁设置有隔热块,隔热块顶部外壁设置有冷凝管,所述提纯箱两端均设置有排气机构,且提纯箱内设置有带动排气机构运转的驱动机构。In order to achieve the above object, the utility model adopts the following technical scheme, a purification device for developing a silane coupling agent, including a heating box and a purification box, the purification box is flexibly connected to the inner wall of the top of the heating box, and the outer wall of the top of the purification box is set There is a heat-insulating block, and the outer wall of the top of the heat-insulating block is provided with a condensing pipe, and both ends of the purification box are provided with an exhaust mechanism, and a driving mechanism for driving the exhaust mechanism is arranged in the purification box.

进一步,所述排气机构内设置有连接管道和出气管,提纯箱两侧外壁均开设有第一固定孔,连接管道设置于第一固定孔内壁,连接管道底部外壁开设有第二固定孔,出气管设置于第二固定孔内壁。Further, the exhaust mechanism is provided with a connecting pipe and an air outlet pipe, the outer walls of both sides of the purification box are provided with first fixing holes, the connecting pipe is arranged on the inner wall of the first fixing hole, and the outer wall of the bottom of the connecting pipe is provided with a second fixing hole, The air outlet pipe is arranged on the inner wall of the second fixing hole.

进一步,所述驱动机构内设置有转动轴。Further, a rotating shaft is arranged in the driving mechanism.

进一步,所述转动轴通过电机设置于提纯箱底部外壁,转动轴外壁设置有搅拌块。Further, the rotating shaft is arranged on the outer wall of the bottom of the purification box through a motor, and a stirring block is arranged on the outer wall of the rotating shaft.

进一步,所述搅拌块一侧外壁开设有多个呈圆周排列的分流孔,且多个分流孔均延伸至搅拌块底部外壁,分流孔横截面为弧形。Further, the outer wall of one side of the stirring block is provided with a plurality of distribution holes arranged in a circle, and the plurality of distribution holes extend to the outer wall of the bottom of the stirring block, and the cross section of the distribution holes is arc-shaped.

进一步,所述转动轴顶部外壁设置有锥形齿轮一,且连接管道一侧外壁转动连接有丝杆,丝杆一侧外壁设置有锥形齿轮二,锥形齿轮二啮合于锥形齿轮一外壁。Further, the top outer wall of the rotating shaft is provided with a bevel gear 1, and the outer wall of one side of the connecting pipe is rotatably connected with a screw rod, and the outer wall of one side of the screw rod is provided with a bevel gear 2, and the bevel gear 2 meshes with the bevel gear 1 outer wall .

进一步,所述连接管道内壁的两端均开设有滑动槽,滑动槽内壁滑动连接有连接滑块,两个连接滑块相对一侧外壁设置有活塞板,活塞板一侧外壁开设有螺纹孔,丝杆螺纹连接于螺纹孔内壁。Further, both ends of the inner wall of the connecting pipe are provided with sliding grooves, the inner wall of the sliding groove is slidably connected with connecting sliders, the outer walls of the opposite sides of the two connecting sliders are provided with piston plates, and the outer walls of one side of the piston plates are provided with threaded holes. The screw rod is threadedly connected to the inner wall of the threaded hole.

进一步,所述活塞板一侧外壁设置有复位弹簧,复位弹簧设置于连接管道一侧外壁。Further, a return spring is provided on one side of the outer wall of the piston plate, and the return spring is provided on the outer wall of the connecting pipe side.

进一步,所述冷凝管内壁设置有筛板,筛板顶部外壁开设有多个呈圆周排列的过滤孔Further, the inner wall of the condensation pipe is provided with a sieve plate, and the outer wall of the top of the sieve plate is provided with a plurality of filter holes arranged in a circle

有益效果Beneficial effect

本实用新型提供了一种用于研制硅烷偶联剂提纯装置。具备以下有益效果:The utility model provides a purification device for developing a silane coupling agent. Has the following beneficial effects:

(1)、该一种用于研制硅烷偶联剂提纯装置,通过设置的排气机构和驱动机构,当开始进行提纯时,此时开启升温箱,升温箱启动对提纯箱进行加热,并将电机开启带动转动轴进行转动,转动轴转动带动搅拌块进行转动,即可带动搅拌块对内部的溶液进行搅拌,并且此时搅拌块上的分流孔能够在搅拌时将上部的液体带入下部,从而能够有效地提高搅拌效率,搅拌更为均匀,同时提高溶液的溶解速率,并且转动轴转动通过锥形齿轮一带动锥形齿轮二进行转动,即可带动丝杆进行转动,丝杆转动带动螺纹连接其上的活塞板进行移动,由于活塞板上的滑动槽滑动连接于连接滑块内部,从而活塞板的移动进行限位,只能进行水平移动,并且活塞板移动时对复位弹簧进行压缩,当复位弹簧上弹力大于活塞板移动时驱动的应力时,此时在复位弹簧弹力的作用下带动活塞板向反方向进行移动,即可带动活塞板在连接管道内来回移动,对提纯箱内部进行吸气,并将气体通过出气管进行排出,从而能够进一步加快提纯速率,提高其效率,节约时间。(1), this one is used to develop the silane coupling agent purification device, through the exhaust mechanism and the drive mechanism provided, when starting to purify, open the heating box at this time, the heating box starts to heat the purification box, and the The motor is turned on to drive the rotating shaft to rotate, and the rotation of the rotating shaft drives the stirring block to rotate, which can drive the stirring block to stir the internal solution, and at this time, the split hole on the stirring block can bring the upper liquid into the lower part during stirring, Thereby, the stirring efficiency can be effectively improved, the stirring is more uniform, and the dissolution rate of the solution is improved at the same time, and the rotating shaft rotates through the bevel gear 1 to drive the bevel gear 2 to rotate, which can drive the screw to rotate, and the screw to drive the thread The piston plate connected to it moves. Since the sliding groove on the piston plate is slidably connected to the inside of the connecting slider, the movement of the piston plate is limited and can only move horizontally, and the return spring is compressed when the piston plate moves. When the elastic force on the return spring is greater than the driving stress when the piston plate moves, at this time, under the action of the elastic force of the return spring, the piston plate is driven to move in the opposite direction, which can drive the piston plate to move back and forth in the connecting pipe, and clean the interior of the purification box. Inhale and discharge the gas through the outlet pipe, which can further speed up the purification rate, improve its efficiency and save time.

(2)、该一种用于研制硅烷偶联剂提纯装置,通过设置的筛板,当进行提纯时,此时提纯箱内会产生大量气体,气体随提纯箱进入冷凝管内部,此时气体接触到冷凝管内壁,由于冷凝管管壁温度较低,从而内部的液体和固体回归原样,由于重力的作用,通过筛板回到提纯箱内部,并且此时内部较大的固定杂质会被筛板过滤,从而能够提高提纯的纯度。(2) This one is used to develop a silane coupling agent purification device. Through the sieve plate provided, when the purification is performed, a large amount of gas will be generated in the purification box at this time, and the gas enters the inside of the condensation tube with the purification box. At this time, the gas When it comes into contact with the inner wall of the condensation tube, due to the low temperature of the tube wall of the condensation tube, the liquid and solid inside return to the original state. Due to the action of gravity, they return to the inside of the purification box through the sieve plate, and at this time, the larger fixed impurities inside will be sieved Plate filtration, which can improve the purity of purification.

附图说明Description of drawings

图1为本实用新型主视图;Fig. 1 is a front view of the utility model;

图2为本实用新型剖视图;Fig. 2 is a sectional view of the utility model;

图3为本实用新型图2的A部分放大图;Fig. 3 is the enlarged view of part A of Fig. 2 of the utility model;

图4为本实用新型图2的B部分放大图。Fig. 4 is an enlarged view of part B of Fig. 2 of the present invention.

图例说明:1、升温箱;2、提纯箱;3、隔热块;4、冷凝管;5、连接管道;6、出气管;7、转动轴;8、搅拌块;9、分流孔;10、活塞板;11、丝杆;12、复位弹簧;13、筛板;14、锥形齿轮一;15、锥形齿轮二;16、滑动槽;17、连接滑块。Legend: 1. Heating box; 2. Purification box; 3. Insulation block; 4. Condenser pipe; 5. Connecting pipe; 6. Outlet pipe; 7. Rotation shaft; 8. Stirring block; 11, screw rod; 12, return spring; 13, sieve plate; 14, bevel gear one; 15, bevel gear two; 16, sliding groove; 17, connecting slider.

具体实施方式Detailed ways

实施例一:一种用于研制硅烷偶联剂提纯装置,如图1-4所示,包括升温箱1和提纯箱2,提纯箱2活动连接于升温箱1顶部内壁,提纯箱2顶部外壁设置有隔热块3,隔热块3顶部外壁设置有冷凝管4,且提纯箱2两端均设置有排气机构,且提纯箱2内设置有带动排气机构运转的驱动机构。Embodiment 1: A purification device for developing a silane coupling agent, as shown in Figure 1-4, includes a heating box 1 and a purification box 2, the purification box 2 is flexibly connected to the top inner wall of the heating box 1, and the top outer wall of the purification box 2 A heat insulating block 3 is provided, and a condensation pipe 4 is provided on the outer wall of the top of the heat insulating block 3, and an exhaust mechanism is arranged at both ends of the purification box 2, and a driving mechanism for driving the exhaust mechanism is arranged inside the purification box 2.

排气机构内设置有连接管道5和出气管6,提纯箱2两侧外壁均开设有第一固定孔,连接管道5设置于第一固定孔内壁,连接管道5底部外壁开设有第二固定孔,出气管6设置于第二固定孔内壁。The exhaust mechanism is provided with a connecting pipe 5 and an air outlet pipe 6, the outer walls of both sides of the purification box 2 are provided with first fixing holes, the connecting pipe 5 is arranged on the inner wall of the first fixing hole, and the outer wall of the bottom of the connecting pipe 5 is provided with a second fixing hole , the air outlet pipe 6 is arranged on the inner wall of the second fixing hole.

驱动机构内设置有转动轴7。A rotating shaft 7 is arranged in the driving mechanism.

转动轴7通过电机设置于提纯箱2底部外壁,转动轴7外壁设置有搅拌块8。The rotating shaft 7 is arranged on the outer wall of the bottom of the purification box 2 through a motor, and the outer wall of the rotating shaft 7 is provided with a stirring block 8 .

搅拌块8一侧外壁开设有多个呈圆周排列的分流孔9,且多个分流孔9均延伸至搅拌块8底部外壁,分流孔9横截面为弧形。The outer wall of one side of the stirring block 8 is provided with a plurality of distribution holes 9 arranged in a circle, and the plurality of distribution holes 9 all extend to the outer wall of the bottom of the stirring block 8, and the cross section of the distribution holes 9 is arc-shaped.

转动轴7顶部外壁设置有锥形齿轮一14,且连接管道5一侧外壁转动连接有丝杆11,丝杆11一侧外壁设置有锥形齿轮二15,锥形齿轮二15啮合于锥形齿轮一14外壁。The top outer wall of the rotating shaft 7 is provided with a bevel gear 1 14, and the outer wall on one side of the connecting pipe 5 is rotatably connected with a screw mandrel 11, and the outer wall on one side of the screw mandrel 11 is provided with a bevel gear 2 15, and the bevel gear 2 15 meshes with the conical gear. Gear one 14 outer walls.

连接管道5内壁的两端均开设有滑动槽16,滑动槽16内壁滑动连接有连接滑块17,两个连接滑块17相对一侧外壁设置有活塞板10,活塞板10一侧外壁开设有螺纹孔,丝杆11螺纹连接于螺纹孔内壁。Both ends of the inner wall of the connecting pipe 5 are provided with sliding grooves 16, the inner walls of the sliding groove 16 are slidably connected with connecting sliders 17, and the outer walls on the opposite side of the two connecting sliders 17 are provided with piston plates 10, and the outer walls on one side of the piston plate 10 are provided with In the threaded hole, the screw rod 11 is threadedly connected to the inner wall of the threaded hole.

活塞板10一侧外壁设置有复位弹簧12,复位弹簧12设置于连接管道5一侧外壁。A return spring 12 is arranged on one side of the outer wall of the piston plate 10 , and the return spring 12 is arranged on one side of the outer wall of the connecting pipe 5 .

通过设置的排气机构和驱动机构,当开始进行提纯时,此时开启升温箱1,升温箱1启动对提纯箱2进行加热,并将电机开启带动转动轴7进行转动,转动轴7转动带动搅拌块8进行转动,即可带动搅拌块8对内部的溶液进行搅拌,并且此时搅拌块8上的分流孔9能够在搅拌时将上部的液体带入下部,从而能够有效地提高搅拌效率,搅拌更为均匀,同时提高溶液的溶解速率,并且转动轴7转动通过锥形齿轮一14带动锥形齿轮二15进行转动,即可带动丝杆11进行转动,丝杆11转动带动螺纹连接其上的活塞板10进行移动,由于活塞板10上的滑动槽16滑动连接于连接滑块17内部,从而活塞板10的移动进行限位,只能进行水平移动,并且活塞板10移动时对复位弹簧12进行压缩,当复位弹簧12上弹力大于活塞板10移动时驱动的应力时,此时在复位弹簧12弹力的作用下带动活塞板10向反方向进行移动,即可带动活塞板10在连接管道5内来回移动,对提纯箱2内部进行吸气,并将气体通过出气管6进行排出,从而能够进一步加快提纯速率,提高其效率,节约时间。Through the exhaust mechanism and the driving mechanism provided, when the purification is started, the heating box 1 is opened at this time, the heating box 1 starts to heat the purification box 2, and the motor is turned on to drive the rotating shaft 7 to rotate, and the rotating shaft 7 rotates to drive The stirring block 8 rotates to drive the stirring block 8 to stir the internal solution, and at this time, the split hole 9 on the stirring block 8 can bring the upper liquid into the lower part during stirring, thereby effectively improving the stirring efficiency. Stir more evenly, increase the dissolution rate of the solution at the same time, and the rotating shaft 7 rotates through the bevel gear 14 to drive the bevel gear 2 15 to rotate, which can drive the screw rod 11 to rotate, and the rotation of the screw rod 11 drives the threaded connection The piston plate 10 moves, because the sliding groove 16 on the piston plate 10 is slidably connected to the inside of the connecting slider 17, so that the movement of the piston plate 10 is limited and can only move horizontally, and when the piston plate 10 moves, the return spring 12 is compressed, when the elastic force on the return spring 12 is greater than the driving stress when the piston plate 10 moves, at this time, under the action of the elastic force of the return spring 12, the piston plate 10 is driven to move in the opposite direction, and the piston plate 10 can be driven in the connecting pipeline. 5 to move back and forth, to inhale the inside of the purification box 2, and discharge the gas through the outlet pipe 6, so that the purification rate can be further accelerated, the efficiency can be improved, and time can be saved.

实施例二:在实施例一的基础上,参考图4,冷凝管4内壁设置有筛板13,筛板13顶部外壁开设有多个呈圆周排列的过滤孔。Embodiment 2: On the basis of Embodiment 1, referring to FIG. 4 , the inner wall of the condensation pipe 4 is provided with a sieve plate 13 , and the top outer wall of the sieve plate 13 is provided with a plurality of circumferentially arranged filter holes.

通过设置的筛板13,当进行提纯时,此时提纯箱2内会产生大量气体,气体随提纯箱2进入冷凝管4内部,此时气体接触到冷凝管4内壁,由于冷凝管4管壁温度较低,从而内部的液体和固体回归原样,由于重力的作用,通过筛板13回到提纯箱2内部,并且此时内部较大的固定杂质会被筛板13过滤,从而能够提高提纯的纯度。Through the sieve plate 13 provided, when purifying, a large amount of gas will be produced in the purification box 2 at this time, and the gas enters the inside of the condensation tube 4 with the purification box 2. At this time, the gas touches the inner wall of the condensation tube 4. The temperature is low, so that the internal liquid and solid return to their original state, and due to the effect of gravity, they return to the inside of the purification box 2 through the sieve plate 13, and at this time, the larger fixed impurities inside will be filtered by the sieve plate 13, thereby improving the efficiency of purification. purity.

以上显示和描述了本实用新型的基本原理和主要特征和本实用新型的优点。本行业的技术人员应该了解,本实用新型不受上述实施例的限制,上述实施例和说明书中描述的只是说明本实用新型的原理,在不脱离本实用新型精神和范围的前提下,本实用新型还会有各种变化和改进,这些变化和改进都落入要求保护的本实用新型范围内。本实用新型要求保护范围由所附的权利要求书及其等效物界定。The basic principles and main features of the present utility model and the advantages of the present utility model have been shown and described above. Those skilled in the industry should understand that the utility model is not limited by the above-mentioned embodiments. The above-mentioned embodiments and descriptions only illustrate the principles of the utility model. Without departing from the spirit and scope of the utility model, the utility model The new model also has various changes and improvements, and these changes and improvements all fall within the scope of the claimed utility model. The scope of protection required by the utility model is defined by the appended claims and their equivalents.

Claims (9)

1. The utility model provides a be used for developing silane coupling agent purification device, includes intensification case (1) and purification case (2), its characterized in that: purification case (2) swing joint is in intensification case (1) top inner wall, and purification case (2) top outer wall is provided with thermal-insulated piece (3), and thermal-insulated piece (3) top outer wall is provided with condenser pipe (4), purification case (2) both ends all are provided with exhaust mechanism, and are provided with the actuating mechanism that drives exhaust mechanism moving in purification case (2).
2. The purification apparatus for developing a silane coupling agent according to claim 1, wherein: be provided with connecting tube (5) and outlet duct (6) in the exhaust mechanism, first fixed orifices have all been seted up to purifying case (2) both sides outer wall, and connecting tube (5) set up in first fixed orifices inner wall, and second fixed orifices have been seted up to connecting tube (5) bottom outer wall, and outlet duct (6) set up in second fixed orifices inner wall.
3. The purification apparatus for developing a silane coupling agent according to claim 2, wherein: a rotating shaft (7) is arranged in the driving mechanism.
4. The purification apparatus for developing a silane coupling agent according to claim 3, wherein: the rotating shaft (7) is arranged on the outer wall of the bottom of the purifying box (2) through a motor, and the stirring block (8) is arranged on the outer wall of the rotating shaft (7).
5. The purification apparatus for developing a silane coupling agent according to claim 4, wherein: a plurality of circumferentially arranged diversion holes (9) are formed in the outer wall of one side of the stirring block (8), the diversion holes (9) extend to the outer wall of the bottom of the stirring block (8), and the cross sections of the diversion holes (9) are arc-shaped.
6. The purification apparatus for developing a silane coupling agent according to claim 5, wherein: the outer wall at the top of the rotating shaft (7) is provided with a first conical gear (14), the outer wall at one side of the connecting pipeline (5) is rotationally connected with a screw rod (11), the outer wall at one side of the screw rod (11) is provided with a second conical gear (15), and the second conical gear (15) is meshed with the outer wall of the first conical gear (14).
7. The purification apparatus for developing a silane coupling agent according to claim 6, wherein: the two ends of the inner wall of the connecting pipeline (5) are provided with sliding grooves (16), the inner wall of each sliding groove (16) is connected with a connecting sliding block (17) in a sliding mode, the outer wall of one side opposite to the two connecting sliding blocks (17) is provided with a piston plate (10), the outer wall of one side of the piston plate (10) is provided with a threaded hole, and a screw rod (11) is connected to the inner wall of the threaded hole in a threaded mode.
8. The purification apparatus for developing a silane coupling agent according to claim 7, wherein: the piston plate (10) is provided with a return spring (12) on one side outer wall, and the return spring (12) is arranged on one side outer wall of the connecting pipeline (5).
9. The purification apparatus for developing a silane coupling agent according to claim 1, wherein: the inner wall of the condensing tube (4) is provided with a sieve plate (13), and the outer wall of the top of the sieve plate (13) is provided with a plurality of circumferentially arranged filtering holes.
CN202223281273.7U 2022-12-05 2022-12-05 A purification device for developing silane coupling agent Expired - Fee Related CN219091098U (en)

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