CN214439056U - Temperature-controllable heating reaction device for production of methyl isobutyrylacetate - Google Patents
Temperature-controllable heating reaction device for production of methyl isobutyrylacetate Download PDFInfo
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- CN214439056U CN214439056U CN202120366092.0U CN202120366092U CN214439056U CN 214439056 U CN214439056 U CN 214439056U CN 202120366092 U CN202120366092 U CN 202120366092U CN 214439056 U CN214439056 U CN 214439056U
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Abstract
The utility model discloses a temperature-controllable isobutyryl methyl acetate production heating reaction device, which belongs to the technical field of chemical production devices and comprises a shell, wherein the inner side of the shell is provided with an inner wall, a heating device is arranged between the shell and the inner wall, one side of the shell is provided with a lateral wall, a lead pipe is connected between the shell and the lateral wall, a valve is arranged on the lead pipe, a rotating rod is arranged inside the inner wall, a motor is arranged above the rotating rod, the inside of the rotating rod is of a hollow structure, a heating wire is arranged inside the rotating rod, a first temperature sensor is arranged on the inner wall, a stirring shaft is arranged inside the lateral wall, a cooling coil is wound on the stirring shaft, a second temperature sensor is arranged on the lateral wall, isobutyryl methyl acetate heating reaction purification can be realized, the effect of temperature rise can be quickly achieved by a double heating device, and the temperature detection and control device can effectively collect and monitor temperature, effectively promotes the working efficiency and solves the problems in the prior art.
Description
Technical Field
The utility model relates to a controllable isobutyryl methyl acetate production heating reaction unit of temperature belongs to chemical production technical field.
Background
Methyl isobutyrylacetate is also called methyl isobutyrylacetate, is liquid at normal temperature, is one kind of organic chemical raw material, methyl isobutyrylacetate is in the in-process of production, need purify methyl isobutyrylacetate, the purification is mainly purified through heating, the heating reaction device structure among the prior art is more complicated, short service life, occupation space is big, the efficiency of simultaneous heating is lower, lack effectual temperature monitoring device, can't realize the control of temperature, need consume a large amount of energy, greatly increased the cost of equipment operation.
SUMMERY OF THE UTILITY MODEL
The not enough to prior art, the utility model aims to provide a controllable isobutyryl methyl acetate production heating reaction unit of temperature has solved the problem that appears among the prior art.
A controllable methyl isobutyrylacetate production heating reaction device of temperature, which comprises an outer shell, the inboard of shell is equipped with the inner wall, be equipped with heating device between shell and the inner wall, one side of shell is equipped with the lateral wall, the hookup has the pipe that leads between shell and the lateral wall, be equipped with the valve on the pipe that leads, the inside of inner wall is equipped with the bull stick, the top of bull stick is equipped with the motor, the inside of bull stick is the hollow structure, the inside of bull stick is equipped with the heater strip, be equipped with first temperature sensor on the inner wall, the inside of lateral wall is equipped with the (mixing) shaft, the winding has cooling coil pipe on the (mixing) shaft, be equipped with second temperature sensor on the lateral wall, the inside of lateral wall still is equipped with the suction tube, be equipped with the suction pump on the suction tube, the outside of device is equipped with the controller, the controller is connected with the host computer of Zigbee, the Zigbee host computer is connected with the Zigbee from the computer, the first temperature sensor in every device is connected to the Zigbee, The controller is connected with a wireless transmission module outside, and the controller is in data communication with the monitoring center through the wireless transmission module.
The inner wall is also internally provided with an auxiliary rotating shaft, and the auxiliary rotating shaft is connected with the rotating rod through a connecting rod.
A material inlet is arranged above the shell.
The valve is an electromagnetic valve.
The controller adopts STM32 type singlechip.
Compared with the prior art, the utility model, following beneficial effect has:
a controllable isobutyryl methyl acetate production heating reaction device of temperature can realize isobutyryl methyl acetate heating reaction purification, possesses dual heating device and can reach the effect of intensification fast, possesses the collection and the monitoring that temperature detection and controlling means can effectually carry out the temperature simultaneously, has effectively promoted work efficiency, has solved the problem that exists among the prior art.
Drawings
Fig. 1 is a schematic structural diagram of an embodiment of the present invention;
FIG. 2 is an electrical connection diagram of an embodiment of the present invention;
in the figure: 1. a motor; 2. a rotating rod; 3. a connecting rod; 4. an auxiliary rotating shaft; 5. a housing; 6. heating wires; 7. a first temperature sensor; 8. an inner wall; 9. a heating device; 10. a valve; 11. a conduit pipe; 12. a second temperature sensor; 13. an outer sidewall; 14. a cooling coil; 15. a stirring shaft; 16. a suction pump; 17. a suction tube; 18. and (4) a material inlet.
Detailed Description
The invention will be further described with reference to the following drawings and examples:
example 1:
as shown in fig. 1-2, the temperature-controllable heating reaction device for producing methyl isobutyrylacetate of the present invention comprises a housing 5, an inner wall 8 is disposed inside the housing 5, a heating device 9 is disposed between the housing 5 and the inner wall 8, an outer wall 13 is disposed on one side of the housing 5, a conduit 11 is connected between the housing 5 and the outer wall 13, a valve 10 is disposed on the conduit 11, a rotating rod 2 is disposed inside the inner wall 8, a motor 1 is disposed above the rotating rod 2, the rotating rod 2 is hollow, a heating wire 6 is disposed inside the rotating rod 2, a first temperature sensor 7 is disposed on the inner wall 8, a stirring shaft 15 is disposed inside the outer wall 13, a cooling coil 14 is wound on the stirring shaft 15, a second temperature sensor 12 is disposed on the outer wall 13, a suction pipe 17 is further disposed inside the outer wall 13, a suction pump 16 is disposed on the suction pipe 17, and a controller is disposed outside the device, the controller is connected with a Zigbee host, the Zigbee host is connected with a Zigbee slave through a Zigbee communication network, the Zigbee slave is connected with a first temperature sensor 7, a second temperature sensor 12, a heating device 9 and a cooling coil 14 in each device, a wireless transmission module is further connected to the outside of the controller, and the controller realizes data communication with the monitoring center through the wireless transmission module.
An auxiliary rotating shaft 4 is further arranged inside the inner wall 8, and the auxiliary rotating shaft 4 is connected with the rotating rod 2 through a connecting rod 3.
A material inlet 18 is arranged above the shell 5.
The valve 10 is a solenoid valve.
The controller adopts STM32 type single chip microcomputer.
The working principle of the embodiment is as follows: during operation, materials in the rotating shaft 2 are stirred through the inner wall, the heating function can be effectively achieved through the heating wire 6 in the rotating shaft 2, meanwhile, the external heating device 9 conducts steam heating on the internal raw materials, the first temperature sensor 7 detects temperature values in real time, the temperature values enter the outer side wall 13 through the lead pipe after the temperature values are completed, rapid cooling is conducted through the cooling coil pipe 14, the second temperature sensor 12 detects the temperature values of the materials in the outer side wall in real time, temperature data are collected by the Zigbee slave machine, the Zigbee slave machine communicates with the Zigbee host machine through the Zigbee communication network, unified temperature collection and management of a plurality of devices in a region are achieved, the Zigbee host machine is connected with the controller, the controller is connected with the monitoring center, and the controller sends control commands to achieve opening and closing of the heating device 9 and the cooling coil pipe 14.
Adopt above to combine the drawing description the utility model discloses a controllable isobutyryl methyl acetate production heating reaction device of temperature of embodiment can realize isobutyryl methyl acetate heating reaction purification, possesses dual heating device and can reach the effect of intensification fast, possesses temperature detection and controlling means simultaneously and can effectually carry out the collection and the monitoring of temperature, has effectively promoted work efficiency, has solved the problem that exists among the prior art. The present invention is not limited to the embodiments described, but rather, variations, modifications, substitutions and alterations from the embodiments described herein are possible without departing from the spirit and scope of the invention.
Claims (5)
1. A temperature-controllable heating reaction device for producing methyl isobutyrylacetate is characterized in that: comprises a shell (5), an inner wall (8) is arranged on the inner side of the shell (5), a heating device (9) is arranged between the shell (5) and the inner wall (8), an outer side wall (13) is arranged on one side of the shell (5), a guide connecting pipe (11) is connected between the shell (5) and the outer side wall (13), a valve (10) is arranged on the guide connecting pipe (11), a rotating rod (2) is arranged in the inner wall (8), a motor (1) is arranged above the rotating rod (2), the rotating rod (2) is of a hollow structure, a heating wire (6) is arranged in the rotating rod (2), a first temperature sensor (7) is arranged on the inner wall (8), a stirring shaft (15) is arranged in the outer side wall (13), a cooling coil (14) is wound on the stirring shaft (15), a second temperature sensor (12) is arranged on the outer side wall (13), a suction pipe (17) is also arranged in the outer side wall (13), the suction pipe (17) is provided with a suction pump (16), the controller is arranged outside the device and connected with a Zigbee host, the Zigbee host is connected with a Zigbee slave through a Zigbee communication network, the Zigbee slave is connected with a first temperature sensor (7), a second temperature sensor (12), a heating device (9) and a cooling coil (14) in each device, the controller is also connected with a wireless transmission module outside, and the controller realizes data communication with the monitoring center through the wireless transmission module.
2. The temperature-controllable heating reaction device for producing methyl isobutyrylacetate according to claim 1, wherein: the inner wall (8) is also internally provided with an auxiliary rotating shaft (4), and the auxiliary rotating shaft (4) is connected with the rotating rod (2) through a connecting rod (3).
3. The temperature-controllable heating reaction device for producing methyl isobutyrylacetate according to claim 1, wherein: a material inlet (18) is arranged above the shell (5).
4. The temperature-controllable heating reaction device for producing methyl isobutyrylacetate according to claim 1, wherein: the valve (10) is an electromagnetic valve.
5. The temperature-controllable heating reaction device for producing methyl isobutyrylacetate according to claim 1, wherein: the controller adopts STM32 type singlechip.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120366092.0U CN214439056U (en) | 2021-02-10 | 2021-02-10 | Temperature-controllable heating reaction device for production of methyl isobutyrylacetate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120366092.0U CN214439056U (en) | 2021-02-10 | 2021-02-10 | Temperature-controllable heating reaction device for production of methyl isobutyrylacetate |
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| CN214439056U true CN214439056U (en) | 2021-10-22 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202120366092.0U Active CN214439056U (en) | 2021-02-10 | 2021-02-10 | Temperature-controllable heating reaction device for production of methyl isobutyrylacetate |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115253964A (en) * | 2022-07-18 | 2022-11-01 | 丽水学院 | A high-efficiency production device for polyurethane waterproof coating |
-
2021
- 2021-02-10 CN CN202120366092.0U patent/CN214439056U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115253964A (en) * | 2022-07-18 | 2022-11-01 | 丽水学院 | A high-efficiency production device for polyurethane waterproof coating |
| CN115253964B (en) * | 2022-07-18 | 2023-11-28 | 丽水学院 | High-efficient apparatus for producing of polyurethane waterproof coating |
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