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CN209530253U - A kind of crystallization solvent recyclable device of sodium ascorbyl phosphate - Google Patents

A kind of crystallization solvent recyclable device of sodium ascorbyl phosphate Download PDF

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Publication number
CN209530253U
CN209530253U CN201821939651.7U CN201821939651U CN209530253U CN 209530253 U CN209530253 U CN 209530253U CN 201821939651 U CN201821939651 U CN 201821939651U CN 209530253 U CN209530253 U CN 209530253U
Authority
CN
China
Prior art keywords
reaction kettle
receiving tank
capping
connecting tube
ascorbyl phosphate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201821939651.7U
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Chinese (zh)
Inventor
杨海
徐建国
吴从新
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HEBEI TIANYIN BIO-TECHNOLOGY CO LTD
Original Assignee
HEBEI TIANYIN BIO-TECHNOLOGY CO LTD
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HEBEI TIANYIN BIO-TECHNOLOGY CO LTD filed Critical HEBEI TIANYIN BIO-TECHNOLOGY CO LTD
Priority to CN201821939651.7U priority Critical patent/CN209530253U/en
Application granted granted Critical
Publication of CN209530253U publication Critical patent/CN209530253U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/141Feedstock

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  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The utility model discloses a kind of crystallization solvent recyclable devices of sodium ascorbyl phosphate, the heating interlayer is arranged inside reaction kettle, the fixed plate is arranged in reaction kettle inner wall, fixed plate is equipped with filter screen and activated charcoal strainer, the capping is arranged in reaction kettle upper end, it covers upper end and is equipped with bracket, the bracket is equipped with gas sampling tank, gas sampling tank lower end is connected with tracheae, the tracheae is pumped equipped with air draught, the capping upper end is equipped with inlet, pressure gauge and thermometer, the steam (vapor) outlet is arranged in reaction kettle left side, the drain pipe is arranged at the center of reaction kettle lower end, the drain pipe lower end is equipped with flange, the flange lower end is connected with connecting tube, the connecting tube right end is connected with receiving tank, the regulating switch is arranged in connecting tube, the receiving tank lower end is equipped with stabilizer blade, institute It states leakage fluid dram to be arranged at the center of receiving tank lower end, the rotating handles setting is in receiving tank front.

Description

A kind of crystallization solvent recyclable device of sodium ascorbyl phosphate
Technical field
The utility model relates to a kind of vitamin C derivatives crystallizer technical field, specifically a kind of vitamin C phosphoric acid The crystallization solvent recyclable device of ester sodium.
Background technique
Sodium ascorbyl phosphate is a kind of vitamin C derivatives, and 2 hydroxyls, which are derived as phosphate, can be improved dimension life The stability of plain C can regenerate vitamin C after being formed by the phosphate hydrolysis that derivative is widely present in vivo, because It is a kind of valuable fine chemicals as the main component that feed addictive, food additive and superior cosmetics brighten.
Existing solvent recovery unit the degree of automation is low, needs manually to participate in, recovery operation low efficiency;Existing solvent Recyclable device purification degree is not high, and solvent recovery effect is poor;It is miscellaneous to be easy accumulation since purification degree is not high for existing solvent recovery unit Matter results in blockage to leakage fluid dram, influences working efficiency and increases work difficulty.
Utility model content
The purpose of this utility model is to provide a kind of crystallization solvent recyclable devices of sodium ascorbyl phosphate, with solution Certainly the problems mentioned above in the background art.
To achieve the above object, the utility model provides the following technical solutions: a kind of crystallization use of sodium ascorbyl phosphate Solvent recovery unit, including reaction kettle, support frame, heating interlayer, fixed plate, filter screen, activated charcoal strainer, capping, bracket, Gas sampling tank, tracheae, air draught pump, inlet, pressure gauge, thermometer, steam (vapor) outlet, drain pipe, flange, connecting tube, control Valve, receiving tank, water pump, stabilizer blade, leakage fluid dram and rotating handles, the reaction kettle lower part are equipped with support frame, and the heating interlayer is set It sets inside reaction kettle, in reaction kettle inner wall, fixed plate is equipped with filter screen and activated charcoal strainer, institute for the fixed plate setting Capping setting is stated in reaction kettle upper end, upper end is covered and is equipped with bracket, the bracket is equipped with gas sampling tank, the gas sampling Tank lower end is connected with tracheae, and the tracheae is pumped equipped with air draught, and the capping upper end is equipped with inlet, pressure gauge and thermometer, The steam (vapor) outlet setting is in reaction kettle left side, and the drain pipe is arranged at the center of reaction kettle lower end, under the drain pipe End is equipped with flange, and the flange lower end is connected with connecting tube, and the connecting tube right end is connected with receiving tank, the regulating switch It is arranged in connecting tube, the receiving tank lower end is equipped with stabilizer blade, and the leakage fluid dram is arranged at the center of receiving tank lower end, the rotation The setting of handle hand is in receiving tank front.
As a further solution of the present invention: there are four fixed plate sets altogether, and specification is consistent, convenient for filter screen and Activated carbon filter layer is fixed.
As a further solution of the present invention: capping side is equipped with bolt, reaction kettle side is correspondingly provided with bolt Screw hole, capping is connected with reaction kettle by screw thread, convenient for dismounting to reaction kettle and capping.
As a further solution of the present invention: pressure gauge maximum gauge pressure is 0.6Mpa, it is able to ascend the work of reaction kettle Make efficiency.
As a further solution of the present invention, rotating handles be worm-gear type structure, be conducive to receiving tank inside into Row cleaning, is convenient for daily maintenance and trouble hunting.
Compared with prior art, the utility model has the beneficial effects that the utility model high degree of automation, is reduced artificial It participates in, is conducive to optimization production, promotes working efficiency;It is equipped with filter screen and activated carbon filter layer in inside, solvent is filtered, Disassembly capping, can clean reaction kettle inside, avoid the blocking at drain and influence working effect;Inside reaction kettle It equipped with heating interlayer, is convenient for being evenly heated, is conducive to promote working efficiency;Rotating handles are worm-gear type structure, are conducive to docking It is cleared up inside closed cans, is convenient for daily maintenance and trouble hunting.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of the crystallization solvent recyclable device of sodium ascorbyl phosphate.
Fig. 2 is the structural schematic diagram of reaction kettle in a kind of crystallization solvent recyclable device of sodium ascorbyl phosphate.
Fig. 3 is the structural schematic diagram of receiving tank amplification in a kind of crystallization solvent recyclable device of sodium ascorbyl phosphate.
In figure: reaction kettle 1, support frame 2, heating interlayer 3, fixed plate 4, filter screen 5, activated charcoal strainer 6, capping 7, branch Frame 8, gas sampling tank 9, tracheae 10, air draught pump 11, inlet 12, pressure gauge 13, thermometer 14, steam (vapor) outlet 15, drain pipe 16, flange 17, connecting tube 18, control valve 19, receiving tank 20, water pump 21, stabilizer blade 22, leakage fluid dram 23, rotating handles 24.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
Please refer to Fig. 1~3, in the utility model embodiment, a kind of crystallization solvent of sodium ascorbyl phosphate recycles dress It sets, including reaction kettle 1, support frame 2, heating interlayer 3, fixed plate 4, filter screen 5, activated charcoal strainer 6, capping 7, bracket 8, useless Gas collecting tank 9, tracheae 10, air draught pump 11, inlet 12, pressure gauge 13, thermometer 14, steam (vapor) outlet 15, drain pipe 16, flange 17, connecting tube 18, control valve 19, receiving tank 20, water pump 21, stabilizer blade 22, leakage fluid dram 23 and rotating handles 24, the reaction kettle 1 Lower part is equipped with support frame 2, and the heating interlayer 3 is arranged inside reaction kettle 1, and the fixed plate 4 is arranged in 1 inner wall of reaction kettle, Fixed plate 4 is equipped with filter screen 5 and activated charcoal strainer 6, and there are four fixed plate 4 is set altogether, and specification is consistent, convenient for filter screen 5 and activated carbon filter layer 6 it is fixed, 7 setting of capping covers 7 sides and is equipped with bolt, 1 side of reaction kettle in 1 upper end of reaction kettle It is correspondingly provided with screw hole with bolt, capping 7 is connected with reaction kettle 1 by screw thread, convenient for being dismounted to reaction kettle 1 and capping 7, 7 upper ends are covered equipped with bracket 8, the bracket 8 is equipped with gas sampling tank 9, and 9 lower end of gas sampling tank is connected with tracheae 10, the tracheae 10 is equipped with air draught pump 11, and 7 upper ends of the capping are equipped with inlet 12, pressure gauge 13 and thermometer 14, pressure The maximum gauge pressure of table 13 is 0.6Mpa, is able to ascend the working efficiency of reaction kettle 1, and the setting of steam (vapor) outlet 15 is left in reaction kettle 1 Side, the drain pipe 16 are arranged at 1 lower end center of reaction kettle, and 16 lower end of drain pipe is equipped with flange 17, the flange 17 lower ends are connected with connecting tube 18, and 18 right end of connecting tube is connected with receiving tank 20, and the setting of regulating switch 21 is even On adapter tube 18,20 lower end of receiving tank is equipped with stabilizer blade 22, and the leakage fluid dram 23 is arranged at 20 lower end center of receiving tank, described The setting of rotating handles 24 is worm-gear type structure in 20 front of receiving tank, rotating handles 24, is conducive to clear to carrying out inside receiving tank 20 Reason is convenient for daily maintenance and trouble hunting.
The working principle of the utility model is: the setting of fixed plate 4, in 1 inner wall of reaction kettle, fixed plate 4 is equipped with filter screen 5 With activated charcoal strainer 6, there are four fixed plate 4 is set altogether, and specification is consistent, convenient for solid to filter screen 5 and activated carbon filter layer 6 Fixed, 7 setting of capping covers 7 sides and is equipped with bolt in 1 upper end of reaction kettle, and 1 side of reaction kettle and bolt are correspondingly provided with screw hole, seal Lid 7 is connected with reaction kettle 1 by screw thread, convenient for being dismounted to reaction kettle 1 and capping 7, filter screen 5 and activated charcoal strainer 6 can be filtered solvent, and disassembly capping 7 can avoid the blocking and shadow at drain to cleaning inside reaction kettle 1 Working effect is rung, heating interlayer 3 is equipped with inside reaction kettle 1, is convenient for being evenly heated, is conducive to promote working efficiency, solvent Entered in reaction kettle 1 by inlet 12, via filter screen 5 and activated charcoal strainer 6, solvent is filtered, by heating interlayer 3 1 internal solvent of reaction kettle is evenly heated, the exhaust gas of generation is sucked exhaust gas in gas sampling tank 9 by air draught pump 11, is kept away Exempt from air pollution, the solvent after the completion of filtering is connected with connecting tube 19 by flange 17 by 16 row of drain pipe, drain pipe 16, The solvent that filtering is completed is collected into receiving tank 20 by water pump 21, is discharged after the completion of collection by leakage fluid dram 23, rotating handles 24 are set It sets in 20 front of receiving tank, rotating handles 24 are worm-gear type structure, conducive to clearing up inside receiving tank 20, are convenient for daily dimension Shield and trouble hunting.
Although the utility model is described in detail with reference to the foregoing embodiments, come for those skilled in the art Say, it is still possible to modify the technical solutions described in the foregoing embodiments, or to part of technical characteristic into Row equivalent replacement, within the spirit and principle of the utility model, any modification, equivalent replacement, improvement and so on should all It is included within the scope of protection of this utility model.

Claims (5)

1. a kind of crystallization solvent recyclable device of sodium ascorbyl phosphate, including reaction kettle, support frame, heating interlayer, fixation Plate, filter screen, activated charcoal strainer, capping, bracket, gas sampling tank, tracheae, air draught pump, inlet, pressure gauge, thermometer, Steam (vapor) outlet, drain pipe, flange, connecting tube, control valve, receiving tank, water pump, stabilizer blade, leakage fluid dram and rotating handles, feature exist In the reaction kettle lower part is equipped with support frame, and the heating interlayer is arranged inside reaction kettle, and the fixed plate setting is being reacted Kettle inner wall, fixed plate are equipped with filter screen and activated charcoal strainer, and the capping setting covers upper end and be equipped in reaction kettle upper end Bracket, the bracket are equipped with gas sampling tank, and gas sampling tank lower end is connected with tracheae, and the tracheae is equipped with air draught Pump, the capping upper end are equipped with inlet, pressure gauge and thermometer, and the steam (vapor) outlet is arranged in reaction kettle left side, described Drain pipe is arranged at the center of reaction kettle lower end, and the drain pipe lower end is equipped with flange, and the flange lower end is connected with connecting tube, The connecting tube right end is connected with receiving tank, and regulating switch is arranged in connecting tube, and the receiving tank lower end is equipped with stabilizer blade, institute It states leakage fluid dram to be arranged at the center of receiving tank lower end, the rotating handles setting is in receiving tank front.
2. a kind of crystallization solvent recyclable device of sodium ascorbyl phosphate according to claim 1, which is characterized in that There are four the fixed plate is set altogether, and specification is consistent.
3. a kind of crystallization solvent recyclable device of sodium ascorbyl phosphate according to claim 1, which is characterized in that The capping side is equipped with bolt, and reaction kettle side and bolt are correspondingly provided with screw hole, and capping is connected with reaction kettle by screw thread.
4. a kind of crystallization solvent recyclable device of sodium ascorbyl phosphate according to claim 1, which is characterized in that The pressure gauge maximum gauge pressure is 0.6Mpa.
5. a kind of crystallization solvent recyclable device of sodium ascorbyl phosphate according to claim 1, which is characterized in that The rotating handles are worm-gear type structure.
CN201821939651.7U 2018-11-23 2018-11-23 A kind of crystallization solvent recyclable device of sodium ascorbyl phosphate Expired - Fee Related CN209530253U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821939651.7U CN209530253U (en) 2018-11-23 2018-11-23 A kind of crystallization solvent recyclable device of sodium ascorbyl phosphate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821939651.7U CN209530253U (en) 2018-11-23 2018-11-23 A kind of crystallization solvent recyclable device of sodium ascorbyl phosphate

Publications (1)

Publication Number Publication Date
CN209530253U true CN209530253U (en) 2019-10-25

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821939651.7U Expired - Fee Related CN209530253U (en) 2018-11-23 2018-11-23 A kind of crystallization solvent recyclable device of sodium ascorbyl phosphate

Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111992161A (en) * 2020-09-04 2020-11-27 江西科技学院 Photocatalytic degradation device for copper slag pollutants and use method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111992161A (en) * 2020-09-04 2020-11-27 江西科技学院 Photocatalytic degradation device for copper slag pollutants and use method thereof

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20191025

CF01 Termination of patent right due to non-payment of annual fee