CN201128726Y - Difluoroethane reactor with mixing function - Google Patents
Difluoroethane reactor with mixing function Download PDFInfo
- Publication number
- CN201128726Y CN201128726Y CNU2007200426955U CN200720042695U CN201128726Y CN 201128726 Y CN201128726 Y CN 201128726Y CN U2007200426955 U CNU2007200426955 U CN U2007200426955U CN 200720042695 U CN200720042695 U CN 200720042695U CN 201128726 Y CN201128726 Y CN 201128726Y
- Authority
- CN
- China
- Prior art keywords
- reaction vessel
- cooling
- stirring
- reactor
- difluoroethane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- NPNPZTNLOVBDOC-UHFFFAOYSA-N 1,1-difluoroethane Chemical compound CC(F)F NPNPZTNLOVBDOC-UHFFFAOYSA-N 0.000 title claims abstract description 13
- 238000003756 stirring Methods 0.000 claims abstract description 52
- 238000006243 chemical reaction Methods 0.000 claims abstract description 28
- 238000001816 cooling Methods 0.000 claims abstract description 21
- 239000000498 cooling water Substances 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000002699 waste material Substances 0.000 claims abstract description 4
- 238000010438 heat treatment Methods 0.000 claims description 3
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 9
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 9
- 239000003054 catalyst Substances 0.000 description 8
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 6
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 6
- 230000000694 effects Effects 0.000 description 3
- 238000007259 addition reaction Methods 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000005587 bubbling Effects 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000006384 oligomerization reaction Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000012852 risk material Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses a difluoroethane reactor provided with a stirrer, consisting of a reaction vessel (1), wherein the upper part of the reaction vessel (1) is provided with an upper inlet orifice I (2), an inlet orifice II (17) and a product output (3); the lower part of the reaction vessel (1) is provided with a waste output (4); the interior part of reaction vessel (1) is provided with two sets of cooling coils (7), wherein the bottom part of each cooling coil (7) is provided with a cooling water inlet I, the top part is provided with a cooling water outlet; the cooling jacket (5) is provided with a cooling water inlet II (10), a cooling water outlet II (11), a hot water inlet I (12) and a hot water outlet I (13); a stirring device is arranged at the central part of the reaction vessel (1), wherein the stirring device consists of a drive set(14)and a stirring shaft (15); the stirring shaft (15) is provided with a stirring paddle (16); the drive set (14) drives the stirring shaft (15) to rotate, and the stirring shaft (15) drives the stirring paddle (16) to rotate.
Description
Technical field
The utility model relates to a kind of difluoroethane reactor with stirring, and it is applicable to the field of acetylene and hydrogen fluoride addition reaction production preparation C2H4F2 C2H4F2 cooling agent.
Background technology
Utilizing acetylene and hydrogen fluoride that addition reaction production C2H4F2 C2H4F2 product takes place under the effect of catalyzer is the C2H4F2 C2H4F2 synthetic route that generally adopts at present.Because the singularity such as inflammable, explosive of acetylene and the severe corrosive of hydrogen fluoride and catalyzer, difluoroethane reactor is the traditional technology that domestic colleague mostly adopts gas-liquid phase bubbling.Because mass transfer and heat transfer are undesirable, for guaranteeing acetylene enough reaction times and lower temperature of reaction are arranged, reactor volume is huge; Simultaneously, owing to do not stir, form local superheating easily, the acetylene autohemagglutination generates a large amount of oligopolymer, not only reduce activity of such catalysts, shorten the reaction one way cycle, and because oligopolymer can stop up the discharge outlet of spent catalyst, thereby in order to reduce the viscosity of discharge, guarantee the smooth discharging of spent catalyst, the hydrogen fluoride that have to keep higher concentration discharges with spent catalyst, causes wastage of material, contaminate environment.
Summary of the invention
The utility model provides a kind of difluoroethane reactor with stirring, and it not only can improve throughput and cut down the consumption of raw materials, but also helps the safety dumping of catalyzer.
The utility model has adopted following technical scheme to be: a kind of difluoroethane reactor with stirring, it comprises reaction vessel, be provided with opening for feed I in the upper end of reaction vessel, opening for feed II and product delivery port, lower end at reaction vessel is provided with waste outlet, outside surface at reaction vessel is with cooling jacket and heating jacket, in reaction vessel, be provided with two groups of spiral coil cooling tubes, the lower end of spiral coil cooling tube is provided with entrance of cooling water I, the upper end of spiral coil cooling tube is provided with cooling water outlet I, be provided with entrance of cooling water II in the bottom of cooling jacket, hot water inlet I and hot water outlet I, at the top of cooling jacket cooling water outlet II, the center that it is characterized in that described reaction vessel inner chamber is provided with whipping appts, whipping appts comprises drive unit and stir shaft, drive unit and stir shaft are drive state, be provided with stirring rake on stir shaft, drive unit drives stir shaft and rotates, and stir shaft drives stirring rake and rotates.
Dead-tight magnetic driving equipment that Porcelain Jar was formed inside and outside described drive unit was served as reasons.Described stirring rake is magnetic force driving, and its blade is pusher blade.Stirring rake (16) is one or more layers stirring rake.
The utlity model has following beneficial effect: the utility model increases whipping appts in chuck or inner coil pipe difluoroethane reactor, not only can prevent to form local superheating, mass transfer, heat transfer are evenly, avoid the acetylene autohemagglutination to generate a large amount of oligopolymer, prolong activity of such catalysts, improve the reaction one way cycle; And can avoid oligomerization of acetylene thing deposition to stop up the discharge outlet of spent catalyst; Also can improve simultaneously the flowability of discharge, guarantee the smooth discharging of spent catalyst, thereby the hydrogen fluoride that reduces higher concentration discharges with spent catalyst, economizes in raw materials, and reduces environmental pollution.The stirring rake of whipping appts of the present utility model is magnetic force driving, and paddle is pusher blade, so blade has self-suction function, can participate in reaction for the acetylene gas of reaction again like this.The utility model adopts the structure formation that stirs with dead-tight magnetic force driving, magnetic driving equipment is a transmission mechanism of being made up of inside and outside Porcelain Jar, stir shaft is not contacted with air, do not have conventional stir shaft and the sealing between the reactor body yet, thereby leaking of high-risk materials such as acetylene and hydrogen fluoride just can not occur avoiding yet.
Description of drawings
Fig. 1 is the utility model structural representation
Embodiment
In Fig. 1, the utility model is a kind of difluoroethane reactor with stirring, it comprises reaction vessel 1, be provided with opening for feed I 2 in the upper end of reaction vessel 1, opening for feed II 17 and product delivery port 3, be provided with waste outlet 4 in the lower end of reaction vessel 1, outside surface at reaction vessel 1 is with cooling jacket 5 and heating jacket 6, in reaction vessel 1, be provided with two groups of spiral coil cooling tubes 7, the lower end of spiral coil cooling tube 7 is provided with entrance of cooling water I, the upper end of spiral coil cooling tube 7 is provided with cooling water outlet I, be provided with entrance of cooling water II 10 in the bottom of cooling jacket 5, hot water inlet I 12 and hot water outlet I 13, at the top of cooling jacket 5 cooling water outlet II11, the center of reaction vessel 1 inner chamber is provided with whipping appts, whipping appts comprises drive unit 14 and stir shaft 15, dead-tight magnetic driving equipment that Porcelain Jar was formed inside and outside drive unit 14 was served as reasons, drive unit 14 is a drive state with stir shaft 15, on stir shaft 15, be provided with stirring rake 16, stirring rake 16 is magnetic force driving, its blade is pusher blade, stirring rake 16 is one or more layers stirring rake, drive unit 14 drives stir shaft 15 and rotates, and stir shaft 15 drives stirring rake 16 and rotates.
Claims (4)
1, a kind of difluoroethane reactor with stirring, it comprises reaction vessel (1), be provided with opening for feed I (2) in the upper end of reaction vessel (1), opening for feed II (17) and product delivery port (3), be provided with waste outlet (4) in the lower end of reaction vessel (1), outside surface at reaction vessel (1) is with cooling jacket (5) and heating jacket (6), in reaction vessel (1), be provided with two groups of spiral coil cooling tubes (7), the lower end of spiral coil cooling tube (7) is provided with entrance of cooling water I, the upper end of spiral coil cooling tube (7) is provided with cooling water outlet I, be provided with entrance of cooling water II (10) in the bottom of cooling jacket (5), hot water inlet I (12) and hot water outlet I (13), at the top of cooling jacket (5) cooling water outlet II (11), the center that it is characterized in that described reaction vessel (1) inner chamber is provided with whipping appts, whipping appts comprises drive unit (14) and stir shaft (15), drive unit (14) is a drive state with stir shaft (15), on stir shaft (15), be provided with stirring rake (16), drive unit (14) drives stir shaft (15) and rotates, and stir shaft (15) drives stirring rake (16) and rotates.
2, the difluoroethane reactor that stirs of band according to claim 1, the dead-tight magnetic driving equipment that it is characterized in that serving as reasons described drive unit (14) inside and outside Porcelain Jar forms.
3, the difluoroethane reactor of band stirring according to claim 1 is characterized in that described stirring rake (16) is magnetic force driving, and its blade is pusher blade.
4, the difluoroethane reactor of band stirring according to claim 3 is characterized in that the stirring rake of stirring rake (16) for one or more layers.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNU2007200426955U CN201128726Y (en) | 2007-11-23 | 2007-11-23 | Difluoroethane reactor with mixing function |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNU2007200426955U CN201128726Y (en) | 2007-11-23 | 2007-11-23 | Difluoroethane reactor with mixing function |
Publications (1)
Publication Number | Publication Date |
---|---|
CN201128726Y true CN201128726Y (en) | 2008-10-08 |
Family
ID=40016564
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CNU2007200426955U Expired - Fee Related CN201128726Y (en) | 2007-11-23 | 2007-11-23 | Difluoroethane reactor with mixing function |
Country Status (1)
Country | Link |
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CN (1) | CN201128726Y (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102593470A (en) * | 2012-03-01 | 2012-07-18 | 华东理工大学 | Device and method for preparing diffusion layer slurry of proton exchange membrane fuel cell |
-
2007
- 2007-11-23 CN CNU2007200426955U patent/CN201128726Y/en not_active Expired - Fee Related
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102593470A (en) * | 2012-03-01 | 2012-07-18 | 华东理工大学 | Device and method for preparing diffusion layer slurry of proton exchange membrane fuel cell |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20081008 Termination date: 20141123 |
|
EXPY | Termination of patent right or utility model |