CN118556897A - Reconstituted tobacco prepared by thick slurry method, preparation method thereof and cigarettes - Google Patents
Reconstituted tobacco prepared by thick slurry method, preparation method thereof and cigarettes Download PDFInfo
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- CN118556897A CN118556897A CN202310181044.8A CN202310181044A CN118556897A CN 118556897 A CN118556897 A CN 118556897A CN 202310181044 A CN202310181044 A CN 202310181044A CN 118556897 A CN118556897 A CN 118556897A
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- tobacco
- reconstituted tobacco
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- thick slurry
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- 241000208125 Nicotiana Species 0.000 title claims abstract description 163
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 163
- 238000007613 slurry method Methods 0.000 title claims abstract description 40
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title abstract description 14
- 239000000853 adhesive Substances 0.000 claims abstract description 49
- 230000001070 adhesive effect Effects 0.000 claims abstract description 49
- 239000000843 powder Substances 0.000 claims abstract description 48
- 239000000835 fiber Substances 0.000 claims abstract description 41
- 239000002994 raw material Substances 0.000 claims abstract description 40
- 239000002002 slurry Substances 0.000 claims abstract description 33
- 239000007790 solid phase Substances 0.000 claims abstract description 17
- 238000002156 mixing Methods 0.000 claims description 48
- 239000000203 mixture Substances 0.000 claims description 40
- 238000000034 method Methods 0.000 claims description 29
- 239000007788 liquid Substances 0.000 claims description 16
- 229920000591 gum Polymers 0.000 claims description 12
- 238000004537 pulping Methods 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 229920002752 Konjac Polymers 0.000 claims description 7
- 229930006000 Sucrose Natural products 0.000 claims description 7
- 235000004298 Tamarindus indica Nutrition 0.000 claims description 7
- 239000000679 carrageenan Substances 0.000 claims description 7
- 235000010418 carrageenan Nutrition 0.000 claims description 7
- 229920001525 carrageenan Polymers 0.000 claims description 7
- 229940113118 carrageenan Drugs 0.000 claims description 7
- 239000005720 sucrose Substances 0.000 claims description 7
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 7
- 108010010803 Gelatin Proteins 0.000 claims description 6
- 229920002907 Guar gum Polymers 0.000 claims description 6
- 150000002016 disaccharides Chemical class 0.000 claims description 6
- 229920000159 gelatin Polymers 0.000 claims description 6
- 239000008273 gelatin Substances 0.000 claims description 6
- 235000019322 gelatine Nutrition 0.000 claims description 6
- 235000011852 gelatine desserts Nutrition 0.000 claims description 6
- 239000000665 guar gum Substances 0.000 claims description 6
- 235000010417 guar gum Nutrition 0.000 claims description 6
- 229960002154 guar gum Drugs 0.000 claims description 6
- 239000011121 hardwood Substances 0.000 claims description 6
- 150000002772 monosaccharides Chemical class 0.000 claims description 6
- 239000011122 softwood Substances 0.000 claims description 6
- 229920002472 Starch Polymers 0.000 claims description 5
- 235000010485 konjac Nutrition 0.000 claims description 5
- 239000008107 starch Substances 0.000 claims description 5
- 235000019698 starch Nutrition 0.000 claims description 5
- 229930091371 Fructose Natural products 0.000 claims description 4
- 239000005715 Fructose Substances 0.000 claims description 4
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 4
- 239000008103 glucose Substances 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 125000000185 sucrose group Chemical group 0.000 claims description 4
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 claims description 3
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 3
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims description 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 3
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 3
- 239000008101 lactose Substances 0.000 claims description 3
- 239000000252 konjac Substances 0.000 claims description 2
- 235000019823 konjac gum Nutrition 0.000 claims description 2
- 240000004584 Tamarindus indica Species 0.000 claims 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 abstract description 27
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 abstract description 21
- 238000012545 processing Methods 0.000 abstract description 13
- 238000010438 heat treatment Methods 0.000 abstract description 12
- 238000004519 manufacturing process Methods 0.000 abstract description 11
- 230000001953 sensory effect Effects 0.000 abstract description 8
- 238000011049 filling Methods 0.000 abstract description 7
- 238000003860 storage Methods 0.000 abstract description 7
- 239000000126 substance Substances 0.000 abstract description 7
- 239000000796 flavoring agent Substances 0.000 abstract description 5
- 235000019634 flavors Nutrition 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 4
- 235000019505 tobacco product Nutrition 0.000 abstract description 3
- 230000000052 comparative effect Effects 0.000 description 11
- 238000001035 drying Methods 0.000 description 9
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical group [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 8
- 239000000945 filler Substances 0.000 description 8
- 238000011156 evaluation Methods 0.000 description 7
- 239000000779 smoke Substances 0.000 description 7
- 125000003118 aryl group Chemical group 0.000 description 6
- 241000596504 Tamarindus Species 0.000 description 5
- 229910052751 metal Inorganic materials 0.000 description 5
- 239000002184 metal Substances 0.000 description 5
- 229910000019 calcium carbonate Inorganic materials 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 238000005266 casting Methods 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 235000013599 spices Nutrition 0.000 description 3
- 238000002485 combustion reaction Methods 0.000 description 2
- 210000000214 mouth Anatomy 0.000 description 2
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- 230000000630 rising effect Effects 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 206010013911 Dysgeusia Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000010009 beating Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- BJHIKXHVCXFQLS-UYFOZJQFSA-N fructose group Chemical group OCC(=O)[C@@H](O)[C@H](O)[C@H](O)CO BJHIKXHVCXFQLS-UYFOZJQFSA-N 0.000 description 1
- 125000002791 glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 210000003928 nasal cavity Anatomy 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 238000010079 rubber tapping Methods 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
- A24B15/14—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/004—Cigars; Cigarettes with a filter located between tobacco rods
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The application provides reconstituted tobacco prepared by a thick slurry method, a preparation method thereof and cigarettes, and relates to the field of reconstituted tobacco production. The raw material components of the thick slurry reconstituted tobacco consist of tobacco powder, sugar, fiber and adhesive, can be used as auxiliary materials to be directly applied to the traditional cigarettes, and have filling performance and processing resistance better than those of the traditional thick slurry reconstituted tobacco, and simultaneously have sensory properties better than those of the papermaking reconstituted tobacco; the reconstituted tobacco with the thick slurry method can also be used in novel tobacco products which are not burnt by heating, and the raw materials of the reconstituted tobacco with the thick slurry method do not contain hydrophilic substances such as glycerol, propylene glycol and the like, so that the difficulty of the production process is reduced, and the reconstituted tobacco with the thick slurry method has the characteristics of good processing resistance, low cost, low storage requirement and the like, and is a novel dual-purpose reconstituted tobacco with the thick slurry method. In addition, the addition of sugar in large amounts can replace the adhesive to form bonds between solid phases, reduce the amount of adhesive or fiber, and reduce non-tobacco flavor imparted by the adhesive and fiber while improving the sensory suitability of the product.
Description
Technical Field
The application relates to the field of reconstituted tobacco production, in particular to thick slurry reconstituted tobacco, a preparation method thereof and cigarettes.
Background
The traditional thick slurry method for reproducing tobacco leaves is to grind tobacco raw materials into fine powder, uniformly disperse the fine powder in water, add adhesives and other additives, uniformly stir the fine powder, spread the fine powder on the surface of a metal sheet evenly, mold and dry the fine powder, and peel the fine powder off the metal sheet after the moisture reaches the index to obtain the tobacco sheets meeting the requirements. The prepared slices enter a tobacco rolling group after being cut into slices, and finally the conventional cigarettes in the market are formed through the process links such as cut tobacco making and the like. However, as the filling value of the conventional thick-pulp reconstituted tobacco is lower, the conventional thick-pulp reconstituted tobacco is easy to crush and has poor processing resistance in the production process, and is gradually replaced by the paper-making reconstituted tobacco, only a few tobacco enterprises still use the conventional thick-pulp reconstituted tobacco at present.
The prior thick paste method heating non-combustion thin sheet is to stir tobacco particles ground into fine powder, glycerol, propylene glycol, adhesive, plant fibers and the like in water to form thick paste, then spread the thick paste on the surface of a metal thin plate flatly for molding and drying, and peel the thick paste from the metal thin plate after the moisture reaches the index to obtain the sheet with the heating non-combustion thick paste method meeting the requirements. The sheet is rolled into a large roll, then the large roll is rewound and divided into small rolls according to design indexes, and the corresponding small rolls are cut into shreds, sticks, cuts, composites and other process links to finally form the conventional ordered heating nonflammable cigarettes in the market. Or directly forming the conventional disordered heating nonflammable cigarettes in the market through the process links of slicing, shredding, blending, forming rods, cutting, compounding and the like. However, the existing thick slurry method is used for heating the incombustible thin sheet, a large amount of hydrophilic substances such as glycerol and propylene glycol are added to cause high production difficulty, and meanwhile, the storage environment of the thick slurry method needs constant temperature and constant humidity, so that the processing resistance is greatly reduced and the thick slurry cannot be normally used once the thick slurry is improperly stored.
Disclosure of Invention
The application aims to provide thick slurry reconstituted tobacco, a preparation method thereof and cigarettes, and aims to solve the problems that the filling value of the existing thick slurry reconstituted tobacco is low, the breakage resistance and the processing resistance are poor in the production process, and the production difficulty is high due to the fact that a large amount of hydrophilic substances such as glycerol and propylene glycol are added into the existing thick slurry heated incombustible sheet, and meanwhile, the storage environment needs constant temperature and humidity, and the processing resistance is greatly reduced due to improper storage, so that the existing thick slurry reconstituted tobacco cannot be normally used.
In order to achieve the purpose, the application provides thick slurry reconstituted tobacco, which comprises the following raw materials in percentage by mass:
70-90% of tobacco powder, 10-30% of sugar, 0-8% of fiber and 0-10% of adhesive.
Preferably, the particle diameter D50 of the tobacco powder is 125-250 mu m.
Preferably, the sugar comprises a monosaccharide or disaccharide;
the monosaccharide comprises any one of glucose and fructose;
The disaccharide comprises any one of sucrose and lactose;
Preferably, the sugar is sucrose.
Preferably, the adhesive is selected from any one or more of guar gum, carrageenan, tamarind gum, konjac gum, starch and gelatin;
Wherein, when the adhesive is selected from any one or a combination of a plurality of carrageenan, tamarind gum, konjak gum and gelatin, the raw material of the thick slurry reconstituted tobacco does not comprise the fiber.
Preferably, the length of the fibers is 200-5000 μm;
The fibers are selected from the group consisting of finished hardwood pulp and/or softwood pulp.
The application also provides a preparation method of the thick slurry reconstituted tobacco, which comprises the steps of mixing raw materials according to a proportion, removing bubbles, feeding, forming and drying to obtain the thick slurry reconstituted tobacco.
Preferably, the "mixing the raw materials according to the proportion" includes:
Mixing the tobacco powder, sugar and adhesive in solid phase to obtain a mixture;
pulping fibers to obtain a slurry;
And carrying out solid-liquid mixing on the slurry and the mixture.
Preferably, the "mixing the raw materials according to the proportion" includes:
mixing the tobacco powder and sugar in a solid phase to obtain a mixture;
preparing an adhesive into a solution;
Solid-liquid mixing the solution with the mixture;
Preferably, the "mixing the raw materials according to the proportion" includes:
Mixing the tobacco powder, sugar and adhesive in solid phase to obtain a mixture;
and mixing water and the mixture in a solid-liquid mode.
The application also provides a cigarette, which comprises a filter section and a tobacco core section, wherein the tobacco core section comprises the thick slurry reconstituted tobacco.
Compared with the prior art, the application has the beneficial effects that:
The raw material components of the thick-pulp reconstituted tobacco provided by the application consist of tobacco powder, sugar, fiber and adhesive, and the thick-pulp reconstituted tobacco can be directly applied to traditional cigarettes as auxiliary materials, has filling performance and processing resistance better than those of the traditional thick-pulp reconstituted tobacco, and has sensory properties better than those of the papermaking reconstituted tobacco; the reconstituted tobacco prepared by the thick slurry method can also be used in novel tobacco products which are not burnt by heating, and the raw materials of the reconstituted tobacco prepared by the thick slurry method do not contain hydrophilic substances such as glycerol, propylene glycol and the like, so that the difficulty of the production process is reduced, and the reconstituted tobacco prepared by the thick slurry method has the characteristics of good processing resistance, low cost, low storage requirement and the like, and is a novel dual-purpose reconstituted tobacco prepared by the thick slurry method. In addition, the addition of sugar in large amounts can replace the adhesive to form bonds between solid phases, reduce the amount of adhesive or fiber, and reduce non-tobacco flavor imparted by the adhesive and fiber while improving the sensory suitability of the product.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present application, the drawings that are needed in the embodiments will be briefly described below, it being understood that the following drawings only illustrate some embodiments of the present application and therefore should not be considered as limiting the scope of the present application.
FIG. 1 is a schematic flow chart of a method for preparing reconstituted tobacco by thick slurry method according to an embodiment of the application;
FIG. 2 is a schematic flow chart of a method for preparing reconstituted tobacco by thick slurry method according to another embodiment of the application;
Fig. 3 is a schematic flow chart of a method for preparing reconstituted tobacco by thick slurry method according to another embodiment of the application.
Detailed Description
The term as used herein:
"prepared from … …" is synonymous with "comprising". The terms "comprising," "including," "having," "containing," or any other variation thereof, as used herein, are intended to cover a non-exclusive inclusion. For example, a composition, step, method, article, or apparatus that comprises a list of elements is not necessarily limited to only those elements but may include other elements not expressly listed or inherent to such composition, step, method, article, or apparatus.
The conjunction "consisting of … …" excludes any unspecified element, step or component. If used in a claim, such phrase will cause the claim to be closed, such that it does not include materials other than those described, except for conventional impurities associated therewith. When the phrase "consisting of … …" appears in a clause of the claim body, rather than immediately following the subject, it is limited to only the elements described in that clause; other elements are not excluded from the stated claims as a whole.
When an equivalent, concentration, or other value or parameter is expressed as a range, preferred range, or a range bounded by a list of upper preferable values and lower preferable values, this is to be understood as specifically disclosing all ranges formed from any pair of any upper range limit or preferred value and any lower range limit or preferred value, regardless of whether ranges are separately disclosed. For example, when ranges of "1 to 5" are disclosed, the described ranges should be construed to include ranges of "1 to 4", "1 to 3", "1 to 2 and 4 to 5", "1 to 3 and 5", and the like. When a numerical range is described herein, unless otherwise indicated, the range is intended to include its endpoints and all integers and fractions within the range.
In these examples, the parts and percentages are by mass unless otherwise indicated.
"Parts by mass" means a basic unit of measurement showing the mass ratio of a plurality of components, and 1 part may be any unit mass, for example, 1g, 2.689g, or the like. If we say that the mass part of the a component is a part and the mass part of the B component is B part, the ratio a of the mass of the a component to the mass of the B component is represented as: b. or the mass of the A component is aK, the mass of the B component is bK (K is any number and represents a multiple factor). It is not misunderstood that the sum of the parts by mass of all the components is not limited to 100 parts, unlike the parts by mass.
"And/or" is used to indicate that one or both of the illustrated cases may occur, e.g., a and/or B include (a and B) and (a or B).
When the reconstituted tobacco prepared by the traditional thick slurry method is applied to conventional cigarettes, the filling value is low, and the breakage resistance and the processing resistance are poor in the production process; when the conventional thick paste method heating nonflammable thin sheet is applied to heating nonflammable cigarettes, the production difficulty is high due to the addition of a large amount of hydrophilic substances such as glycerol and propylene glycol, meanwhile, the storage environment needs constant temperature and constant humidity, and once the thin sheet is improperly stored, the processing resistance is greatly reduced and cannot be normally used.
In order to solve the technical problems of the conventional thick-slurry reconstituted tobacco and the thick-slurry heated nonflammable sheet, the application provides the thick-slurry reconstituted tobacco which is suitable for conventional cigarettes and heated nonflammable cigarettes, and comprises the following raw materials in percentage by mass: 70-90% of tobacco powder, 10-30% of sugar, 0-8% of fiber and 0-10% of adhesive.
The tobacco powder is fine powder obtained by grinding tobacco raw materials, and the tobacco raw materials can be flue-cured tobacco, burley tobacco, aromatic tobacco and the like, and the dosage of the tobacco powder can be 70%, 75%, 80%, 85% or 90%, for example. The particle diameter D50 of the tobacco powder is 125-250 μm, for example, 125-150 μm, 150-200 μm, or 180-250 μm.
The amount of sugar may be, for example, 10%, 15%, 20%, 25% or 30%. Sugar includes mono-or disaccharides; the monosaccharide comprises any one of glucose and fructose; the disaccharide comprises any one of sucrose and lactose.
In a preferred embodiment, the sugar is sucrose.
Wherein the adhesive is selected from any one of guar gum, carrageenan, tamarind gum, konjak gum, starch and gelatin; when the adhesive is selected from any one of carrageenan, tamarind gum, konjak gum and gelatin, the raw materials of the thick slurry reconstituted tobacco can not comprise the fibers. The mass percentage of the adhesive may be, for example, 0 to 5%, or 5 to 10%, more specifically, for example, 0%, 1%, 2%, 3%, 4%, 5%, 6%, 7%, 8%, 9% or 10%.
Wherein the length of the fibers is 200 to 5000 μm, for example, 200 to 500 μm, or 500 to 1000 μm, or 800 to 1500 μm, or 1000 to 2000 μm, or 2000 to 5000 μm; more specifically, for example, 200 μm, 300 μm, 400 μm, 500 μm, 600 μm, 700 μm, 800 μm, 900 μm, 1000 μm, 2000 μm, 3000 μm, 4000 μm or 5000 μm may be mentioned.
The fibers are selected from the group consisting of finished hardwood pulp and/or softwood pulp. The mass percentage of the fibers may be, for example, 0% to 4%, or 4% to 8%, more specifically, 0%, 1%, 2%, 3%, 4%, 5%, 6%, 7% or 8%.
The application also provides a preparation method of the thick slurry reconstituted tobacco, which comprises the steps of mixing raw materials according to a proportion, removing bubbles, feeding, forming and drying to obtain the thick slurry reconstituted tobacco.
The bubble removal means that tiny bubbles in thick slurry obtained by mixing raw materials according to a proportion are discharged, so that micropores are prevented from being generated in the forming process, and a vacuum bubble removal mode is preferably adopted.
Wherein, the feeding forming refers to the process of evenly casting thick slurry obtained by mixing raw materials according to a proportion on a metal sheet to form an even casting layer.
Wherein drying refers to the process of removing water from the casting layer to finally form a sheet.
Wherein, the post-treatment refers to processing the dried thick slurry reconstituted tobacco into cut tobacco.
In one embodiment, referring to fig. 1, the "mixing the raw materials according to the mixture ratio" includes:
The tobacco powder, sugar and adhesive are subjected to solid phase mixing by using a mixing device to obtain a mixture.
Pulping the fibers to obtain pulp, wherein the pulping of the fibers refers to that the hardwood pulp and the softwood pulp are processed to the required degree through a pulping machine according to a certain proportion; preferably, the fiber slurry has a degree of tapping of 35 to 85 ° SR and a wet weight of 0.5 to 2.4g.
And carrying out solid-liquid mixing on the slurry and the mixture.
In another embodiment, referring to fig. 2, the "mixing the raw materials according to the mixture ratio" includes:
The tobacco powder and sugar are subjected to solid phase mixing by using a mixing device to obtain a mixture.
Preparing the adhesive into a solution by means of steaming and boiling;
And mixing the solution with the mixture in a solid-liquid manner.
In yet another embodiment, referring to fig. 3, the "mixing the raw materials according to the mixture ratio" includes:
The tobacco powder, sugar and adhesive are subjected to solid phase mixing by using a mixing device to obtain a mixture.
And (3) carrying out solid-liquid mixing on water and the mixture, wherein the water temperature of the water needs to be controlled so as to meet the dispersion requirement of the adhesive.
The application also provides a cigarette which can be a conventional cigarette or a heated non-combustible cigarette, wherein the cigarette comprises a filtering section and a tobacco core section, and the tobacco core section comprises the reconstituted tobacco by the thick slurry method.
The raw material components of the thick-pulp reconstituted tobacco provided by the application consist of tobacco powder, sugar, fiber and adhesive, and the thick-pulp reconstituted tobacco can be directly applied to traditional cigarettes as auxiliary materials, has filling performance and processing resistance better than those of the traditional thick-pulp reconstituted tobacco, and has sensory properties better than those of the papermaking reconstituted tobacco; the reconstituted tobacco prepared by the thick slurry method can also be used in novel tobacco products which are not burnt by heating, and the raw materials of the reconstituted tobacco prepared by the thick slurry method do not contain hydrophilic substances such as glycerol, propylene glycol and the like, so that the difficulty of the production process is reduced, and the reconstituted tobacco prepared by the thick slurry method has the characteristics of good processing resistance, low cost, low storage requirement and the like, and is a novel dual-purpose reconstituted tobacco prepared by the thick slurry method. In addition, the addition of sugar in large amounts can replace the adhesive to form bonds between solid phases, reduce the amount of adhesive or fiber, and reduce non-tobacco flavor imparted by the adhesive and fiber while improving the sensory suitability of the product.
Embodiments of the present application will be described in detail below with reference to specific examples, but it will be understood by those skilled in the art that the following examples are only for illustrating the present application and should not be construed as limiting the scope of the present application. The specific conditions are not noted in the examples and are carried out according to conventional conditions or conditions recommended by the manufacturer. The reagents or apparatus used were conventional products commercially available without the manufacturer's attention.
Example 1
The raw materials of the reconstituted tobacco by the thick slurry method in the embodiment 1 comprise the following components in percentage by mass: 70% of tobacco powder, 20% of sugar, 5% of adhesive and 5% of fiber. Wherein, the grain diameter D50 of the tobacco powder is 125-250 mu m, and the raw materials of the tobacco powder are as follows: flue-cured tobacco, burley tobacco, aromatic tobacco (6:2:2); the sugar is sucrose; the adhesive is carrageenan; the length of the fiber is 200-5000 mu m, and the fiber is any one of hardwood pulp and softwood pulp or is matched according to proportion.
A schematic flow chart of a preparation method of reconstituted tobacco by thick slurry method in embodiment 1 is shown in fig. 1, and the preparation method comprises the following steps:
firstly, carrying out solid-phase mixing on the smoke powder, sugar and adhesive in mixing equipment to obtain a mixture;
pulping the fibers by a pulping machine to obtain fiber pulp, wherein the beating degree of the fiber pulp is 35-85 DEG SR, the wet weight of the fiber pulp is 0.5-2.4 g, and carrying out solid-liquid mixing on the fiber pulp and the mixture;
finally, the process of defoaming, feeding, forming, drying and post-treatment is carried out to obtain the reconstituted tobacco of the thick slurry method in the embodiment 1.
Example 2
The raw materials of the reconstituted tobacco by the thick slurry method in the embodiment 2 comprise the following components in percentage by mass: 75% of tobacco powder, 20% of sugar and 5% of adhesive. Wherein, the grain diameter D50 of the tobacco powder is 125-250 mu m, and the raw materials of the tobacco powder are as follows: flue-cured tobacco, burley tobacco, aromatic tobacco (6:2:2); the sugar is fructose, the adhesive is tamarind gum and konjak gum (9:1).
A schematic flow chart of a preparation method of reconstituted tobacco by thick slurry method in embodiment 2 is shown in fig. 2, and the preparation method comprises the following steps:
firstly, carrying out solid phase mixing on the tobacco powder and sugar to obtain a mixture;
preparing the adhesive into a solution, and carrying out solid-liquid mixing on the solution and the mixture;
Finally, the process of defoaming, feeding, forming, drying and post-treatment is carried out to obtain the reconstituted tobacco of the thick slurry method in the embodiment 2.
Example 3
The raw materials of the reconstituted tobacco by the thick slurry method in the embodiment 3 comprise the following components in percentage by mass: 75% of tobacco powder, 20% of sugar and 5% of adhesive. Wherein, the grain diameter D50 of the tobacco powder is 125-250 mu m, and the raw materials of the tobacco powder are as follows: flue-cured tobacco, burley tobacco, aromatic tobacco (6:2:2); the sugar is glucose, and the adhesive is guar gum.
A schematic flow chart of a preparation method of reconstituted tobacco by thick slurry method in embodiment 3 is shown in fig. 3, and the preparation method comprises the following steps:
firstly, carrying out solid phase mixing on the tobacco powder, sugar and adhesive to obtain a mixture;
then mixing water with the mixture in a solid-liquid manner;
Finally, the process of defoaming, feeding, forming, drying and post-treatment is carried out to obtain the reconstituted tobacco of the thick slurry method in the embodiment 3.
Comparative example 1
Comparative example 1 is a reconstituted tobacco prepared by a traditional thick slurry method, and comprises the following raw materials in percentage by mass: 75% of tobacco powder, 15% of filler and 10% of adhesive. Wherein, the grain diameter of the tobacco powder is 34-78 mu m, and the raw materials of the tobacco powder are as follows: flue-cured tobacco, burley tobacco and aromatic tobacco (6:2:2), wherein the filler is calcium carbonate, and the adhesive is guar gum and starch (3:1).
The preparation method of the reconstituted tobacco by the traditional thick slurry method comprises the following steps:
firstly, carrying out solid phase mixing on the smoke powder and the calcium carbonate to obtain a mixture;
preparing the adhesive into a solution, and carrying out solid-liquid mixing on the solution and the mixture;
Finally, the conventional thick slurry reconstituted tobacco of comparative example 1 is obtained through the processes of defoaming, feeding, forming, drying and post-treatment.
Comparative example 2
Comparative example 2 is a prior thick paste method heating non-combustible sheet, and comprises the following raw materials in percentage by mass: 55% of tobacco powder, 15% of filler, 20% of glycerol, 3% of adhesive and 7% of fiber, and 25% of essence and spice. Wherein, the grain diameter of the tobacco powder is less than or equal to 120 mu m, and the raw materials of the tobacco powder are as follows: flue-cured tobacco, burley tobacco and aromatic tobacco (6:2:2), wherein the filler is as follows: calcium carbonate and adhesive are: guar gum, starch (3:1), fiber is: hardwood pulp, softwood pulp (5:5), essence and spice are: special flavors and fragrances or tobacco raw materials flavors and fragrances.
The existing thick paste method for preparing the heating non-combustible thin sheet comprises the following steps:
Firstly, carrying out solid phase mixing on the smoke powder and calcium carbonate to obtain a first mixture;
Preparing an adhesive into a solution, and carrying out solid-liquid mixing on the solution and the first mixture to obtain a second mixture;
Pulping the fibers by a pulping machine to obtain fiber pulp, and carrying out solid-liquid mixing on the fiber pulp and the second mixture to obtain a third mixture;
Then, the glycerol, the essence and the spice are mixed with the third mixture in a solid-liquid manner;
Finally, the process of defoaming, feeding forming, drying and post-treatment is carried out to obtain the reconstituted tobacco of the thick slurry method of the comparative example 2.
Test example 1
Shredding the reconstituted tobacco with the thick slurry method in the embodiment 1, wherein the length of the tobacco is about 1.5-2.5 cm. The tobacco shreds prepared by the reconstituted tobacco with the thick slurry method of comparative example 2 are mixed according to the proportion shown in the following table 1, and a heated non-combustible cigarette is prepared for sensory evaluation. Wherein, the aroma is pleasant smell during suction, and the evaluation organ is nasal cavity; the smoke (smog) refers to the total amount of some gases including aroma, miscellaneous gases, fuming agents (the conventional cigarettes do not contain the substances) and the like, and the evaluation organ is an oral cavity, and the evaluation mode is that the impact (expansion) feeling of the whole gases on the periphery of the oral cavity is felt.
TABLE 1 use proportion of reconstituted tobacco cut filler and existing cut filler by thick slurry method and evaluation result
Numbering device | Example 1 | Related patent | Fragrance release amount | Smoke quantity |
1 | 25% | 75% | 70% | 60% |
2 | 50% | 50% | 80% | 50% |
3 | 75% | 25% | 90% | 40% |
The evaluation result shows that the aroma release amount is increased along with the increase of the usage amount of the thick slurry reconstituted tobacco, but the smoke amount is reduced along with the decrease of the usage amount of related patent products, so that certain balance is achieved in the sample No. 2, the problems of stimulation, aftertaste and the like are avoided, and the aroma is mellow and long-lasting.
Test example 2
The reconstituted tobacco obtained in example 1, example 2, comparative example 1 and paper-making process was cut into shreds with a length of about 1.5 to 2.5cm. The tobacco rods were prepared by manual smoking by mixing the tobacco rods with tobacco shreds of the finished cigarettes at a ratio of 5%, and the obtained tobacco rods were evaluated as shown in Table 2.
TABLE 2 usage proportion of reconstituted tobacco cut filler and finished cigarette cut filler by thick slurry method and evaluation result
Shredding and crushing conditions: example 1. Gtoreq.example 2. Apprxeq. Papermaking reconstituted tobacco > comparative example 1.
Cigarette filling condition (cigarette weight): example 1. Apprxeq. Example 2. Apprxeq. Papermaking process reconstituted tobacco < comparative example 1.
Sensory example 1. Apprxeq. Example 2 > papermaking reconstituted tobacco > comparative example 1. The slurry reconstituted tobacco has the main advantages of less miscellaneous gas, good coordination, rising smoke concentration and rising aroma.
Finally, it should be noted that: the above embodiments are only for illustrating the technical solution of the present application, and not for limiting the same; although the application has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical scheme described in the foregoing embodiments can be modified or some or all of the technical features thereof can be replaced by equivalents; such modifications and substitutions do not depart from the spirit of the application.
Furthermore, those skilled in the art will appreciate that while some embodiments herein include some features but not others included in other embodiments, combinations of features of different embodiments are meant to be within the scope of the application and form different embodiments. For example, in the claims below, any of the claimed embodiments may be used in any combination. The information disclosed in this background section is only for enhancement of understanding of the general background of the application and should not be taken as an acknowledgement or any form of suggestion that this information forms the prior art already known to a person skilled in the art.
Claims (10)
1. The reconstituted tobacco by thick slurry method is characterized by comprising the following raw materials in percentage by mass:
70-90% of tobacco powder, 10-30% of sugar, 0-8% of fiber and 0-10% of adhesive.
2. The thick stock reconstituted tobacco according to claim 1, wherein the particle size D50 of the tobacco powder is 125-250 μm.
3. The thick stock reconstituted tobacco of claim 1, wherein the sugar comprises a monosaccharide or disaccharide;
the monosaccharide comprises any one of glucose and fructose;
The disaccharide comprises any one of sucrose and lactose;
Preferably, the sugar is sucrose.
4. The thick stock reconstituted tobacco according to claim 1, wherein the adhesive is selected from any one or more of guar gum, carrageenan, tamarind gum, konjac gum, starch, gelatin;
Wherein, when the adhesive is selected from any one or a combination of a plurality of carrageenan, tamarind gum, konjak gum and gelatin, the raw material of the thick slurry reconstituted tobacco does not comprise the fiber.
5. The thick stock reconstituted tobacco according to claim 1, wherein the length of the fibers is 200-5000 μm;
The fibers are selected from the group consisting of finished hardwood pulp and/or softwood pulp.
6. The method for preparing reconstituted tobacco by thick stock method according to any one of claims 1 to 5, wherein the raw materials are mixed according to a proportion, defoamed, fed for forming and dried to obtain the reconstituted tobacco by thick stock method.
7. The method according to claim 6, wherein the step of mixing the raw materials in the mixture ratio comprises:
Mixing the tobacco powder, sugar and adhesive in solid phase to obtain a mixture;
pulping fibers to obtain a slurry;
And carrying out solid-liquid mixing on the slurry and the mixture.
8. The method according to claim 6, wherein the step of mixing the raw materials in the mixture ratio comprises:
mixing the tobacco powder and sugar in a solid phase to obtain a mixture;
preparing an adhesive into a solution;
And mixing the solution with the mixture in a solid-liquid manner.
9. The method according to claim 6, wherein the step of mixing the raw materials in the mixture ratio comprises:
Mixing the tobacco powder, sugar and adhesive in solid phase to obtain a mixture;
and mixing water and the mixture in a solid-liquid mode.
10. A cigarette comprising a filter segment and a core segment, the core segment comprising the thick stock reconstituted tobacco of any one of claims 1 to 5.
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