CN115364008A

CN115364008A - Cherry blossom repairing and tightening composition and application thereof

Info

Publication number: CN115364008A
Application number: CN202210415499.7A
Authority: CN
Inventors: 张训庭; 钟卫芳
Original assignee: Zhejiang Kangmanjia Commodity Co ltd
Current assignee: Zhejiang Kangmanjia Commodity Co ltd
Priority date: 2022-04-18
Filing date: 2022-04-18
Publication date: 2022-11-22

Abstract

The invention belongs to the technical field of skin care products, the IPC classification number is A61K8/9789, and particularly relates to a cherry blossom repairing and tightening composition and application thereof. The cherry blossom repairing and tightening composition comprises a composition A, a composition B and a composition C; the composition A comprises oriental cherry extract and amino acid compounds; the composition B comprises oriental cherry extract and turmeric gel; the composition C comprises cherry blossom extract and collagen. The composition A has good water replenishing and locking effects, and is beneficial to the absorption of active ingredients in the composition B, and then the composition C can be used for replenishing collagen well and locking nutritional active ingredients at the same time, so that the aims of strengthening the barrier function of stratum corneum well and moisturizing and refining the skin are fulfilled.

Description

Cherry blossom repairing and tightening composition and application thereof

Technical Field

The invention belongs to the technical field of skin care products, the IPC classification number is A61K8/9789, and particularly relates to a cherry blossom repairing and tightening composition and application thereof.

Technical Field

The oriental cherry extract has a good antioxidant effect and a skin whitening effect, and is usually added into some skin care products in the market to have the effects of whitening and removing freckles.

Patent CN112043645B uses the cherry blossom extract and anthocyanin to compound, which has an obvious inhibiting effect on the saccharification reaction between ribose and protein in the environment with pH between 5.5 and 7.5, and can better overcome the effect that the single cherry blossom extract cannot fully exert the antioxidant effect, but does not disclose the cherry blossom extract having a better repairing effect.

Disclosure of Invention

In order to solve the technical problems, the invention provides a cherry blossom repairing and tightening composition which comprises a composition A, a composition B and a composition C.

The composition A comprises oriental cherry extract and amino acid compounds; the weight ratio of the cherry blossom extract to the amino acid compound in the composition A is 1: (0.1-1); preferably 1: (0.3 to 0.7), for example, 1:0.3, 1:0.4, 1:0.5, 1:0.6, 1:0.7, etc.

The cherry extract refers to a single cherry extract or a compound containing the cherry extract, and in the invention, the single cherry extract or the compound containing the cherry extract is suitable for the system, and the cherry extract can be obtained from the market, and from the market purchase perspective, the compound containing the cherry extract is usually used as a selling raw material, and the cherry extract in the invention is a compound containing the cherry extract, for example, the compound containing the cherry extract has the following components: water, oriental cherry (Prunus Specisosa) flower extract, butylene glycol, 1, 2-hexanediol, and ethylhexylglycerin. In some embodiments, the cherry extract is purchased from shanghai zhen trade.

The cherry blossom extract is extracted from cherry blossom which is super-liked by oriental women, contains sakuranetin and sakuranetin, belongs to flavonoid substances, has certain functions of resisting oxidation and removing free radicals, and can achieve the effects of improving darkness, whitening skin and moisturizing and tendering skin. Although the oriental cherry extract has a certain antioxidant effect, the antioxidant effect is brought by flavonoids, the effect of the antioxidant effect is realized by using Schiff base reaction under alkaline conditions, human skin is in a weakly acidic environment, the skin care product is also in a weakly acidic state when the corresponding skin care product of the composition product is used for maintaining the steady state balance of the human skin, and the antioxidant property of the oriental cherry extract alone cannot be fully exerted.

Preferably, the amino acid compound is selected from one or more of lysine, tryptophan, arginine, phenylalanine, threonine, leucine, valine and cystine; more preferably, the amino acid compound is arginine. The arginine can be obtained from the market, and the purchase manufacturers include but are not limited to the Shanghai Yaolan trade.

However, the inventor finds that the composition has a better antioxidant effect in use, probably because arginine is a basic amino acid, when the composition A is used for preparing a corresponding product, the synergistic effect of arginine and the cherry blossom extract can better increase the inhibitory effect of the cherry blossom extract on ribose saccharification in the skin, and simultaneously arginine can improve the water content of the skin to a certain extent and increase the metabolism of epidermal cells, and the cherry blossom extract can better remove free radicals in the metabolism process.

To further increase the moisturizing effect of composition a, in some embodiments, the composition a further comprises a polysaccharide.

In some embodiments, the weight ratio of the polysaccharide to the amino acid compound is (3 to 5): 1;

the polysaccharide comprises a soluble proteoglycan or a complex thereof; soluble proteoglycan complexes refer to proteoglycans containing soluble proteoglycans.

According to research, the soluble proteoglycan mainly plays a role in the invention, and the soluble proteoglycan alone or the proteoglycan containing the soluble proteoglycan is suitable for the system of the invention and can be obtained in the market, and from the market purchase perspective, the proteoglycan containing the soluble proteoglycan is usually used as a sales product by common raw material suppliers, and in some embodiments, the components in the proteoglycan containing the soluble proteoglycan comprise water, 1, 2-hexanediol, butanediol and the soluble proteoglycan, and the purchasing manufacturer can be named as the proteoglycan by Shanghai Jinlu biology.

In some embodiments, the polysaccharide further comprises rhamnose; the weight ratio of rhamnose to proteoglycan of soluble proteoglycan is 1: (0.8-1.2); preferably 1:1. the rhamnose is commercially available and purchased from commercial sources including, but not limited to, shanghai Holly.

The inventor finds that the composition has better water replenishing and moisture retaining properties and ensures that effective components in the composition B can be fully absorbed and utilized by adding some soluble proteoglycan and rhamnose, and the soluble proteoglycan can be equivalent to a growth factor in a system and can better activate dermal fibroblasts to synthesize components such as collagen and the like, so that the repairing effect on the skin is improved.

The composition B comprises cherry blossom extract and turmeric gel.

The weight ratio of the oriental cherry extract to the turmeric gel in the composition B is (0.5-3): 1; preferably, the weight ratio of the oriental cherry extract to the turmeric gel in the composition B is (1-2): 1, for example 1:1. 1.2: 1. 1.5: 1. 1.8: 1.2:1, etc.

In some preferred embodiments, the active host ingredient in the turmeric gel comprises turmeric (CURCUMALONGA) root extract, lactobacillus fermentation product. The turmeric gel may be obtained by self-production or commercially available, for example, from Shanghai Holothuria.

The turmeric root extract has good biological activity and pharmacological effects such as anti-inflammation and antioxidation, but the turmeric root extract or the cherry blossom extract alone cannot show good antioxidation when in use, but the composition A, the composition B and the composition C have good antioxidation when in synergistic use, and one aspect is probably because turmeric gel mainly comprising the turmeric root extract and a lactobacillus fermentation product in the invention can well interact with the cherry blossom extract, so that the integral antioxidation effect is improved. The turmeric may have yellow discoloration on the skin due to its own cause when used, and although the yellow discoloration does not harm the skin, the consumer experience is poor, but the inventor also finds that the composition B does not have yellow discoloration on the skin due to the addition of the turmeric when prepared into a corresponding skin care product, possibly due to some effects of certain ingredients in the cherry blossom extract on the turmeric.

In some preferred embodiments, the composition B further comprises a macromolecular glycophorin complex.

The weight ratio of the macromolecular sugar-egg compound to the turmeric gel is (0.5-3): 1; preferably, the weight ratio of the macromolecular sugar-egg compound to the turmeric gel is (1-2): 1, for example 1:1. 1.2: 1. 1.5: 1. 1.8: 1.2:1, etc.

The inventor finds that the stability of the composition can be further improved by adding the macromolecular sugar-egg complex, and the macromolecular sugar-egg complex contains a polysaccharide component, so that the interface activity of the system can be favorably improved in the composition, a relatively stable film is formed, and the stability of the composition is improved. However, it was found in the research that the stability of the composition is rather lowered when the content of the polymer-coated sugar-egg complex is too high, and the flocculation phenomenon may occur due to the increase of the electrostatic effect of the polymer-coated sugar-egg complex due to the too high concentration of the polymer-coated sugar-egg complex.

Preferably, the macromolecular glycoprotein complex is a composition of marine glycoprotein and fibronectin.

The marine glycoprotein alone and fibronectin or a complex of the marine glycoprotein or fibronectin are suitable for the system of the present invention, and are commercially available, and from the viewpoint of commercial purchase, general suppliers often sell the marine glycoprotein complex or fibronectin complex. The present invention is directed to a complex of the present invention, which is an ocean glycoprotein and fibronectin. For example, the complex of marine glycoprotein comprises water, 1, 2-hexanediol, butanediol, soluble proteoglycan components; the fibronectin complexes include water, fibronectin, sodium chloride, propylene glycol, glycerol, and p-hydroxyacetophenone components. The marine glycoprotein and fibronectin of the invention are commercially available, and are obtained from Jinluo Shanghai; the fibronectin was purchased from Shanghai Moire.

The health line (health line) suggests that turmeric may generate allergic reaction which causes irritation and swelling to some people, but the sensitive group of the skin care product prepared by the composition of the invention can also be used, probably because the special macromolecular glycoconjugate and the cherry blossom extract which are used in the invention are mutually cooperated to better inhibit the release of factors which are verified to be turmeric allergy in the skin, thereby regulating the balance of cell-related factors, or the cherry blossom extract can promote the release of some enzymes, the macromolecular glycoconjugate stabilizes mast cell membranes, and inhibits the degranulation of mast cells, so that the synergistic effect of the two inhibit the rate allergy phenomenon.

The weight ratio of the marine glycoprotein to the fibronectin is (0.1-1): 1; preferably, the weight ratio of the marine glycoprotein to fibronectin is (0.3-0.7): 1, for example 0.3: 1. 0.4: 1. 0.5:1. 0.6: 1. 0.7:1, etc.

The marine glycoprotein has good moisturizing effect, fibronectin has the effects of regulating cells, moisturizing and the like, but fibronectin is high-molecular-weight glycoprotein and cannot enter the surface layer even if the composition is used in the skin, and research and development find that the marine glycoprotein and the fibronectin used in the composition have good effect of repairing the skin barrier in the composition B and have good repairing effect, probably because the marine glycoprotein is equivalent to a growth factor and a promoting factor and can well promote the fibronectin to enter the skin to be combined with certain cell ligands to exert the biological activity of the composition B, and then the composition B is combined with lactobacillus fermentation product promoters in the turmeric gel to effectively promote the synthesis of integrins, fibroblast collagen IV, type VII and the like.

To further increase moisture retention, in some embodiments, composition B further comprises an extract of a fruit body of tremella (tremelafuciformis). The extract of Tremella (Tremellafuciformis) fruiting body has good moisture keeping and antioxidant effects.

The composition C comprises oriental cherry extract and collagen.

The weight ratio of the oriental cherry extract to the collagen in the composition C is (0.5-5): 1; preferably, the weight ratio of the oriental cherry extract to the collagen in the composition C is (1.5-2.5): 1.

collagen alone or a collagen complex is suitable for use in the system of the present invention, and is commercially available, and from the viewpoint of the market purchase, collagen complexes are often sold by general suppliers. The collagen is a collagen compound and comprises water, collagen, 1, 2-hexanediol and 1, 2-pentanediol, and the purchasing manufacturers of the collagen can be listed as Zhejiang Chongshan organisms.

The collagen of collagen macromolecules hardly enters the surface layer of the skin when in use, but the composition C is used in the invention to realize the effects of repairing skin barriers and tightening the skin, probably because the skin has good humidity after absorbing the components in the composition A and the composition B, the collagen can be better absorbed by the skin, fibronectin in the composition B enters between dermis and epidermis, then the collagen in the composition C enters the dermis and the epidermis to interact to strengthen the connection between the dermis and the epidermis and tighten the skin, and meanwhile, the triple moisturizing effect ensures that the moisture and nutrition in the dermis are required to be transmitted to the epidermis, the cell metabolic activity is improved, a network system with more collagen fibers and proteins is formed in the system, and a better path is provided for macromolecular components to enter the skin.

In order to further increase moisture retention, rhamnose is also included in the component C; the weight ratio of the rhamnose to the cherry blossom extract in the composition C is (0.1-1): 1; preferably, the weight ratio of the rhamnose to the cherry blossom extract in the composition C is (0.3-0.7): 1; further preferably, the weight ratio of rhamnose to the cherry blossom extract in composition C is 0.5:1.

in some embodiments, the component C further comprises a plant extract or a mixture comprising plant extract components. In some embodiments, the component C further comprises a mixture of Calmyang (a component comprising butylene glycol, water, CENTELLA ASIATICA (CENTELLA ASIATICA) extract, polygonum CUSPIDATUM (Polygonum CUSPIDATUM) root extract, scutellaria BAICALENSIS (Scutellaria BAICALENSIS) root extract, camellia SINENSIS (Camellia SINENSIS) leaf extract, glycyrrhiza glabra (Glycyrrhiza glabra) root extract, matricaria CHAMOMILLA (Chamomilla RECUTITA) flower extract, and Rosmarinus OFFICINALIS (Rosmarinus OFFICINALIS) leaf extract); the Calmyang is available from Shanghai Ruima chemical industry. In some embodiments, the weight ratio of the Calmyang to oriental cherry extract in composition C is 1: (2-5); preferably 1: (3.5-4.5).

In a second aspect of the invention, there is provided the use of a cherry blossom repairing and tightening composition for a skin care product.

Preferably, the skin care product has a pH of 5 to 6 (preferably 5.5 to 6).

The skin care product is selected from one or more of toner, moisturizing water, astringent water, solid water, emulsion, patting milk, sunscreen water, essence, cream, eye cream, facial mask, sunscreen cream, BB cream, acne lotion, essential oil and shampoo, wherein the skin care products prepared from the composition A, the composition B and the composition C are the same or different in type.

Preferably, the skin care product containing composition a is applied to the skin, then the skin care product containing composition B is applied to the skin, and finally the skin care product containing composition C is applied to the skin at the time of use.

In some embodiments, the skin care product comprises solid water comprising composition a, essence comprising composition B, and patty milk comprising composition C.

In some embodiments, the solid water comprises 0.01 to 10wt% of composition a, preferably 0.1 to 5wt% of composition a; further preferably, the solid water raw material contains 0.3 to 1wt% of the composition a.

In some embodiments, the solid water comprises, by mass, 0.3 to 1% of the composition a, 0.01 to 0.03% of the chelating agent a, 3.5 to 4.5% of the first humectant a, 0.08 to 0.12% of the first thickener a, 0.3 to 0.5% of the second humectant a, 2 to 3% of the second thickener a, 0.001 to 0.005% of the solubilizer a, and water up to 100%.

In some embodiments the solid water feedstock comprises 0.3 to 0.7wt% of antioxidant a.

The antioxidant A is an antioxidant commonly used in the art and includes, but is not limited to, p-hydroxyacetophenone.

In some embodiments, the solid water comprises 0.0005-0.0015 wt% of essence A, which can be selected according to needs, including but not limited to cherry blossom RLW-1912 of Shanghai Zhen trade.

Chelating agent a is a chelating agent commonly used in the art, including but not limited to disodium EDTA.

The first humectant A is a polyhydric alcohol humectant such as glycerin, 1, 2-hexanediol, etc.

The first thickener A is selected from acrylate, alkyl methacrylate copolymer or its salt, carboxyvinyl polymer or its salt, hydroxypropyl cellulose, alginate, alginic acid polyol ester, polyvinylpyrrolidone, sodium acrylate, carrageenan, carbomer, xanthan gum or their complex. In some embodiments, the first thickener A is an acrylic acid/C10-30 alkanol acrylate crosspolymer, commercially available from Shanghai Chemicals under the trade designation U21.

The second humectant A is a polyhydric alcohol humectant such as glycerin, 1, 2-hexanediol, or the like.

The second thickener a is selected from the group consisting of acrylates, alkyl methacrylate copolymers or salts thereof, carboxyvinyl polymers or salts thereof, hydroxypropylcellulose, alginates, polyol esters of alginic acid, polyvinylpyrrolidone, sodium acrylate, carrageenan, carbomers, xanthan gum or complexes thereof, such as the complex of PEG-240/HDI copolymer bis-decyltetradecyltetradecyltetradecyltehy-20 ether, in some embodiments the components of the complex of PEG-240/HDI copolymer bis-decyltetradecyltetradecyltehylether-20 ether, butylene glycol, water, potassium laurate, tocopherol (vitamin E), commercially available, such as from the shanghai dynasty, chemical model No. GT-730.

The solubilizer A is selected from one or more of PEG-40 hydrogenated castor oil, polyethylene glycol-60 hydrogenated castor oil, polypropylene glycol-26, polyoxypropylene-26-buthanol polyether-26, polyoxypropylene-1-polyethylene glycol-9 lauryl glycol ether, PPG-26-buthanol polyether-26, coco alcohol polyoxyethylene ether-7, tween-20, span 60 or a mixture thereof. In some embodiments, the solubilizer a is a mixture of PPG-26-buthaneth-26, PEG-40 hydrogenated castor oil, water, commercially available, for example, from shanghai, 28156sen chemical, under the trade designation LRI.

In some embodiments, the method for preparing solid water comprises the steps of:

(1) Adding a first thickening agent A into a water phase pot containing water and a chelating agent, soaking and completely wetting, stirring at 25-40 Hz, heating to 80-90 ℃ until the first thickening agent A is dissolved uniformly, and pumping into a main preparation pot;

(2) Then sequentially adding the first humectant A, one polysaccharide in the composition A and the antioxidant A into a main preparation pot at 25-40 Hz, and stirring until the first humectant A, the one polysaccharide in the composition A and the antioxidant A are dissolved uniformly;

(3) Cooling to 40-60 ℃, adding the second thickening agent A into a preparation pot, stirring at 45-60 Hz under the vacuum condition of-0.03-0.05 MPa until the mixture is uniform, and then adding the dissolved amino acid compound in the composition A and the second humectant A into the preparation pot;

(4) Continuously stirring at 25-35 Hz, cooling to below 40 ℃, sequentially adding the rest components in the composition A into a preparation pot, and stirring at 20-30 Hz under the vacuum condition of-0.03 to-0.05 MPa until the components are uniform;

(5) Adding the solubilized solubilizer and the essence into a preparation pot, continuously stirring the mixture to be uniform under the vacuum condition of-0.03 to-0.05 MPa and at the frequency of 20 to 30Hz, taking the materials, detecting, and directly discharging the materials after the materials are qualified.

The solid water in the invention can effectively wrap the components in the composition A, so that mailbox components can be more effectively protected, the solid water can be in a mist shape when in use, the active energy of the released water can deeply supplement water, the skin is touched to condense and lock the skin surface, an internal water active circulation is formed, and the solid-mist-water has unique experience feeling and different water supplementing and locking effects, and meanwhile, the solid water is free of preservatives, pigments and alcohol, so that the use is safer.

In some embodiments, the essence comprises 0.5-15 wt% of composition B; preferably, the essence contains 1-10 wt% of the composition B; further preferably, the essence contains 2 to 6wt% of the composition B.

In some embodiments, the raw materials of the essence comprise, by mass, 2-6% of a composition B, 0.02-0.05% of a chelating agent B, 4-6% of a first moisturizing agent B, 9-11% of a thickening agent B, 0.7-1% of an emulsifying agent B, 5-8% of an emollient B, 0.01-0.03% of a pH adjusting agent B, 1-2% of a second moisturizing agent B, and water to make up to 100%.

In some embodiments, the raw materials of the essence further comprise 0.1-1 wt% of antioxidant B, wherein the antioxidant B comprises, but is not limited to, p-hydroxyacetophenone.

In some embodiments, the raw materials of the essence further comprise 0.01-0.05 wt% of essence B; the essence B includes but is not limited to cherry blossom RLW-1912 purchased from Shanghai Zhen trade.

Chelating agent B is a chelating agent commonly used in the art, including but not limited to disodium EDTA.

The first humectant B is a polyhydric alcohol, such as one or more of glycerol, ethylene glycol, diethylene glycol, butylene glycol and propylene glycol, and in one embodiment, the humectant B is a composition of glycerol and butylene glycol, wherein the weight ratio of the glycerol to the butylene glycol is (2-4): (1.5-2.5).

The thickener B is one or more selected from hydrolyzed sclerotium rolfsii gum, hydroxyethyl cellulose, polyethylene glycol-90M, cetearyl alcohol, xanthan gum, carbomer and fenugreek gum. In some embodiments, the thickener B is a combination of carbomer, hydrolyzed sclerotinia sclerotiorum gum, fenugreek gum; the weight ratio of the carbomer to the hydrolyzed sclerotium rolfsii gum to the fenugreek gum is (0.07-0.12): (0.03-0.07): 10.

the carbomer is purchased from Shanghai Mega chemostat; the hydrolyzed sclerotium rolfsii gum is purchased from Shanghai Jianlai industry; fenugreek gum was purchased from shanghai boshu industries.

The emulsifier B is selected from one or more of PEG-8 caprylic/capric glycerides, coco glucoside/coco alcohol, span-20, span-80, PPG-4-cetyl polyether-20, hydrogenated phosphatidylcholine, egg yolk lecithin, tween-80, tween-20, polyglycerol-6-dioleate, polyglycerol-6-stearate, polyoxyethylene-8-caprylic glycerol and laureth-7 or a mixture containing any one of the above components. In some embodiments, the emulsifier B is a mixture of hydrogenated phosphatidylcholine and Seppic305 (laureth-7, C13-14 isoalkane, polyacrylamide, water); the weight ratio of the hydrogenated phosphatidylcholine to Seppic305 is 1: (0.5-1). The hydrogenated phosphatidylcholine can be purchased from Shanghai Haoyun chemical industry; the Seppic305 is available from shanghai seifof chemical.

The emollient B is one or more selected from squalane, behenyl alcohol, polydimethylsiloxane, hydrogenated polyisobutene, pentaerythritol tetraester, polyethylene glycol-32, polyethylene glycol-8, betaine, trehalose, bis-PEG-18 methyl ether dimethylsilane, squalane, water-soluble olive oil and polyglycerol-10 myristate or a mixture containing the components. In some embodiments, the emollient B is a mixture comprising polyglycerol-10 myristate in combination with polydimethylsiloxane; the weight ratio of the mixture containing polyglycerol-10 myristate to polydimethylsiloxane is 5: (1.5-2.5). The mixture of polyglycerol-10 myristate is commercially available, for example, as sold under the model SELAEA-999 (components including dimethicone/vinyl dimethicone crosspolymer, water, butylene glycol, ethylhexylglycerin, carbomer, arginine, polyglycerol-10 myristate), available from Kogyan, shanghai, industry. The polydimethylsiloxane is available from 5cst, shanghai Dry fly chemical industry.

The pH adjuster B includes, but is not limited to, sodium hydroxide.

The second humectant B is a mixed humectant containing a polyol component; for example, PHL humectant (composed of 1, 3-propylene glycol, 1, 2-hexanediol, caprylyl hydroximic acid) and 301BG humectant (composed of water, butanediol, tremella FUCIFORMIS (Tremella FUCIFORMIS) polysaccharide, sodium hyaluronate, tremella FUCIFORMIS (Tremella FUCIFORMIS) fruiting body extract); the weight ratio of the PHL humectant to the 301BG humectant is (0.2-0.5): 1. the PH L humectant is purchased from Shanghai Haoyun chemical industry; the 301BG moisturizing agent is purchased from Shanghai Yijie.

In some embodiments, the method of preparing the serum comprises the steps of:

(1) Adding carbomer into a water phase pot containing water and the chelating agent B under the stirring of 40-60 Hz, heating to 80-90 ℃ until the carbomer is dissolved uniformly, and pumping into a main preparation pot;

(2) Adding the predispersed raw materials of butanediol and hydrolyzed sclerotium rolfsii gum into a main preparation pot, and then sequentially adding glycerol, fenugreek gum and an antioxidant B into the main preparation pot at 25-35 Hz and stirring until the materials are uniformly dissolved;

(3) Adding hydrogenated phosphatidylcholine into a main preparation pot, quickly stirring to dissolve the hydrogenated phosphatidylcholine uniformly at 40-60 Hz, sequentially adding the emollient B into the preparation pot, vacuumizing to-0.03-0.05mpa, homogenizing at 50-65 Hz for 1-10 min, and stirring at 25-35 Hz for cooling;

(4) Dissolving a pH regulator into a solution with the weight percent of 10 by water, adding the solution into a preparation pot, stirring the solution to be uniform at 25-35 Hz, and then cooling the solution;

(5) Cooling to 35-45 ℃, sequentially adding the rest raw materials into a preparation pot, continuously stirring at 25-35 Hz until the mixture is uniform, taking the materials, detecting, and directly discharging after the materials are qualified.

In some embodiments, the raw material of the patting milk contains 0.5 to 20wt% of composition C; preferably, the raw materials of the patting milk contain 1 to 10 weight percent of the composition C; more preferably, the raw material of the patting milk contains 3 to 6wt% of the composition C.

In some embodiments, the raw materials of the patting milk comprise, by mass fraction, 3 to 6% of the composition C, 0.02 to 0.05% of the chelating agent C, 2 to 3% of the first humectant C, 0.2 to 0.5% of the thickener C, 0.8 to 1.2% of the first emulsifier C, 0.15 to 0.25% of the co-emulsifier C, 2 to 4% of the emollient C, 0.3 to 0.5% of the second emulsifier C, 1 to 2% of the second humectant C, 0.15 to 0.25% of the fiber-drawing agent C, 1.5 to 2.5% of the third humectant C, and water to make up to 100%.

In some embodiments, the raw material of the patting milk further comprises 0.3 to 0.7wt% of a first antioxidant C; the first antioxidant C includes, but is not limited to, p-hydroxyacetophenone.

In some embodiments, the raw material of the beat milk further comprises 0.08 to 0.15wt% of a second antioxidant C; the second antioxidant C includes, but is not limited to, tocopherol acetate; the tocopheryl acetate is purchased from Shanghai autumn-armor commercial trade and is sold under the name VE acetate.

In some embodiments, the raw material of the patting milk further comprises 0.03-0.07 wt% of essence C, such as cherry blossom RLW-1912.

The chelating agent C includes, but is not limited to, disodium EDTA.

The first humectant C is one or more selected from sodium hyaluronate, 1, 3-propylene glycol, glycerol, tremella polysaccharide, butanediol, 1, 2-hexanediol and diethylene glycol or a mixture of the components. In some embodiments, the first humectant C is a combination of 1, 3-propanediol and a mixture of a Tremella-containing polysaccharide component. The weight ratio of the 1, 3-propanediol to the mixture of the components containing the tremella polysaccharide is 2: (0.3 to 0.7); the Tremella polysaccharide-containing mixture is available from Shanghai Yiniao, and is 301BG humectant (composed of water, butanediol, tremella FUCIFORMIS (Tremella FUCIFORMIS) polysaccharide, sodium hyaluronate, and Tremella FUCIFORMIS (Tremella FUCIFORMIS) fruiting body extract).

The thickening agent C is selected from one or more of acrylate, alkyl methacrylate copolymer or salt thereof, carboxyl vinyl polymer or salt thereof, acryloyl dimethyl taurate/VP copolymer, hydroxypropyl cellulose, alginate, polyol ester of alginic acid, polyvinylpyrrolidone, sodium acrylate, carrageenan, carbomer, xanthan gum or a compound thereof. In some embodiments, the thickener C is ammonium acryloyldimethyl taurate/VP copolymer. The acryloyl dimethyl taurate/VP copolymer is purchased from Shanghai Orxue chemical industry and is sold under the name of AVC.

The first emulsifier C is one or more selected from the group consisting of ceteth-6, lecithin (lecithin), acacia gum, soya lecithin (Soya phosphatydilcholine), polyethylene glycol 40 hydrogenated castor oil (Cremophor RH 40), sucrose esters of lauric acid type (LWA-1570), cetearyl alcohol, caprylic/capric polyethylene glycol glycerol ester, polysorbate 80 (Tween 80), olive oil PEG-7 esters, and polyglycerol-3 diisostearate. In some embodiments, the first emulsifier C is cetearyl alcohol, which is available from higher Shanghai.

The auxiliary emulsifier C is one or more selected from glyceryl stearate, C12-18 alkyl glucoside, monoglyceride, hydrogenated phosphatidyl choline, and sodium lactate hydrogenated lecithin. In some embodiments, the co-emulsifier is hydrogenated phosphatidylcholine. Hydrogenated phosphatidylcholine was purchased from Shanghai Haoyun chemical industry.

Emollient C is an emollient commonly used in the art, and in some embodiments, is a component of fermented olive oil and polydimethylsiloxane; the weight ratio of the fermented olive oil to the polydimethylsiloxane is (1.5-2.5): 1. the fermented olive oil (components including Candida beehives/glucose/methyl rapeseed oleate fermentation product, oleyl alcohol, octyldodecanol, butyrospermum PARKII (Butyrrose PARKII) fruit fat, glycine SOJA (Glycine SOJA) sterols, and tocopherol (vitamin E)) is purchased from Shanghai European thawing organism. Polydimethylsiloxane is available from Shanghai Dry fly chemical under the trade name polydimethylsiloxane (100 cst).

The second emulsifier C includes but is not limited to Seppic305 (components including polyacrylamide, C13-14 isoparaffin, laureth-7, water) available from Shanghai Saiful chemical.

The second moisturizer C includes, but is not limited to, a combination of perhexiline (components including water, butylene glycol, CITRUS RETICULATA (CITRUS RETICULATA) fruit extract) and PHL moisturizer (components including 1, 3-propylene glycol, 1, 2-hexanediol, caprylhydroxamic acid) in a weight ratio of (0.2-0.8): 1; PHL moisturizers are available from shanghai haoyun chemical; \24709Funingis available from Shanghai Gajia leaf chemical industry.

The drawing agent C is selected from one or more of polyethylene oxide polymers, egg white powder, sodium polyacrylate and polyethylene glycol-90M. In some embodiments, the wiredrawing agent C is polyethylene glycol-90M. The polyethylene glycol-90M is purchased from Shanghai Dry fly chemical industry and sold under the brand number WSR301.

The third humectant C is a polyhydric alcohol humectant including, but not limited to, 1, 3-propylene glycol.

In some embodiments, the method for preparing the patting milk comprises the following steps:

(1) Adding the thickener C into a main preparation pot containing water and a chelating agent C under the condition of rapid stirring at 45-60 Hz, heating to 80-90 ℃ until the mixture is dissolved uniformly, and then sequentially adding the rhamnose, the first humectant C, the first antioxidant C and the thickener C in the composition C into the main preparation pot at 25-35 Hz and stirring until the mixture is dissolved uniformly;

(2) Adding a first emulsifier C into a main preparation pot, quickly stirring at 45-60 Hz until the first emulsifier C is uniformly dissolved, then sequentially adding a co-emulsifier C, an emollient C, a first antioxidant C and a second emulsifier C into the preparation pot, vacuumizing to-0.03-0.05mpa, homogenizing at 50-70 Hz for 1-10 min, and then stirring at 25-35 Hz for cooling;

(3) Cooling to 35-45 ℃, sequentially adding the components in the rest component C, the second humectant C and the essence C into a preparation pot, and stirring uniformly at 25-35 Hz;

(4) Pre-dispersing the wire drawing agent C and the third humectant C at normal temperature, slowly stirring with water until the materials are uniformly dissolved, adding the materials into a preparation pot, continuously stirring at 15-25 Hz until the materials are uniformly dissolved, taking the materials, detecting, and directly discharging the materials after the materials are qualified.

Wherein, the patting milk can draw and explode water mist, and meanwhile, the components in the patting milk can supplement collagen and tighten skin.

The invention has the following conception and beneficial effects:

the composition A has good moisturizing performance, and after the skin absorbs the active ingredients of the composition A, the skin water content is improved, and the metabolism of epidermal cells is increased; then, when the product containing the composition B is used, the components in the composition B can better enter the skin to play a role in repairing the skin barrier, and meanwhile, the moisturizing effect is further improved; finally, the product containing composition C is reused, thus achieving a firmer effect on the skin to be repaired and a more comprehensive protection. Namely, the composition A has good water replenishing and locking effects, which are beneficial to the absorption of active ingredients in the composition B, and then the composition C can be used for replenishing collagen better and locking nutritional active ingredients at the same time, so that the aims of strengthening the barrier function of the stratum corneum and moisturizing and refining the skin are fulfilled.

Detailed Description

Example 1

In a first aspect of this embodiment, a cherry blossom repairing and tightening composition is provided, comprising composition a, composition B, composition C;

the composition A comprises oriental cherry extract, amino acid compounds and polysaccharide;

the weight ratio of the oriental cherry extract to the amino acid compounds in the composition A is 1:0.5;

the weight ratio of the polysaccharide to the amino acid compound is 4:1;

the amino acid compound is arginine (purchased from Shanghai Yaolan trade);

the polysaccharides include proteoglycan (purchased from golden marigold) and rhamnose (purchased from sea-holding organisms);

the weight ratio of the proteoglycan to the rhamnose is 1:1;

the composition B comprises oriental cherry extract, turmeric gel and macromolecular sugar-egg complex;

the weight ratio of the oriental cherry extract to the turmeric gel in the composition B is 1.5:1;

the weight ratio of the polymer sugar egg compound to the turmeric gel is 1.5:1;

active main ingredient of Curcuma rhizome gel (obtained from Shanghai Hayata) comprises Curcuma rhizome (Curcuma LONGA) root extract, lactobacillus fermentation product;

the macromolecular glycoprotein complex is a composition of marine glycoprotein (purchased from Shanghai Jinluo biology) and fibronectin (Shanghai Moire biology);

the weight ratio of the marine glycoprotein to fibronectin is 0.5:1;

the composition C comprises oriental cherry extract, collagen, rhamnose, calmyang (obtained from Shanghai Ruima chemical industry, and comprises butylene glycol, water, herba Centellae (CENTELLA ASIATICA) extract, rhizoma Polygoni Cuspidati (Polygonum CUSPIDATUM) root extract, radix Scutellariae (Scutellaria BAICALENSIS) root extract, folium Camelliae SINENSIS (Camellia SINENSIS) extract, radix Glycyrrhizae (Glycyrrhiza GLABRA) root extract, flos Matricariae Chamomillae (Chamomilla RECUTITA) flower extract, and herba Rosmarini OFFICINALIS (Rosmarinus OFFICINALIS) leaf extract);

the weight ratio of the oriental cherry extract to the collagen in the composition C is 2:1;

the weight ratio of rhamnose to the cherry blossom extract in composition C is 0.5:1;

the weight ratio of the Calmyang to the cherry extract in composition C was 1:4;

the oriental cherry extract is purchased from Shanghai Zhen trade;

a second aspect of the present embodiment provides a skin care product, which comprises solid water containing composition a, essence containing composition B, and pat milk containing composition C;

the solid water comprises raw materials, by mass, 0.7% of a composition A, 0.02% of a chelating agent A (disodium EDTA), 4% of a first humectant A (1, 3-propylene glycol), 0.1% of a first thickener A (acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, which is purchased from Shanghai Mega chemical engineering and has a sale mark of U21), 0.5% of an antioxidant A (p-hydroxyacetophenone), 0.4% of a second humectant A (1, 2-hexanediol), 2.5% of a second thickener A (GT-730 and has a sale mark of LRI), 2.5% of a PPG-26-butanol polyether-26, PEG-40 hydrogenated castor oil and water, which are purchased from Shanghai 28156sen chemical engineering and has a sale mark of LRI, 0.003% of essence, and water which is supplemented to 100%;

the preparation method of the solid water comprises the following steps:

(1) Adding the first thickening agent A into a water phase pot containing water and a chelating agent, soaking and completely wetting, stirring at 30Hz, heating to 85 ℃ until the first thickening agent A is dissolved uniformly, and pumping into a main preparation pot;

(2) Then sequentially adding the first humectant A, rhamnose and the antioxidant A into a main preparation pot at 30Hz, and stirring until the first humectant A, the rhamnose and the antioxidant A are dissolved uniformly;

(3) Cooling to 50 ℃, adding the second thickening agent A into the preparation pot, stirring under-0.04 MPa vacuum and 50Hz until the mixture is uniform, and then adding the dissolved arginine and the second humectant A into the preparation pot;

(4) Continuously stirring at 30Hz, cooling to below 40 ℃, sequentially adding the rest components in the composition A into a preparation pot, and stirring at 25Hz under the vacuum condition of-0.04 MPa until the mixture is uniform;

(5) Adding the solubilized solubilizer and essence into a preparation pot, continuously stirring under-0.04 MPa vacuum condition at 25Hz until the mixture is uniform, taking the materials, detecting, and directly discharging after the materials are qualified;

according to a method for measuring GB T13531.1-2008pH, the pH value of the solid water is 5.83 through a pH meter test;

the raw materials of the essence comprise, by mass, 4% of composition B, 0.03% of chelating agent B (disodium EDTA), 5% of a first humectant B (a combination of glycerol and butylene glycol, in a weight ratio of 3: 2), 10.15% of a thickener B (a combination of carbomer, hydrolyzed sclerotium rolfsii and fenugreek gum, in a weight ratio of 0.1;

the preparation method of the essence comprises the following steps of:

(1) Adding carbomer into a water phase pot containing water and disodium EDTA under stirring at 50Hz, heating to 85 deg.C for dissolving, and pumping into a main preparation pot;

(2) Adding the predispersed raw materials of butanediol and hydrolyzed sclerotium rolfsii gum into a main preparation pot, sequentially adding glycerol, fenugreek gum and p-hydroxyacetophenone into the main preparation pot for 30Hz stirring until the materials are uniformly dissolved;

(3) Adding hydrogenated phosphatidylcholine into a main preparation pot, rapidly stirring at 50Hz until the hydrogenated phosphatidylcholine and the Seppic305 are dissolved uniformly, sequentially adding the hydrogenated phosphatidylcholine and the Seppic305 into the preparation pot, vacuumizing to-0.04mpa, homogenizing at 60Hz for 5min, and stirring at 30Hz for cooling;

(4) Dissolving sodium hydroxide into 10wt% solution with water, adding into a preparation pot, stirring at 30Hz until the solution is uniform, and cooling;

(5) Cooling to 40 ℃, sequentially adding the rest raw materials into a preparation pot, continuously stirring at 30Hz until the mixture is uniform, taking the materials, detecting, and directly discharging after the materials are qualified;

according to a determination method of GB T13531.1-2008pH, the pH value of the essence is 5.72 through a pH meter test.

A third aspect of this embodiment provides a method of using the skin care product described above: the solid water containing the composition A is firstly applied to the skin, then the essence containing the composition B is applied to the skin, and finally the patting milk containing the composition C is applied to the skin.

Example 2

the composition A comprises a cherry blossom extract, an amino acid compound and polysaccharide;

the weight ratio of the oriental cherry extract to the amino acid compounds in the composition A is 1:0.4;

the weight ratio of the polysaccharide to the amino acid compound is 5:1;

the amino acid compound is arginine (purchased from Shanghai Yaolan trade);

the weight ratio of the proteoglycan to the rhamnose is 1:0.8;

the composition B comprises oriental cherry extract, turmeric gel and macromolecular sugar egg compound;

the weight ratio of the oriental cherry extract to the turmeric gel in the composition B is 1.2:1;

the weight ratio of the polymer sugar egg compound to the turmeric gel is 1:1;

the weight ratio of the marine glycoprotein to fibronectin is 0.4:1;

said composition C comprises cherry blossom extract, collagen, rhamnose, calmyang (available from Shanghai Rimu chemical industry, and comprises butylene glycol, water, CENTELLA ASIATICA (CENTELLA ASIATICA) extract, polygonum CUSPIDATUM (Polygonum CUSPIDATUM) root extract, scutellaria BAICALENSIS (Scutellaria BAICALENSIS) root extract, camellia SINENSIS (Camellia SINENSIS) leaf extract, glycyrrhiza GLABRA (Glycyrrhiza GLABRA) root extract, chamomilla RECUTITA (Chamomilla RECUTITA) flower extract, and Rosmarinus OFFICINALIS (Rosmarinus OFFICINALIS) leaf extract);

the weight ratio of the oriental cherry extract to the collagen in the composition C is 1.5:1;

the weight ratio of rhamnose to the oriental cherry extract in the composition C is 0.7:1;

the weight ratio of the Calmyang to the oriental cherry extract in the composition C is 1:4;

the oriental cherry extract is purchased from Shanghai Zhen trade;

a second aspect of this example provides a skin care product comprising solid water comprising composition a, a serum comprising composition B, a patting milk comprising composition C;

the raw materials of the solid water comprise, by mass, 0.52% of a composition A, 0.01% of a chelating agent A (disodium EDTA), 3.5% of a first humectant A (1, 3-propylene glycol), 0.3% of a first thickener A (acrylic acid (acrylate)/C10-30 alkanol acrylate cross-linked polymer which is purchased from Shanghai Mega Chemicals and has a sale mark of U21), 0.08% of a first humectant A (p-hydroxyacetophenone), 0.3% of a second humectant A (1, 2-hexanediol), 2% of a second thickener A (GT-730 and has a sale mark of Shanghai Mega Chemicals), 2% of a solubilizer A (PPG-26-butanol polyether-26, PEG-40 hydrogenated castor oil and water which are purchased from Shanghai 28156sen chemical and has a sale mark of LRI), 0.001% of essence and water which are supplemented to 100%;

the preparation method of the solid water comprises the following steps:

(1) Adding the first thickening agent A into a water phase pot containing water and a chelating agent, soaking and completely wetting, stirring at 25Hz, heating to 90 ℃ until the first thickening agent A is dissolved uniformly, and pumping into a main preparation pot;

(2) Then sequentially adding the first humectant A, rhamnose and the antioxidant A into a main preparation pot, and stirring until the components are dissolved uniformly at 30 Hz;

(3) Cooling to 40 ℃, adding the second thickening agent A into the preparation pot, stirring under-0.05 MPa vacuum at 60Hz until the mixture is uniform, and then adding the dissolved arginine and the second humectant A into the preparation pot;

(4) Continuing to stir at 30Hz and cool to below 40 ℃, sequentially adding the rest components in the composition A into a preparation pot, and stirring at 20Hz to be uniform under the vacuum condition of-0.05 MPa;

(5) Adding the solubilized solubilizer and essence into a preparation pot, continuously stirring under-0.05 MPa vacuum condition and 20Hz to be uniform, taking materials, detecting, and directly discharging after qualification;

the raw materials of the essence include, in parts by weight, 3.2% of composition B, 0.02% of chelating agent B (disodium EDTA), 4% of a first humectant B (2% by weight of glycerin and butylene glycol, a combination of 2% by weight of glycerin and butylene glycol), 10% of a thickener B (a combination of carbomer, hydrolyzed sclerotium rolfsii gum, and fenugreek gum, a combination of 0.07% by weight of carbomer, 0.03: 10% by weight of carbomer, 0.3% by weight of hydrolyzed sclerotium rolfsii gum, 10.1% by weight of fenugreek gum, 0.3% of antioxidant B (acetophenone), 0.7% of emulsifier B (a combination of hydrogenated phosphatidylcholine and Seppic305, 1.75% by weight of hydrogenated phosphatidylcholine, 1% by weight of sepium, 305 from sepium, 0.7% by weight of cipic humectant B, 0.7% by weight of humectant B (a combination of mixture of polyglycerol-10 myristate and dimethicone, a combination of 5.5% by weight of dimethicone, 5% by weight of dimethicone, 0.5% by weight of acacia, 5% by weight of dimethicone, 0.01% by weight of acacia seudnervosa, 0% by weight of dimethicone, 1% by weight of acacia, 0.01% by weight of silicone, 1% by weight of seudura No. 5, 301% by weight of a mixture, 5% by weight of acacia seudura, 0.01% by weight of acacia seudura, 0.5, and 1% by weight of dimethicone, 0.01% by weight of dimethicone, and 1% by weight of a humectant B, and 1% by weight of dimethicone, and 1.5% by weight of dimethicone, 301% by weight of a mixture of dimethicone, commercially available from seiko, and 1% by weight of acacia sei, and 1.01% by weight of sakura, 0.3, and 1.3% by weight of silicone;

the preparation method of the essence comprises the following steps:

(1) Adding carbomer into a water phase pot containing water and EDTA disodium under stirring at 40Hz, heating to 90 deg.C for dissolving, and pumping into a main preparation pot;

(2) Adding the predispersed raw materials of butanediol and hydrolyzed sclerotium rolfsii gum into a main preparation pot, sequentially adding glycerol, fenugreek gum and p-hydroxyacetophenone into the main preparation pot at 25Hz, and stirring until the materials are uniformly dissolved;

(3) Adding hydrogenated phosphatidylcholine into a main preparation pot, rapidly stirring at 40Hz until the hydrogenated phosphatidylcholine is uniformly dissolved, sequentially adding the hydrogenated phosphatidylcholine and Seppic305 into the preparation pot, vacuumizing to-0.05mpa, homogenizing at 50Hz for 7min, and stirring at 25Hz for cooling;

(4) Dissolving sodium hydroxide into 10wt% solution with water, adding into a preparation pot, stirring at 25Hz until the solution is uniform, and cooling;

(5) Cooling to 40 ℃, sequentially adding the rest raw materials into a preparation pot, continuously stirring to be uniform at 25Hz, taking materials, detecting, and directly discharging after the materials are qualified;

the raw materials of the pat milk comprise, by mass, 3.7% of a composition C, 0.02% of a chelating agent C (disodium EDTA), 2.3% of a first humectant C (a combination of 1, 3-propylene glycol and 301BG in a weight ratio of 2: 0.3 301bg from shanghai creature), 0.4% of a first antioxidant C (p-hydroxyacetophenone), 0.8% of a thickener C (an ammonium acryloyldimethyl taurate/VP copolymer, available from shanghai snow chemical, sold under the model AVC), 0.2% of a first emulsifier C (cetearyl alcohol, available from shanghai zhen trade), 0.15% of a co-emulsifier C (hydrogenated phosphatidylcholine, available from shanghai haoton chemical), 0.15% of an emollient C (a combination of fermented olive oil and polydimethylsiloxane in a weight ratio of 1.5: polydimethylsiloxane is purchased from Shanghai dry flying chemical industry with the sale name of polydimethylsiloxane (100 cst)) 2.5%, second antioxidant C (prochloraz, shanghai Bauzyan commercial trade with the sale name of VE acetate) 0.08%, second emulsifier C (Seppic 305, from Shanghai Saifu chemical industry) 0.4%, second humectant C (a combination of PHL humectant and 24709funinin, the weight ratio of the PHL humectant is 0.25 Supplementing water to 100%;

the preparation method of the patting milk comprises the following steps:

(1) Adding the thickener C into a main preparation pot containing water and a chelating agent C under rapid 45Hz stirring, heating to 80 ℃ until the mixture is dissolved uniformly, and then sequentially adding the rhamnose, the first humectant C, the first antioxidant C and the thickener C in the composition C into the main preparation pot for 25Hz stirring until the mixture is dissolved uniformly;

(2) Adding a first emulsifier C into a main preparation pot, rapidly stirring at 45Hz until the first emulsifier C is dissolved uniformly, then sequentially adding a co-emulsifier C, an emollient C, a first antioxidant C and a second emulsifier C into the preparation pot, vacuumizing to-0.05mpa, homogenizing at 50Hz for 3min, and then stirring at 25Hz for cooling;

(3) Cooling to 40 ℃, sequentially adding the components in the rest component C, the second humectant C and the essence C into a preparation pot, and stirring uniformly at 25 Hz;

(4) Pre-dispersing the wire drawing agent C and the third humectant C at normal temperature, slowly stirring with water until the materials are dissolved uniformly, adding into a preparation pot, continuously stirring at 15Hz until the materials are dissolved uniformly, taking the materials for detection, and directly discharging the materials after the materials are qualified.

A third aspect of this embodiment provides a method of using the above skin care product: applying the solid water containing the composition A to the skin, applying the essence containing the composition B to the skin, and applying the patted milk containing the composition C to the skin.

Example 3

In a first aspect of this embodiment, there is provided a cherry blossom repairing and tightening composition comprising composition a, composition B, composition C;

the weight ratio of the oriental cherry extract to the amino acid compounds in the composition A is 1:0.7 of the total weight of the mixture;

the weight ratio of the polysaccharide to the amino acid compound is 3:1;

the amino acid compound is arginine (purchased from Shanghai Yao lan trade);

the polysaccharides include proteoglycan (from Shanghai Jinluo organism) and rhamnose (from Shanghai Hayata);

the weight ratio of the proteoglycan to the rhamnose is 1:1;

the weight ratio of the oriental cherry extract to the turmeric gel in the composition B is 1.8:1;

the weight ratio of the macromolecular sugar-egg compound to the turmeric gel is 2:1;

the active main ingredients of Curcuma rhizome gel (purchased from Shanghai Hayata) comprise Curcuma rhizome (Curcuma LONGA) root extract, and lactobacillus fermentation product;

the weight ratio of the marine glycoprotein to fibronectin is 0.6:1;

the oriental cherry extract is purchased from shanghai zhen trade;

in some embodiments, the solid water raw material comprises, in parts by mass, composition a0.95%, chelating agent a (as disodium EDTA) 0.03%, first humectant a (as 1, 3-propanediol) 4.5%, first thickener a (acrylates/C10-30 alkanol acrylate crosspolymer, available from shanghai chemostat, sales brand U21) 0.12%, antioxidant a (as p-hydroxyacetophenone) 0.7%, second humectant a (1, 2-hexanediol) 0.5%, second thickener a (GT-730, available from shanghai chemostat) 3%, solubilizing agent a (as PPG-26-butanolpolyether-26, PEG-40 hydrogenated castor oil, water mixture, available from shanghai 28156565630, sales brand LRI) 0.005%, perfume 0.0015%, water make-up to 100%.

The preparation method of the solid water comprises the following steps:

(1) Adding the first thickening agent A into a water phase pot containing water and a chelating agent, soaking and completely wetting, stirring at 40Hz, heating to 80 ℃ until the first thickening agent A is dissolved uniformly, and pumping into a main preparation pot;

(2) Then sequentially adding the first humectant A, rhamnose and the antioxidant A into a main preparation pot, and stirring until the first humectant A, the rhamnose and the antioxidant A are dissolved uniformly;

(3) Cooling to 60 ℃, adding the second thickening agent A into the preparation pot, stirring under-0.03 MPa vacuum and at 45Hz until the mixture is uniform, and then adding the dissolved arginine and the second humectant A into the preparation pot;

(4) Continuously stirring at 35Hz, cooling to below 40 ℃, sequentially adding the rest components in the composition A into a preparation pot, and stirring at 20Hz under the vacuum condition of-0.03 MPa until the components are uniform;

(5) Adding the solubilized solubilizer and essence into a preparation pot, continuously stirring under-0.03 MPa and vacuum at 20Hz until the mixture is uniform, taking the materials, detecting, and directly discharging the materials after the materials are qualified;

the essence comprises the following raw materials, by mass, 5.76% of a composition B, 0.05% of a chelating agent B (disodium EDTA), 5.5% of a first humectant B (a combination of glycerol and butanediol, wherein the weight ratio is 3.5), 0.07: 10% of a thickening agent B (a combination of carbomer, hydrolyzed sclerotium rolfsii gum and fenugreek gum, wherein the carbomer is purchased from Shanghai Minghai Chemicals, and the weight ratio of carbomer to fenugreek gum is 0.12: hydrolyzed sclerotium rolfsii gum is obtained from Shanghai Jianlai, fenugreek gum is obtained from Shanghai Boehao, 10.19%, antioxidant B (p-hydroxyacetophenone) 0.5%, emulsifier B (a combination of hydrogenated phosphatidylcholine and Seppic305, in a weight ratio of 1;

the preparation method of the essence comprises the following steps:

(1) Adding carbomer into a water phase pot containing water and disodium EDTA under stirring at 60Hz, heating to 80 deg.C for dissolving, and pumping into a main preparation pot;

(2) Adding the predispersed raw materials of butanediol and hydrolyzed sclerotium rolfsii gum into a main preparation pot, sequentially adding glycerol, fenugreek gum and p-hydroxyacetophenone into the main preparation pot at 35Hz, and stirring until the materials are uniformly dissolved;

(3) Adding hydrogenated phosphatidylcholine into a main preparation pot, rapidly stirring at 60Hz until the hydrogenated phosphatidylcholine is uniformly dissolved, sequentially adding the hydrogenated phosphatidylcholine and Seppic305 into the preparation pot, vacuumizing to-0.03mpa, homogenizing at 65Hz for 3min, and stirring at 35Hz for cooling;

(4) Dissolving sodium hydroxide into 10wt% solution with water, adding into a preparation pot, stirring at 35Hz until the solution is uniform, and cooling;

(5) Cooling to 40 ℃, sequentially adding the rest raw materials into a preparation pot, continuously stirring to be uniform at 35Hz, taking materials, detecting, and directly discharging after the materials are qualified;

the raw materials of the pat milk comprise, by mass, 5.4% of a composition C, 0.02% of a chelating agent C (disodium EDTA), 2.97% of a first humectant C (a combination of 1, 3-propylene glycol and 301BG, the weight ratio of which is 2: 0.7 and 301BG obtained from Haichai Haichao Heiyao), 0.7% of a first antioxidant C (p-hydroxyacetophenone), 0.5% of a thickener C (an ammonium acryloyldimethyltaurate/VP copolymer obtained from Haichao Seisakusho chemical, the sale model of which is AVC), 0.5% of a first emulsifier C (cetearyl alcohol obtained from Shanghai commerce), 1.2% of a co-emulsifier C (hydrogenated phosphatidylcholine obtained from Haichao Cishi chemical), 0.5% of a skin moisturizing agent C (a combination of fermented olive oil and polydimethylsiloxane, the weight ratio of which is 2.5, 1, and the fermented olive oil obtained from European thawing biological material in Shanghai Haichia; polydimethylsiloxane is purchased from Shanghai dry fly chemical industry and sold under the name of polydimethylsiloxane (100 cst)) 3.75%, second antioxidant C (tocopherol acetate, sold under the name of VE acetate) 0.15%, second emulsifier C (Seppic 305, sold under the name of Shanghai Saifu chemical industry) 0.5%, second humectant C (a combination of PHL humectant and 24709funinin, the weight ratio of the PHL humectant is 0.8 Supplementing water to 100%;

the preparation method of the patting milk comprises the following steps:

(1) Adding the thickener C into a main preparation pot containing water and a chelating agent C under rapid 60Hz stirring, heating to 90 ℃ until the mixture is dissolved uniformly, and then sequentially adding the rhamnose, the first humectant C, the first antioxidant C and the thickener C in the composition C into the main preparation pot for 35Hz stirring until the mixture is dissolved uniformly;

(2) Adding a first emulsifier C into a main preparation pot, rapidly stirring at 60Hz until the first emulsifier C is dissolved uniformly, then sequentially adding a co-emulsifier C, an emollient C, a first antioxidant C and a second emulsifier C into the preparation pot, vacuumizing to 0.03mpa, homogenizing at 70Hz for 5min, and then stirring at 35Hz for cooling;

(3) Cooling to 45 ℃, sequentially adding the components in the rest component C, the second humectant C and the essence C into a preparation pot, and stirring uniformly at 35 Hz;

(4) Pre-dispersing the wire drawing agent C and the third humectant C at normal temperature, slowly stirring with water until the materials are uniformly dissolved, adding the materials into a preparation pot, continuously stirring at 25Hz until the materials are uniformly dissolved, taking the materials, detecting, and directly discharging the materials after the materials are qualified.

A third aspect of this embodiment provides a method of using the skin care product described above: applying the solid water containing the composition A to the skin, applying the essence containing the composition B to the skin, and applying the patted milk containing the composition C to the skin.

Example 4

In a first aspect of this example, a cherry blossom repairing and tightening composition is provided, which is embodied in the same manner as in example 1, except that composition B is free of cherry blossom extract.

In a second aspect, this example provides a skin care product comprising solid water containing composition a, a serum containing composition B, and a patting milk containing composition C, as described in example 1.

Example 5

In a first aspect, this example provides a cherry blossom repairing and firming composition, which is similar to that of example 1, except that composition B is free of the polymeric glycocalyx, composition a is free of the polysaccharide, and composition C is free of the rhamnose.

According to a second aspect of the present example, a skin care product is provided, which comprises solid water containing composition a, essence containing composition B, and pat milk containing composition C, and is specifically implemented in the same manner as in example 1.

Example 6

In a first aspect of this embodiment, a cherry blossom repairing and tightening composition is provided, which is similar to that in embodiment 1, except that the weight ratio of the polymer-egg complex to the turmeric gel is 4:1.

the second aspect of this embodiment provides a skin care product, which includes solid water containing composition a, essence containing composition B, and pat milk containing composition C, and the specific implementation manner of this embodiment is the same as that in embodiment 1, except that the mass percentage of composition B in the essence is 12%.

Performance testing

1. And (3) stability testing: the skin care products provided in examples 1 to 6 were used as samples for stability testing:

(1) And (3) testing heat resistance: putting the sample into a constant-temperature incubator at the temperature of (50 +/-1) DEG C for 24h, and observing whether phenomena such as thinning, discoloration, layering, precipitation change and the like exist after the temperature is recovered to the room temperature;

(2) Cold resistance test: the skin care product is put into a refrigerator with the temperature of minus 5 to minus 10 +/-1 ℃ for 24 hours, and the phenomena of thinning, discoloration, layering, precipitation change and the like are observed after the room temperature is recovered.

Evaluation criteria: grading is carried out according to the phenomena of thinning, color change, layering, precipitation change and the like of the sample before and after the test, and the grading is totally 0-4 grades, wherein the 0 grade is no thinning, color change, layering and precipitation change, the 1 grade is slight thinning, color change, layering and precipitation change, the 2 grade is color change and thinning phenomenon increase, layering phenomenon is avoided, a small amount of precipitation is generated, the 3 grade is slight layering phenomenon, the precipitation is obviously increased, and the 4 grade is obvious layering and precipitation change.

2. The obtained essence is smeared on the back of hand uniformly (smearing area is about 4 square centimeters), and after 3min, whether yellow discoloration exists or not is observed.

The test results are shown in table 1:

TABLE 1

3. The moisture content of the horny layer of the skin, the water loss rate of the epidermis and the elasticity of the skin are tested: the efficacy of the samples for repair, moisturization, firming, etc. was verified by measuring the stratum corneum moisture content, the trans-epidermal moisture loss rate, the skin elasticity of 31 sensitive muscle female subjects before and after the samples were tested using example 1, and by analyzing the skin color (red-green) value a x value, etc.

Wherein, (1) the sample application method is as follows:

(2) Subject information is as follows:

sex of the subject	Female with a pattern of holes
		Age of subject	18-40
Number of subjects included in the population	35
		Number of persons who failed to complete the test	4*
Data analysis of effective number of persons	31

Remarking: * 7. Subjects 13, 26, and 31 were withdrawn from the test for personal reasons.

Subject inclusion and exclusion criteria were as follows:

and (3) inclusion standard:

female subjects, age 18-40 years;

subjects were a sensitive skin population (as per D0 lactic acid sting results) with facial skin satisfying TEWL simultaneously>15g/h/m ² Moisture content of stratum corneum<60a.u.(D0)；

Patients without severe systemic disease, immunodeficiency or autoimmune disease, the subject site has not received skin treatment, cosmetic and other tests that may affect outcome;

those with inactive allergic disease;

hormone drugs and immunosuppressants have not been used in the last month;

the tested part does not participate in other clinical testers at present or in the near 30 days;

can be matched with testers well;

all contents of the informed consent can be read and understood, and the informed consent can be voluntarily signed;

only the indicated skin care products were used during the test;

during the test period, the use of any cosmetics, drugs and health products having an influence on the results was not agreed.

Exclusion criteria:

all conditions that must be excluded from the study

The facial skin diseases may affect the judgment of the test result;

those with high allergic constitution;

those with a history of cosmetic allergy;

a female who is pregnant, lactating, or intended to be pregnant during the test;

severe center of gravity, liver and kidney function damage and severe immunologic hypofunction;

those with mental disorders, severe endocrine disorders, and oral contraceptives;

patients with significant malnutrition

The drug clinical testers or other testers are involved in 31 days, or the drug which has influence on the test result is systematically used in nearly 1 week;

those who had oral and topical cosmetic products within 2 weeks that may have an effect on the outcome of the test;

the test person can not be matched;

the investigator considered not appropriate for attending the investigator.

(3) The test conditions were as follows: and (3) controlling the test environment condition in the whole test process: temperature 20-22 ℃, humidity: 40-60% RH.

(4) The instrument measurement parameters and related equipment are as follows:

(5) The data statistics method is as follows:

descriptive statistics:

the mean, standard deviation, maximum, minimum, median of each parameter of the skin at each time point was calculated.

Normal distribution test:

and (3) carrying out normal distribution test on the average value, wherein the progressive significance (bilateral) value of the normal test is greater than 0.050, and then the series of data obeys normal distribution.

And (3) differential analysis:

performing difference analysis on the average value, and when the two groups of data are normally distributed at the same time, analyzing the difference between the two groups of data by using a paired T test; when the two sets of data are not normally distributed at the same time, the difference between the two sets of data is analyzed using a rank sum test.

And (4) judging the standard:

(ii) if the statistical significance level p <0.050 indicates that the subject is statistically significantly different before and after sample administration;

if the statistical significance level p.gtoreq.0.050, the subject is prompted to have no statistically significant difference before and after sample use.

(6) And (3) judging standard:

(1) moisture retention efficacy determination indexes:

compared with the samples before use, the moisture content of the horny layer of the skin is remarkably increased (p is less than 0.050) or the water loss rate of the skin per epidermis is remarkably reduced (p is less than 0.050) after the samples are used, and the samples have the moisturizing effect.

(2) Judging indexes of repair efficacy:

compared with the sample before use, the transepidermal water loss rate of the skin after the sample is used is remarkably reduced (p is less than 0.050), and the sample has the repairing effect. Can be matched with skin color (red-green) value a to show significant reduction (p < 0.050).

(3) The compact efficacy determination index is as follows:

the skin elasticity R2 or F3/F4 was significantly increased (p < 0.050) after the sample was used compared to before the sample was used, indicating that the sample had a firming effect.

The skin tightening parameter F4 was significantly reduced after sample application (p < 0.050) compared to before sample application, indicating that the sample has a tightening effect.

(the change result of any parameter in the related parameters is obviously different (p < 0.050), the sample is determined to have corresponding efficacy)

(7) Testing;

before use of the sample:

(1) inclusion: volunteer subjects were enrolled as required and signed written informed consent. Carrying out lactic acid sting test before entering the group, and inquiring the subject about a series of problems such as disease history and health condition according to the selection and exclusion criteria;

(2) clean face and wait: subjects cleanse their face and dry their skin with dry facial tissue, sit still for 30 minutes in a laboratory at a temperature of 21 ± 1 ℃,50 ± 10% rh;

(3) and (3) testing: testing the skin percutaneous water loss rate, the stratum corneum water content and the skin elasticity of a test subject by a laboratory technician, and acquiring an image by using Visia-CR;

(4) product distribution and instructions: the laboratory technician instructs the subject on the product, dispatches the test product and provides written instructions and a log of use of the product.

After 14 days using the samples:

(1) clean face and wait: the subjects cleansed their face and dried their skin with dry facial tissue, sitting still for 30 minutes in a laboratory at a temperature of 21 + -1 deg.C, 50 + -10% RH;

(2) and (3) testing: testing the skin percutaneous water loss rate, the stratum corneum water content and the skin elasticity of a subject by a laboratory technician, and acquiring an image by using Visia-CR; the subjects filled out a self-assessment questionnaire.

After 28 days using the sample:

(2) and (3) testing: testing the skin percutaneous water loss rate, the stratum corneum water content and the skin elasticity of a test subject by a laboratory technician, and acquiring an image by using Visia-CR; the subjects filled out a self-assessment questionnaire.

(3) And (5) recovering the product.

The test results are shown in Table 2.

TABLE 2

In addition, the subjects used the example 1 product self-assessment method as follows:

the feeling after using the sample was evaluated by means of questionnaire after using the sample for 14 days and 28 days:

the satisfaction calculation method is as follows:

after 28 days of continuous use of the sample of example 1, the overall satisfaction with the product was 67.7% for 31 subjects.

According to the tests, the test sample has moisturizing, repairing and tightening effects after being used for 28 days.

Claims

1. A cherry blossom repairing and tightening composition is characterized by comprising a composition A, a composition B and a composition C; the composition A comprises oriental cherry extract and amino acid compounds; the composition B comprises oriental cherry extract and turmeric gel; the composition C comprises oriental cherry extract and collagen.

2. The oriental cherry repairing and tightening composition according to claim 1, wherein the oriental cherry extract and the amino acid compound are present in the composition A in a weight ratio of 1: (0.1 to 1); the amino acid compound is selected from one or more of lysine, tryptophan, arginine, phenylalanine, threonine, leucine, valine and cystine.

3. The oriental cherry repairing and tightening composition according to claim 1 or 2, wherein the composition A further comprises a polysaccharide, and the weight ratio of the polysaccharide to the amino acid compound is (3-5): 1.

4. the oriental cherry repairing and tightening composition of claim 3, wherein the polysaccharide comprises a soluble proteoglycan or a complex thereof.

5. The oriental cherry repairing and tightening composition of claim 1, wherein the composition B further comprises a macromolecular sugar-egg complex.

6. The oriental cherry repairing and tightening composition as claimed in claim 5, wherein the macromolecular glycoprotein complex is a combination of a marine glycoprotein and fibronectin.

7. The oriental cherry repairing and tightening composition as claimed in claim 1, wherein the oriental cherry extract and the collagen in the composition C are in a weight ratio of (0.5-5): 1.

8. use of a cherry blossom repairing and tightening composition according to any one of claims 1 to 7, wherein the cherry blossom repairing and tightening composition is used in a skin care product.

9. The use of the oriental cherry nourishing and tightening composition according to claim 8, characterized in that the skin care product has a pH of from 5 to 6.

10. The use of the oriental cherry repairing and tightening composition according to claim 8 or 9, wherein the skin care product is selected from one or more of toner, moisturizing lotion, astringent lotion, solid water, lotion, patting lotion, sunscreen lotion, essence, cream, eye cream, mask, sunscreen cream, BB cream, acne lotion, essential oil, shampoo, etc.