CN111166683A

CN111166683A - Fullerene anti-aging antioxidant beauty and skin care cosmetic and preparation method thereof

Info

Publication number: CN111166683A
Application number: CN201911385056.2A
Authority: CN
Inventors: 卿德武
Original assignee: Jiawen Cosmetics Dongguan Co Ltd
Current assignee: Jiawen Cosmetics Dongguan Co Ltd
Priority date: 2019-12-28
Filing date: 2019-12-28
Publication date: 2020-05-19

Abstract

The invention discloses a fullerene anti-aging antioxidant beauty and skin care cosmetic and a preparation method thereof, wherein the fullerene anti-aging antioxidant beauty and skin care cosmetic comprises (A)7.05-22.1 wt% of an anti-aging antioxidant nutritional composition and (B) optional common components in the skin care cosmetic. The anti-aging nutritional composition comprises: fullerene, phytosterol isostearate, acetyl chitosamine, hydrolyzed collagen, palmitoyl pentapeptide-4, nicotinamide, palmitoyl hexapeptide-8, agave stem extract, and herba Centellae extract. The invention has the beneficial effects that: the skin care product can obviously improve the effects of skin anti-aging, anti-oxidation, beauty and skin care products, and can greatly reduce the damage of free radicals to the skin of a human body, effectively delay the early aging of the skin, improve the skin moistening and moisturizing capability, enhance the skin elasticity, reduce the generation of fine wrinkles and young wrinkles, and simultaneously improve the skin color and luster.

Description

Fullerene anti-aging antioxidant beauty and skin care cosmetic and preparation method thereof

Technical Field

The invention relates to the field of skin care products, and mainly relates to a fullerene anti-aging antioxidant beauty and skin care cosmetic and a preparation method thereof.

Background

The human being enters the early aging stage after age 25, anti-aging is not a proper term for the elderly, and early 90 provides for the prevention of aging! With the development of skin care products with low age, the concepts of anti-aging, anti-saccharification and anti-oxidation are aroused, how enterprises meet different requirements of people of different age groups is the subject of research and development of effective anti-aging series products.

The damage to the skin of a human body is accelerated due to factors such as air pollution, invasion of environmental allergens, irradiation of sunlight, great pressure of modern work and life, unsafe cosmetics and the like, so that the early aging of the skin is accelerated, and anti-aging and anti-oxidation products are needed in the current market.

Although a plurality of anti-aging products are available on the market, the anti-aging cosmetic is developed according to aged people, the used raw materials are commonly used, anti-aging antioxidant active components are not well subdivided into different age groups, especially the skin of young people is fragile and easy to allergy, great care and caution are needed when a new product is developed, no addition and no allergy of the product are achieved, the effect nutrition combination plays an extremely good role in soothing and sensitizing, repairing and anti-aging effects on the skin of the face, and the anti-aging cosmetic is a problem to be solved in urgent research on the existing anti-aging antioxidant cosmetic with fullerene.

Therefore, the prior art still needs to be upgraded and improved.

Disclosure of Invention

Based on the above, the invention aims to provide the fullerene anti-aging antioxidant beauty and skin care cosmetic and the preparation method thereof, the cosmetic composition can obviously improve the skin anti-aging antioxidant beauty and skin care cosmetic effect, and the reasonable formula combination is designed according to different age groups, so that the skin aging is effectively delayed in advance, the skin moistening and moisturizing capability is improved, the skin elasticity is enhanced, the generation of fine wrinkles is reduced, and the skin color and the skin luster are improved. The fullerene anti-aging antioxidant beauty and skin care cosmetic provided by the invention contains any additional water, but does not exclude the water added in the adopted fullerene anti-aging antioxidant nutrition combination and a small amount or trace amount of water inevitably introduced in other components.

In order to realize the purpose of the invention, the invention adopts the following technical scheme:

the fullerene anti-aging antioxidant cosmetic for beauty and skin care is characterized by comprising the following components:

(A) 7.05-22.1% by weight of an anti-aging and anti-oxidant nutritional composition,

(B) optionally, ingredients commonly used in skin care cosmetics;

wherein the above percentage amounts comprise water, which is usually added as a separate component, calculated on the total weight of the cosmetic.

Preferably, the fullerene anti-aging antioxidant beauty and skin care cosmetic comprises: (A) 7.05-22.1% of anti-aging and anti-oxidation nutritional composition and (B) 92.95-77.9% of other ingredients commonly used in cosmetics.

Preferably, the anti-aging and anti-oxidation nutritional composition comprises:

preferably, (B) optionally, other ingredients commonly used for skin care cosmetics are cosmetic ingredients commonly used in the production of lotions, creams, masks, lotions or essences, and the skin care cosmetics may be lotions, creams, masks, lotions or essences depending on the commonly used ingredients.

The preparation method of the fullerene anti-aging antioxidant beauty and skin care cosmetic is characterized by comprising the following steps:

1) putting water-soluble substances into a water phase pot, putting oil-soluble substances into an oil phase pot, and respectively heating the water phase and the oil phase to 82-85 ℃; wherein, the raw materials which are easy to agglomerate are pre-dispersed by a disperser; after the dissolution is finished, conveying the oil phase and the water phase into a vacuum homogenizing and emulsifying pot, and homogenizing and emulsifying for about 5-15 minutes;

2) after emulsification is finished, continuously stirring and cooling, adding the anti-aging and anti-oxidation nutrition combination of fullerene when the temperature is reduced to 50 ℃, and continuously stirring and dispersing uniformly;

3) when the temperature is reduced to 45 ℃, adding the preservative, and stirring and dispersing uniformly;

4) when the temperature is reduced to 40 ℃, adding essence, and stirring and dispersing uniformly;

5) when the temperature is reduced to 38 ℃, adding the pH regulator component, stirring for 10-20 minutes, uniformly dispersing, and continuously cooling to room temperature;

6) supplementing the evaporated water, stirring, filtering, and discharging.

The anti-aging and anti-oxidation essence of fullerene comprises the following substances:

the invention has the beneficial effects that: the skin care product can obviously improve the effects of skin anti-aging, anti-oxidation, beauty and skin care products, and can greatly reduce the damage of free radicals to the skin of a human body, effectively delay the early aging of the skin, improve the skin moistening and moisturizing capability, enhance the skin elasticity, reduce the generation of fine wrinkles and young wrinkles, and simultaneously improve the skin color and luster. The anti-aging facial mask has the advantages of delaying skin aging, providing a scientific anti-aging nutritional combination for facial skin, keeping the facial skin moist, bright and elastic by insisting on using, reducing the generation of wrinkles and fine lines, and delaying the skin aging process.

Detailed Description

In order to facilitate an understanding of the present invention, a more complete description of the present invention is provided below. Preferred embodiments of the present invention are given below. This invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.

Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used herein in the description of the invention is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.

The technical solution of the present patent will be described in further detail with reference to the following embodiments.

The invention provides a fullerene anti-aging antioxidant cosmetic for beauty and skin care and a preparation method thereof, and the invention is further explained in detail below in order to make the purpose, technical scheme and effect of the invention clearer and more clear. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.

The fullerene is a substance formed by carbon with the same component, is a third allotrope in which simple substance carbon is found, and is divided into a series of fullerenes such as C60, C70, Gd @ C82 and the like according to the difference of the number of contained carbon atoms and the difference of embedded substances, wherein the fullerene applied in the cosmetic field is mainly C60 which is a three-dimensional hollow molecule formed by 60 carbon atoms, 12 five-membered rings and 20 six-membered rings and shaped like a football; fullerene was first produced in 1985 by three researchers, Harprod Wolter Crotto (Eng), Robert Keel (Mei), and Rickett Stomoli (Mei), who won the Nobel prize in 1996 for their discovery of fullerene. The research results of the last 30 years show that the metal fullerene inlaid on the wall of the tumor vessel can effectively destroy the tumor vessel when the nano particles explode, then quickly block the nutrient supply to the tumor, and completely starve the tumor cells within a few hours. Therefore, the metal fullerene embedded with Gd atoms is also called a molecular scalpel aiming at solid tumors.

Research also finds that fullerene has super-strong capability of eliminating free radicals of human bodies, strong and stable antioxidant effect, is recorded in an SFDA directory, has the antioxidant capability of 172 times that of VC and 50 times that of SOD, and is known as the king of oxidation resistance; in 6 months and 30 days in 2014, fullerene is formally recorded in catalog of names of used cosmetic raw materials by the State food and drug administration.

The fullerene has a core value in the field of beauty and skin care, fullerene-free radical killers, after the fullerene adsorbs free radicals, two adjacent free radicals adsorbed on the same covalent bond are combined by electrons to form a new compound and are separated from fullerene molecules, and after the free radicals are adsorbed by the fullerene molecules to form the new compound, the fullerene molecules have a complete structure and can continuously adsorb the free radicals.

Just because the fullerene has peculiar efficacy in the aspect of beauty and skin care, researches find that the fullerene is good in matching compatibility with other known cosmetic raw materials, and the beauty and skin care cosmetic with the functions of anti-aging and anti-oxidation can be developed by adopting scientific, organic and reasonable combination proportion, so that the fullerene is a fashionable product which is in line with perfect pursuit of the current market.

Agave stem extract, english name: AGAVEAMERICANASTTEMEXTRACT has the effects of moisturizing, relieving allergy, resisting ultraviolet rays and repairing skin.

Chitosamine, english name: acetylglucopamine, CAS No.: 7512-17-6, has excellent percutaneous absorbability, is a natural cutin regulator, can promote synthesis of hyaluronic acid of skin cells, and inhibit glycosylation of tyrosinase, thereby inhibiting tyrosinase maturation, reducing melanin synthesis, scavenging free radicals, reducing free radical injury to human body, removing wrinkle, resisting aging, and improving skin tissue repair ability.

Nicotinamide, the alias nicotinamide, CASNO: 98-92-0, application: vitamins are involved in metabolism in vivo, and can be used for preventing and treating niacin deficiency such as pellagra.

Phytosterol isostearate, english name: PHYTOSTERYLISOSTEARATE, CAS number: 83615-24-1, can strengthen the skin barrier, thereby protecting the skin from the external environment, greatly reduce the percutaneous water loss rate of the skin, have excellent repairing effect on the epidermis and dermis, and are high-efficiency skin moisturizers and emollients.

Palmitoyl pentapeptide-4, english name: palmitoylpentapeptide-4, CAS number 214047-00-4, purpose of use: the cosmetic polypeptide can penetrate dermis to increase hydrolyzed collagen, and reverse skin aging process through reconstruction from inside to outside; cosmetic pentapeptides are in fact hydrolyzed C-terminal fragments of collagen I, with efficacy similar to laser surgery; stimulating the proliferation of hydrolyzed collagen, elastic fiber and hyaluronic acid, improving the water content and water locking degree of skin, increasing the thickness of skin and reducing fine wrinkles; the absorption effect can be increased.

Acetyl hexapeptide-8, english name: acetylhexapeptide-8, CAS number: 616204-22-9, purpose of use: is a bioactive polypeptide, which can reduce existing facial wrinkles and effectively prevent new wrinkles. The release of the nerve conduction element acetylcholine (acetylcholine) is inhibited to reduce the contraction of muscles, thereby achieving the purpose of reducing the generation of dynamic lines and expression lines.

Hydrolyzed collagen, english name: hydrolyzed COLLAGEN, a small biological molecule, has effects in building up body, and making skin tender, smooth, firm and elastic; the activity of hydrolyzed collagen in the skin is enhanced, the metabolism of skin tissues is promoted, and good moistening, moisturizing, wrinkle-removing and beautifying effects are generated on the skin.

Centella asiatica extract: english name: centella asiaticaxtract, CASNO: 84696-21-9, the main active components of centella asiatica extract, asiaticoside and madecassoside, are widely used for removing scars and promoting wound healing.

The invention provides a fullerene anti-aging antioxidant cosmetic for beauty and skin care, which is prepared by scientifically and organically matching and combining fullerene, phytosterol isostearate, acetyl chitosamine, nicotinamide, hydrolyzed collagen, palmitoyl pentapeptide-4, acetyl hexapeptide-8, agave tongue (AGAVEAMERICANA) stem extract and centella asiatica (CENTELLAASIATICA) extract according to weight percentage and then placing the mixture into a known formula system of the cosmetic for refining. The key components playing a role in anti-aging care on facial skin are present in the fullerene nutrient composition, and the fullerene in the anti-aging and anti-oxidation effect composition has the effects of ultra-strong oxidation resistance and skin free radical elimination, and the damage of free radicals to human skin is greatly reduced, so that the beautifying and skin care effects are exerted, the proliferation of hydrolyzed collagen, elastic fibers and hyaluronic acid is stimulated, the water content and the water locking degree of the skin are improved, the skin thickness is increased, wrinkle fine lines are reduced, the skin aging is delayed, a scientific anti-aging nutrient composition is provided for the facial skin, the facial skin can be kept moist, bright and elastic after the facial skin is insisted for use, the generation of the wrinkle fine lines is reduced, and the skin aging process is delayed.

The fullerene anti-aging antioxidant beautifying and skin-care cosmetic composition optionally also comprises a component (B) which is a component commonly used in skin-care cosmetics and comprises a medium, an active component, auxiliary materials and the like. Component (B) is known in the art and can be specifically selected by those skilled in the art in terms of type and amount as desired. Typically, component (B) is present in the compositions of the present invention in an amount of from 92.95 to 77.9 weight percent, based on the total weight percent of the composition.

Such as diluents, dispersants or carriers, and the like. All these vehicles are known in the art and the type and amount thereof can be specifically selected by the skilled person as desired. For example, the vehicle includes water, surfactants and emulsifiers, thickeners, and the like;

such active ingredients include, for example, emollients, humectants, skin conditioning agents, and the like. All these active ingredients are known in the art and the type and amount thereof can be specifically selected by the skilled person as desired.

Such adjuvants include, for example, preservatives, fragrances, colorants, chelating agents, pH adjusters, all of which are known in the art, the type and amount of which can be specifically selected by one skilled in the art as desired.

The surfactant, which is used to reduce the surface tension of the interface for the purpose of cleaning, emulsifying, stabilizing the system, can be any type of surfactant commonly used in cosmetics, the type and amount of which can be selected by the skilled person as desired. For example, the surfactant may include, but is not limited to, fatty acid soaps (e.g., sodium laurate, sodium palmitate, etc.), higher alkyl sulfates (e.g., sodium lauryl sulfate, etc.), alkyl ether sulfates (e.g., PEG-triethanolamine lauryl sulfate, PEG-sodium lauryl sulfate, etc.), alkyl betaines, amido betaines, sulfobetaines, hydrogenated castor oil derivatives, glyceryl alkyl ethers, etc., PEG-glyceryl fatty acid esters (e.g., PEG-glyceryl monostearate, PEG-glyceryl monoisostearate, etc.), sucrose fatty acid esters, and the like. The amount of surfactant present in the composition is known in the art. Generally, the surfactant based on the total weight of the components in the compositions of the present invention will depend on the particular formulation.

For example, the emulsifier includes, but is not limited to, one or more of cetearyl olive oleate, sorbitan olive oleate, polysorbate-60, polysorbate-80, methylglucose sesquistearate, PEG-20 methylglucose sesquistearate, PEG-40 hydrogenated castor oil, PPG-26-buthylpolyether-26, steareth-2, steareth-21, cetearyl glucoside, PEG-100 stearate, glyceryl stearate SE, sucrose stearate, sucrose polystearate, and the like. The amount of the emulsifier in the composition is known in the art. Generally, the total weight of the emulsifier in the composition of the present invention is a function of the particular formulation.

For example, the thickener includes, but is not limited to, one or more of carbomers, acrylates and derivatives thereof, xanthan gum, hydroxyethyl cellulose, hydroxypropyl methyl cellulose, and like high molecular polymers. The amount of the thickener in the composition is known in the art. Generally, the thickener component content in the compositions of the present invention will depend on the particular formulation.

For example, the emollient includes, but is not limited to, one or more of olive oil, macadamia nut oil, sweet almond oil, grape seed oil, meadowfoam seed oil, jojoba seed oil, sunflower seed oil, squalane, ethylhexyl palmitate, isopropyl myristate, hydrogenated polyisobutene, isohexadecane, isododecane, diethylhexyl carbonate, dioctyl carbonate, isononyl isononanoate, hydrogenated polydecene, tris (ethylhexanoate) glyceride, cetyl ethylhexanoate, caprylic/capric triglyceride, octyldodecanol, polydimethylsiloxane, and the like. The solid emollient described herein includes, but is not limited to, one or more of cetyl alcohol, stearyl alcohol, cetostearyl alcohol, behenyl alcohol, batyl alcohol, lauric acid, myristic acid, palmitic acid, stearic acid, hydrogenated coconut oil glycerides, shea butter, saw palmetto seed fat, and the like. The amount of the emollient in the composition is known in the art. Generally, in the compositions of the present invention, is the emollient present in the total weight? It is required to be adjusted according to the characteristics of the product and the formula.

For example, the moisturizer includes, but is not limited to, one or more of glycerin, propylene glycol, 1, 3-propanediol, 1, 2-pentanediol, polyethylene glycol-8, polyethylene glycol-32, methyl gluceth-10, glycerol polyether-26, glycerol glucoside, PPG-10 methyl glucose ether, trehalose, rhamnose, mannose, raffinose, betaine, erythritol, sodium hyaluronate, sodium polyglutamate, hydrolyzed sclerotium gum, tremella polysaccharides, tamarind seed polysaccharides, and the like. The amount of the humectant in the composition is known in the art. Generally, how much of the total weight is the humectant in the compositions of the present invention? It is required to be adjusted according to the characteristics of the product and the formula.

The skin conditioner may include active ingredients for moisturizing, anti-wrinkle, spot removing, acne removing, oil control, etc., including, but not limited to, one or more of ascorbic acid, ascorbyl glucoside, arbutin, tranexamic acid, niacinamide, phytosterols, phenethyl resorcinol, turmeric root extract, white birch bark extract, ceramide 2, ceramide 3, resveratrol, Pterocarpus marsupium bark extract, pepper seed extract, ubiquinone, cholesterol, cholesteryl stearate, ascorbyl dipalmitate, tocopherol (vitamin E), tocopheryl acetate, bisabolol, ascorbyl tetraisopalmitate, retinol palmitate, phytosterol macadamia oleate, various peptides, various plant extracts, etc. The level of the skin conditioning agent in the composition is known in the art. Generally, how are conditioner ingredients selected in the compositions of the present invention? How much of the skin conditioning agent is based on total weight? It is required to be adjusted according to the characteristics of the product and the formula.

Such adjuvants include, but are not limited to, preservatives, fragrances, colorants, chelating agents, pH adjusting agents, and the like. All these auxiliary ingredients are known in the art and the type and amount thereof can be specifically selected by the skilled person as desired.

For example, the preservatives include, but are not limited to, one or more of methylparaben, propylparaben, phenoxyethanol, benzyl alcohol, phenylethyl alcohol, bis (hydroxymethyl) imidazolidinyl urea, potassium sorbate, sodium benzoate, chlorphenesin, sodium dehydroacetate, and the like. The amount of the preservative in the composition is known in the art. Generally, the preservative component content in the compositions of the present invention will depend on the particular formulation.

The aromatic comprises natural essence, artificial essence, essential oil, etc.

The colorant comprises carmine pigment (CI16255), brilliant blue 85 pigment (CI42090), lemon yellow 60 pigment (CI19140), sunset yellow 60 pigment (CI15985) and the like.

The chelating agent comprises disodium EDTA (EDTA-2Na), tetrasodium EDTA (EDTA-4Na) and the like.

Such pH adjusting agents include, but are not limited to, arginine, triethanolamine, citric acid, sodium citrate, sodium hydroxide, potassium hydroxide, and the like.

The fullerene anti-aging and anti-oxidation cosmetic for beautifying and protecting skin provided by the invention can be prepared by any suitable method known in the field. For example, it can be prepared by using a vessel such as a liquid washing pot, a vacuum homogenizing and emulsifying pot, a disperser, a transfer pump, etc., which are generally used in the field of cosmetics. The preparation method comprises putting water soluble substance into water phase pot, putting oil soluble substance into oil phase pot, respectively heating water phase and oil phase to about 85 deg.C, wherein the raw material easy to agglomerate can be pre-dispersed with disperser. After the dissolution is finished, conveying the oil phase and the water phase into a vacuum homogenizing and emulsifying pot, and homogenizing and emulsifying for about 5-15 minutes; after emulsification is finished, stirring and cooling are continued, fullerene anti-aging and anti-oxidation nutrition combination is added at 50 ℃, essence, preservative and the like are optionally added, the pH of the product is adjusted according to needs, stirring and cooling are continued, the temperature of the material body is reduced to normal temperature, and the material body can be filled and delivered after relevant detection indexes are qualified. The preparation method can be deleted or adjusted according to the requirements of the preparation formulation, and various preparation formulations such as emulsion, cream, facial mask, toner, essence and the like can be prepared according to the requirements.

The invention provides a fullerene anti-aging antioxidant beauty and skin care cosmetic, which is really a fullerene anti-aging nourishing beauty essence. It consists of the following substances:

in a preferred embodiment, the invention provides a fullerene anti-aging and anti-oxidation cosmetic and skin care cosmetic with the following formula, preferably fullerene anti-aging nourishing cosmetic essence, which shows excellent anti-aging and anti-oxidation, repairing and anti-allergy and enhances skin elasticity and is a good product for delaying skin aging.

TABLE 1

Weighing the raw materials corresponding to the examples according to the data in table 1, and preparing according to the following steps:

1) sequentially adding a P1 phase (water, glycerol, xanthan gum, ammonium acryloyldimethyl taurate/VP copolymer, sodium hyaluronate and EDTA-2Na) into a liquid washing pot, stirring and dispersing, heating to 82-85 ℃, keeping the temperature and stirring for 30-40 minutes, starting cooling water after solid phase substances are completely dissolved and dispersed, and adding a P2 phase (triethanolamine and adding a proper amount of water to dissolve in advance for later use) at 70 ℃;

2) cooling to 50 deg.C, adding P3 phase (fullerene, phytosterol isostearate, acetyl chitosamine, nicotinamide, hydrolyzed collagen, palmitoyl pentapeptide-4, acetyl hexapeptide-8, herba agaves Variegatae (AGAVE AMERICANA) stem extract, and herba Centellae (CENTELLA ASIATICA) extract), and stirring to disperse uniformly;

3) cooling to 45 deg.C, adding P4 phase (phenoxyethanol, 1, 3-butanediol, 1, 2-hexanediol, P-hydroxyacetophenone, and ethylhexylglycerin), stirring, and dispersing;

4) cooling to 40 deg.C, adding P5 phase (essence, PEG-40 hydrogenated castor oil, pre-dispersed for use), stirring for 10-20 min, dispersing, and cooling;

5) adding pH regulator (arginine and citric acid) when the temperature is reduced to 38 deg.C, stirring for 10-20 min, dispersing, and cooling to room temperature;

6) supplementing the evaporated water, stirring, filtering, and discharging.

The 1-4 fullerene anti-aging nourishing beauty essence prepared in the embodiment adopts a sensory evaluation method, and the specific implementation mode is as follows:

100 office workers (60 women, 22-45 years old; 40 men, 25-50 years old) were selected for testing, and the fullerene anti-aging nourishing beauty essence prepared in examples 1-4 was respectively used for testing 100 subjects. Smearing anti-aging, nourishing and beautifying fullerene essence once every morning and evening by a subject, and gently patting and massaging the skin by hands until the skin is completely absorbed; each example of the fullerene anti-aging nourishing beauty essence is continuously used for four weeks, the skin is graded according to the feelings of the testees, the grading is 10 minutes, 2 is the worst, 5 is the moderate, 10 is the best, the higher the grading is, the better the moisturizing, conditioning and anti-aging effects of the fullerene anti-aging nourishing essence are, the grading of 100 testees is 2-4 minutes before use, and the evaluation results of the effects of moisturizing, repairing, allergy, elasticity, skin tendering, wrinkle resistance and the like after use are shown in Table 2.

The invention provides fullerene anti-aging nourishing beauty essence which is prepared by adding mild and safe anti-aging and anti-oxidation nutrition combination into an essence formula, can effectively relieve and repair skin, reduce the generation of free radicals on the surface of the skin, resist the aging process of the skin and enhance the elasticity of the skin, and is proved by example tests to have quite good effect, and the fullerene anti-aging nourishing beauty essence is highly favored by tested users to continue using the fullerene anti-aging nourishing beauty essence.

TABLE 2

In a preferred embodiment, the present invention provides a fullerene anti-aging and anti-oxidation cosmetic skin care product, preferably a fullerene anti-aging skin rejuvenation cream, having the following formulation.

TABLE 3

In a preferred embodiment, the present invention provides a fullerene anti-aging antioxidant cosmetic for skin care having a formulation, preferably a fullerene anti-aging skin rejuvenation cream, which shows excellent anti-oxidation, reduction of skin wrinkle lines, enhancement of skin elasticity, and restoration of water-moist and silky youth of skin, as shown in table 3.

Weighing the raw materials corresponding to the examples according to the data in table 3, and preparing according to the following steps:

1) sequentially adding a P1 phase (water, 1, 3-butanediol, allantoin, EDTA-2Na, ammonium acryloyldimethyl taurate/VP copolymer and sodium hyaluronate) into a water phase pot, stirring and dispersing, heating to 82-85 ℃, keeping the temperature and stirring for 15-30 minutes, adding a P2 phase (cetostearyl alcohol, cetostearyl glucoside, glyceryl stearate, PEG-100 stearate, squalane, caprylic/capric triglyceride, isononyl isononanoate, Butyrospermum PARKII (Butyrum PARKII) fruit fat, hydrogenated coconut oil glycerides and sweet almond oil) into an oil phase pot, stirring and heating to 85 ℃, melting and dispersing a solid phase, and keeping the temperature for 10-20 minutes;

2) pumping the P1 and P2 phases into a vacuum mean value emulsifying pot, keeping the mean value for 5-15 minutes, stirring for 15 minutes for defoaming, then starting cooling water to cool, adding the P3 phases (water and arginine) at 65 ℃, keeping the mean value for 1-3 minutes, and continuing cooling and stirring;

3) cooling to 50 deg.C, adding P4 phase (fullerene, phytosterol isostearate, acetyl chitosamine, nicotinamide, hydrolyzed collagen, palmitoyl pentapeptide-4, acetyl hexapeptide-8, herba agaves Variegatae (AGAVE AMERICANA) stem extract, and herba Centellae (CENTELLA ASIATICA) extract), and stirring to disperse uniformly;

4) cooling to 45 deg.C, adding P5 phase (phenoxyethanol, P-hydroxyacetophenone, 1, 3-butanediol, 1, 2-hexanediol, ethylhexyl glycerol, and orange peel oil), stirring, dispersing, and cooling;

5) when the temperature is reduced to 38 ℃, the cooling water is closed to stop cooling;

6) supplementing the evaporated water, stirring, filtering, and discharging.

The 1-4 fullerene anti-aging skin-tendering cream prepared in the embodiment adopts a sensory evaluation method, and the specific implementation mode is as follows:

200 office workers (120 women, 20-55 years old; 80 men, 25-60 years old) were selected for testing, and the fullerene anti-aging skin-rejuvenating cream prepared as described in examples 1-4 was used for testing of 200 subjects, respectively. Smearing the anti-aging fullerene skin-tendering cream on a subject in the morning and at night each day, and gently massaging the subject with hands until the anti-aging fullerene skin-tendering cream is completely absorbed; each example of the fullerene anti-aging skin-tendering cream is continuously used for four weeks, a subject scores the skin-tendering cream according to own feelings, the score is 10 minutes, 2 is the worst score, 5 is the moderate score, 10 is the best score, the higher the score is, the better the anti-aging, anti-oxidation and anti-wrinkle effects of the fullerene anti-aging skin-tendering cream are achieved, the score is 2-4 minutes before the use of 200 subjects, and the evaluation results of the effects of moistening, moisturizing, allergy, elasticity, skin-tendering, anti-wrinkle and the like after the use are shown in Table 2.

TABLE 4

Examples of the invention	Moistening	Moisture retention	Allergy (S)	Elasticity	Light color	Anti-wrinkle	Results
								1	5	4	3	2	3	3	3.33
2	6	5	5	6	6	7	5.83
								3	7	6	7	7	8	7	7.00
4	8	8	8	7	8	8	7.83

The invention provides a fullerene anti-aging skin-tendering cream which is prepared by adding mild and safe anti-aging and anti-oxidation nutrition combination into a high cream formula, can effectively relieve and repair skin, reduce the generation of free radicals on the surface of the skin, resist the aging process of the skin and enhance the elasticity of the skin, and is proved to have quite good effect by example test and is well accepted by tested users and is willing to continue to use the product.

In a preferred embodiment, the present invention provides a fullerene anti-aging antioxidant cosmetic for skin care, preferably a fullerene anti-aging skin rejuvenation mask having a formulation which shows excellent anti-aging antioxidant properties, fine wrinkle repair properties, and skin elasticity enhancement, and is a good mask for delaying skin aging.

TABLE 5

Weighing the raw materials corresponding to the examples according to the data in table 5, and preparing according to the following steps:

1) sequentially adding a P1 phase (water, glycerol, propylene glycol, xanthan gum, carbomer, sodium hyaluronate and EDTA-2Na) into a liquid washing pot, stirring for dispersion, heating to 82-85 ℃, keeping the temperature and stirring for 30-40 minutes, starting cooling water to cool after the solid phase is completely dissolved and dispersed, and adding a P2 phase (TEA, adding a proper amount of water and dissolving for later use);

3) cooling to 45 deg.C, adding P4 phase (phenoxyethanol, butanediol, hexanediol, P-hydroxyacetophenone, and ethylhexyl glycerol), and stirring for dispersing;

6) supplementing the evaporated water, stirring, filtering, and discharging.

The yellow fullerene anti-aging skin-tendering mask is prepared by putting mask cloth into a bag, and then pouring essence and sealing, wherein the mask cloth is made of one of copper ammonia fiber, nano-Sael fiber, bamboo charcoal mask fiber, chitosan fiber and plant fiber.

The 1-4 fullerene anti-aging skin-tendering mask prepared in the embodiment is subjected to a sensory evaluation method, and the specific implementation mode is as follows:

100 office people (60 women, age 22-45 years; 40 men, age 25-50 years) were selected for testing, and the fullerene anti-aging skin-rejuvenating facial mask prepared as described in examples 1-4 was used for testing of 100 subjects, respectively. Smearing the fullerene anti-aging skin-tendering mask on a subject in the morning and at night every day, and gently patting and massaging the subject by hands until the fullerene anti-aging skin-tendering mask is completely absorbed; each example of the fullerene anti-aging and skin-tendering mask is continuously used for four weeks, the skin-tendering mask is graded by the testees according to the feelings of the testees, the grading is 10 minutes, 2 is the worst, 5 is the moderate, 10 is the best, the moisturizing and conditioning anti-aging effect of the fullerene anti-aging and skin-tendering mask is better when the grading is higher, the grading of 100 testees is 2-4 minutes before use, and the evaluation results of the effects of moisturizing, fine lines, allergy, elasticity, skin tendering, wrinkle resistance and the like after use are shown in Table 6.

The fullerene anti-aging skin-tendering mask provided by the invention is prepared by adding mild and safe anti-aging and anti-oxidation nutrition combination into a mask essence formula, can effectively relieve and nourish skin, reduce fine wrinkles, enhance skin elasticity and resist the skin aging process, and is proved to have quite good effect through example tests, and the fullerene anti-aging skin-tendering mask is highly favored by testees and is willing to continue to use the fullerene anti-aging skin-tendering mask.

TABLE 6

Examples	Moistening condition	Reduction of fine lines	Hypersensitivity to skin	Elasticity of skin	Brightening skin color	Anti-wrinkle condition	Conclusion
								1	5	5	5	5	4	5	4.83
2	5	6	5	6	5	6	5.5
								3	7	7	6	7	6	8	6.83
4	8	8	9	7	8	8	8

In a preferred embodiment, the invention provides a fullerene anti-aging and anti-oxidation cosmetic skin care cosmetic with a formula, preferably fullerene anti-aging and anti-oxidation toner, which shows excellent anti-aging and anti-oxidation effects, skin tenderness, skin firming, pore shrinking and skin elasticity enhancing, and is a toner with the effect of delaying skin aging.

Weighing the raw materials corresponding to the examples according to the data in table 7, and preparing according to the following steps:

1) sequentially adding a P1 phase (water, glycerol, propylene glycol, sodium hyaluronate, EDTA-2Na) into a liquid washing pot, stirring and dispersing, heating to 82-85 ℃, preserving heat and stirring for 30-40 minutes, and starting cooling water after solid phase substances are completely dissolved and dispersed;

2) cooling to 50 deg.C, adding P2 phase (fullerene, phytosterol isostearate, acetyl chitosamine, nicotinamide, hydrolyzed collagen, palmitoyl pentapeptide-4, acetyl hexapeptide-8, herba agaves Variegatae (AGAVE AMERICANA) stem extract, and herba Centellae (CENTELLA ASIATICA) extract), and stirring to disperse uniformly;

3) cooling to 45 deg.C, adding P3 phase (phenoxyethanol, 1, 3-butanediol, 1, 2-hexanediol, P-hydroxyacetophenone, and ethylhexylglycerin), stirring, and dispersing;

4) cooling to 40 deg.C, adding P4 phase (essence, PEG-40 hydrogenated castor oil, pre-dispersed for use), stirring for 10-20 min, dispersing, and cooling;

6) supplementing the evaporated water, stirring, filtering, and discharging.

The 1-4 fullerene anti-aging firming toner prepared in the example is subjected to a sensory evaluation method, and the specific implementation mode is as follows:

100 office workers (60 women, 22-45 years old; 40 men, 25-50 years old) were selected for testing, and the fullerene anti-aging firming toner prepared as described in examples 1-4 was used for testing in 100 subjects, respectively. Smearing the anti-aging firming toner of the fullerene once in the morning and at night every day by a subject, and gently patting and massaging the skin by hands until the skin is completely absorbed; each example of the fullerene anti-aging compact toner is continuously used for four weeks, the skin of a subject is graded according to the self feeling, the grading is carried out by 10 minutes, 2 is the worst, 5 is the moderate, 10 is the best, the higher the grading is, the moisturizing, conditioning, elasticity, skin tendering and anti-aging effects of the fullerene anti-aging compact toner are better, the grading of 100 subjects before use is 2-4 minutes, and the evaluation results of the effects of moisturizing, fine lines, allergy, elasticity, skin tendering and anti-wrinkle are shown in Table 8.

TABLE 8

Examples	Moistening condition	Tender skin	Hypersensitivity to skin	Elasticity of skin	Firming skin	Anti-wrinkle condition	Conclusion
								1	5	4	3	3	4	4	3.83
2	6	6	5	6	5	6	5.67
								3	6	7	7	7	7	7	6.83
4	8	8	8	8	8	7	7.83

The fullerene anti-aging firming toner provided by the invention is prepared by adding mild and safe anti-aging and anti-oxidation nutrition combination into a toner formula, can effectively relax and nourish the skin, firms the skin, enhances the skin elasticity and resists the skin aging process, and the effect is proved to be quite good by example tests, so that the fullerene anti-aging firming toner is highly favored by testees to continue using the fullerene anti-aging firming toner.

In a preferred embodiment, the present invention provides a fullerene anti-aging antioxidant cosmetic skin care cosmetic with a formulation, preferably fullerene anti-aging nourishing skin rejuvenating cream, which shows excellent anti-oxidation, reduction of skin wrinkle fine lines, enhancement of skin elasticity, reduction of skin sagging, and restoration of your firm and alive healthy skin, as shown in table 9.

TABLE 9

The raw materials corresponding to the examples were weighed according to the data in table 9, and prepared according to the following steps:

3) sequentially adding a P1 phase (water, 1, 3-butanediol, glycerol, allantoin, EDTA-2Na, ammonium acryloyldimethyl taurate/VP copolymer and sodium hyaluronate) into a water phase pot, stirring and dispersing, heating to 82-85 ℃, keeping the temperature and stirring for 15-30 minutes, adding a P2 phase (cetostearyl alcohol, glyceryl stearate, PEG-100 stearate, olive oil, caprylic/capric triglyceride, isononyl isononanoate, shea butter (Butyripenum Parkii) fruit fat, hydrogenated polyisobutene and tocopheryl acetate) into an oil phase pot, stirring and heating to 85 ℃, melting and dispersing a solid phase, and keeping the temperature for 10-20 minutes;

4) pumping the P1 and P2 phases into a vacuum mean value emulsifying pot, keeping the mean value for 5-15 minutes, stirring for 15 minutes for defoaming, then starting cooling water to cool, adding the P3 phases (water and arginine) at 65 ℃, keeping the mean value for 1-3 minutes, and continuing cooling and stirring;

4) cooling to 45 deg.C, adding P5 phase (phenoxyethanol, menthone, 1, 3-butanediol, 1, 2-hexanediol, ethylhexyl glycerol, and Rosa CANINA (Rosa CANINA) fruit oil), stirring, dispersing, and cooling;

7) supplementing the evaporated water, stirring, filtering, and discharging.

The 1-4 fullerene anti-aging nourishing and skin-tendering milk prepared in the embodiment adopts a sensory evaluation method, and the specific implementation mode is as follows:

200 office workers (120 women, 20-55 years old; 80 men, 25-60 years old) were selected for testing, and the fullerene anti-aging nourishing and skin-tendering creams prepared as described in examples 1-4 were respectively tested for 200 subjects. Smearing fullerene anti-aging nourishing skin-tendering emulsion on a subject in the morning and at night every day, and gently massaging the subject with hands until the fullerene anti-aging nourishing skin-tendering emulsion is completely absorbed; each example of the fullerene anti-aging nourishing and skin-tendering lotion is continuously used for four weeks, the skin-reviving lotion is graded by the test subjects according to the feelings of the test subjects, the grading is 10 minutes, 2 is the worst, 5 is the moderate, 10 is the best, the skin-moisturizing, relaxing, compacting, elasticity and anti-wrinkle effects of the fullerene anti-aging nourishing and skin-tendering lotion are better when the grading is higher, the grading before the use of 200 test subjects is 2-4 minutes, and the evaluation results of the effects of moisturizing, relaxing, allergy, elasticity, compacting and anti-wrinkle after the use are shown in the table 10.

Watch 10

The fullerene anti-aging nourishing skin-tendering lotion provided by the invention is prepared by adding mild and safe anti-aging and anti-oxidation nutrition combination into a lotion formula, can effectively relax and nourish skin, compact skin, enhance skin elasticity and resist the process of skin relaxation and aging, and is proved to have quite good effect through example test, so that the lotion is highly favored by testees to continue using the lotion.

The technical solutions of the above-described embodiments are preferred embodiments of the present invention, and several modifications and changes can be made without departing from the principle of the present invention, and these modifications and changes should also be considered as being within the protection scope of the present invention.

Claims

1. The fullerene anti-aging antioxidant cosmetic for beauty and skin care is characterized by comprising the following components:

(B) optionally, ingredients commonly used in skin care cosmetics;

2. The fullerene anti-aging antioxidant cosmetic for beauty and skin care according to claim 1, comprising: (A) 7.05-22.1% of anti-aging and anti-oxidation nutritional composition and (B) 92.95-77.9% of other ingredients commonly used in cosmetics.

3. The fullerene anti-aging antioxidant cosmetic for beauty and skin care of claim 1 or 2, characterized in that the anti-aging antioxidant nutritional composition comprises:

4. the fullerene anti-aging antioxidant cosmetic for skin care of claim 1 or 2, wherein the (B) optional, other ingredients commonly used for skin care cosmetics are cosmetic ingredients commonly used in the production of lotions, creams, masks, lotions or essences.

5. The preparation method of the fullerene anti-aging antioxidant beauty and skin care cosmetic is characterized by comprising the following steps:

6) supplementing the evaporated water, stirring, filtering, and discharging.

6. A fullerene cosmetic for resisting aging, oxidation and beautifying and protecting skin is composed of the following substances:

7. the fullerene anti-aging and anti-oxidation beauty and skin care cosmetic as claimed in claim 6, which is essence.