CN114894095B - Cantilever beam displacement measuring device and measuring method - Google Patents
Cantilever beam displacement measuring device and measuring method Download PDFInfo
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Abstract
本发明提供一种悬臂梁位移测量装置和测量方法。本发明的悬臂梁位移测量装置,包括悬臂梁、激光器、光学干涉系统、光电探测器,还包括第一控制器,其根据激光器的检测温度值与目标温度之差来生成用于控制激光器的温度的控制信号,来将激光器的温度控制成目标温度;和第二控制器,其根据光电探测器输出的干涉光光强电压信号与规定的基准电压值之差生成悬臂梁的位移信号,并将该位移信号作为目标温度相关信号输出到第一控制器,通过使第一控制器控制激光器的温度来改变所输出的激光的波长,来对光强电压信号进行反馈控制。采用本发明的装置和方法,能够提高悬臂梁静态位移测量的灵敏度和动态范围。
The invention provides a cantilever beam displacement measuring device and a measuring method. The cantilever beam displacement measuring device of the present invention includes a cantilever beam, a laser, an optical interference system, a photodetector, and a first controller, which generates a temperature for controlling the laser according to the difference between the detected temperature value of the laser and the target temperature control signal to control the temperature of the laser to the target temperature; and a second controller, which generates the displacement signal of the cantilever beam according to the difference between the interference light intensity voltage signal output by the photodetector and the specified reference voltage value, and The displacement signal is output to the first controller as a target temperature-related signal, and the first controller controls the temperature of the laser to change the wavelength of the output laser, thereby performing feedback control on the light intensity voltage signal. By adopting the device and method of the invention, the sensitivity and dynamic range of the static displacement measurement of the cantilever beam can be improved.
Description
技术领域technical field
本发明属于灵敏力探测研究领域,具体涉及基于激光干涉测距法的悬臂梁位移测量装置和测量方法。The invention belongs to the research field of sensitive force detection, and in particular relates to a cantilever beam displacement measuring device and a measuring method based on a laser interference ranging method.
背景技术Background technique
悬臂梁位移测量是灵敏力探测的重要方法之一,比如对纳米尺度磁性样品的磁扭矩测量,卡西米尔力(Casimir effect),磁共振力测试等。悬臂梁包括固定端和自由端,能够用于测量作用在磁性样品上面的扭矩。扭矩使悬臂梁发生弯曲,测量悬臂梁弯曲也就是测量悬臂梁自由端的位移。由于悬臂梁的位移与悬臂梁受到的扭矩是对应的,故在本说明书中悬臂梁位移测量和悬臂梁扭矩测量的意思是大致相同的,混合使用两种表述。Cantilever beam displacement measurement is one of the important methods for sensitive force detection, such as magnetic torque measurement of nanoscale magnetic samples, Casimir effect, magnetic resonance force test, etc. A cantilever beam with a fixed end and a free end can be used to measure torque acting on a magnetic sample. Torque causes the cantilever to bend, and to measure the cantilever bend is to measure the displacement of the free end of the cantilever. Since the displacement of the cantilever beam corresponds to the torque received by the cantilever beam, the meanings of cantilever beam displacement measurement and cantilever beam torque measurement in this specification are roughly the same, and the two expressions are mixed.
悬臂梁的位移测量,目前采用的方法主要分为电学方式和光学方式两类。The displacement measurement of the cantilever beam is mainly divided into two types: electrical method and optical method.
用电学方式测量悬臂梁位移的方法主要有电容耦合、压阻效应和压电效应三种,悬臂梁的弯曲引起悬臂梁和基片上的电容、压阻和压电电压的改变,通过电容、电阻和电压的读取来判别悬臂梁所受的扭矩大小。利用电容耦合效应来测量悬臂梁位移时,悬臂梁与基片形成一个平行板电容,悬臂梁产生位移后,平行板电容值改变,电容的改变对应悬臂梁的位移,在悬臂梁的力学线性区内,通过电容的读取来判断悬臂梁上所受到的扭矩大小。利用压阻效应来测量悬臂梁位移时,在悬臂梁根部附近,也就是悬臂梁弯曲幅度最大的位置采用压阻材料制备,当悬臂梁受到扭矩弯曲时,压阻材料受到压力引起它的电阻改变。利用压电效应来测量悬臂梁位移的悬臂梁结构与压阻效应类似。There are three main methods to measure the displacement of the cantilever beam electrically: capacitive coupling, piezoresistive effect, and piezoelectric effect. The bending of the cantilever beam causes changes in the capacitance, piezoresistance and piezoelectric voltage on the cantilever beam and the substrate. The reading of the voltage is used to determine the magnitude of the torque on the cantilever beam. When the capacitive coupling effect is used to measure the displacement of the cantilever beam, the cantilever beam and the substrate form a parallel plate capacitance. After the cantilever beam is displaced, the capacitance value of the parallel plate changes, and the change of capacitance corresponds to the displacement of the cantilever beam. In the mechanical linear region of the cantilever beam Inside, judge the torque on the cantilever beam by reading the capacitance. When the piezoresistive effect is used to measure the displacement of the cantilever beam, the piezoresistive material is used near the root of the cantilever beam, that is, the position where the cantilever beam has the largest bending range. When the cantilever beam is bent by torque, the piezoresistive material is subjected to pressure to cause its resistance to change. . Cantilever structures that use the piezoelectric effect to measure cantilever displacement are similar to the piezoresistive effect.
光学方法通常利用激光在悬臂梁表面的反射与光纤出射端面的反射光形成干涉信号,用光学方式测量悬臂梁位移的光纤干涉测量系统的构成例如图1所示。图1所示的测量系统包括激光器101、光纤耦合器103、光纤104、透镜105、悬臂梁106和光电探测器102。来自激光器101的激光经由光纤耦合器103、光纤104和透镜105聚焦在悬臂梁106的反射面上,在该反射面上反射的光返回到光纤104中,与光纤出射端面的反射光发生光学干涉形成干涉光信号。干涉光信号经过光纤耦合器103传递给光电探测器102转变成电压信号。Optical methods usually use the reflection of the laser on the surface of the cantilever beam and the reflected light from the exit end of the fiber to form an interference signal. The measurement system shown in FIG. 1 includes a laser 101 , a fiber coupler 103 , an optical fiber 104 , a lens 105 , a cantilever beam 106 and a photodetector 102 . The laser light from the laser 101 is focused on the reflective surface of the cantilever beam 106 through the fiber coupler 103, the optical fiber 104 and the lens 105, and the light reflected on the reflective surface returns to the optical fiber 104 and optically interferes with the reflected light at the exit end face of the optical fiber Interfering optical signals are formed. The interference light signal is transmitted to the photodetector 102 through the fiber coupler 103 and converted into a voltage signal.
悬臂梁力探测的光学方法与电学方法相比,前者具有更高的灵敏度。这是由于电学方法所使用的悬臂梁需要集成电容耦合、压阻效应和压电效应的功能,这使得这些悬臂梁不可能有很低的弹性系数。应用于激光干涉测量的悬臂梁就没有这个限制,它可以采用纯硅的悬臂梁,弹性系数可以达到1mN/m的量级。Optical methods of cantilever beam force detection are more sensitive than electrical methods. This is because the cantilevers used in the electrical method need to integrate the functions of capacitive coupling, piezoresistive effect and piezoelectric effect, which makes it impossible for these cantilever beams to have a very low elastic coefficient. The cantilever beam used in laser interferometry does not have this limitation. It can use pure silicon cantilever beam, and the elastic coefficient can reach the order of 1mN/m.
发明内容Contents of the invention
本发明要解决的技术问题The technical problem to be solved in the present invention
悬臂梁力探测的光学方式,悬臂梁与光纤光出射端面之间形成干涉腔,悬臂梁的位移引起干涉腔长度的变化,将引起干涉光强的变化。图2是表示改变干涉腔长度时的干涉信号强度变化的曲线图。如图2 所示,在激光干涉测量时,改变干涉腔长度(悬臂梁距离光纤出射端面的距离),干涉信号呈周期变化,干涉信号为正弦函数形。从图2 可以明显的看出,悬臂梁位移与干涉信号的强弱并非线性的关系,如果采用这种方式测量悬臂梁位移,其测量信号的动态范围将极小。所以采用激光干涉法和悬臂梁来进行弱力探测时通常是测量悬臂梁共振频率的变化,来表征力的强弱,这就是力探测的动态模式。因为测量悬臂梁共振频率时,只需要保持悬臂梁的振动幅度控制在极小的范围,不会超出干涉信号的动态范围,如图2中正弦线上加粗部分。In the optical method of cantilever beam force detection, an interference cavity is formed between the cantilever beam and the light emitting end face of the fiber. The displacement of the cantilever beam causes the change of the length of the interference cavity, which will cause the change of the interference light intensity. Fig. 2 is a graph showing changes in the intensity of interference signals when the length of the interference cavity is changed. As shown in Figure 2, when the length of the interference cavity is changed (the distance between the cantilever beam and the exit end face of the fiber) during laser interferometry, the interference signal changes periodically, and the interference signal is sinusoidal. It can be clearly seen from Figure 2 that the relationship between the displacement of the cantilever beam and the strength of the interference signal is not linear. If the displacement of the cantilever beam is measured in this way, the dynamic range of the measurement signal will be extremely small. Therefore, when laser interferometry and cantilever beams are used for weak force detection, the change of the resonant frequency of the cantilever beam is usually measured to characterize the strength of the force. This is the dynamic mode of force detection. Because when measuring the resonant frequency of the cantilever beam, it is only necessary to keep the vibration amplitude of the cantilever beam in a very small range, and will not exceed the dynamic range of the interference signal, as shown in the thickened part on the sinusoidal line in Figure 2.
但是动态测量法存在局限性,下面以动态磁扭矩测量来加以说明。首先,动态测量法测量的是悬臂梁的共振频率,通过共振频率的变化来反映悬臂梁受到的扭矩的大小,然而共振频率的变化并不能直接的反映扭矩的大小。共振频率的变化是由样品的磁化强度M和磁各向异性系数H共同决定,这使得应用动态测量法时,从共振频率变化来推演出样品磁化强度等有用参量变得异常困难。相较而言,直接测量磁性样品在磁场中受到的扭矩而引起悬臂梁的位移的方法,也叫悬臂梁静态测量,位移与磁化强度之间的关系就简单得多。However, there are limitations in the dynamic measurement method, which will be described below with dynamic magnetic torque measurement. First of all, the dynamic measurement method measures the resonant frequency of the cantilever beam. The change of the resonant frequency reflects the magnitude of the torque on the cantilever beam. However, the change of the resonant frequency cannot directly reflect the magnitude of the torque. The change of resonance frequency is jointly determined by the magnetization M of the sample and the magnetic anisotropy coefficient H, which makes it extremely difficult to deduce useful parameters such as the magnetization of the sample from the change of resonance frequency when applying the dynamic measurement method. In comparison, the method of directly measuring the displacement of the cantilever caused by the torque of the magnetic sample in the magnetic field is also called static measurement of the cantilever, and the relationship between the displacement and the magnetization is much simpler.
另外,动态测量法测量扭矩的灵敏度取决于悬臂梁的弹性系数k 和品质因子Q。在动态磁扭矩测量中由于样品磁化态的不同都会影响到悬臂梁的Q值。例如对MnSi纳米片进行的动态磁扭矩测试中磁场大于0.4T后有明显的磁化损耗,这个磁场区间内,悬臂梁的Q值减小,测量共振频率的信噪比降低,在测量曲线上对应噪声的增加。In addition, the sensitivity of the dynamic measurement method to measure torque depends on the elastic coefficient k and quality factor Q of the cantilever beam. In the dynamic magnetic torque measurement, the Q value of the cantilever beam will be affected by the difference of the magnetization state of the sample. For example, in the dynamic magnetic torque test of MnSi nanosheets, there is obvious magnetization loss after the magnetic field is greater than 0.4T. In this magnetic field range, the Q value of the cantilever beam decreases, and the signal-to-noise ratio of the measured resonance frequency decreases, which corresponds to increase in noise.
虽然目前普遍存在的电学测距的悬臂梁也可以实现静态的扭矩测量,但是其灵敏度无法与光学干涉测量法相比。Although the current ubiquitous electrical ranging cantilever can also achieve static torque measurement, its sensitivity cannot be compared with that of optical interferometry.
本发明是针对上述问题做出的,其目的在于提供一种适用于激光干涉测量法的悬臂梁位移测量装置和方法,其能够实现提高了灵敏度和动态范围的悬臂梁位移静态测量。The present invention is made in response to the above problems, and its purpose is to provide a cantilever beam displacement measurement device and method suitable for laser interferometry, which can realize static measurement of cantilever beam displacement with improved sensitivity and dynamic range.
解决技术问题的技术方案Technical solutions to technical problems
为了解决上述技术问题,本发明提供一种悬臂梁位移测量装置,其特征在于,包括:悬臂梁,其能够载置被测物,包括固定端和自由端,在所述自由端具有光反射面;激光器,其能够通过控制其温度而改变所输出的激光的波长;光学干涉系统,所述激光器输出的激光能够经由该光学干涉系统照射到所述悬臂梁的所述光反射面,在所述光反射面反射的光能够返回到所述光学干涉系统并发生光的干涉,生成干涉光;光电探测器,其能够检测所述干涉光而将所述干涉光的光强转换成光强电压信号;第一控制器,其根据所述激光器的检测温度值与目标温度之差来生成用于控制所述激光器的温度的控制信号,来将所述激光器的温度控制成目标温度;和第二控制器,其根据所述光电探测器输出的光强电压信号与规定的基准电压值之差生成所述悬臂梁的位移信号,并将该位移信号作为目标温度相关信号输出到所述第一控制器,通过使所述第一控制器控制所述激光器的温度来改变所输出的激光的波长,来对所述光强电压信号进行反馈控制。In order to solve the above technical problems, the present invention provides a cantilever beam displacement measuring device, which is characterized in that it includes: a cantilever beam, which can carry the object to be measured, including a fixed end and a free end, and the free end has a light reflecting surface the laser, which can change the wavelength of the output laser by controlling its temperature; the optical interference system, the laser output by the laser can be irradiated to the light reflecting surface of the cantilever beam through the optical interference system, in the The light reflected by the light-reflecting surface can return to the optical interference system and interfere with light to generate interference light; a photodetector can detect the interference light and convert the light intensity of the interference light into a light intensity voltage signal a first controller, which generates a control signal for controlling the temperature of the laser according to the difference between the detected temperature value of the laser and the target temperature, to control the temperature of the laser to the target temperature; and the second control A device, which generates a displacement signal of the cantilever beam according to the difference between the light intensity voltage signal output by the photodetector and a specified reference voltage value, and outputs the displacement signal to the first controller as a target temperature-related signal , performing feedback control on the light intensity voltage signal by causing the first controller to control the temperature of the laser to change the wavelength of the output laser light.
优选所述规定的基准电压值是所述光强电压信号相对于所述波长的变化或所述悬臂梁的位移的变化率成为最大值的所述光强电压信号的电压值。Preferably, the predetermined reference voltage value is a voltage value of the light intensity voltage signal at which a change rate of the light intensity voltage signal with respect to a change in the wavelength or a displacement of the cantilever beam becomes a maximum value.
优选所述规定的基准电压值是通过获取所述光强电压信号的最大值和最小值,并计算所述最大值和所述最小值的平均值而得到的。Preferably, the specified reference voltage value is obtained by obtaining the maximum value and the minimum value of the light intensity voltage signal, and calculating the average value of the maximum value and the minimum value.
优选所述第一控制器为第一PID控制器,所述激光器的检测温度值和目标温度相关信号为其输入信号,所述用于控制所述激光器的温度的控制信号为其输出信号,所述第二控制器为第二PID控制器,所述光电探测器输出的光强电压信号和规定的基准电压值为其输入信号,所述悬臂梁的位移信号为其输出信号,该输出信号作为目标温度相关信号被输出到所述第一PID控制器。Preferably, the first controller is a first PID controller, the detected temperature value of the laser and the target temperature-related signal are its input signals, and the control signal for controlling the temperature of the laser is its output signal, so The second controller is a second PID controller, the light intensity voltage signal output by the photodetector and the specified reference voltage are its input signals, the displacement signal of the cantilever beam is its output signal, and the output signal is used as A target temperature related signal is output to the first PID controller.
优选所述光学干涉系统包括光纤耦合器和光纤,所述激光器所输出的激光经由所述光纤耦合器进入所述光纤,从所述光纤的光出射端出射的激光照射到所述悬臂梁的所述光反射面,在所述光反射面反射的光经所述光纤的光出射端返回到所述光纤中,与在所述光纤的光出射端反射的光发生光学干涉,所述光电探测器与所述光纤耦合器耦合来接收所述干涉光。Preferably, the optical interference system includes a fiber coupler and an optical fiber, the laser output by the laser enters the optical fiber through the optical fiber coupler, and the laser light emitted from the light output end of the optical fiber irradiates the cantilever beam. The light reflecting surface, the light reflected on the light reflecting surface returns to the optical fiber through the light exit end of the optical fiber, and optically interferes with the light reflected at the light exit end of the optical fiber, and the photodetector coupled with the optical fiber coupler to receive the interference light.
优选所述激光器为波长可调半导体激光器。Preferably, the laser is a wavelength-tunable semiconductor laser.
优选所述悬臂梁由纯硅制成。Preferably said cantilevers are made of pure silicon.
优选所述被测物是磁性样品,所述外力是通过外加磁场来施加的。Preferably, the measured object is a magnetic sample, and the external force is applied by an external magnetic field.
此外,本发明提供一种悬臂梁位移测量方法,使用上述悬臂梁位移测量装置来测量所述悬臂梁的位移,其特征在于,包括:在所述悬臂梁上载置被测物的步骤;通过控制激光器的温度改变激光的波长,对悬臂梁照射激光使得发生光的干涉,来获取所述干涉光的光强电压信号,基于所述光强电压信号来确定所述光强电压信号的基准电压值的步骤;通过利用所述第一控制器和所述第二控制器进行反馈控制将所述光强电压信号锁定在所述基准电压值的步骤;对所述被测物施加外力使其发生位移,基于所述第二控制器输出的所述位移信号来测量所述位移的步骤。In addition, the present invention provides a method for measuring the displacement of a cantilever beam, using the above-mentioned cantilever beam displacement measuring device to measure the displacement of the cantilever beam, which is characterized in that it includes: the step of placing the measured object on the cantilever beam; The temperature of the laser changes the wavelength of the laser, irradiating the laser on the cantilever beam to cause light interference to obtain the light intensity voltage signal of the interference light, and determining the reference voltage value of the light intensity voltage signal based on the light intensity voltage signal the step of locking the light intensity voltage signal at the reference voltage value by using the first controller and the second controller to perform feedback control; applying an external force to the measured object to cause displacement , the step of measuring the displacement based on the displacement signal output by the second controller.
有益效果Beneficial effect
1、本发明通过改变激光器的波长对激光干涉光强(测距)信号进行工作点锁定和实时补偿,使原本非线性的测量关系变得线性从而提高了灵敏度,使得改进后的测量系统变得适合进行静态位移测量。1. The present invention locks the working point and compensates in real time on the laser interference light intensity (ranging) signal by changing the wavelength of the laser, so that the original nonlinear measurement relationship becomes linear, thereby improving the sensitivity, and making the improved measurement system become Suitable for static displacement measurements.
2、因为能够通过改变激光的波长来补偿位移量,将干涉光强信号拉回到锁定的工作点,故大大提高了测量的动态范围。2. Because the displacement can be compensated by changing the wavelength of the laser, the interference light intensity signal can be pulled back to the locked working point, so the dynamic range of the measurement is greatly improved.
3、就悬臂梁而言,由于悬臂梁的静态位移测量灵敏度取决于悬臂梁的弹性系数而与悬臂梁的品质因子无关,所以采用静态位移测量对悬臂梁品质的要求更加宽容。采用纯硅材质悬臂梁能实现更低的弹性系数,进一步提高灵敏度。3. As far as the cantilever beam is concerned, since the static displacement measurement sensitivity of the cantilever beam depends on the elastic coefficient of the cantilever beam and has nothing to do with the quality factor of the cantilever beam, the static displacement measurement is more tolerant to the quality of the cantilever beam. The cantilever beam made of pure silicon can achieve a lower elastic coefficient and further improve the sensitivity.
附图说明Description of drawings
图1是用于测量悬臂梁位移的光纤干涉测量系统的示意图。Figure 1 is a schematic diagram of a fiber optic interferometry system for measuring the displacement of a cantilever beam.
图2是表示改变干涉腔长度时的干涉信号强度变化的曲线图。Fig. 2 is a graph showing changes in the intensity of interference signals when the length of the interference cavity is changed.
图3是表示本发明的一个实施方式进行工作点锁定和温度补偿的反馈控制结构的示意图。Fig. 3 is a schematic diagram showing a feedback control structure for operating point locking and temperature compensation according to an embodiment of the present invention.
图4是表示PID控制器的内部电路结构之一例的电路图。FIG. 4 is a circuit diagram showing an example of an internal circuit configuration of a PID controller.
图5A是表示MnSi微米片的SEM照片,图5B是表示将MnSi微米片载置到悬臂梁上的状态的SEM照片。FIG. 5A is an SEM photograph showing a MnSi microsheet, and FIG. 5B is an SEM photograph showing a state in which an MnSi microsheet is mounted on a cantilever beam.
图6A是测量共振频率变化的动态测量法的测试结果,图6B是采用了温度补偿的静态测量法测量的悬臂梁的静态位移的测试结果。FIG. 6A is the test result of the dynamic measurement method for measuring the change of resonance frequency, and FIG. 6B is the test result of the static displacement of the cantilever beam measured by the static measurement method using temperature compensation.
具体实施方式Detailed ways
下面结合附图,对本发明的具体实施方式进行说明。The specific implementation manners of the present invention will be described below in conjunction with the accompanying drawings.
以下实施方式中,在提及要素的数字等(包括个数、数值、量、范围等)的情况下,除了特别明确说明的情况和从原理上明显限定为特定数字的情况之外,并不限定于该特定数字,可为特定数字以上或以下。In the following embodiments, when referring to numbers and the like (including numbers, values, amounts, ranges, etc.) of elements, except for the cases where it is particularly clearly stated and the case where it is clearly limited to a specific number in principle, it does not mean Limited to the specific number, may be above or below the specific number.
另外,在以下的实施方式中,其结构要素(包括步骤要素等)除了特别明确说明的情况和从原理上明显理解为是必须的情况之外,都不一定是必须的,并且也可以包括说明书中未明确提及的要素,这无需明言。In addition, in the following embodiments, the structural elements (including step elements, etc.) are not necessarily essential except for the case where it is particularly clearly stated and the case where it is clearly understood as essential in principle, and the description may also be included. Elements not expressly mentioned in , need not be stated.
本发明是基于激光干涉测距系统的悬臂梁位移测量装置和方法。具体而言,本发明的一个实施方式采用了图1所示的用于测量悬臂梁位移的光纤干涉测量系统,其包括激光器101、光纤耦合器103、光纤 104、透镜105、悬臂梁106和光电探测器102。来自激光器101的激光经由光纤耦合器103、光纤104和透镜105聚焦在悬臂梁106的反射面上,在该反射面上反射的光返回到光纤104中,与光纤出射端面的反射光发生光学干涉形成干涉光信号。干涉光信号经过光纤耦合器103 传递给光电探测器102转变成电压信号。The invention is a cantilever beam displacement measuring device and method based on a laser interference ranging system. Specifically, one embodiment of the present invention adopts the optical fiber interferometry system for measuring the displacement of a cantilever shown in FIG. Detector 102. The laser light from the laser 101 is focused on the reflective surface of the cantilever beam 106 through the fiber coupler 103, the optical fiber 104 and the lens 105, and the light reflected on the reflective surface returns to the optical fiber 104 and optically interferes with the reflected light at the exit end face of the optical fiber Interfering optical signals are formed. The interference light signal is transmitted to the photodetector 102 through the fiber coupler 103 and converted into a voltage signal.
然而,本发明的用于测量悬臂梁位移的光学干涉系统不限于采用具有光纤耦合器和光纤的光纤干涉系统。根据后文的记载可知,本发明采用的技术手段是对干涉光强信号锁定工作点和进行补偿,因此只要是能够与来自悬臂梁的反射光产生光学干涉的光学干涉系统(例如偏振分束器、半透半反镜和4分之一波片的组合),采用本发明的技术方案就能够实现提高了灵敏度和动态范围的悬臂梁位移静态测量。However, the optical interference system for measuring the displacement of a cantilever beam of the present invention is not limited to the use of an optical fiber interference system having a fiber coupler and an optical fiber. According to the following description, it can be seen that the technical means adopted in the present invention is to lock the working point and compensate the interference light intensity signal, so as long as it is an optical interference system (such as a polarizing beam splitter) that can generate optical interference with the reflected light from the cantilever , a half-mirror and a quarter-wave plate), the adoption of the technical solution of the present invention can realize the static measurement of the cantilever beam displacement with improved sensitivity and dynamic range.
本发明的目的在于提供一种适用于激光干涉测量法的悬臂梁位移测量装置和方法,其能够实现提高了灵敏度和动态范围的悬臂梁位移静态测量。本发明所披露的测量装置和方法,其解决技术问题的主要手段是锁定工作点与补偿,使原本非线性的测量关系变得线性从而提高了测量信号的灵敏度和动态范围。The object of the present invention is to provide a cantilever beam displacement measurement device and method suitable for laser interferometry, which can realize static measurement of cantilever beam displacement with improved sensitivity and dynamic range. The measuring device and method disclosed in the present invention mainly solve technical problems by locking the working point and compensating, so that the original nonlinear measurement relationship becomes linear, thereby improving the sensitivity and dynamic range of the measurement signal.
图2是表示改变激光波长或干涉腔长度时的干涉信号强度变化的曲线图。如图2所示,在激光干涉测量时,改变干涉腔长度(悬臂梁距离光纤出射端面的距离),干涉信号呈周期变化,干涉信号为正弦函数形。在正弦形的干涉信号上斜率最大处为a、b两点,也就是说悬臂梁位移相同的量,在a或b对应的电压变化最大,也就是在a、b位置测量位移最灵敏。为了始终得到最佳的灵敏度,最佳的状态是一直工作在干涉信号上的a或b点,但是当悬臂梁产生位移,干涉信号必然偏离a或b点。Fig. 2 is a graph showing the change in the intensity of the interference signal when the laser wavelength or the length of the interference cavity is changed. As shown in Figure 2, when the length of the interference cavity is changed (the distance between the cantilever beam and the exit end face of the fiber) during laser interferometry, the interference signal changes periodically, and the interference signal is sinusoidal. On the sinusoidal interference signal, the slope of the maximum point is a and b, that is to say, the cantilever beam has the same displacement, and the voltage change corresponding to a or b is the largest, that is, the displacement measurement at a and b is the most sensitive. In order to always get the best sensitivity, the best state is to always work on point a or b on the interference signal, but when the cantilever beam is displaced, the interference signal must deviate from point a or b.
发明人注意到,不仅是悬臂梁的位移能引起干涉信号的产生,激光波长的变化也能引起干涉信号,那么这就可以用激光的波长变化去补偿悬臂梁的位移变化,使干涉信号一直保持在a或b。例如,初始时干涉信号位于a点,电压为V,悬臂梁上的样品受到扭矩使悬臂梁位移了10nm,使干涉腔缩短了,对应的干涉信号偏离a点向右移动,到了V+ΔV;为了使干涉信号保持在V,可以改变激光的波长,波长增加对应于图2中的干涉曲线向右移动,改变适当大小的波长Δλ使干涉信号改变-ΔV,就可以将悬臂梁位移引起的干涉信号变化ΔV补偿掉,从而将干涉信号始终锁定在a点。可以看出,波长的变化Δλ与悬臂梁的位移成正比,所以通过调整激光波长将干涉信号的工作点锁定在a,激光波长的变化也就是悬臂梁的位移变化量。因为a点的斜率最大,所以测量位移最为灵敏。此外,因为够通过改变激光的波长来补偿该位移量,将干涉信号拉回到a点或b点,故测量的动态范围要远高于干涉信号的线性区。The inventor noticed that not only the displacement of the cantilever beam can cause the interference signal, but also the change of the laser wavelength can cause the interference signal, then the wavelength change of the laser can be used to compensate the displacement change of the cantilever beam, so that the interference signal can always be maintained in a or b. For example, the initial interference signal is at point a, and the voltage is V. The sample on the cantilever beam is subjected to torque to displace the cantilever beam by 10nm, shortening the interference cavity, and the corresponding interference signal deviates from point a and moves to the right, reaching V+ΔV; In order to keep the interference signal at V, the wavelength of the laser can be changed. The increase of the wavelength corresponds to the rightward movement of the interference curve in Figure 2. Changing the wavelength Δλ of an appropriate size makes the interference signal change -ΔV, and the interference caused by the displacement of the cantilever beam can be reduced The signal change ΔV is compensated, so that the interference signal is always locked at point a. It can be seen that the change of wavelength Δλ is proportional to the displacement of the cantilever beam, so the working point of the interference signal is locked at a by adjusting the laser wavelength, and the change of the laser wavelength is the displacement change of the cantilever beam. Because point a has the largest slope, it is the most sensitive to measure displacement. In addition, because the displacement can be compensated by changing the wavelength of the laser, the interference signal can be pulled back to point a or point b, so the dynamic range of the measurement is much higher than the linear region of the interference signal.
图3是表示本发明的一个实施方式进行工作点锁定和温度补偿的反馈控制结构的示意图。对图3所示的反馈控制结构,将在实施例部分进行详细说明,这里主要说明其工作原理。激光的波长可通过控制激光器的温度来实现,为了精确的控制激光器的温度,需要对激光器进行温度控制。在本实施方式中,使用PID控制进行控温。前面所说的锁定干涉信号上斜率最大的工作点也需要进行反馈控制。在本实施方式中,同样使用PID方法进行反馈控制。所以本实施方式的测量系统包含两个PID控制单元,即图3所示的PID1和PID2。PID1用于精确控制激光器温度,PID2用于锁定工作点于干涉曲线上的斜率最大点。Fig. 3 is a schematic diagram showing a feedback control structure for operating point locking and temperature compensation according to an embodiment of the present invention. The feedback control structure shown in FIG. 3 will be described in detail in the embodiment part, and its working principle is mainly explained here. The wavelength of the laser can be achieved by controlling the temperature of the laser. In order to accurately control the temperature of the laser, it is necessary to control the temperature of the laser. In this embodiment, temperature control is performed using PID control. The above-mentioned operating point with the largest slope on the locking interference signal also requires feedback control. In this embodiment, the feedback control is also performed using the PID method. Therefore, the measurement system in this embodiment includes two PID control units, namely PID1 and PID2 shown in FIG. 3 . PID1 is used to precisely control the temperature of the laser, and PID2 is used to lock the working point on the maximum slope point on the interference curve.
PID控制器是反馈回路部件,它把收集到的数据和一个参考值进行比较,然后把这个差别用于计算新的输入值,这个新的输入值的目的是可以让系统的数据达到或者保持在参考值。和其他简单的控制运算不同,PID控制器可以根据历史数据和差别的出现率来调整输入值,这样可以使系统更加准确,更加稳定。The PID controller is a feedback loop component that compares the collected data with a reference value, and then uses this difference to calculate a new input value. The purpose of this new input value is to make the data of the system reach or maintain at Reference. Different from other simple control operations, the PID controller can adjust the input value according to the historical data and the occurrence rate of the difference, which can make the system more accurate and stable.
在信号补偿方法中,锁定工作点于最大斜率的功能优选使用PID 控制技术来实现,PID是目前应用最为广泛的调节器,控制规律为比例 (Proportional)、积分(Integral)、微分(Derivative)控制,简称 PID控制,它实际上是一种算法。In the signal compensation method, the function of locking the operating point at the maximum slope is preferably realized using PID control technology. PID is currently the most widely used regulator, and the control law is proportional (Proportional), integral (Integral), and differential (Derivative) control , referred to as PID control, it is actually an algorithm.
然而,对激光器的温度控制和用于锁定干涉信号的工作点的反馈控制不限于采用PID控制,也可以通过其他方式来实现。例如,可以通过计算机程序来构成第一控制器和第二控制器,由它们来分别实现图3所示的PID1和PID2的功能。However, the temperature control of the laser and the feedback control for locking the operating point of the interference signal are not limited to PID control, and can also be implemented in other ways. For example, the first controller and the second controller can be configured by a computer program, and they respectively realize the functions of PID1 and PID2 shown in FIG. 3 .
优选的是,使用本身包含温度控制部件的激光器,例如波长可调半导体激光器。半导体激光器的TEC±是温度控制部件的引脚,用于控制半导体激光器温度,Thermistor是温度传感器的引脚,用于测量半导体激光器的温度。将测量到的温度与目标温度进行差分,作为PID1 的输入,PID1的输出用来激励TEC控制温度。It is preferred to use a laser which itself contains temperature control components, such as a wavelength tunable semiconductor laser. The TEC± of the semiconductor laser is the pin of the temperature control component, which is used to control the temperature of the semiconductor laser, and the Thermistor is the pin of the temperature sensor, which is used to measure the temperature of the semiconductor laser. The difference between the measured temperature and the target temperature is used as the input of PID1, and the output of PID1 is used to stimulate the TEC to control the temperature.
PID2用于锁定干涉信号工作点的位置,选定光强电压信号相对于波长的变化或悬臂梁的位移的变化率成为最大值的光强电压信号。具体而言,选定正弦形的干涉信号的a或b点为工作点,如图2所示,a 点斜率为负,PID反馈为负向,b点斜率为正,PID反馈为正向。如果选择a点为工作点,将激光器的温度调整到与a点对应的激光器温度,这时光电转换器对应a点的输出的电压为V,用PID控制单元反馈控制激光器温度,使光电转换器的电压锁定在V,这样就固定工作点在干涉曲线上的最大斜率处了。工作点a与b的区别在于斜率不同,一个用正反馈,在另一个工作点时用负反馈。PID2 is used to lock the position of the working point of the interference signal, and select the light intensity voltage signal whose change rate of the light intensity voltage signal relative to the wavelength or the displacement of the cantilever beam becomes the maximum value. Specifically, point a or point b of the sinusoidal interference signal is selected as the working point, as shown in Figure 2, the slope of point a is negative, the PID feedback is negative, the slope of point b is positive, and the PID feedback is positive. If point a is selected as the working point, the temperature of the laser is adjusted to the laser temperature corresponding to point a. At this time, the output voltage of the photoelectric converter corresponding to point a is V, and the PID control unit is used to control the temperature of the laser with feedback, so that the photoelectric converter The voltage of V is locked at V, so that the fixed operating point is at the maximum slope on the interference curve. The difference between operating point a and b is that the slope is different, one uses positive feedback, and the other uses negative feedback.
优选的是,锁定的工作点电压信号通过获取光强电压信号的最大值和最小值,并计算所述最大值和所述最小值的平均值来得到。如图2 所示,改变激光器的温度,光干涉信号的光强会周期变化。在本实施方式中,光电探测器测量到的光强的变化,转换成电压信号用数据采集卡采集,可以得到如图2所示的正弦曲线图形,图形上最大值与最小值的平均值即为斜率最大处,如图2中的a与b点,干涉信号采集进入电脑后,可通过软件编程求取图形上的最大与最小值然后去平均来确定a点与b点的电压值。Preferably, the locked operating point voltage signal is obtained by obtaining the maximum value and the minimum value of the light intensity voltage signal, and calculating the average value of the maximum value and the minimum value. As shown in Figure 2, when the temperature of the laser is changed, the light intensity of the optical interference signal will change periodically. In this embodiment, the change of the light intensity measured by the photodetector is converted into a voltage signal and collected by a data acquisition card, and the sinusoidal graph shown in Figure 2 can be obtained, and the average value of the maximum and minimum values on the graph is It is the point with the largest slope, as shown in point a and b in Figure 2. After the interference signal is collected and entered into the computer, the maximum and minimum values on the graph can be obtained through software programming and then averaged to determine the voltage value of point a and point b.
工作点对应干涉信号中斜率最大时的电压值,当施加了外力时悬臂梁位移,也就是干涉腔长度变化,工作点在干涉曲线上发生移动。如果控制激光器的波长(温度),使工作点在干涉曲线上向着反方向移动,则可保持工作点位于干涉曲线上的斜率最大点。这一过程通过 PID2来进行控制,即将干涉信号中斜率最大时的电压值作为基准电压值输入到PID2,实时地锁定工作点位于涉曲线上的斜率最大位置。而激光器的波长(温度)的改变正比于悬臂梁的位移,反映了作用在悬臂梁上扭矩的大小,PID2的输出就是静态位移测量的信号。The working point corresponds to the voltage value when the slope of the interference signal is the largest. When an external force is applied, the cantilever beam is displaced, that is, the length of the interference cavity changes, and the working point moves on the interference curve. If the wavelength (temperature) of the laser is controlled so that the working point moves in the opposite direction on the interference curve, the working point can be kept at the point with the maximum slope on the interference curve. This process is controlled by PID2, that is, the voltage value at the time of the maximum slope in the interference signal is input to PID2 as the reference voltage value, and the working point is locked in real time at the maximum slope position on the interfering curve. The change of the wavelength (temperature) of the laser is proportional to the displacement of the cantilever beam, which reflects the magnitude of the torque acting on the cantilever beam. The output of PID2 is the signal of static displacement measurement.
使用本发明的悬臂梁位移测量装置来测量所述悬臂梁的位移悬臂梁位移测量方法,可以包括以下步骤:Use the cantilever beam displacement measuring device of the present invention to measure the displacement of the cantilever beam The cantilever beam displacement measuring method may include the following steps:
在悬臂梁上载置被测物的步骤;The step of placing the object under test on the cantilever beam;
通过控制激光器的温度改变激光的波长,对悬臂梁照射激光使得发生光的干涉,来获取所述干涉光的光强电压信号,基于所述光强电压信号来确定所述光强电压信号的基准电压值的步骤;By controlling the temperature of the laser to change the wavelength of the laser, irradiating the cantilever beam with laser light to cause light interference to obtain the light intensity voltage signal of the interference light, and determine the reference of the light intensity voltage signal based on the light intensity voltage signal step of voltage value;
通过利用第一控制器和第二控制器进行反馈控制将光强电压信号锁定在基准电压值的步骤;a step of locking the light intensity voltage signal at a reference voltage value by performing feedback control using the first controller and the second controller;
对所述被测物施加外力使其发生位移,基于所述第二控制器输出的所述位移信号来测量所述位移的步骤。A step of applying an external force to the measured object to cause displacement, and measuring the displacement based on the displacement signal output by the second controller.
(实施例)(Example)
下面参照附图来说明本发明的一个具体实施例。A specific embodiment of the present invention will be described below with reference to the accompanying drawings.
本发明是基于激光干涉测距系统的悬臂梁位移测量装置和方法。具体而言,本实施例采用了图1所示的用于测量悬臂梁位移的光纤干涉测量系统。该系统中,激光器使用的是亢特科技(Kongtum)出品的 DFB半导体激光器,由该激光器产生单模激光,波长为1100-2000nm。温度测量原件和控温原件集成在该激光器内部,其中,Thermistor端子为热敏电阻端口,用于测量激光器温度;TEC±端子为温度控制部件的端口,用于控制激光器温度。The invention is a cantilever beam displacement measuring device and method based on a laser interference ranging system. Specifically, this embodiment adopts the optical fiber interferometry system shown in FIG. 1 for measuring the displacement of a cantilever beam. In this system, the laser used is a DFB semiconductor laser produced by Kongtum, which generates single-mode laser with a wavelength of 1100-2000nm. The temperature measurement element and the temperature control element are integrated inside the laser. The Thermistor terminal is the thermistor port for measuring the laser temperature; the TEC± terminal is the port of the temperature control component for controlling the laser temperature.
从激光器出射的激光经过thorlabs出品的90∶10单模光纤耦合器导入到光纤,经过透镜聚焦在悬臂梁上,悬臂梁反射的光和光纤出射端面反射的光发生光学干涉,干涉光信号经光纤耦合器传出,由光电探测器转换为电压信号。The laser light emitted from the laser is introduced into the optical fiber through the 90:10 single-mode fiber coupler produced by Thorlabs, and focused on the cantilever beam through the lens. The output of the coupler is converted into a voltage signal by the photodetector.
图3是表示本发明的一个实施方式进行工作点锁定和温度补偿的反馈控制结构的示意图。该反馈控制结构包括两个PID控制单元。其中,PID1的反馈电压端与激光器201的热敏电阻端口连接,PID1的目标电压端与PID2的输出电压端连接,PID1的输出电压端即控制端与激光器201的温度控制部件的端口连接。PID2的反馈电压端与光电探测器202连接,光强电压信号的基准电压值输入到PID2的目标电压端, PID2的输出电压端即控制端与PID1的目标电压端连接。Fig. 3 is a schematic diagram showing a feedback control structure for operating point locking and temperature compensation according to an embodiment of the present invention. The feedback control structure includes two PID control units. Wherein, the feedback voltage terminal of PID1 is connected to the thermistor port of the laser 201, the target voltage terminal of PID1 is connected to the output voltage terminal of PID2, and the output voltage terminal of PID1, namely the control terminal, is connected to the port of the temperature control part of the laser 201. The feedback voltage terminal of PID2 is connected to the photodetector 202, the reference voltage value of the light intensity voltage signal is input to the target voltage terminal of PID2, and the output voltage terminal of PID2, namely the control terminal, is connected to the target voltage terminal of PID1.
PID1的作用是对半导体激光器进行精确控温,也就是精确控制激光的波长。在测量激光器温度时,恒定电流经过温度传感器,热敏电阻端口的电压值等效为激光器温度作为PID1的反馈信号(Feedback Signal)。PID1的预期值(Desired State)就是温度(波长)的补偿值。The function of PID1 is to precisely control the temperature of the semiconductor laser, that is, to precisely control the wavelength of the laser. When measuring the laser temperature, a constant current passes through the temperature sensor, and the voltage value at the thermistor port is equivalent to the laser temperature as the feedback signal (Feedback Signal) of PID1. The expected value (Desired State) of PID1 is the compensation value of temperature (wavelength).
PID2的作用是对悬臂梁位移进行补偿。它的预期值(Desired State) 就是需要锁定的干涉曲线上的斜率最大点即基准电压值,反馈信号 (Feedback Signal)为由光电探测器输出的干涉电压信号,控制端(Control Signal)的输出为位移信号,其与一个固定的比例系数相乘就是激光器需要达到的目标温度,这就是PID1的预期值(Desired State)。因此PID2的控制端输出的位移信号,是激光器的目标温度相关信号。The function of PID2 is to compensate the displacement of the cantilever beam. Its expected value (Desired State) is the maximum slope point on the interference curve that needs to be locked, that is, the reference voltage value, the feedback signal (Feedback Signal) is the interference voltage signal output by the photodetector, and the output of the control terminal (Control Signal) is The displacement signal, multiplied by a fixed proportional coefficient is the target temperature that the laser needs to reach, which is the expected value of PID1 (Desired State). Therefore, the displacement signal output by the control terminal of PID2 is the target temperature-related signal of the laser.
图4是表示PID控制器的内部电路结构之一例的电路图。内部电路中所用到的运算放大器均为opa627,其中U2,U3,U4对应的运算放大器和电阻电容分别实现比例、积分和微分功能,可变电阻R16、 R17、R18分别控制比例系数、积分系数和微分系数。U5是将最后PID控制电路的输出进行放大或缩小。FIG. 4 is a circuit diagram showing an example of an internal circuit configuration of a PID controller. The operational amplifiers used in the internal circuit are all opa627, in which the operational amplifiers and resistors and capacitors corresponding to U2, U3, and U4 respectively realize proportional, integral and differential functions, and the variable resistors R16, R17, and R18 respectively control the proportional coefficient, integral coefficient and differential coefficient. U5 is to amplify or reduce the output of the final PID control circuit.
为了验证激光干涉测距的悬臂梁静态扭矩的测量方法,以悬臂梁磁扭矩测量为例来证明本发明的具体效果。In order to verify the method for measuring the static torque of the cantilever beam by laser interferometric ranging, the specific effect of the present invention is demonstrated by taking the measurement of the magnetic torque of the cantilever beam as an example.
在该实验中以MnSi微米片为测试对象,其为磁性样品。MnSi微米片是采用聚焦离子束刻蚀技术从MnSi块体上切下的一块。图5A为 MnSi微米片位于Si片上的SEM照片,MnSi微米片尺寸为7μm×15μm ×1μm的薄片,图5B为该MnSi微米片载置到Si悬臂梁上的状态的SEM照片。悬臂梁为纯硅,例如单晶硅制成,其自由端的扩宽的平面是用于激光测距时的反射面。In this experiment, MnSi microsheets are used as the test object, which is a magnetic sample. MnSi microflakes are cut from a MnSi bulk by focused ion beam etching. Figure 5A is an SEM photo of a MnSi microsheet on a Si sheet, and the size of the MnSi microsheet is a sheet of 7 μm x 15 μm x 1 μm, and Figure 5B is a SEM photo of the state where the MnSi microsheet is mounted on a Si cantilever beam. The cantilever beam is made of pure silicon, such as single crystal silicon, and the widened plane at its free end is a reflection surface for laser ranging.
就悬臂梁而言,光学干涉法采用的纯硅材质悬臂梁能实现更低的弹性系数,进一步提高灵敏度。具体而言,悬臂梁的静态位移测量灵敏度取决于悬臂梁的弹性系数,而灵敏的动态扭矩测量不仅需要更低的弹性系数,而且悬臂梁的品质因子越高越灵敏。因而,制备用于光干涉法静态位移测量的悬臂梁只需要考虑如何降低悬臂梁的弹性系数,而不用顾及悬臂梁高的品质因子。所以,采用静态位移测量对悬臂梁品质的要求具有更加宽容。As far as the cantilever beam is concerned, the pure silicon cantilever beam used in optical interferometry can achieve a lower elastic coefficient and further improve sensitivity. Specifically, the static displacement measurement sensitivity of the cantilever depends on the elastic coefficient of the cantilever, while the sensitive dynamic torque measurement not only requires a lower elastic coefficient, but also the higher the quality factor of the cantilever, the more sensitive it is. Therefore, to prepare a cantilever beam for static displacement measurement by optical interferometry, it is only necessary to consider how to reduce the elastic coefficient of the cantilever beam, without considering the high quality factor of the cantilever beam. Therefore, the use of static displacement measurement has a more tolerant requirement on the quality of the cantilever beam.
实验中,采用激光干涉测量法来测量悬臂梁的位移,在外加磁场的作用下,悬臂梁自由端的磁性样品受到扭矩的作用,使悬臂梁弯曲并且改变了悬臂梁的共振频率。实验中分别进行了动态磁扭矩测量与静态磁扭矩测量,以此来反应磁性样品的磁化特性。测试温度为22K,扫场为从-1T到+1T(-10000Oe到+10000Oe)的循环,磁场沿着微米片的面内方向。In the experiment, laser interferometry was used to measure the displacement of the cantilever beam. Under the action of an external magnetic field, the magnetic sample at the free end of the cantilever beam was subjected to torque, which made the cantilever beam bend and changed the resonance frequency of the cantilever beam. In the experiment, dynamic magnetic torque measurement and static magnetic torque measurement were carried out to reflect the magnetization characteristics of magnetic samples. The test temperature is 22K, the sweep field is a cycle from -1T to +1T (-10000Oe to +10000Oe), and the magnetic field is along the in-plane direction of the microsheet.
动态测量方法是实时测量悬臂梁共振频率随磁场的变化,悬臂梁共振频率的测量采取了常用的锁相环(PLL)技术,实现该功能的仪器使用苏黎世仪器公司的HF。静态测量法则使用了本发明的技术。激光光路和电信号转化系统如图2所示,PID控制单元的电路图如图4所示,整个测量系统即反馈控制结构如图3所示,其中PID2的输出电压端口的输出即是静态测量的位移信号。The dynamic measurement method is to measure the change of the resonance frequency of the cantilever beam with the magnetic field in real time. The measurement of the resonance frequency of the cantilever beam adopts the commonly used phase-locked loop (PLL) technology, and the instrument that realizes this function uses the HF of Zurich Instruments. The static measurement method uses the technique of the present invention. The laser optical path and electrical signal conversion system are shown in Figure 2, the circuit diagram of the PID control unit is shown in Figure 4, and the entire measurement system, that is, the feedback control structure, is shown in Figure 3, where the output of the output voltage port of PID2 is the static measurement displacement signal.
图6A是测量共振频率变化的动态测量法的测试结果,图6B是采用了温度补偿的静态测量法测量的悬臂梁的静态位移的测试结果。其中,图6A表示采用动态测量法测量的MnSi微米片面外方向的磁特性,图6B表示采用静态测量法测量的MnSi微米片面外方向的磁性。从图中可以看出动态和静态的磁扭矩测量都反映出了MnSi纳米片的磁性质,但是图6A曲线中有一段的噪声较大,这是由于磁场在±0.4T到± 1T这一段,由于样品磁化态引起的磁损耗导致悬臂梁的Q值降低所引起。FIG. 6A is the test result of the dynamic measurement method for measuring the change of resonance frequency, and FIG. 6B is the test result of the static displacement of the cantilever beam measured by the static measurement method using temperature compensation. 6A shows the magnetic properties of the MnSi micro-sheets in the out-of-plane direction measured by the dynamic measurement method, and FIG. 6B shows the magnetic properties in the out-of-plane direction of the MnSi micro-sheets measured by the static measurement method. It can be seen from the figure that both the dynamic and static magnetic torque measurements reflect the magnetic properties of MnSi nanosheets, but there is a section of the curve in Figure 6A with relatively high noise, which is due to the fact that the magnetic field is in the section from ±0.4T to ±1T. It is caused by the reduction of the Q value of the cantilever due to the magnetic loss caused by the magnetization state of the sample.
通过磁扭矩的测试,说明本发明的静态测量方法能够进行基于激光干涉法的悬臂梁扭矩测量。两种测量方法的对比,静态磁扭矩测量方法得到的数据更加干净,受其它因素的影响也较小。Through the test of the magnetic torque, it shows that the static measurement method of the present invention can measure the torque of the cantilever beam based on the laser interferometry. Compared with the two measurement methods, the data obtained by the static magnetic torque measurement method is cleaner and less affected by other factors.
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