CN114732146A - Method for preparing non-tobacco-agilawood type cigarette material by wet papermaking powder forming technology - Google Patents
Method for preparing non-tobacco-agilawood type cigarette material by wet papermaking powder forming technology Download PDFInfo
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
Landscapes
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a method for preparing a non-tobacco-agilawood type tobacco material by using a wet papermaking powder forming technology, which comprises the following steps: a. pretreating an agilawood raw material; b. preparing superfine powder by using the pretreated agilawood raw material; c. extracting ultrafine powder of lignum Aquilariae Resinatum prepared from lignum Aquilariae Resinatum raw material, and performing solid-liquid separation to obtain solid phase X and filtrate Y; d. pulping and manufacturing the obtained solid-phase substance X to obtain a non-tobacco-heavy fragrance type tobacco material sheet base, and concentrating the filtrate Y to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain the non-tobacco-agilawood-type tobacco material. Solves the problem that the non-tobacco-heavy flavor type cigarette material is prepared by adopting a formula of taking non-tobacco raw materials as main leaf groups and adopting an ultramicro crushing technology and a wet paper-making technology without utilizing processed products (shovelling and hooking) of the stems of the agilawood and natural plant fibers in the prior art.
Description
Technical Field
The invention relates to the technical field of tobacco sheet production by a paper making method (wet method), in particular to a method for preparing a non-tobacco-agilawood type tobacco material by using a wet method paper making powder forming technology.
Background
The production process technology of the tobacco sheet (also called reconstituted tobacco) is developed for more than half a century and mainly goes through three stages of a rolling method, a thick pulp method and a paper-making method, and the paper-making method (wet method) production process technology is dominant in the market of China due to strong plasticity and good filling property. Paper-making (wet) tobacco sheet production the main raw material sources are tobacco by-products such as: tobacco fragments, tobacco dust, tobacco stems, ash, and the like. At present, the tobacco sheets become an indispensable part in Chinese style cigarette leaf group formulas, and the tobacco sheets applied to the cigarette leaf group formulas have the functions of reducing harm and tar, stabilizing product quality, highlighting cigarette style characteristics and the like.
The cigarette paper of the cigarette and the inner cigar sleeve of the machine-made cigar are used as the essential cigarette auxiliary material for designing the cigarette and the machine-made cigar and can be used for wrapping and forming cigarette tobacco shreds (cigar cores of the machine-made cigars). The cigarette paper of cigarettes sold in the market of China and the inner cigar sleeve of a machine-made cigar are basically designed, produced and processed by taking different types and proportions of wood pulp, hemp pulp, straw pulp and the like as raw materials.
Internationally, WTO is added in self countries, particularly after the tobacco control framework convention takes effect formally, Chinese tobacco faces more serious challenges, and the domestic tobacco industry faces new normality under new economic environment after continuous high growth. Therefore, the innovation of cigarette design and development is increased by various cigarette industry enterprises in China, new cigarettes are developed in recent years, and no matter the cigarette package design is changed, the appearance of the cigarettes with different flavors and tastes is changed, so that more opportunities are provided for tobacco consumers to select the cigarettes and the mechanism cigars. However, with the increasing demands of tobacco consumers on the safety, functionality and individuality of cigarettes and mechanism cigars, the innovation of tobacco materials is a problem to be solved urgently in high-quality development of the industry. The traditional tobacco sheet takes tobacco byproducts as raw materials, is applied to a cigarette leaf group formula, mainly represents the original tobacco fragrance, and has limited effect of highlighting other fragrance notes; the cigarette paper and the machine-made cigar inner cover which are designed and produced by only taking wood pulp, hemp pulp, straw pulp and the like as raw materials generally have the problems of wood miscellaneous gas or other miscellaneous gas and the like, and have negative influence on sensory quality.
Aquilaria sinensis is the main resource of Chinese eaglewood, and is mainly distributed in Guangdong and Hainan. Is a traditional and rare medicinal material in China, Japan, India and middle east China, and has various pharmacological effects of spasmolysis, asthma relieving, sedation, analgesia, blood pressure reduction, antibiosis and the like. The ancient expression "heavy sandalwood dragon musk" means agilawood, which is listed as the top-class fragrance since ancient times and is always used as high-grade perfume.
The superfine grinding technology is a new technology developed in recent decades and is a science and technology for researching the special phenomena and functions of micron-sized and even nano-sized substances. As a new processing technology, the superfine grinding technology is mainly applied to the traditional Chinese medicine industry in China, and has the new physical and chemical characteristics of high solubility, high dispersibility, high fluidity and the like by changing the chemical and physical characteristics of raw materials.
In recent years, innovative research on tobacco materials by industrial workers is uninterrupted, and the tobacco sheets prepared from ginkgo leaves, fennel, gynostemma pentaphylla, ginseng, scutellaria baicalensis, platycodon grandiflorum, liquorice, reed rhizome and tobacco byproducts by Zhengchengqian and the like fully retain insoluble effective medicinal components and are coordinated with tobacco fragrance and good in safety; the magnolia flower is added into the tobacco sheet coating liquid in a powder form, such as Zhang wenlong, and the like, so that the effects of covering miscellaneous gases and reducing smoke stimulation are achieved to a certain extent; plum mothers and the like use tea leaves and tea stems as raw materials to manufacture tea leaf sheets for cigarettes, and the influence of the tea leaf sheets on the sensory quality of the cigarettes is researched; chenyinghua invention (patent number: 201210165130.0) combines the powder of agilawood leaf and tobacco component into agilawood tobacco sheet to enrich the tobacco fragrance; the invention relates to a plum noble life invention (patent number: 201310137653. X), which is characterized in that agilawood slices are prepared by adding adhesive and alcoholizing biological agent into agilawood leaf powder and utilizing a thick pulp method; xueshigao et al (patent number: 201310207429.3) discloses a method for preparing agilawood tobacco sheets for cigarette leaf groups by extracting agilawood powder with alcohol, pulping, and mixing with tobacco pulp; the invention of Haiying et al (patent number: 201610252062.0) discloses a method for processing interlayer agilawood reconstituted tobacco by adjusting paper making and forming processes of alcohol extraction, pulping and tobacco pulp of agilawood powder; the invention of Zhougui Yuan et al (patent number: 201610252063.5) discloses a method for preparing reconstituted agilawood tobacco leaves by mixing agilawood powder in a coating liquid and coating with the help of ultrasound assistance. However, on the basis of the formula of the processed product of the stem of the agilawood (namely, shovelling and hooking), natural plant fibers and the like, which all use non-tobacco raw materials as main leaf groups, the contents of preparing the non-tobacco-heavy fragrance type tobacco material by combining the ultramicro crushing technology with the wet papermaking process are not reported.
Disclosure of Invention
The invention aims to provide a method for preparing a non-tobacco-agilawood type tobacco material by using a wet papermaking powder forming technology, and solves the problem that the non-tobacco-agilawood type tobacco material is prepared by using an agilawood stem processing product (shoveling and shredding), natural plant fibers and the like which all use non-tobacco raw materials as main leaf group formulas and combining an ultramicro crushing technology with the wet papermaking technology in the prior art.
In order to solve the technical problems, the invention adopts the following technical scheme:
a method for preparing a non-tobacco-agilawood type cigarette material by using a wet papermaking powder forming technology comprises the following steps: a. pretreating an agilawood raw material; b. preparing superfine powder by using the pretreated agilawood raw material; c. extracting the agilawood superfine powder prepared from the agilawood raw material, and performing solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; d. pulping and manufacturing the obtained solid-phase substance X to obtain a non-tobacco-heavy fragrance type tobacco material sheet base, and concentrating the filtrate Y to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain the non-tobacco-agilawood-type tobacco material.
The solid phase substance X is the residue of the extraction of the agilawood ultrafine powder, the natural plant fiber is any one or the combination of softwood pulp, hardwood pulp, hemp pulp, straw pulp and cotton pulp, after the non-tobacco-agilawood-type tobacco material is obtained, different treatment processes are adopted according to the final application target of the tobacco material, for example, the application targets are cigarette paper of cigarettes and inner eggplant sleeves of machine-made cigars, and the tobacco material can be further calendered, cut and rewound in the production process link according to the actual requirements of the application targets; the calendering refers to calendering the tobacco material by a calender under a certain rolling condition so as to change the physical properties of the tobacco material, such as smoothness, air permeability and the like, and it needs to be stated that not all the tobacco materials need to be calendered, which depends on the product design requirements; the cutting-rewinding refers to that in the production process link, a cutting-rewinding machine is utilized to cut and rewind a mother roll of the cigarette material according to the design requirement so as to obtain the cigarette paper of the cigarette and the required width of the inner cigar sleeve of the machine-made cigar;
compared with the prior art, the process flow disclosed in the application does not need to add other production process equipment, the method is simple and efficient, the implementation is easy, meanwhile, the non-tobacco-heavy fragrance type sheet and the auxiliary materials are prepared according to the adjustment of the raw material formula, the coating liquid formula, the process parameters and the like, and the non-tobacco-agilawood type sheet can be applied to the cigarette leaf group formula to partially or completely replace the traditional tobacco sheet; the auxiliary material of the non-tobacco-agilawood type can be applied to cigarettes and machine-made cigars to replace cigarette paper of the traditional cigarettes and inner cigar sleeves of the machine-made cigars; compared with the process of directly pulping, papermaking and forming by using the agilawood and the natural plant fiber, the method has the advantages that the extraction efficiency of the raw materials is higher by combining the ultramicro crushing technology with the wet papermaking process, and the prepared non-tobacco-heavy fragrance type cigarette material has smoother and finer surface, better compactness and physical property; compared with the traditional tobacco sheet using tobacco as raw material, and the cigarette paper and the machine-made cigar inner eggplant sleeve which only use plant fiber as raw material, the invention selects the tobacco material prepared by non-tobacco raw materials such as agilawood and natural plant fiber, etc., thereby enlarging the application range of the agilawood and improving the economic value of the agilawood; the cigarette additive is applied to cigarette products, and has the function of improving the sensory quality of cigarettes: for example, the aroma of the cigarette product such as agilawood, costustoot and honey is increased, the aroma of the tobacco is enriched, bad miscellaneous gas is covered, the sensory stimulation is reduced, and the like, thereby providing a material basis for the diversified and personalized development of Chinese style cigarettes and comprehensively improving the competitiveness of the Chinese tobacco market.
As a further preferred aspect of the present invention, the agilawood raw material in step a is any one or a combination of shoveling and shredding stems of aquilaria sinensis belonging to the family of reshorridae; the pretreatment of the agilawood raw material in the step a comprises the steps of removing foreign matters, pathological changes and mildewed parts of the agilawood raw material after the agilawood raw material is identified by artificial naked eyes, and drying the agilawood raw material by using an oven at 40 ℃ until the water content is 9-12%.
The shovelling refers to small pieces of Chinese eaglewood bark shoveled off by roughly processed Chinese eaglewood pieces, and the oil content is low; the thread hooking is the crushed material hooked by the fine-processing eaglewood blocks, is closer to the agilawood core material than shoveled and crushed, and contains a small amount of grease.
As a further preferable mode of the invention, the mesh number of the agilawood ultra-fine powder prepared by the pretreated agilawood raw material in the step b is 20-800 m.
The 20-800m superfine powder is obtained by measuring with a laser particle size distribution instrument, representing the particle size with a median particle size D50 index, and converting the mesh number with reference to a mesh number and particle size conversion relation table.
As a further preferred aspect of the present invention, the extraction step in step c is: mixing the agilawood superfine powder and water according to the weight ratio of 1:5-20, and extracting for 1-3h at the temperature of 50-90 ℃.
In a further preferred aspect of the present invention, the pulping and papermaking in step d is that natural plant fibers are pulped by a pulping machine to obtain natural plant fiber pulp, then the solid matter X is uniformly mixed with the natural plant fiber pulp and is formed into pulp by a dynamic or static paper former, and the pulping degree of the natural plant fibers pulped by the pulping machine is 15 ° SR to 90 ° SR.
In a further preferred embodiment of the present invention, when the solid substance X is uniformly mixed with the natural plant fiber slurry, the mass of the solid substance X is 5 to 70 parts by weight by oven dry, and the mass of the natural plant fiber is 30 to 95 parts by weight by oven dry.
Along with the improvement of the proportion of the agilawood ultrafine powder extract residues in the 'non-tobacco-heavy fragrance type' sheet integral formula, the style characteristics of the agilawood are enhanced, the richness of the fragrance is improved, the irritation is reduced, and the comfort is improved.
As a further preference of the invention, when the application of the prepared smoking material is aimed at replacing the traditional tobacco sheet, the absolute dry basis weight of the sheet of the 'non-tobacco-agilawood type' sheet in the step d is 35g/m2～80g/m2When the application target of the manufactured tobacco material is to replace cigarette paper of the traditional cigarette and an inner eggplant sleeve of a machine-made cigar, the absolute dry basis weight of the film base of the auxiliary material of the non-tobacco-agilawood type in the step d is 20g/m2～45g/m2。
In a further preferred embodiment of the present invention, the filtrate Y is concentrated in step d under reduced pressure using a rotary evaporator.
In a further preferred embodiment of the present invention, the coating liquid mixed with the concentrated solution Z in the step e is obtained by adding any one or a combination of propylene glycol, glycerol and an agilawood extract having an agilawood characteristic to the concentrated solution Z, which have a moisturizing effect, and sufficiently mixing the mixture.
And fully mixing to obtain a coating liquid, wherein the solid content percentage of each material in the coating liquid is as follows:
as a further preference of the present invention, the drying temperature in the step e is 100-120 ℃.
Compared with the prior art, the invention can at least achieve one of the following beneficial effects:
1. the adjustment of the raw material formula, the coating liquid formula and the process parameters meets the physical performance requirements of machining the non-tobacco-heavy fragrance type thin sheet and the auxiliary materials when producing cigarettes or machine-made cigars, and simultaneously obtains better sensory experience when smoking.
2. The application range of the agilawood is expanded, and the economic value of the agilawood is improved.
3. The raw materials are extracted more efficiently by combining the superfine grinding technology with the wet papermaking technology, and the prepared non-tobacco-heavy fragrance type cigarette material has smoother and finer surface, better compactness and physical properties.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Specific example 1:
a method for preparing a non-tobacco-agilawood type cigarette material by using a wet papermaking powder forming technology comprises the following steps: a. pretreating an agilawood raw material; b. preparing superfine powder by using the pretreated agilawood raw material; c. extracting the agilawood superfine powder prepared from the agilawood raw material, and performing solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; d. pulping and manufacturing the obtained solid-phase substance X to obtain a non-tobacco-fragrant tobacco material sheet base, and concentrating the filtrate Y to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain the non-tobacco-agilawood-type tobacco material.
Specific example 2:
this example further illustrates, on the basis of specific example 1, a method for preparing a "non-tobacco-agilawood-type" tobacco material by using a wet papermaking powder forming technique, including the steps of: a. pretreating lignum Aquilariae Resinatum raw material, namely removing foreign matter, pathological changes and mildewed parts of the lignum Aquilariae Resinatum raw material after artificial visual identification, and drying the lignum Aquilariae Resinatum raw material in an oven at 40 ℃ until the water content is 9%; b. preparing superfine powder of pretreated lignum Aquilariae Resinatum raw material into 50m lignum Aquilariae Resinatum superfine powder; c. extracting the agilawood superfine powder prepared from the agilawood raw material, mixing the agilawood superfine powder and water according to the weight ratio of 1:5 during extraction, extracting for 1h at 50 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; d. pulping and manufacturing the obtained solid-phase substance X to obtain a non-tobacco-fragrant sediment tobacco material sheet base, wherein in the pulping and manufacturing process, the pulping degree of natural plant fiber pulping by using a pulping machine is 15 DEG SR, when the solid-phase substance X and the natural plant fiber pulp are uniformly mixed, the mass of the solid-phase substance X is 50 absolute dry weight parts, the mass of the natural plant fiber is 50 absolute dry weight parts, the absolute dry weight of the sheet base formed by papermaking is 35g/m, and meanwhile, concentrating the filtrate Y to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain a non-tobacco-agilawood-type tobacco material, wherein the solid content percentage of each material in the coating liquid mixed with the concentrated solution Z is as follows: mixing concentrate C5%, propylene glycol 0.01%, glycerol 0.01%, and lignum Aquilariae Resinatum extract 0.0001% to obtain coating solution; the drying temperature in step e is 100 ℃.
Specific example 3:
this example further illustrates, on the basis of specific example 1, a method for preparing a "non-tobacco-agilawood-type" tobacco material by using a wet papermaking powder forming technique, including the steps of: a. pretreating lignum Aquilariae Resinatum raw material, namely removing foreign matter, pathological changes and mildewed parts of the lignum Aquilariae Resinatum raw material after artificial visual identification, and drying the lignum Aquilariae Resinatum raw material in an oven at 40 ℃ until the water content is 12%; b. preparing superfine powder of pretreated lignum Aquilariae Resinatum raw material into 800m lignum Aquilariae Resinatum superfine powder; c. extracting the agilawood superfine powder prepared from the agilawood raw material, mixing the agilawood superfine powder and water according to the weight ratio of 1:20 during extraction, extracting for 3 hours at 90 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; d. pulping and papermaking by using the obtained solid-phase substance X to obtain a non-tobacco-heavy fragrance type tobacco material sheet base, wherein in the pulping and papermaking process, the pulping degree of pulping natural plant fibers by using a pulping machine is 90 DEG SR, when the solid-phase substance X is uniformly mixed with natural plant fiber pulp, the mass of the solid-phase substance X is 50 absolute dry weight parts, the mass of the natural plant fibers is 50 absolute dry weight parts, the absolute dry weight of the sheet base formed by papermaking is 80g/m, and meanwhile, concentrating the filtrate Y to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain a non-tobacco-agilawood-type tobacco material, wherein the solid content percentage of each material in the coating liquid mixed with the concentrated solution Z is as follows: mixing the concentrate C40%, propylene glycol 5.0%, glycerol 5.0%, and lignum Aquilariae Resinatum extract 5.0% to obtain coating solution, and drying at 120 deg.C in step e.
Specific example 4:
this example further illustrates, on the basis of specific example 1, a method for preparing a "non-tobacco-agilawood-type" tobacco material by using a wet papermaking powder forming technique, including the steps of: a. pretreating lignum Aquilariae Resinatum raw material, namely removing foreign matter, pathological changes and mildewed parts of the lignum Aquilariae Resinatum raw material after artificial visual identification, and drying the lignum Aquilariae Resinatum raw material at 40 ℃ until the water content is 10%; b. preparing ultramicro powder from the pretreated agilawood raw material to prepare 300m agilawood ultramicro powder; c. extracting the agilawood superfine powder prepared from the agilawood raw material, mixing the agilawood superfine powder and water according to the weight ratio of 1:10 during extraction, extracting for 1.5h at the temperature of 60 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; d. pulping and papermaking are carried out by utilizing the obtained solid-phase substance X to obtain a non-tobacco-heavy fragrance type tobacco material sheet base, in the pulping and papermaking process, the pulping degree of pulping natural plant fibers by utilizing a pulping machine is 65 DEG SR, when the solid-phase substance X is uniformly mixed with natural plant fiber pulp, the mass of the solid-phase substance X is 50 absolute dry weight parts, the mass of the natural plant fibers is 50 absolute dry weight parts, the absolute dry weight of the sheet base molded by papermaking is 55g/m, and meanwhile, the filtrate Y is concentrated to obtain concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain a non-tobacco-agilawood-type tobacco material, wherein the coating liquid mixed with the concentrated solution Z contains the following materials in percentage by solid content: mixing the concentrate C20%, propylene glycol 2.5%, glycerol 2.0%, and lignum Aquilariae Resinatum extract 3.0% to obtain coating solution, and drying at 115 deg.C in step e.
The non-tobacco-agilawood type slices obtained in examples 2 to 4 were cut into shreds by a shredder, and the shreds were rolled into the same blank tobacco tube, and sensory quality was judged by professional smokers, and the comprehensive sensory quality ranking was: example 4 is superior to example 3 and to example 2.
On the basis of example 4, the influence of the oven dry ingredient ratio of the raw materials on the sensory quality of the non-tobacco-agilawood type sheet is researched, and comparative examples 1 to 3 and example 4 are only different in oven dry ingredient ratio of the raw materials, and are detailed in table 1:
TABLE 1 Effect of raw material oven dry mix ratio on organoleptic quality of non-tobacco-eaglewood type sheets
| Raw material seed Class I | Comparative example 1 | Comparative example 2 | Example 4 | Comparative example 3 |
| Solid phase A (Chenxiang super) Micro powder lifter Residue of material) | 5% | 30% | 50% | 70% |
| Natural plant Biological fiber | 95% | 70% | 50% | 30% |
| Sensory quality Quantitative evaluation | Chen Xiang is weak in style and manifested as heavy Fragrant, roasted fragrant, nasal cavity has strong fragrance A rough, burning sensation and a dry throat Thorns, oral stings | The style and characteristics of Chinese eaglewood are more obvious Now is the fragrant of Chinese eaglewood, roasted fragrance and nose A burred, glowing and dry throat Thorns, oral stings | The style of Chinese eaglewood is obvious Now is lignum Aquilariae Resinatum, baked incense and sweet The smell, the burr and burning of the nasal cavity, oral cavity sting | The style and the characteristics of the agilawood are obvious, is prepared from eaglewood, baked incense, Sweet and fragrant, and nasal hair Thorns, oral stings |
As shown in the table above, sensory quality determination was performed by ranking method, and the overall quality ranking was: comparative example 3 > example 4 > comparative example 2 > comparative example 1.
According to sensory quality judgment, through adjustment of the oven-dry ratio of the raw materials, along with improvement of the proportion of the agilawood ultrafine powder extract residues in the overall formula of the non-tobacco-agilawood-type sheet, the style characteristics of the agilawood are enhanced, the aroma richness is improved, the irritation is reduced, and the comfort is improved.
Specific example 5:
this example further illustrates, on the basis of specific example 1, a method for preparing a "non-tobacco-agilawood" type tobacco material by using a wet papermaking powder forming technology, including the steps of: a. pretreating lignum Aquilariae Resinatum raw material, namely removing foreign matter, pathological changes and mildewed parts of the lignum Aquilariae Resinatum raw material after artificial visual identification, and drying the lignum Aquilariae Resinatum raw material at 40 ℃ until the water content is 10%; b. preparing superfine powder of pretreated lignum Aquilariae Resinatum raw material into 100m lignum Aquilariae Resinatum superfine powder; c. extracting the agilawood superfine powder prepared from the agilawood raw material, mixing the agilawood superfine powder and water according to the weight ratio of 1:7 during extraction, extracting for 2 hours at the temperature of 65 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; d. pulping and papermaking are carried out by utilizing the obtained solid-phase substance X to obtain a non-tobacco-heavy fragrance type tobacco material sheet base, in the pulping and papermaking process, the pulping degree of the pulping of the broad leaf wood pulp fibers by utilizing a pulping machine is 70 DEG SR, when the solid-phase substance X and the broad leaf wood pulp fiber slurry are uniformly mixed, the mass of the solid-phase substance X is 40 absolute dry weight parts, the mass of the broad leaf wood pulp fibers is 60 absolute dry weight parts, the absolute dry weight of the sheet base formed by papermaking is 60g/m, and meanwhile, the filtrate Y is concentrated to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, drying to obtain a non-tobacco-agilawood-type tobacco material, wherein the solid content percentages of the materials in the coating liquid mixed with the concentrated solution Z are respectively configured according to the following table 2: the drying temperature in step e was 116 ℃.
Comparative examples 4 to 7 in table 2 differ only in the composition of the coating liquid, and the "non-tobacco-agilawood-type" sheets obtained in comparative examples 4 to 7 were cut into pieces by a shredder and wrapped in the same blank tobacco tube, and subjected to sensory quality judgment by a professional inspector to study the influence of the composition of the coating liquid on the sensory quality of the "non-tobacco-agilawood-type" sheets.
TABLE 2 Effect of coating liquid composition on the sensory quality of "non-tobacco-eaglewood-type" sheets
| Coating composition Cloth Liquid for treating urinary tract infection Group of Portions are | Comparative example 4 | Comparative example 5 | Comparative example 6 | Comparative example 7 |
| Concentration Shrinking device Liquid C | — | 20% | — | 20% |
| C3 II Alcohol(s) | — | — | 1.5% | 1.5% |
| Third to fourth III Alcohol(s) | — | — | 1.5% | 1.5% |
| Sink with a metal plate Incense stick Lifting device Get Article (A) | — | — | 1.5% | 1.5% |
| Feeling of Officer Quality of food Measurement of Review of Price of | The wood gas is relatively obvious, and the wood gas is relatively obvious, nasal cavity and throat thorns A burning sensation Strong, mouth stings | The agilawood has more obvious style and characteristics Is prepared from lignum Aquilariae Resinatum, baked incense, and sweet aroma, woody-qi manifesting as nasal burr and oral cavity Relatively clean and slightly marked with stings | Slightly obvious flavor and characteristics of Chen Xiang Is prepared from lignum Aquilariae Resinatum, baked incense and wood gas Obviously, the nasal cavity is scorched and the throat is dry and stabbed, slightly residual and coating feeling in the oral cavity | The agilawood has more obvious style characteristics and is represented as Agilawood, roasted incense, costustoot and honey sweet note, rich fragrance, slightly burr in nasal cavity and mouth feeling Slight sting and coating sensation in the cavity |
As shown in the table above, sensory quality determination was performed by ranking method, and the comprehensive quality ranking was: comparative example 7 > comparative example 5 > comparative example 6 > comparative example 4.
The sensory quality judgment shows that the adjustment of the components of the coating liquid has influence on the sensory quality of the non-tobacco-heavy fragrance type sheet, and compared with the comparative example 4, the increase of the concentrated solution C or the addition of the humectant and the agilawood extract in a certain range has different contributions to the improvement of the sensory quality.
Specific example 6:
this example further illustrates, on the basis of specific example 1, a method for preparing a "non-tobacco-agilawood" type tobacco material by using a wet papermaking powder forming technology, including the steps of: a. pretreating lignum Aquilariae Resinatum raw material, namely removing foreign matter, pathological changes and mildewed parts of the lignum Aquilariae Resinatum raw material after artificial visual identification, and drying the lignum Aquilariae Resinatum raw material at 40 ℃ until the water content is 10%; b. preparing superfine powder from the pretreated agilawood raw material, and preparing the superfine powder into agilawood superfine powder according to the table 3; c. extracting the agilawood superfine powder prepared from the agilawood raw material, mixing the agilawood superfine powder and water according to the weight ratio of 1:13 during extraction, extracting for 1h at 70 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; d. pulping and papermaking by using the obtained solid-phase substance X to obtain a non-tobacco-heavy fragrance type tobacco material sheet base, wherein in the pulping and papermaking process, the pulping degree of the softwood pulp fiber pulping by using a pulping machine is 80 DEG SR, when the solid-phase substance X and the softwood pulp fiber pulp are uniformly mixed, the mass of the solid-phase substance X is 50 absolute dry weight parts, the mass of the softwood pulp fiber is 50 absolute dry weight parts, the absolute dry weight of the sheet base formed by papermaking is 35g/m, and meanwhile, the filtrate Y is concentrated to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain a non-tobacco-agilawood-type tobacco material, wherein the coating liquid mixed with the concentrated solution Z contains the following materials in percentage by solid content: mixing concentrate C25%, propylene glycol 1.5%, glycerol 1.5%, and lignum Aquilariae Resinatum extract 1.5% to obtain coating solution, and drying at 105 deg.C in step e.
Comparative examples 8 to 10 in table 3 are different only in the mesh number of the agilawood ultra-fine powder, the non-tobacco-agilawood auxiliary materials obtained in comparative examples 8 to 10 are rolled and formed to prepare samples to replace cigarette paper of cigarettes or inner cigar sleeves of machine-made cigars, the influence of the agilawood ultra-fine powder with different mesh numbers on the sensory quality and the rolling and forming of samples prepared from the non-tobacco-agilawood auxiliary materials is researched, and sensory evaluation is carried out by professional smokers after sample preparation.
TABLE 3 influence of different mesh number of superfine powder on sensory quality and rolling formation of "non-tobacco-eaglewood type" auxiliary material sample
| Sink with a metal plate Incense stick Super-super Micro-meter Powder | Comparative example 8 | Comparative example 9 | Comparative example 10 |
| Eyes of a user Number of （m） | 20 | 350 | 800 |
| Feeling of Officer Quality of food Measurement of Review of Price of | The agilawood has more obvious style characteristics and is dry Grass flavor, agilawood, baking flavor and honey-sweet flavor, a slight burr in the nasal cavity and a sweet and fluid-producing oral cavity Feel good | The agilawood has more obvious style and characteristics and is represented as hay Fragrant, eaglewood, roasted fragrant, sweet and fragrant, nasal cavity A slight burr and moist and sweet mouth and promoting the production of body fluid Cool feeling | The agilawood has more obvious style and characteristics and is represented as hay Fragrant, eaglewood, roasted fragrant, sweet and fragrant, nasal cavity A slight burr and a sweet mouth and promoting the production of body fluid Cool feeling |
| Roll of paper System for making Become into Model (III) | The paper has good tensile property and is easy to roll; the paper surface has a grainy and rough feel Displaying; the powder is separated from the paper | The paper has good tensile property and is easy to roll; paper The surface of the sheet is smoother; no powder separation occurs Paper phenomenon | The paper has good tensile property and is easy to roll; paper Smooth surface, good soft feeling and no appearance Powder separation from paper |
As shown in the table above, for the cigarette paper based on the non-tobacco-agilawood auxiliary material for replacing cigarettes or the inner cigar sleeve rolling forming sample of the machine-made cigar, the ultrafine powder with different meshes has little influence on the sensory quality of the sample of the non-tobacco-agilawood auxiliary material, and the main influence is shown in the rolling forming process. Within a certain range, with the increase of the mesh number of the superfine powder, the surface of the auxiliary material becomes smoother and more flexible, and the phenomenon of paper powder falling is improved.
Specific example 7:
this example further illustrates, on the basis of specific example 1, a method for preparing a "non-tobacco-agilawood" type tobacco material by using a wet papermaking powder forming technology, including the steps of: a. pretreating lignum Aquilariae Resinatum raw material, namely removing foreign matter, pathological changes and mildewed parts of the lignum Aquilariae Resinatum raw material after artificial visual identification, and drying the lignum Aquilariae Resinatum raw material at 40 ℃ until the water content is 10%; b. preparing ultramicro powder from the pretreated agilawood raw material to prepare 300m agilawood ultramicro powder; c. extracting the agilawood superfine powder prepared from the agilawood raw material, mixing the agilawood superfine powder and water according to the weight ratio of 1:15 during extraction, extracting for 1.2h at 63 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; d. pulping and manufacturing the obtained solid-phase substance X to obtain a non-tobacco-heavy fragrance type tobacco material sheet base, wherein in the pulping and manufacturing process, a pulping degree of pulping hemp pulp fibers by using a pulping machine is 55 DEG SR, when the solid-phase substance X and the hemp pulp fibers are uniformly mixed, the mass of the solid-phase substance X is 45 absolute dry weight parts, the mass of the hemp pulp fibers is 55 absolute dry weight parts, the sheet base is manufactured and formed according to the absolute dry quantitative paper manufacturing of the table 4, and meanwhile, the filtrate Y is concentrated to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain a non-tobacco-agilawood-type tobacco material, wherein the coating liquid mixed with the concentrated solution Z contains the following materials in percentage by solid content: mixing the concentrate C22.0%, propylene glycol 1.2%, glycerol 1.2%, and lignum Aquilariae Resinatum extract 1.2% to obtain coating solution, and drying at 108 deg.C in step e.
Comparative examples 11 to 13 in table 4 are different only in the quantitative absolute dry basis of the sheet, the auxiliary materials of the "non-tobacco-agilawood type" obtained in comparative examples 11 to 13 are used for replacing cigarette paper of cigarettes or inner cigar sleeve rolling and forming samples of machine-made cigars, the quantitative absolute dry basis of different sheets is studied, the influence on the sensory quality and the rolling and forming of the samples of the auxiliary materials of the "non-tobacco-agilawood type" is studied, and sensory quality judgment is carried out by professional smokers after sample preparation.
TABLE 4 influence of different base absolute dry quantities on sensory quality and roll forming of "non-tobacco-eaglewood type" auxiliary material sample preparation
| Sheet Base of | Comparative example 11 | Comparative example 12 | Comparative example 13 |
| Insulation for a building Dry matter Stator Measurement of （g/ m²） | 20 | 30 | 45 |
| Feeling of Official officer Quality of food Measurement of Review of Price of | The agilawood has more obvious style characteristics and is represented as Dried grass flavor, agilawood, roasted flavor and sweet flavor Yun, a slightly burred nasal cavity and a moist oral cavity Sweet and producing saliva with slight cooling sensation | The agilawood has more obvious style and characteristics and is represented as hay Fragrant, eaglewood, roasted fragrant, sweet and fragrant, and tactile sensation Slightly coarse, slightly burred nasal cavity and moist oral cavity Sweet and promoting the production of body fluid with a slight cooling feeling | The agilawood has more obvious style characteristics and is expressed by dry grass flavor, Agalloch eaglewood, roasted incense, costustoot, sweet and fragrant flavor and coarse texture Coarse, the nasal cavity has slight burrs, the oral cavity is sweet and generates body fluid, has slight cool feeling and coating feeling |
| Roll of paper Making (A) a To become Model (II) | Poor tensile properties and low tendency to curl Preparing; the surface of the paper is smoother; is not out The phenomenon that the powder is separated from the paper | The paper has good tensile property and is easy to roll; paper The surface of the sheet is smoother; no powder detachment Paper phenomenon | Good tensile properties of paper, but in high quantitative amounts, the same applies Easy 'cracking' under the glue amount and failure probability of sample preparation Higher; the surface of the paper is smoother; no powder appeared Phenomenon of paper separation |
As shown in the table above, the cigarette paper based on the non-tobacco-agilawood auxiliary material for replacing cigarettes or the inner eggplant sleeve roll forming sample of the machine-made cigar, and the main influence of different sheet base absolute dry weight on the sample preparation sample of the non-tobacco-agilawood auxiliary material comprises the sensory quality and the roll forming process links. The absolute dry quantity of the film base is too low and too high, which affects the roll forming of the sample; sensory quality judgment is carried out by a sorting method, and comprehensive quality sorting comprises the following steps: comparative example 12 > comparative example 11 > comparative example 13.
Although the invention has been described with reference to a number of illustrative embodiments thereof, it should be understood that numerous other modifications and embodiments can be devised by those skilled in the art that will fall within the scope and spirit of the principles of this disclosure. More specifically, various variations and modifications are possible in the component parts and/or arrangements of the subject combination arrangement within the scope of the disclosure and claims of this application. In addition to variations and modifications in the component parts and/or arrangements, other uses will also be apparent to those skilled in the art.
Claims (10)
1. A method for preparing a non-tobacco-agilawood type tobacco material by using a wet papermaking powder forming technology is characterized by comprising the following steps: the method comprises the following steps: a. pretreating an agilawood raw material; b. preparing superfine powder by using the pretreated agilawood raw material; c. extracting the agilawood superfine powder prepared from the agilawood raw material, and performing solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; d. pulping and manufacturing the obtained solid-phase substance X to obtain a non-tobacco-heavy fragrance type tobacco material sheet base, and concentrating the filtrate Y to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain the non-tobacco-agilawood-type tobacco material.
2. The method for preparing the non-tobacco-agilawood-type cigarette material by using the wet papermaking powder forming technology as claimed in claim 1, wherein the method comprises the following steps: the agilawood raw material in the step a is any one or a combination of shoveling and hooking stems of aquilaria sinensis of the Thymelaeaceae family; and a step a of pretreating the agilawood raw material, which is to remove foreign matters, pathological changes and mildewed parts of the agilawood raw material after the agilawood raw material is identified by naked eyes, and dry the agilawood raw material by using an oven at 40 ℃ until the water content is 9-12%.
3. The method for preparing the non-tobacco-agilawood type tobacco material by using the wet papermaking powder forming technology as claimed in claim 1, wherein the method comprises the following steps: the mesh number of the agilawood superfine powder prepared by the pretreated agilawood raw material in the step b is 20-800 m.
4. The method for preparing the non-tobacco-agilawood type tobacco material by using the wet papermaking powder forming technology as claimed in claim 1, wherein the method comprises the following steps: the extraction step in the step c is as follows: mixing the agilawood superfine powder and water according to the weight ratio of 1:5-20, and extracting for 1-3h at the temperature of 50-90 ℃.
5. The method for preparing the non-tobacco-agilawood-type cigarette material by using the wet papermaking powder forming technology as claimed in claim 1, wherein the method comprises the following steps: the pulping and papermaking in the step d is to pulp natural plant fibers by using a pulping machine to obtain natural plant fiber slurry, then uniformly mix the solid-phase substance X with the natural plant fiber slurry and then use a dynamic or static paper former to make and form, and the pulping degree of the natural plant fiber pulping by using the pulping machine is 15-90 DEG SR.
6. The method for preparing the non-tobacco-agilawood-type cigarette material by using the wet papermaking powder forming technology as claimed in claim 5, wherein the method comprises the following steps: when the solid phase substance X and the natural plant fiber slurry are uniformly mixed, the mass of the solid phase substance X is 5-70 absolute dry weight parts, and the mass of the natural plant fiber is 30-95 absolute dry weight parts.
7. The method for preparing the non-tobacco-agilawood-type cigarette material by using the wet papermaking powder forming technology as claimed in claim 1, wherein the method comprises the following steps: when the application of the prepared tobacco material aims at replacing the traditional tobacco sheets, the absolute dry basis weight of the sheets of the non-tobacco-agilawood type sheets in the step d is 35g/m2～80g/m2When the application target of the prepared tobacco material is to replace the cigarette paper of the traditional cigarette and the inner eggplant sleeve of the machine-made cigar, the absolute dry basis weight of the base of the auxiliary material of the non-tobacco-agilawood type in the step d is 20g/m2～45g/m2。
8. The method for preparing the non-tobacco-agilawood-type cigarette material by using the wet papermaking powder forming technology as claimed in claim 1, wherein the method comprises the following steps: and d, concentrating the filtrate Y in the step d by adopting a rotary evaporator for reduced pressure concentration.
9. The method for preparing the non-tobacco-agilawood type tobacco material by using the wet papermaking powder forming technology as claimed in claim 1, wherein the method comprises the following steps: the coating liquid mixed with the concentrated solution Z in the step e is obtained by adding any one or combination of propylene glycol, glycerol and agilawood extract with agilawood characteristic with moisturizing effect into the concentrated solution Z and fully mixing.
10. The method for preparing the non-tobacco-agilawood-type cigarette material by using the wet papermaking powder forming technology as claimed in claim 1, wherein the method comprises the following steps: the drying temperature in the step e is 100-.
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| CN103238922A (en) * | 2013-05-29 | 2013-08-14 | 云南烟草科学研究院 | Method of preparing tobacco sheet with agilawood characteristic |
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| WO2020167805A1 (en) * | 2019-02-11 | 2020-08-20 | Schweitzer-Mauduit International, Inc. | Aerosol generating material comprising reconstituted cocoa husk fiber material |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103238922A (en) * | 2013-05-29 | 2013-08-14 | 云南烟草科学研究院 | Method of preparing tobacco sheet with agilawood characteristic |
| CN103783651A (en) * | 2014-01-22 | 2014-05-14 | 江苏中烟工业有限责任公司 | Application of supercritically-extracted aquilaria sinensis in tobacco reproduction technology with paper making method |
| CN107183778A (en) * | 2017-07-03 | 2017-09-22 | 中烟施伟策（云南）再造烟叶有限公司 | A kind of papermaking-method reconstituted tobaccos preparation method of the natural plant powder containing ultra micro |
| WO2020167805A1 (en) * | 2019-02-11 | 2020-08-20 | Schweitzer-Mauduit International, Inc. | Aerosol generating material comprising reconstituted cocoa husk fiber material |
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Application publication date: 20220712 |