CN114469792A - A cosmetic composition containing folium Cannabis extract and its preparation method - Google Patents
A cosmetic composition containing folium Cannabis extract and its preparation method Download PDFInfo
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- CN114469792A CN114469792A CN202011145325.0A CN202011145325A CN114469792A CN 114469792 A CN114469792 A CN 114469792A CN 202011145325 A CN202011145325 A CN 202011145325A CN 114469792 A CN114469792 A CN 114469792A
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 52
- 239000000203 mixture Substances 0.000 title claims abstract description 52
- 239000000284 extract Substances 0.000 title claims abstract description 15
- 241000218236 Cannabis Species 0.000 title claims description 12
- 238000002360 preparation method Methods 0.000 title abstract description 9
- 239000000419 plant extract Substances 0.000 claims abstract description 36
- 244000269722 Thea sinensis Species 0.000 claims abstract description 24
- 235000009569 green tea Nutrition 0.000 claims abstract description 23
- 244000025254 Cannabis sativa Species 0.000 claims abstract description 21
- 241000196324 Embryophyta Species 0.000 claims abstract description 20
- 235000012766 Cannabis sativa ssp. sativa var. sativa Nutrition 0.000 claims abstract description 19
- 235000012765 Cannabis sativa ssp. sativa var. spontanea Nutrition 0.000 claims abstract description 19
- 235000009120 camo Nutrition 0.000 claims abstract description 19
- 235000005607 chanvre indien Nutrition 0.000 claims abstract description 19
- 239000011487 hemp Substances 0.000 claims abstract description 19
- 239000000463 material Substances 0.000 claims abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 229940070641 chamomile flowers Drugs 0.000 claims abstract description 7
- 150000001875 compounds Chemical class 0.000 claims abstract description 6
- 241000167550 Centella Species 0.000 claims abstract description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 23
- 244000146462 Centella asiatica Species 0.000 claims description 18
- 235000004032 Centella asiatica Nutrition 0.000 claims description 18
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 claims description 18
- POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 claims description 16
- 239000002904 solvent Substances 0.000 claims description 16
- -1 polydimethylsiloxane Polymers 0.000 claims description 15
- 239000002562 thickening agent Substances 0.000 claims description 15
- 244000042664 Matricaria chamomilla Species 0.000 claims description 14
- 239000003995 emulsifying agent Substances 0.000 claims description 14
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 claims description 14
- 238000001914 filtration Methods 0.000 claims description 13
- 239000004519 grease Substances 0.000 claims description 13
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 13
- 235000007232 Matricaria chamomilla Nutrition 0.000 claims description 12
- 239000003906 humectant Substances 0.000 claims description 12
- 239000003755 preservative agent Substances 0.000 claims description 12
- 235000007866 Chamaemelum nobile Nutrition 0.000 claims description 10
- 230000002335 preservative effect Effects 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
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- 239000004264 Petrolatum Substances 0.000 claims description 9
- 235000018597 common camellia Nutrition 0.000 claims description 9
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 9
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 9
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 claims description 9
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims description 9
- 229940066842 petrolatum Drugs 0.000 claims description 9
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- 238000003756 stirring Methods 0.000 claims description 9
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 claims description 9
- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 claims description 8
- SNPLKNRPJHDVJA-ZETCQYMHSA-N D-panthenol Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCCO SNPLKNRPJHDVJA-ZETCQYMHSA-N 0.000 claims description 8
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- 238000000034 method Methods 0.000 claims description 8
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- NLMKTBGFQGKQEV-UHFFFAOYSA-N 2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-(2-hexadecoxyethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethanol Chemical compound CCCCCCCCCCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO NLMKTBGFQGKQEV-UHFFFAOYSA-N 0.000 claims description 7
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 7
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- 229920002125 Sokalan® Polymers 0.000 claims description 7
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- 239000008367 deionised water Substances 0.000 claims description 7
- 229910021641 deionized water Inorganic materials 0.000 claims description 7
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 7
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 claims description 7
- 239000000194 fatty acid Substances 0.000 claims description 7
- 229930195729 fatty acid Natural products 0.000 claims description 7
- 125000005456 glyceride group Chemical group 0.000 claims description 7
- 239000002540 palm oil Substances 0.000 claims description 7
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 239000003607 modifier Substances 0.000 claims description 6
- 239000003921 oil Substances 0.000 claims description 5
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- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 4
- 244000044822 Simmondsia californica Species 0.000 claims description 4
- 235000004433 Simmondsia californica Nutrition 0.000 claims description 4
- NENOAJSZZPODGJ-OIMNJJJWSA-N [(2r)-2-[(2r,3r,4s)-3,4-dihydroxyoxolan-2-yl]-2-hydroxyethyl] octanoate Chemical compound CCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O NENOAJSZZPODGJ-OIMNJJJWSA-N 0.000 claims description 4
- 241000628997 Flos Species 0.000 claims description 3
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- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 claims description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 2
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 2
- XPFCZYUVICHKDS-UHFFFAOYSA-N 3-methylbutane-1,3-diol Chemical compound CC(C)(O)CCO XPFCZYUVICHKDS-UHFFFAOYSA-N 0.000 claims description 2
- 235000018936 Vitellaria paradoxa Nutrition 0.000 claims description 2
- 241001135917 Vitellaria paradoxa Species 0.000 claims description 2
- 230000002421 anti-septic effect Effects 0.000 claims description 2
- 229940056318 ceteth-20 Drugs 0.000 claims description 2
- 229920001577 copolymer Polymers 0.000 claims description 2
- 239000006071 cream Substances 0.000 claims description 2
- 229940008099 dimethicone Drugs 0.000 claims description 2
- 229960005150 glycerol Drugs 0.000 claims description 2
- 229940075529 glyceryl stearate Drugs 0.000 claims description 2
- 229920002674 hyaluronan Polymers 0.000 claims description 2
- 229960003160 hyaluronic acid Drugs 0.000 claims description 2
- AEIJTFQOBWATKX-UHFFFAOYSA-N octane-1,2-diol Chemical compound CCCCCCC(O)CO AEIJTFQOBWATKX-UHFFFAOYSA-N 0.000 claims description 2
- 229960005323 phenoxyethanol Drugs 0.000 claims description 2
- 229960004063 propylene glycol Drugs 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- 229940057910 shea butter Drugs 0.000 claims description 2
- 239000002671 adjuvant Substances 0.000 claims 2
- 239000007858 starting material Substances 0.000 claims 1
- 239000004480 active ingredient Substances 0.000 abstract description 3
- 230000000694 effects Effects 0.000 description 26
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 12
- 206010033425 Pain in extremity Diseases 0.000 description 11
- 230000036620 skin dryness Effects 0.000 description 9
- 238000012360 testing method Methods 0.000 description 9
- 239000000126 substance Substances 0.000 description 8
- 235000011187 glycerol Nutrition 0.000 description 5
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 4
- 239000002024 ethyl acetate extract Substances 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 4
- 150000003254 radicals Chemical class 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 238000010992 reflux Methods 0.000 description 3
- 230000002000 scavenging effect Effects 0.000 description 3
- 238000002791 soaking Methods 0.000 description 3
- 235000008697 Cannabis sativa Nutrition 0.000 description 2
- 206010013786 Dry skin Diseases 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 238000007605 air drying Methods 0.000 description 2
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 description 2
- 235000020346 chamomile tea Nutrition 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 2
- 230000037336 dry skin Effects 0.000 description 2
- 239000000469 ethanolic extract Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- 239000000399 hydroalcoholic extract Substances 0.000 description 2
- 238000002386 leaching Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000013641 positive control Substances 0.000 description 2
- 241000208173 Apiaceae Species 0.000 description 1
- 241000208838 Asteraceae Species 0.000 description 1
- 235000009024 Ceanothus sanguineus Nutrition 0.000 description 1
- 240000003553 Leptospermum scoparium Species 0.000 description 1
- 235000015459 Lycium barbarum Nutrition 0.000 description 1
- 229920002385 Sodium hyaluronate Polymers 0.000 description 1
- GLEVLJDDWXEYCO-UHFFFAOYSA-N Trolox Chemical compound O1C(C)(C(O)=O)CCC2=C1C(C)=C(C)C(O)=C2C GLEVLJDDWXEYCO-UHFFFAOYSA-N 0.000 description 1
- 206010048222 Xerosis Diseases 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 210000004204 blood vessel Anatomy 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000010835 comparative analysis Methods 0.000 description 1
- 238000007405 data analysis Methods 0.000 description 1
- 230000009849 deactivation Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 230000007760 free radical scavenging Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 238000005325 percolation Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 210000001732 sebaceous gland Anatomy 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000002884 skin cream Substances 0.000 description 1
- 229940010747 sodium hyaluronate Drugs 0.000 description 1
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 235000013616 tea Nutrition 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/007—Preparations for dry skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a cosmetic composition containing a hemp leaf extract and a preparation method thereof. The cosmetic composition consists of a plant extract and auxiliary materials acceptable in cosmetics, wherein the plant extract is a compound extract, and plant raw materials of the plant extract comprise hemp leaves, centella, chamomile flowers and green tea. The cosmetic composition takes natural plant extracts as active ingredients, is safe and efficient, is applied to feet, can effectively relieve pain of shanks and feet, improves the dry condition of plantar skin, and is particularly suitable for women who wear high-heeled shoes for a long time in daily life.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a cosmetic composition (especially a skin cream) containing a hemp leaf extract and a preparation method thereof.
Background
The cosmetic is a chemical industrial product or a fine chemical product which is applied to any part of the surface of a human body, such as skin, hair, nails, lips, and teeth, by painting, spraying, or the like, in order to clean, maintain, beautify, modify, and change the appearance, or correct the odor of the human body, and maintain a good state.
The active ingredients in the cosmetics are usually chemical compositions, the using effect is poor and unsafe, as the market of the cosmetics becomes mature, the consumer demand for the cosmetics tends to be rational, the safety of the cosmetics is emphasized when the effects such as beauty and the like are pursued, and particularly, the cosmetics which need to be used for a long time such as moisturizing, water controlling and wrinkle preventing are used.
The feet are the moving organs of the human body, the places where the meridians are concentrated, and a large number of blood vessels and nerves are distributed, which are called as the second heart of the human body. The soles of people do not have sebaceous glands, can not secrete grease, and the skin of feet is rough, dry and even chapped, which often troubles many people. In addition, many women often wear high-heeled shoes for commuting, shopping or standing for a long time, and the legs and feet are painful due to uneven stress on the legs. At present, no cosmetics specially used for relieving foot pain and dry skin are available on the market.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention provides a cosmetic composition which consists of plant extracts and auxiliary materials acceptable in cosmetics.
Specifically, the plant extract is a compound extract, and the plant raw materials comprise hemp leaves, centella asiatica, chamomile flowers and green tea.
Specifically, in the cosmetic composition, the amount of the plant extract is 1-10 parts (specifically, 1, 2, 3, 4, 5, 6, 7, 8, 9, 10 parts), such as 5 parts.
Specifically, the ratio of folium Cannabis, herba Centellae, flos Matricariae Chamomillae and green tea in the above plant materials is 1-5:1-3:1-2:1-2 (weight ratio).
In an embodiment of the present invention, the ratio of cannabis leaves, centella asiatica, chamomile flowers and green tea in the plant material is 1-5:1:1, such as 1:1:1:1, 1.5:1:1:1, 2:1:1:1, 3:1:1:1, 4:1:1:1, 5:1:1: 1.
The above plant extracts can be prepared by conventional methods in the art, for example, by mixing the extract parts of the corresponding plants with a solvent, such as water, ethanol, etc., and extracting by conventional methods in the art, such as soaking, percolation, decoction, reflux extraction, continuous extraction, etc.
In one embodiment of the present invention, the preparation method of the plant extract comprises the following steps:
(1) adding plant materials into ethanol water solution, soaking, ultrasonic extracting, reflux extracting, filtering to obtain water-ethanol extract, and air drying the solid obtained by filtering;
(2) adding ethyl acetate into the solid obtained by filtering in the step (1), leaching, evaporating the ethyl acetate to obtain an extractum-shaped substance, dissolving the extractum-shaped substance in butanediol, and filtering to obtain an ethyl acetate extract;
optionally, (3) adding the hydroalcoholic extract obtained in the step (1) into the ethyl acetate extract obtained in the step (2), dissolving, and filtering to obtain the plant extract.
Specifically, the auxiliary materials acceptable in the cosmetic field comprise: one or more of humectant, oil, emulsifier, thickener, antiseptic, skin feeling regulator and solvent.
In particular, the above-mentioned moisturizers may be those commonly used in the art, and may be selected, for example, from: glycerin, allantoin, panthenol, propylene glycol, hyaluronic acid and its salt (such as sodium hyaluronate).
Specifically, in the cosmetic composition, the humectant is used in an amount of 1 to 15 parts (specifically, 1, 2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15 parts).
In one embodiment of the present invention, the humectant includes: 1-5 parts of glycerol, 1-5 parts of allantoin and 1-5 parts of panthenol.
In one embodiment of the present invention, the above-mentioned moisturizer comprises: 3 parts of glycerol, 1 part of allantoin and 3 parts of panthenol.
Specifically, the above-mentioned grease may be a grease commonly used in the art, and for example, may be selected from: petrolatum, caprylic/capric triglyceride, dimethicone, camellia seed oil, squalane, sorbitan caprylate, jojoba seed oil, shea butter, and the like.
Specifically, the amount of the oil or fat in the cosmetic composition is 10 to 30 parts (specifically, 10, 12, 14, 16, 18, 20, 22, 24, 26, 28, 30 parts).
In one embodiment of the present invention, the fat or oil is selected from the group consisting of: 1-2 parts of petrolatum, 1-2 parts of caprylic/capric triglyceride, 2-4 parts of polydimethylsiloxane, 2-4 parts of camellia seed oil, 2-4 parts of squalane, 2-4 parts of sorbitan caprylate and 1-2 parts of jojoba seed oil.
In one embodiment of the present invention, the grease includes: 2 parts of petrolatum, 2 parts of caprylic/capric triglyceride, 4 parts of polydimethylsiloxane, 4 parts of camellia seed oil and 4 parts of squalane.
In particular, the above-mentioned emulsifiers may be those commonly used in the art, and may be selected, for example, from: one or more of glyceryl stearate, cetyl alcohol, PEG-75 fatty acid ester, ceteth-20, etc.
Specifically, in the above cosmetic composition, the emulsifier is used in an amount of 1 to 10 parts (specifically, 1, 2, 3, 4, 5, 6, 7, 8, 9, 10 parts).
In one embodiment of the present invention, the above emulsifier comprises: 2 parts of cetyl alcohol, 2 parts of PEG-75 fatty acid ester and 202 parts of ceteth.
In particular, the above-mentioned thickeners may be thickeners commonly used in the art, for example, selected from: PEG-240/HDI copolymer bis-decyltetradecylpolyether-20 ether, carbomer, and the like.
Specifically, in the cosmetic composition, the thickener is used in an amount of 0.1 to 0.5 parts (specifically, 0.1, 0.2, 0.3, 0.4, 0.5 parts).
In one embodiment of the present invention, the above thickener comprises: and 0.3 part of carbomer.
In particular, the above-mentioned preservatives may be those commonly used in the art, and may be selected, for example, from: one or more of isoprene glycol, caprylyl glycol, dipropylene glycol, phenoxyethanol, etc.
Specifically, in the cosmetic composition, the preservative is used in an amount of 0.1-0.5 parts (specifically, 0.1, 0.2, 0.3, 0.4, 0.5 parts)
In one embodiment of the present invention, the above-mentioned preservatives include: 0.5 part of dipropylene glycol.
Specifically, the above-mentioned skin-feel modifier may be a skin-feel modifier commonly used in the art, for example, hydrogenated palm oil glyceride and the like.
Specifically, in the above cosmetic composition, the skin feel modifier is used in an amount of 1 to 5 parts (specifically, 1, 2, 3, 4, 5 parts).
In one embodiment of the present invention, the skin-feel modifier comprises: 1 part of hydrogenated palm oil glyceride.
Specifically, the above solvent may be a solvent conventional in the art, such as water (specifically, deionized water), and the amount of the solvent is an amount conventional in the art.
In one embodiment of the present invention, the raw materials of the above cosmetic composition comprise components A to F,
wherein:
the component A comprises: 1-15 parts of a humectant and 10-50 parts of a solvent;
the component B comprises: 10-30 parts of grease and 1-10 parts of emulsifier;
the component C comprises: 0.1-0.5 part of thickening agent and 5-10 parts of solvent;
the component D comprises: 0.1-0.5 part of preservative;
the component E comprises: 1-5 parts of a skin feel regulator;
the component F comprises: 1-10 parts of plant extract;
wherein, the plant extract, the humectant, the grease, the emulsifier, the thickener, the preservative, the skin feeling regulator and the solvent have the corresponding definitions of the invention.
In one embodiment of the present invention, the raw materials of the above cosmetic composition comprise a-F components, wherein:
the component A comprises: 3 parts of glycerol, 1 part of allantoin, 3 parts of panthenol and 10-50 parts of deionized water;
and B component: 2 parts of petrolatum, 2 parts of caprylic/capric triglyceride, 4 parts of polydimethylsiloxane, 4 parts of camellia seed oil and 4 parts of squalane; 2 parts of cetyl alcohol, 2 parts of PEG-75 fatty acid ester and 202 parts of ceteth;
and C, component C: 0.3 part of carbomer and 5-10 parts of deionized water;
and (D) component: 0.5 part of dipropylene glycol;
and E, component (E): 1 part of hydrogenated palm oil glyceride;
and F component: 5 parts of plant extract;
wherein the plant material of the plant extract comprises Cannabis sativa leaf, centella asiatica, Matricaria chamomilla flower and green tea, wherein the ratio of Cannabis sativa leaf, centella asiatica, Matricaria chamomilla flower and green tea is 1-5:1:1:1 (especially 1-2:1:1: 1).
Specifically, the cosmetic composition is in the form of a cream.
The invention also provides a preparation method of the cosmetic composition, which comprises the step of mixing the raw material components.
In one embodiment of the present invention, the above preparation method comprises the steps of:
(1) adding the component A into an emulsifying pot, stirring and heating to 80-85 ℃ until the component A is completely dissolved into transparent liquid;
(2) adding the component D and the component E into the transparent liquid obtained in the step (1), and uniformly stirring to obtain a mixture 1;
(3) preserving the heat of the mixture 1 obtained in the step (2), adding the component B and the component C, and homogenizing to be uniform to obtain a mixture 2;
(4) cooling the mixture 2 obtained in the step (3) to normal temperature, adding the component F, uniformly stirring, filtering and discharging;
the component A comprises a humectant and a solvent, the component B comprises grease and an emulsifier, the component C comprises a thickener and a solvent, the component D comprises a preservative, the component E comprises a skin feel regulator, and the component F comprises a plant extract; wherein, the plant extract, the humectant, the grease, the emulsifier, the thickener, the preservative, the skin feeling regulator and the solvent have the corresponding definitions of the invention.
The invention also provides an application of the plant extract in a cosmetic composition, wherein the plant extract is a compound extract, and plant raw materials of the plant extract comprise hemp leaves, centella, chamomile flowers and green tea.
Specifically, the ratio of folium Cannabis, herba Centellae, flos Matricariae Chamomillae and green tea in the above plant materials is 1-5:1-3:1-2: 1-2.
In one embodiment of the present invention, the ratio of cannabis leaves, centella asiatica, chamomile flowers and green tea in the plant material is 1-5:1:1:1 (particularly 1-2:1:1: 1).
The cosmetic composition provided by the invention takes the natural plant extract as the active ingredient, is safe and efficient, is used for feet, can effectively relieve the pain of shanks and feet, improves the dry condition of the skin of the soles, and is particularly suitable for women who wear high-heeled shoes for a long time in daily life.
Detailed Description
Unless defined otherwise, all scientific and technical terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention pertains.
The raw materials of the hemp in the invention are industrial hemp, and are simply referred to as hemp.
The parts referred to in the present invention are parts by weight.
In the present invention, "chamomile" refers to a flower of chamomile, a plant of the family Compositae.
In the present invention, "centella asiatica" refers to dried whole plant of centella asiatica, a plant of the family Umbelliferae.
In the invention, the green tea is one of the main types of tea leaves, is prepared by adopting new leaves or buds of tea trees, is not fermented, and is prepared by processes of enzyme deactivation, shaping, drying and the like.
The technical solutions of the present invention will be described clearly and completely with reference to the following embodiments of the present invention, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1: preparation of plant extract
The method comprises the following steps:
(1) adding plant materials into ethanol water solution, soaking, ultrasonic extracting, reflux extracting, filtering to obtain water-ethanol extract, and air drying the solid obtained by filtering;
(2) adding ethyl acetate into the solid obtained by filtering in the step (1), leaching, evaporating the ethyl acetate to obtain an extractum-shaped substance, dissolving the extractum-shaped substance in butanediol, and filtering to obtain an ethyl acetate extract;
(3) adding the hydroalcoholic extract obtained in the step (1) into the ethyl acetate extract obtained in the step (2), dissolving, and filtering to obtain a plant extract.
Example 2: DPPH free radical scavenging experiment
The plant extract obtained in example 1 was mixed with DPPH (final concentration: 100. mu.M) and reacted, 8 replicate wells were set, a drug-free blank control well and a Trolox positive control well were set, OD was measured at 30 ℃ for 1 hour with an enzyme reader, the detection wavelength was 515nm, and the oxidation resistance was calculated according to the following formula, and the results are shown in Table 1.
The oxidation resistance (%) (1-experimental well OD515 nm/blank well OD515nm) × 100%.
Plant extract samples were numbered as follows, depending on the plant material used in example 1:
sample No. 1: hemp leaf;
sample No. 2: hempseed leaf, centella asiatica, chamomile 1:1: 1;
sample No. 3: hemp leaf, centella asiatica, green tea 1:1: 1;
sample No. 4: hemp leaf, chamomile, green tea 1:1: 1;
sample No. 5: hemp leaf, centella asiatica, chamomile and green tea in the ratio of 0.5 to 1;
sample No. 6: hempseed leaf, centella asiatica, chamomile, green tea, 1:1: 1;
sample No. 7: hemp leaf, centella asiatica, chamomile, green tea 1.5:1:1: 1;
sample No. 8: hempseed leaf, centella asiatica, chamomile and green tea in a ratio of 2:1:1: 1.
TABLE 1 scavenging of free radicals by combination of various functional substances
| Sample numbering | Sample No. 1 | Sample No. 2 | Sample No. 3 | Sample No. 4 | Sample No. 5 | Sample No. 6 | Sample No. 7 | Sample No. 8 | Positive control |
| Clearance rate | 69.33％ | 70.21％ | 68.16％ | 72.38％ | 75.15％ | 80.33％ | 81.21％ | 82.16％ | 92.15％ |
Analysis table 1 shows that the effect of scavenging free radicals is not the best when only the cannabis leaf extract is used, the effect is improved to different degrees when the cannabis leaf extract and other functional substances are combined, and the effect of scavenging free radicals is the best when only the cannabis leaf is combined with a compound extract of centella asiatica, chamomile flower and green tea, and is higher than that of the single cannabis leaf extract; from the samples No. 6-8, it can be seen that the radical clearance rate is significantly improved with the increase of the addition amount of the hemp leaves, but No. 7 is not greatly improved compared with No. 6, so the optimum addition amount is 1 part of the hemp leaf extract.
Example 3
Cosmetic samples were prepared according to the following raw material composition and method:
the component A comprises: 3 parts of glycerol, 1 part of allantoin, 3 parts of panthenol and 10-50 parts of deionized water;
and B component: 2 parts of petrolatum, 2 parts of caprylic/capric triglyceride, 4 parts of polydimethylsiloxane, 4 parts of camellia seed oil and 4 parts of squalane; 2 parts of cetyl alcohol, 2 parts of PEG-75 fatty acid ester and 202 parts of ceteth;
and C, component C: 0.3 part of carbomer and 5-10 parts of deionized water;
and (D) component: 0.5 part of dipropylene glycol;
and E, component (E): 1 part of hydrogenated palm oil glycerides;
and F component: a plant extract;
the plant extract was sample No. 8 described in example 2.
Cosmetic sample preparation step:
(1) adding the component A into an emulsifying pot, stirring and heating to 80-85 ℃ until the component A is completely dissolved into transparent liquid;
(2) adding the component D and the component E into the transparent liquid obtained in the step (1), and uniformly stirring to obtain a mixture 1;
(3) preserving the heat of the mixture 1 obtained in the step (2), adding the component B and the component C, and homogenizing to be uniform to obtain a mixture 2;
(4) and (4) cooling the mixture 2 obtained in the step (3) to normal temperature, adding the component F, uniformly stirring, filtering and discharging.
Example 4
The cosmetics obtained in example 3 were evaluated for the pain relief care effect and the improvement effect on the dry skin condition of the sole of the foot of 10 patients who wear high-heeled shoes for a long time in the age of 25 to 35 years old or had pain in the lower leg and foot for 28 days, respectively, by comparative analysis. The results of the feedback trials are summarized in tables 2-11, respectively.
Feedback results for test subject No. 21 in Table 21
| Is very obvious | Is more obvious | In general | Has a little effect | Has no effect | |
| Relieving foot pain | √ | ||||
| Relieving shank pain | √ | ||||
| Improving plantar skin dryness | √ |
Feedback results for test subject No. 32 in Table 32
| Is quite obvious | Is more obvious | In general | Has a little effect | Has no effect | |
| Relieving foot pain | √ | ||||
| Relieving shank pain | √ | ||||
| Improving plantar skin dryness | √ |
Feedback results for test subject No. 43 in Table 43
TABLE 54 feedback results of the test subjects
| Is quite obvious | Is more obvious | In general | Has a little effect | Has no effect | |
| Relieving foot pain | √ | ||||
| Relieving shank pain | √ | ||||
| Improving plantar skin dryness | √ |
Table 65 feedback results of Subjects
| Is quite obvious | Is more obvious | In general | Has a little effect | Has no effect | |
| Relieving foot pain | √ | ||||
| Relieving shank pain | √ | ||||
| Improving plantar skin dryness | √ |
Feedback results for test subject No. 76 in Table 76
| Is quite obvious | Is more obvious | In general | Has a little effect | Has no effect | |
| Relieving foot pain | √ | ||||
| Relieving shank pain | √ | ||||
| Improving plantar skin dryness | √ |
Feedback results for test subject No. 87
| Is quite obvious | Is more obvious | In general | Has a little effect | Has no effect | |
| Relieving foot pain | √ | ||||
| Relieving shank pain | √ | ||||
| Improving plantar skin dryness | √ |
Feedback results for test subject No. 98 in Table
| Is quite obvious | Is more obvious | In general | Has a little effect | Has no effect | |
| Relieving foot pain | √ | ||||
| Relieving shank pain | √ | ||||
| Improving plantar skin dryness | √ |
Table 109 feedback results from Subjects
| Is quite obvious | Is more obvious | In general | Has a little effect | Has no effect | |
| Relieving foot pain | √ | ||||
| Relieving shank pain | √ | ||||
| Improving plantar skin dryness | √ |
Table 1110 feedback results for test subject
| Is quite obvious | Is more obvious | In general | Has a little effect | Has no effect | |
| Relieving foot pain | √ | ||||
| Relieving shank pain | √ | ||||
| Improving plantar skin dryness | √ |
From the data analysis in tables 2-11, it can be seen that: the product has very obvious and relatively obvious good evaluation rate of 80 percent for evaluating the foot pain relief; the product has very obvious and relatively obvious favorable evaluation rate of 60 percent on the evaluation of shank pain relief, which shows that the product has certain effect but is not very obvious on shank pain relief; the product has very obvious and relatively obvious favorable evaluation rate of 90 percent for evaluating the relief of plantar xerosis cutis; because the sample trial test is carried out in autumn and winter, the sole skin is generally dry, and the sole is not conscious of skin care at ordinary times, most people feel that the sole skin is dry after the product is tried, and the condition is relieved.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents and the like that are within the spirit and principle of the present invention are included in the present invention.
The foregoing embodiments and methods described in this disclosure may vary based on the abilities, experience, and preferences of those skilled in the art.
The mere order in which the steps of a method are listed in the present invention does not constitute any limitation on the order of the steps of the method.
Claims (16)
1. A cosmetic composition comprises plant extract and cosmetically acceptable adjuvants, wherein the plant extract is compound extract, and its plant materials include folium Cannabis, herba Centellae, flos Matricariae Chamomillae and green tea.
2. The cosmetic composition according to claim 1, wherein the amount of the plant extract used in the cosmetic composition is 1 to 10 parts;
the weight ratio of hemp leaf, centella asiatica, chamomile flower and green tea in the plant raw materials is 1-5:1-3:1-2:1-2, and preferably 1-5:1:1: 1.
3. The cosmetic composition of claim 1, wherein the cosmetically acceptable adjuvant comprises: one or more of humectant, oil, emulsifier, thickener, antiseptic, skin feeling regulator and solvent.
4. The cosmetic composition of claim 3, wherein the humectant comprises: a combination of one or more of glycerol, allantoin, panthenol, propylene glycol, hyaluronic acid, and salts thereof; the dosage of the humectant is 1-15 parts;
preferably, the moisturizer comprises: 1-5 parts of glycerol, 1-5 parts of allantoin and 1-5 parts of panthenol.
5. The cosmetic composition of claim 3, wherein the oil or fat is selected from the group consisting of: one or more of petrolatum, caprylic/capric triglyceride, dimethicone, camellia seed oil, squalane, sorbitan caprylate, jojoba seed oil, and shea butter; the using amount of the grease is 10-30 parts;
preferably, the grease is selected from: 1-2 parts of petrolatum, 1-2 parts of caprylic/capric triglyceride, 2-4 parts of polydimethylsiloxane, 2-4 parts of camellia seed oil, 2-4 parts of squalane, 2-4 parts of sorbitan caprylate and 1-2 parts of jojoba seed oil;
more preferably, the grease comprises: 2 parts of petrolatum, 2 parts of caprylic/capric triglyceride, 4 parts of polydimethylsiloxane, 4 parts of camellia seed oil and 4 parts of squalane.
6. The cosmetic composition of claim 3, wherein the emulsifier is selected from the group consisting of: one or more of glyceryl stearate, cetyl alcohol, PEG-75 fatty acid ester, and ceteth-20; the dosage of the emulsifier is 1-10 parts;
preferably, the emulsifier comprises: 2 parts of cetyl alcohol, 2 parts of PEG-75 fatty acid ester and 202 parts of ceteth.
7. The cosmetic composition of claim 3, wherein said thickener is selected from the group consisting of: one or more of PEG-240/HDI copolymer bis-decyl tetradecyl polyether-20 ether and carbomer; the using amount of the thickening agent is 0.1-0.5 part;
preferably, the thickener comprises: and 0.3 part of carbomer.
8. The cosmetic composition of claim 3, wherein the preservative is selected from the group consisting of: one or more of isoprene glycol, caprylyl glycol, dipropylene glycol and phenoxyethanol; the dosage of the preservative is 0.1-0.5 part;
preferably, the preservative comprises: 0.5 part of dipropylene glycol.
9. The cosmetic composition of claim 3, wherein said skin feel modifier is hydrogenated palm oil glyceride; the dosage of the skin feel regulator is 1-5 parts;
preferably, the skin feel modifier comprises: 1 part of hydrogenated palm oil glyceride.
10. The cosmetic composition of any one of claims 1 to 9, wherein the starting materials of the cosmetic composition comprise a-F components, wherein:
the component A comprises: 1-15 parts of a humectant and 10-50 parts of a solvent;
the component B comprises: 10-30 parts of grease and 1-10 parts of emulsifier;
the component C comprises: 0.1-0.5 part of thickening agent and 5-10 parts of solvent;
the component D comprises: 0.1-0.5 part of preservative;
the component E comprises: 1-5 parts of a skin feel regulator;
the component F comprises: 1-10 parts of plant extract.
11. The cosmetic composition of claim 10, wherein the raw materials of the cosmetic composition comprise a-F components, wherein:
the component A comprises: 3 parts of glycerol, 1 part of allantoin, 3 parts of panthenol and 10-50 parts of deionized water;
and B component: 2 parts of petrolatum, 2 parts of caprylic/capric triglyceride, 4 parts of polydimethylsiloxane, 4 parts of camellia seed oil and 4 parts of squalane; 2 parts of cetyl alcohol, 2 parts of PEG-75 fatty acid ester and 202 parts of ceteth;
and C, component C: 0.3 part of carbomer and 5-10 parts of deionized water;
and (D) component: 0.5 part of dipropylene glycol;
and E, component (E): 1 part of hydrogenated palm oil glyceride;
and F component: 5 parts of plant extract;
wherein the plant material of the plant extract comprises hemp leaf, centella asiatica, chamomile flower and green tea, wherein the weight ratio of the hemp leaf, the centella asiatica, the chamomile flower and the green tea is 1-5:1:1: 1.
12. The cosmetic composition of claim 11, wherein the cosmetic composition is in the form of a cream.
13. A method for preparing the cosmetic composition according to any one of claims 1 to 12, comprising the step of mixing the raw material components.
14. The method of claim 13, comprising the steps of:
(1) adding the component A into an emulsifying pot, stirring and heating to 80-85 ℃ until the component A is completely dissolved into transparent liquid;
(2) adding the component D and the component E into the transparent liquid obtained in the step (1), and uniformly stirring to obtain a mixture 1;
(3) preserving the heat of the mixture 1 obtained in the step (2), adding the component B and the component C, and homogenizing to be uniform to obtain a mixture 2;
(4) cooling the mixture 2 obtained in the step (3) to normal temperature, adding the component F, uniformly stirring, filtering and discharging;
the component A comprises a humectant and a solvent, the component B comprises grease and an emulsifier, the component C comprises a thickener and a solvent, the component D comprises a preservative, the component E comprises a skin feel regulator, and the component F comprises a plant extract.
15. The application of a plant extract in a cosmetic composition is characterized in that the plant extract is a compound extract, and plant raw materials of the plant extract comprise hemp leaves, centella, chamomile flowers and green tea.
16. Use according to claim 15, wherein the weight ratio of cannabis leaves, centella asiatica, chamomile flowers and green tea in the plant material is 1-5:1-3:1-2:1-2, preferably 1-5:1:1: 1.
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