CN105853300B - One kind is deoiled anti-dandruff and itching-relieving moist type shampoo paste and preparation method thereof - Google Patents

Abstract

The invention discloses a kind of anti-dandruff antipruritic moist type shampoo pastes and preparation method thereof to deoil of Chinese medicine, and the shampoo paste contains：Sodium laureth sulfate, sodium lauroyl glutamate, MES, GOC, EG, watermiscible vitamin E, amino acid surfactant, coix seed extracting solution, lemon juice extracting solution, ginger extract, peppermint extracting solution, Radix Sophorae Flavescentis extractive liquid, Miconazole aqueous solution, zinc pyrithione, climbazole, glycerine, pearling agent, ethylparaben, olive oil, camellia seed oil, cationic melon glue, carbomer gel liquid, sodium carboxymethylcellulose, sodium alginate gel liquid, distilled water, essence.The shampoo paste property of the present invention is mild, safe, and removal hair is greasy, effectively antipruritic, and inhibits the generation of dandruff, and hair nutrient can be supplemented, profit hair is nourished, improves scalp blood circulation, boosts metabolism, strong root of hair, prevents epilation, promotes kainogenesis long, keeps the submissive show of hair bright.

Description

Oil-removing, anti-dandruff, anti-itch and moisturizing shampoo and preparation method thereof

technical field

The invention relates to a shampoo, in particular to an oil-removing, anti-dandruff, anti-itch and moisturizing shampoo and a preparation method thereof.

Background technique

How to improve oily hair? Whether you are at school or working, whether you are a man or a woman, you often have oily hair, which leads to greasy hair. Even after you wash it not long ago, you will feel that a layer of oil has covered your scalp when you touch it. This feeling is very bad. , especially when students are busy with their studies, they use their brains too much, and their hair is very oily. After washing their hair, it will be greasy and stick together the next day. There are also people who work under high pressure at work, and their hair is prone to serious oily phenomena. , especially when the head is connected to the face, sometimes the entire forehead will be greasy and acne will appear, which is also caused by greasy skin, which greatly affects the normal life and mood of many people.

What causes oily hair? Sebaceous gland secretion is the direct cause, it is affected by androgen, and is related to factors such as heredity, living habits, and environment.

The scalp is the same as the skin on the face, arms and other parts, and it can also be divided into oily, normal and dry. When we were children, we would not have skin problems such as oily scalp, pimples, and acne, but when we were young, with the secretion of male hormones, we gradually began to be "entangled" by them. Oily scalp is also a normal physiological phenomenon. A certain amount of oil will protect the skin, but excessive secretion will become an annoying problem like acne. In fact, the sebaceous gland secretion of the scalp is higher than that of the facial skin, even compared with the most oily forehead, it is almost twice as much.

Dandruff is the white or gray scales that appear when there are abnormal lesions on the scalp. It is caused by fungal infection and belongs to the category of skin diseases. This kind of scale particles are relatively large, attached to the surface of the scalp or hair, and it is easy to fall off to the shoulder clothes when combing or scratching.

There are also many reasons for dandruff: people with a strong metabolism are prone to dandruff; excessive use of the brain and irregular life will cause dandruff; climate change, eating irritating food, smoking and drinking, excessive stress, etc. Too much dandruff...

Whether it is excessive oily scalp or excessive dandruff, it will bring a lot of troubles to life. At this time, you can consider integrating the essence of traditional Chinese medicine into hair care products, which will be the research and development trend of modern hair care technology. Using advanced technology to extract the essence of traditional Chinese medicine, the active ingredients can fully contact with the hair, penetrate deep into the hair follicles, deeply control oil, reduce the occurrence of dandruff, and play a better role. For busy office workers and students, using anti-oil, anti-dandruff, nourishing shampoo and hair care products containing traditional Chinese medicine essence is a scientific and convenient method.

Contents of the invention

The first technical problem to be solved by the present invention is to provide a new oil-removing, dandruff-relieving, itching-relieving and moisturizing shampoo containing natural component extracts.

The 2nd technical problem to be solved by the present invention is the preparation method of above-mentioned shampoo cream.

The technical problem solved by the present invention is: an oil-removing, anti-dandruff, anti-itch and moisturizing shampoo and its preparation method. The shampoo contains the following raw material components:

The coix seed extract is prepared by the following method:

Weigh an appropriate amount of coix seed, crush it and soak for 0.15-0.8h, heat and decoct for extraction 3 times, add 10-18 times the amount of water for the first time, extract for 0.5-2h, add 8-15 times the amount of water for the second time, extract 0.5 -1.5h, add 8-10 times the amount of water for the third time, extract for 0.5-1.5h, filter each time, combine the filtrate, concentrate the volume of the filtrate to 3-6 times the weight of coix seed g/ml, and filter to obtain.

Described lemon juice extract is prepared by the following method:

Weigh an appropriate amount of fresh lemon, cut it open, soak for 0.15-0.8h, heat and decoct to extract 3 times, add 8-15 times the amount of water for the first time, extract for 0.5-2h, add 8-10 times the amount of water for the second time, extract 0.5-1.5h, add 8-10 times the amount of water for the third time, extract for 0.5-1.5h, filter each time, combine the filtrate, concentrate the volume of the filtrate to 3-6 times the weight of the lemon g/ml, and filter to obtain.

Described ginger extract is prepared by the following method:

Weigh an appropriate amount of ginger, cut into thin slices, and reflux with water to extract 3 times. For the first time, use 10-18 times the amount of water, extract for 0.5-2.5h, filter, and use 8-15 times the amount of water for the second time, extract for 0.5-2.5h , the third time with 6-12 times the amount of water, extract 0.5-1.5h, filter respectively, combine the filtrates, concentrate under reduced pressure to 6-10 times the weight of ginger g/ml, and set aside.

Described peppermint extract is prepared by the following method:

Weigh a certain amount of fresh mint, put it into a round bottom flask, add 10-18 times of distilled water, place it in an electric heating mantle, use a volatile oil extractor to reflux and extract for 5-6 hours, cool to room temperature, and cover with a double-layer gauze Filter the extract and set aside.

Described sophora flavescens extract is prepared by the following method:

Weigh an appropriate amount of Sophora flavescens, crush it, soak it for 0.15-0.8h, heat and decoct it for 3 times, add 10-18 times the amount of water for the first time, extract 0.5-2h, add 10-12 times the amount of water for the second time, extract 0.5 -1.5h, add 8-12 times the amount of water for the third time, extract for 0.5-1.5h, filter each time, combine the filtrate, concentrate the volume of the filtrate to 3-6 times g/ml of the weight of Sophora flavescens, and filter to obtain.

The essence is milk essence, peach essence, lily essence, jasmine essence, osmanthus essence, rose essence.

The preparation method of the described a kind of oil-removing, dandruff-relieving and itching-relieving moisturizing shampoo cream comprises the following steps:

a) Weigh 0.06-0.6g of cationic guar gum, add it to 50-100ml of distilled water, heat it in a water bath at 60-80°C, stir while heating, wait until it is evenly mixed, let it stand for full swelling, and obtain cationic guar gum glue gel liquid, set aside;

b) Weigh 0.05-1.5g of carbomer, add it to a beaker with 50-100ml of distilled water, heat it in a water bath at 60-80°C, stir while heating, let it swell fully, and form a carbomer gel ,stand-by;

c) Weigh 0.08-1.5g of sodium carboxymethyl cellulose, add it to a beaker containing 50-100ml of distilled water, heat in a water bath at 40-50°C, stir while heating, and let it swell fully to form carboxymethyl Sodium cellulose gel, for use;

d) Weigh 0.06-2g of sodium alginate, add it to a beaker containing 50-100ml of distilled water, heat in a water bath at 60-80°C, stir while heating, let it stand still to fully swell, and form a sodium alginate gel liquid, stand-by;

e) Weigh 1-15g of miconazole, add it to a beaker containing 10-100ml of distilled water, stir evenly with a glass rod, and obtain a miconazole solution for use;

f) Take 2-8g of sodium lauryl ether sulfate, 1-10g of sodium lauroyl glutamate, 4-12g of amino acid surfactants, 1-15g of MES, 2-16g of zinc pyrithione, 1-10g of campanol, Put 2-10g of water-soluble vitamin E and 10-50ml of distilled water in beaker 1, put it in a constant temperature water bath at 60-90°C and stir to dissolve, and form solution 1 after completely dissolving, ready for use;

g) Take coix seed extract 0.7-3.5ml, lemon juice extract 0.5-3.2ml, ginger extract 0.5-2.8ml, peppermint extract 0.6-3.0ml, Sophora flavescens extract 0.8-3.0ml, miconazole The solution is placed in beaker 1, and stirred evenly to form solution 2, which is ready for use;

h) Weigh 1.5-3.5g of camellia oleifera seed oil, 1.2-4.5g of olive oil, 1-9g of simple emulsifier GOC, and 1-9g of emulsifier EG, and place them on a water bath at 60-90°C as the oil phase for later use;

i) Measure 12-25ml of distilled water, place it on a water bath at 60-90°C as the water phase, and set aside;

j) When the oil phase and the water phase reach the same temperature, add the water phase into the oil phase in a thin stream, and stir while adding, until a milky white fine and uniform emulsion matrix is formed;

k) Add solution 1, solution 2, cationic guar gum gel, sodium alginate gel, carbomer gel, glycerin 2-7ml, 2% ethylparaben 75% ethanol to the emulsion base Mix 0.5-3.5ml of the solution, 0.08-0.35ml of essence and 0.5-1.2g of pearlescent agent, and stir evenly with a glass rod to obtain an oil-removing, anti-dandruff, anti-itch, moisturizing shampoo cream.

Various compositions among the present invention are as follows:

The main components of coix seed are protein, vitamin B ₁ and B ₂ , which can soften the cutin of the skin and have the functions of whitening and removing spots. "Compendium of Materia Medica" says that coix seed "invigorates the spleen and stomach, nourishes the lungs and clears heat, dispels wind and dampness, and nourishes the skin." Keeps the appearance, lightens the body and prolongs life.” Coix seed used for hair can nourish the hair, prevent hair loss, and make the hair smooth and supple.

Lemons contain more citric acid. This acid can not only promote the secretion of gastric juice and help digestion, but also neutralize alkalinity, prevent pigmentation, and have a bleaching effect on the skin. Lemon juice contains a lot of provitamin A, which can make the skin absorb and moisturize the skin. Washing hair with lemon juice can promote the growth and development of hair, because citric acid can neutralize the alkaline components in hair, thus playing a hair care effect.

Gingerol, zingiberene oil and other ingredients in ginger can normalize the blood circulation of the head skin, promote scalp metabolism, activate hair follicle tissue, effectively prevent hair loss and gray hair, stimulate new hair growth, and inhibit scalp itching. Strengthens hair roots. Apply ginger directly to the affected part of the head for alopecia areata. For several days, new hair can grow on the bald part. Shampoo containing ginger has the effects of cleaning the scalp, removing dandruff, and preventing hair loss. Especially in winter, when you wash your hair and massage your scalp, it feels relaxed and warm.

Peppermint is a pungent and cool sweating and antipyretic medicine. The anti-dandruff factor of mint has the effect of anti-inflammatory and sterilizing, decomposing lipids, effectively improving the troubles of dandruff and scalp itching, and effectively inhibiting dandruff and itching. External use can cure skin itching, rash and eczema, etc. It can regulate unclean and blocked skin. It has a cool feeling, can shrink capillaries, eliminate toxins in the body, improve eczema, ringworm, relieve itching, inflammation and burns, and soften the skin. Beneficial for oily hair. It can clear hair follicles, fight hair follicle aging, repair, nourish and protect dry hair, and make hair and scalp full of health and vitality. feel. Peppermint is also anti-inflammatory and analgesic, making it suitable for scalp itching.

Sophora flavescens can clear away heat and dampness, kill insects and relieve itching, and has a good effect on alleviating skin itching. Sophora flavescens, with its bitter and cold nature, can effectively clean up the toxins deposited in the hair follicles of the scalp, and has a significant improvement effect on hair loss and broken hair caused by mites and sebum clogging hair follicles, recreating a healthy scalp ecological environment. It has the effect of tonifying the kidney, the kidney governs the bones and hair, and when the kidney qi is strong, the hair will be dense, black and shiny.

Miconazole is a highly effective, safe and broad-spectrum antifungal drug, which is effective against almost all pathogenic fungi. Its mechanism is to inhibit the synthesis of sterols in the fungal cell membrane, affect the permeability of the cell membrane, inhibit the growth of fungi, and lead to death. Concentrations below 4 μg/ml can inhibit most clinically isolated fungi, among which Cryptococcus neoformans, Candida and spores are sensitive to this product, dermatitis blastomyces and histoplasma are highly sensitive to this product, but Aspergillus Mold is poor. In addition, miconazole also has antibacterial effects on Staphylococcus aureus, Streptococcus, Gram-positive cocci and anthrax. For skin fungal infections, such as hand, foot, body, jock itch.

Zinc pyrithione (ZPT) is an excellent anti-scaling agent and anti-grease agent, which can effectively kill the fungus that produces dandruff. Safe Anti-Itch and Anti-Dandruff.

Campanile has broad-spectrum bactericidal properties, and is mainly used in anti-itch and anti-dandruff conditioning shampoos and hair care shampoos, and can also be used in antibacterial soaps, shower gels, drug toothpaste, mouthwash and other high-end washing products.

Camellia oleifera seed oil has a delicate smell and unique flavor. It is known as "Oriental olive oil". It is found that the fatty acid composition of camellia oil is very similar to that of olive oil. The content of linoleic acid is more than 80%, and the content of unsaturated fatty acid in camellia oil is as high as 90%. It is easy to be absorbed by the body, and it can also promote the body's absorption of fat-soluble fiber and trace elements such as calcium, iron, and zinc. Camellia oleifera seed oil also contains biologically active substances such as camellia glycosides, camellia saponins, and tea polyphenols that are not found in olive oil. Natural tea tree oil is mild in nature, can supplement the nutrition of the scalp and skin, promote hair growth, sterilize and relieve itching, and has obvious effects on the treatment of scalp oil, dermatitis, eczema and dandruff, and can regulate oily skin. It is a very effective antibacterial and anti-dandruff product . It has obvious improvement effect on scalp itching, chapped skin, eczema, and after-sun repair. It has strong cleaning ability and keeps scalp and skin fresh, healthy and comfortable.

Cationic guar gum plays a good role in foam stabilization, antistatic and thickening in shampoo products. It can also improve the wet combing and dry combing properties of the hair, keep the hair shiny, soft and elastic for a long time, and reduce the irritation of the detergent to the skin.

Sodium alginate plays a good role in thickening, antistatic and foam stabilization in shampoo products. In addition, it improves the moisture retention of the hair, leaving it soft and supple for a long time. It is a common thickener and moisturizer in shampoo products.

Some natural plant extracts are first added to the shampoo prescription. It can reduce the growth of bacteria and fungi and prevent hair loss by cleaning the scalp and hair and controlling the water-oil balance of the head skin. Ingredients such as lemon juice and mint can clean and care for the scalp and hair very well, and the texture is mild and not easy to damage the skin; camellia seed oil can regulate the oil secretion of the scalp and keep the scalp in a state of water and oil balance for a long time; ginger extract can effectively Prevents hair loss.

Secondly, use antibacterial and anti-inflammatory drugs to achieve the effect of anti-dandruff and relieve itching. For example, zinc pyrithione, miconazole, and campanol can effectively kill fungi and bacteria on the head, and relieve scalp itching symptoms caused by fungi and bacteria.

These natural extracts and antibacterial drugs added contain a large amount of nourishing hair care ingredients and a variety of important trace elements. While effectively cleaning and removing dandruff, it can speed up scalp metabolism, promote new hair growth, and make hair roots strong and difficult Broken, the hair is black and shiny.

In short, this shampoo can inhibit the growth of bacteria and fungi, regulate the water-oil balance of the head skin, achieve the effect of cleaning and removing dandruff, can supplement the nutrition and moisture needed by the hair and scalp, reduce scalp itching, prevent hair loss, and split ends and fungus growth, can improve blood circulation in the scalp, promote metabolism, make hair roots strong, hair thick and supple.

The shampoo cream prepared by the invention is milky white, suitable in viscosity, smooth and rich in foam, fine and uniform, good in spreadability, cool and comfortable, good in stability and fragrant in smell.

Detailed ways

The present invention will be further described below in conjunction with the examples.

Zinc pyrithione, miconazole, and campanola of the present invention are commercially available.

Amino acid surfactant (GCK-12K), simple emulsifier GOC (glyceryl oleate citrate), emulsifier EG (sodium acrylate/sodium dimethacryl taurate and isohexadecane, polysorbate Ester 80) were provided by Beijing Xinnuo Jiuheng Technology and Trade Co., Ltd.

Example 1

1.1 Preparation of coix seed extract

Weigh 60g of coix seed, crush it, soak for 0.5h, heat and decoct for extraction 3 times, add 18 times the amount of water for the first time, extract for 2 hours, add 12 times the amount of water for the second time, extract for 1 hour, and add 10 times the amount for the third time water, extract for 0.5h, filter each time with 3 layers of gauze, combine the filtrate, and concentrate the volume of the filtrate to 3 times the weight of coix seed g/ml, set aside.

1.2 Preparation of lemon juice extract

Weigh 50g of fresh lemon, soak for 0.5h, heat and decoct to extract, extract 3 times, add 12 times the amount of water for the first time, extract for 1.5h, use 10 times the amount of water for the second time, extract for 1.5h, and use 8 times for the third time Double the amount of water, extract for 1 hour, filter each time with double-layer gauze, combine the filtrate, and concentrate the volume of the filtrate to 3 times the weight of the lemon g/ml, and set aside.

1.3 Preparation of ginger extract

Weigh 50g of ginger, cut into thin slices, reflux and extract with water for 3 times, the first time use 16 times the amount of water, extract for 1 hour, filter, the second time use 12 times the amount of water, extract for 1 hour, and the third time use 10 times the amount of water, Extract for 0.5h, filter separately, combine the filtrates, concentrate under reduced pressure to 6 times the weight of ginger, g/ml, and set aside.

1.4 Preparation of peppermint extract

Weigh 50g of fresh mint, put it into a round bottom flask, add 17 times of distilled water, place it in an electric heating mantle, use a volatile oil extractor to reflux and extract for 5 hours, cool to room temperature, and filter the extract with double-layer gauze. stand-by.

1.5 Preparation of Sophora flavescens extract

Weigh 60g of Sophora flavescens, crush and soak for 0.8h, heat and decoct for extraction 3 times, use 18 times of water for the first time, extract for 1 hour, use 12 times of water for the second time, extract for 1 hour, and use 10 times of water for the third time, extract After 0.5h, the extracts were combined and filtered with double-layer gauze, and the volume of the filtrate was concentrated to 3 times g/ml of the weight of Sophora flavescens for use.

1.6 Preparation of Shampoo Cream

a) Weigh 0.3 g of cationic guar gum, add it to 70 ml of distilled water, heat in a water bath at 60° C., stir while heating, and after mixing evenly, leave it to swell fully to obtain cationic guar gum gel liquid, wait use;

b) Weigh 0.9g of carbomer, add it to a beaker with 80ml of distilled water, heat it in a water bath at 60°C, stir while heating, let it stand still to fully swell, and form a carbomer gel, which is ready for use;

c) Weigh 0.5 g of sodium carboxymethyl cellulose, add it to a beaker with 80 ml of distilled water, heat it in a water bath at 50° C., stir while heating, let it stand to swell fully, and form a sodium carboxymethyl cellulose condensate. stand-by;

d) Weigh 0.3 g of sodium alginate, add it to a beaker with 70 ml of distilled water, heat it in a water bath at 60°C, stir while heating, let it stand still to fully swell, and form a sodium alginate gel liquid, which is ready for use;

e) Weigh 2 g of miconazole, add it to a beaker with 30 ml of distilled water, stir it evenly with a glass rod, and obtain a miconazole solution for use;

f) Take 4g of sodium lauryl ether sulfate, 5g of sodium lauroyl glutamate, 6g of amino acid surfactants, 6g of MES, 8g of zinc pyrithione, 5g of campanola, 4g of water-soluble vitamin E, and 50ml of distilled water in beaker 1, Put it in a constant temperature water bath at 70°C and stir to dissolve, and form solution 1 after complete dissolution, which is ready for use;

g) Take coix seed extract 2ml, lemon juice extract 2ml, ginger extract 2ml, peppermint extract 2ml, Sophora flavescens extract 2ml, and miconazole solution in beaker 1, and stir evenly to form solution 2, stand-by;

h) Weigh 2g of camellia oleifera seed oil, 2g of olive oil, 2g of simple emulsifier GOC, and 1g of emulsifier EG, and place them on a water bath at 80°C as the oil phase, and set aside;

i) Measure 12ml of distilled water and place it on a water bath at 80°C as the water phase for later use;

j) When the oil phase and the water phase reach the same temperature, add the water phase into the oil phase in a thin stream, and stir while adding, until a milky white fine and uniform emulsion matrix is formed;

k) Add solution 1, solution 2, cationic guar gum gel, sodium alginate gel, carbomer gel, glycerin 7ml, 2% ethylparaben 75% ethanol solution 2ml to the emulsion matrix , Essence 0.08ml and pearlescent agent 1g, stir well with a glass rod to get oil-removing, anti-dandruff, anti-itch and moisturizing shampoo.

Example 2

2.1 Preparation of coix seed extract

Weigh 100g of coix seed, crush it, soak for 0.5h, heat and decoct for extraction 3 times, add 15 times the amount of water for the first time, extract for 2 hours, add 10 times the amount of water for the second time, extract for 1 hour, and add 10 times the amount for the third time water, extract for 0.5h, filter each time with 3 layers of gauze, combine the filtrate, and concentrate the volume of the filtrate to 5 times the weight of coix seed g/ml, and set aside.

2.2 Preparation of lemon juice extract

Weigh 80g of fresh lemon, extract 3 times, heat and decoct and extract 3 times, add 15 times the amount of water for the first time, extract for 1.5h, use 9 times for the second time, extract for 1.5h, and use 9 times the amount of water for the third time, Extract for 1 hour, filter each time with double-layer gauze, combine the filtrate, and concentrate the volume of the filtrate to 5 times the weight of the lemon g/ml, and set aside.

2.3 Preparation of ginger extract

Weigh 90g of ginger, cut into thin slices, and extract 3 times under reflux with water. For the first time, use 14 times the amount of water, extract for 1 hour, filter, use 12 times the amount of water for the second time, extract for 1 hour, and use 8 times the amount of water for the third time. Extract for 0.5h, filter separately, combine the filtrates, concentrate under reduced pressure to 8 times the weight of ginger, g/ml, and set aside.

2.4 Preparation of peppermint extract

Weigh 80g of fresh mint, put it into a round bottom flask, add 15 times of distilled water, place it in an electric heating mantle, use a volatile oil extractor to reflux extract for 5.5 hours, cool to room temperature, filter the extract with double gauze, stand-by.

2.5 Preparation of Sophora flavescens extract

Weigh 80g of Sophora flavescens, crush and soak for 0.5h, heat and decoct for extraction 3 times, use 15 times of water for the first time, extract for 1 hour, use 11 times of water for the second time, extract for 1 hour, and use 10 times of water for the third time, extract After 0.5h, the extracts were combined and filtered with double-layer gauze, and the volume of the filtrate was concentrated to 6 times g/ml of the weight of Sophora flavescens for later use.

2.6 Preparation of Shampoo Cream

a) Weigh 0.6g of cationic guar gum, add it to 100ml of distilled water, heat in a water bath at 80°C, stir while heating, and after mixing evenly, let it stand to swell fully to obtain cationic guar gum gel liquid, wait use;

b) Weigh 0.5g of carbomer, add it to a beaker with 80ml of distilled water, heat it in a water bath at 70°C, stir while heating, let it stand still to fully swell, and form a carbomer gel, which is ready for use;

c) Weigh 0.7 g of sodium carboxymethyl cellulose, add it to a beaker with 70 ml of distilled water, heat it in a water bath at 50° C., stir while heating, let it stand to swell fully, and form a sodium carboxymethyl cellulose condensate. stand-by;

d) Weigh 0.8 g of sodium alginate, add it to a beaker with 7 ml of distilled water, heat it in a water bath at 80 ° C, stir while heating, let it stand still to fully swell, and form a sodium alginate gel liquid, which is ready for use;

e) Weigh 3g of miconazole, add it to a beaker with 30ml of distilled water, stir it evenly with a glass rod, and obtain a miconazole solution for use;

f) Take 4g of sodium lauryl ether sulfate, 5g of sodium lauroyl glutamate, 5g of amino acid surfactants, 5g of MES, 8g of zinc pyrithione, 3g of campanolin, 40g of water-soluble vitamin E, and 30ml of distilled water in beaker 1, and place Stir and dissolve in a constant temperature water bath at 60°C, and form solution 1 after complete dissolution, ready for use;

g) Take coix seed extract 3ml, lemon juice extract 2ml, ginger extract 2ml, peppermint extract 3ml, Sophora flavescens extract 2.0ml, and miconazole solution in beaker 1, and stir evenly to form solution 2 ,stand-by;

h) Weigh 2g of camellia oleifera seed oil, 3g of olive oil, 2g of simple emulsifier GOC, and 1.5g of emulsifier EG, put them on a water bath at 90°C, and use them as the oil phase for later use;

i) Measure 13ml of distilled water, place it on a water bath at 70°C, and use it as the water phase for later use;

j) When the oil phase and the water phase reach the same temperature, add the water phase into the oil phase in a thin stream, and stir while adding, until a milky white fine and uniform emulsion matrix is formed;

k) Add solution 1, solution 2, cationic guar gum gel, sodium alginate gel, carbomer gel, glycerin 7ml, 2% ethylparaben 75% ethanol solution 2.0 to the emulsion matrix ml, 0.15ml of essence and 0.6g of pearlescent agent, and stir evenly with a glass rod to obtain an oil-removing, anti-dandruff, anti-itch and moisturizing shampoo.

Example 3

3.1 Preparation of coix seed extract

Weigh 80g of coix seed, crush it, soak for 0.5h, heat and decoct for extraction 3 times, add 16 times the amount of water for the first time, extract for 2 hours, add 12 times the amount of water for the second time, extract for 1 hour, and add 8 times the amount for the third time water, extract for 0.5h, filter each time with 3 layers of gauze, combine the filtrate, and concentrate the volume of the filtrate to 4 times the weight of coix seed g/ml, and set aside.

3.2 Preparation of lemon juice extract

Weigh 70g of fresh lemon, extract 3 times, heat and decoct and extract 3 times, add 15 times of water for the first time, extract for 1.5h, use 10 times for the second time, extract for 1.5h, use 10 times of water for the third time, Extract for 1 hour, filter each time with double-layer gauze, combine the filtrates, concentrate the volume of the filtrates to 4 times the weight of the lemon g/ml, and set aside.

3.3 Preparation of ginger extract

Weigh 70g of ginger, cut into thin slices, reflux with water and extract 3 times, the first time use 14 times the amount of water, extract for 2.0h, filter, the second time use 10 times the amount of water, extract for 1.8h, the third time use 8 times the amount of water water, extract for 1.0 h, filter separately, combine the filtrates, concentrate under reduced pressure to 7 times the weight of ginger, g/ml, and set aside.

3.4 Preparation of peppermint extract:

Weigh 70g of fresh mint, put it into a round bottom flask, add 16 times of distilled water, place it in an electric heating mantle, use a volatile oil extractor to reflux extract for 5.5 hours, cool to room temperature, and filter the extract with double gauze. stand-by.

3.5 Preparation of Sophora flavescens extract

Weigh 70g of Sophora flavescens, crush and soak for 0.15h, heat and decoct for extraction 3 times, use 15 times the amount of water for the first time, extract for 1 hour, use 12 times the amount of water for the second time, extract for 1 hour, and use 10 times the amount for the third time water, extracted for 0.5h, and the extracts were combined and filtered with double-layer gauze, and the volume of the filtrate was concentrated to 4 times g/ml of the weight of Sophora flavescens, and set aside.

3.6 Preparation of Shampoo Cream

a) Weigh 0.6g of cationic guar gum, add it to 100ml of distilled water, heat in a water bath at 80°C, stir while heating, and after mixing evenly, let it stand to swell fully to obtain cationic guar gum gel liquid, wait use;

b) Weigh 1.0g of carbomer, add it to a beaker with 100ml of distilled water, heat it in a water bath at 80°C, stir while heating, let it stand still to fully swell, and form a carbomer gel liquid, which is ready for use;

c) Weigh 1.0 g of sodium carboxymethyl cellulose, add it to a beaker with 100 ml of distilled water, heat it in a water bath at 50 ° C, stir while heating, let it stand still to fully swell, and form a sodium carboxymethyl cellulose condensate, stand-by;

d) Weigh 1.5 g of sodium alginate, add it to a beaker with 100 ml of distilled water, heat it in a water bath at 80°C, stir while heating, let it stand still to fully swell, and form a sodium alginate gel liquid, which is ready for use;

e) Take miconazole 15g, add in the beaker that 100ml distilled water is housed, stir evenly with glass rod, obtain miconazole solution, stand-by;

f) Take 8g of sodium lauryl ether sulfate, 10g of sodium lauroyl glutamate, 12g of amino acid surfactants, 15g of MES, 16g of zinc pyrithione, 10g of clambolin, 10g of water-soluble vitamin E, and 50ml of distilled water in beaker 1, Put it in a constant temperature water bath at 80°C and stir to dissolve, and form solution 1 after complete dissolution, which is ready for use;

g) Take coix seed extract 2ml, lemon juice extract 3.2ml, ginger extract 2.8ml, peppermint extract 3.0ml, Sophora flavescens extract 3.0ml, miconazole solution in beaker 1, and stir evenly, Form solution 2, stand-by;

h) Weigh 3.5g of camellia oleifera seed oil, 4.5g of olive oil, 5g of simple emulsifier GOC, and 3g of emulsifier EG, put them on a water bath at 80°C, and use them as the oil phase for later use;

i) Take 25ml of distilled water and place it on a water bath at 80°C as the water phase for use;

j) When the oil phase and the water phase reach the same temperature, add the water phase into the oil phase in a thin stream, and stir while adding, until a milky white fine and uniform emulsion matrix is formed;

k) Add solution 1, solution 2, cationic guar gum gel, sodium alginate gel, carbomer gel, glycerin 5ml, 2% ethylparaben 75% ethanol solution 3ml to the emulsion base , Essence 0.35ml and pearlescent agent 1.2g, stir evenly with a glass rod to get oil-removing, anti-dandruff, anti-itch and moisturizing shampoo.

Example 4:

The physicochemical index of embodiment 1,2,3 is as follows:

4.1 Traits

This product is a milky white shampoo with suitable viscosity, smooth and rich foam, fine and uniform, and good spreadability.

4.2 pH check

Dip a small amount of shampoo with moistened pH test paper, the pH is 6-7.

4.3 Hot and cold test

Package the shampoo in a transparent cosmetic bottle and refrigerate it in a refrigerator at 4°C for about a week to observe that there is no delamination. In a constant temperature box at 55°C for 24 hours, the soap liquid has no phenomena such as stratification, emulsification and odor change.

4.4 Centrifugal test

Pack the shampoo cream into a stoppered test tube and centrifuge at 3000r/min for 20min without delamination.

4.5 Irritation test, allergy test

The hair on the back of the mouse was cut off, and the hair shampoo prepared in Examples 1 and 2 was applied to the cut hair respectively, and compared with the unpainted part, the result was no irritation and allergic reaction.

Get 1 gram of Example and apply it to volunteers (16-70 years old, 60 people) on their hands, observe after 30 minutes, and there is no redness, rash, and blistering.

4.6 Placement experiment at room temperature

The shampoo cream prepared in Examples 1 and 2 is placed in a cosmetic bottle, and left standing at room temperature for 6 months, no delamination phenomenon, no change in feeling after use, and no change in smell.

4.7 Anti-dandruff effect

Volunteers (16-70 years old, 60 people) were selected, and the prepared shampoo was used on the volunteers' hair, mixed with a small amount of water and scrubbed repeatedly. It was found that the foam was rich, and the volunteers generally felt smooth and comfortable, with better. Hair combs well both dry and wet. After washing with water, the hair is soft as silk, fluffy and non-greasy, with good moisturizing effect, no scalp itching after washing, and no need to use conditioner. After a month of continuous use, the hair is visibly shiny, soft, and dandruff is significantly reduced.

Example 5:

Investigation on the Comprehensive Effect of the Shampoo

The efficacy of the shampoos produced in Examples 1 and 2 will be evaluated by using the trial experience below. Adopt public opinion survey scoring method, select 50 women in the age group of 18-60 as trial objects, arbitrarily divide into two groups equally, wash hair with the shampoo cream prepared in embodiment 1, 2 respectively. Use twice a week for two months. The total score of each effect is 5: 5 is the highest score, which means very good and very satisfied; 4 is good; 3 is acceptable; below 3 is bad and unacceptable. Below are the average scores for each category. The results are shown in Table 1:

Table 1 Comprehensive effect investigation

To sum up, the shampoo prepared by the present invention is rich in foam, has good degreasing properties, decontamination properties, wet combing properties, and nourishing properties. It feels refreshing and comfortable when used. After use, the hair has good elasticity and has oil-removing properties. , hair care, anti-itch dandruff, prevent hair loss effect.

Claims (8)

1. Anti-dandruff and itching-relieving moist type shampoo paste and preparation method thereof 1. one kind is deoiled, it is characterised in that：Match containing following in shampoo paste The raw material components of ratio：

   Sodium laureth sulfate 2-8g

   Sodium lauroyl glutamate 1-10g

   GCK-12K 4-12g

   Dodecyl Polyoxyethylene Ether sulfosuccinate disodium MES 1-15g

   Simple emulsifier GOC 1-9g

   Emulsifier EG 1-9g

   Watermiscible vitamin E 2-10g

   Coix seed extracting solution 0.7-3.5ml

   Lemon extract 0.5-3.2ml

   Ginger extract 0.5-2.8ml

   Peppermint extracting solution 0.6-3.0ml

   Radix Sophorae Flavescentis extractive liquid 0.8-3.0ml

   Miconazole 1-15g

   Zinc pyrithione 2-16g

   Climbazole 1-10g

   Glycerine 2-7ml

   Pearling agent 0.5-1.2g

   Olive oil 1.2-4.5g

   Camellia seed oil 1.5-3.5g

   Cationic melon glue 0.06-0.6g

   Carbomer 0.05-1.5g

   Sodium carboxymethylcellulose 0.08-1.5g

   Sodium alginate 0.06-2.0g

   Distilled water 232-575ml

   Essence 0.08-0.35ml

   2% ethylparaben, 75% ethanol solution 0.5-3.5ml.
2. The anti-dandruff and itching-relieving moist type shampoo paste 2. one kind according to claim 1 is deoiled, it is characterised in that：The coix seed Extracting solution is to be prepared by the following method：

   It is appropriate to weigh coix seed, 0.15-0.8h is impregnated after crushing, heating decocts extraction 3 times, the 1st time plus 10-18 times and measures water, carries It takes 0.5-2h, measures water the 2nd time plus 8-15 times, extract 0.5-1.5h, measure water the 3rd time plus 8-10 times, extract 0.5-1.5h, filter every time It crosses, merging filtrate, the volume concentration of filtrate is filtered to 3-6 times of g/ml of coix seed weight to obtain the final product.
3. The anti-dandruff and itching-relieving moist type shampoo paste 3. one kind according to claim 1 is deoiled, it is characterised in that：The lemon carries Liquid is taken to be prepared by the following method：

   It is appropriate to weigh lemon, 0.15-0.8h is impregnated after incision, heating decocts extraction 3 times, the 1st time plus 8-15 times and measures water, extracts 0.5-2h, the 2nd time plus 8-10 times measure water, extract 0.5-1.5h, measure water the 3rd time plus 8-10 times, extract 0.5-1.5h, filter every time It crosses, merging filtrate, the volume concentration of filtrate is filtered to 3-6 times of g/ml of lemon weight to obtain the final product.
4. The anti-dandruff and itching-relieving moist type shampoo paste 4. one kind according to claim 1 is deoiled, it is characterised in that：The ginger carries Liquid is taken to be prepared by the following method：

   It is appropriate to weigh ginger, thinly slices, with water refluxing extraction 3 times, measures water with 10-18 times for the first time, extracts 0.5-2.5h, mistake Filter measures water with 8-15 times for the second time, extracts 0.5-2.5h, measures water with 6-12 times for the third time, extracts 0.5-1.5h, filters respectively, The 6-10 times of g/ml for ginger weight is concentrated under reduced pressure, for use in merging filtrate.
5. The anti-dandruff and itching-relieving moist type shampoo paste 5. one kind according to claim 1 is deoiled, it is characterised in that：The peppermint carries Liquid is taken to be prepared by the following method：

   It is a certain amount of to weigh fresh mint, is put into round-bottomed flask, and 10-18 times of distilled water is added, is positioned in electric jacket, uses It after 5-6 hour of volatile oil extractor refluxing extraction, is cooled to room temperature, filters extracting solution with double gauze, for use.
6. The anti-dandruff and itching-relieving moist type shampoo paste 6. one kind according to claim 1 is deoiled, it is characterised in that：The kuh-seng carries Liquid is taken to be prepared by the following method：

   It is appropriate to weigh kuh-seng, 0.15-0.8h is impregnated after crushing, heating decocts extraction 3 times, the 1st time plus 10-18 times and measures water, extracts 0.5-2h, the 2nd time plus 10-12 times measure water, extract 0.5-1.5h, measure water the 3rd time plus 8-12 times, extract 0.5-1.5h, filter every time It crosses, merging filtrate, the volume concentration of filtrate is filtered to 3-6 times of g/ml of kuh-seng weight to obtain the final product.
7. The anti-dandruff and itching-relieving moist type shampoo paste 7. one kind according to claim 1 is deoiled, it is characterised in that：The essence is Milk flavour, peach flavor, lily essence, cream jasmin france, osmanthus flower fragrance, flavoring rose essence.
8. 8. a kind of preparation method of anti-dandruff and itching-relieving moist type shampoo paste that deoils according to claim 1, it is characterised in that：

   a）Cationic melon glue 0.06-0.6g is weighed, is added in the distilled water of 50-100ml, 60-80 DEG C of heating water bath, side Heat side stirring, it is to be mixed uniformly after, standing allows it to be fully swollen, and obtains cationic melon gelling glue, for use；

   b）Carbomer 0.05-1.5g is weighed, is added in the beaker equipped with 50-100ml distilled water, 60-80 DEG C of heating water bath, side Side stirring is heated, standing allows it to be fully swollen, and forms carbomer gel liquid, for use；

   c）Sodium carboxymethylcellulose 0.08-1.5g is weighed, is added in the beaker equipped with 50-100ml distilled water, 40-50 DEG C of water Bath heating, heats while stirring, and standing allows it to be fully swollen, and forms sodium carboxymethylcellulose lime set, for use；

   d）Sodium alginate 0.06-2g is weighed, is added in the beaker equipped with 50-100ml distilled water, 60-80 DEG C of heating water bath, side Side stirring is heated, standing allows it to be fully swollen, and forms sodium alginate gel liquid, for use；

   e）Miconazole 1-15g is weighed, is added in the beaker equipped with 10-100ml distilled water, is stirred evenly with glass bar, obtain miaow Health azoles solution, for use；

   f）Take respectively sodium laureth sulfate 2-8g, sodium lauroyl glutamate 1-10g, GCK-12K 4-12g, MES 1-15g, Zinc pyrithione 2-16g, climbazole 1-10g, watermiscible vitamin E 2-10g, distilled water 10-50ml are placed in beaker 1 Stirring and dissolving in 60-90 DEG C of thermostat water bath forms solution 1, for use after being completely dissolved；

   g）Coix seed extracting solution 0.7-3.5ml, lemon extract 0.5-3.2ml, ginger extract 0.5-2.8ml, thin is taken respectively Lotus extracting solution 0.6-3.0ml, Radix Sophorae Flavescentis extractive liquid 0.8-3.0ml, Miconazole solution are placed in beaker 1, and stir evenly, and are formed Solution 2, for use；

   h）Camellia seed oil 1.5-3.5g, olive oil 1.2-4.5g, simple emulsifier GOC 1-9g, emulsifier EG 1-9g are weighed, is set In in 60-90 DEG C of water-bath, as oil phase, for use；

   i）12-25ml distilled water is measured, is placed in 60-90 DEG C of water-bath, as water phase, for use；

   j）When equal oil phases reach mutually synthermal with water phase, water phase is added in thread shape in oil phase, it is stirring while adding, until being formed The fine and smooth uniform emulsion bases of milky；

   k）It is solidifying that solution 1, solution 2, cationic melon gelling glue, sodium alginate gel liquid, carbomer are added into emulsion bases Glue, glycerine 2-7ml, 2% ethylparaben, 75% ethanol solution 0.5-3.5ml, essence 0.08-0.35ml and pearling agent 0.5- 1.2g stirs evenly the anti-dandruff and itching-relieving moist type shampoo paste that deoils to obtain the final product with glass bar.