CN114150287A - Thin film deposition method and equipment - Google Patents
Thin film deposition method and equipment Download PDFInfo
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- CN114150287A CN114150287A CN202111505256.4A CN202111505256A CN114150287A CN 114150287 A CN114150287 A CN 114150287A CN 202111505256 A CN202111505256 A CN 202111505256A CN 114150287 A CN114150287 A CN 114150287A
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/54—Controlling or regulating the coating process
- C23C14/542—Controlling the film thickness or evaporation rate
- C23C14/545—Controlling the film thickness or evaporation rate using measurement on deposited material
- C23C14/547—Controlling the film thickness or evaporation rate using measurement on deposited material using optical methods
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- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
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- C23C14/35—Sputtering by application of a magnetic field, e.g. magnetron sputtering
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Abstract
本发明提供了一种薄膜沉积方法及设备,方法包括:对圆晶进行多个分步沉积;在分步沉积之间,进行多点的前步沉积厚度检测,得到多点的前步沉积厚度;根据多点的前步沉积厚度分析前步沉积均匀度;判断前步沉积均匀度是否满足要求,若不满足则根据不均匀点分布情况,调整检测的后步沉积的各点局部沉积速率,在检测后继续进行的后步沉积中进行沉积厚度的均匀度补偿。设备包括PVD沉积腔体、光学测试腔体和控制器;用以采用前述方法进行圆晶沉积工艺。本发明通过将同一沉积层薄膜的沉积工艺分为多个分步沉积,在分步沉积之间,进行多点的前步沉积厚度检测及均匀度补偿,使得沉积后的沉积层薄膜厚度均匀,简化后续生产流程,提高生产效率,降低生产成本。
The invention provides a method and equipment for film deposition. The method includes: performing multiple step-by-step deposition on a wafer; between the step-by-step depositions, performing multi-point pre-deposition thickness detection to obtain the multi-point pre-deposition thickness ; Analyze the pre-deposition uniformity according to the multi-point pre-deposition thickness; judge whether the pre-deposition uniformity meets the requirements, if not, adjust the local deposition rate of the detected post-deposition points according to the uneven point distribution, The uniformity compensation of the deposition thickness is performed in the subsequent deposition that continues after the inspection. The equipment includes a PVD deposition chamber, an optical test chamber and a controller; it is used for the wafer deposition process using the aforementioned method. The invention divides the deposition process of the same deposition layer film into multiple step-by-step depositions, and performs multi-point pre-deposition thickness detection and uniformity compensation between the step-by-step depositions, so that the thickness of the deposited layer film after deposition is uniform. Simplify the follow-up production process, improve production efficiency and reduce production costs.
Description
技术领域technical field
本发明涉及半导体器件制备中的沉积工艺及设备技术领域,特别涉及一种薄膜沉积方法及设备。The invention relates to the technical field of deposition process and equipment in the preparation of semiconductor devices, in particular to a thin film deposition method and equipment.
背景技术Background technique
圆晶沉积工艺是半导体器件制备中最常用的工艺之一,目前,用于圆晶沉积工艺的薄膜沉积机台,如图1所示,都是无区别地在晶圆上一次性沉积一定厚度(设计厚度)的薄膜。The wafer deposition process is one of the most commonly used processes in the preparation of semiconductor devices. At present, the thin film deposition machines used in the wafer deposition process, as shown in Figure 1, are indiscriminately depositing a certain thickness on the wafer at one time. (design thickness) of the film.
但是,传统沉积方式的弊端是:受制于机台硬体设备,随着设备使用时间的增长,设备会存在耗损,或者受到其它因素影响,会导致沉积的薄膜均匀度变差,导致硅片上厚度不均匀,对圆晶的加工产生不利影响,使得产品的品质下降,降低了产品的良品率;为了防止这种情况发生往往需要在后续的工艺中增加圆晶的表面修复或者补偿工序,使得后续生产流程复杂化,降低了生产效率,提高了生产成本。However, the disadvantages of the traditional deposition method are: subject to the hardware equipment of the machine, with the increase of the use time of the equipment, the equipment will be worn out, or affected by other factors, which will lead to the deterioration of the uniformity of the deposited film, resulting in the loss of the silicon wafer. The uneven thickness has an adverse effect on the processing of the wafer, which reduces the quality of the product and reduces the yield of the product; in order to prevent this from happening, it is often necessary to increase the surface repair or compensation process of the wafer in the subsequent process, so that the The subsequent production process is complicated, which reduces the production efficiency and increases the production cost.
发明内容SUMMARY OF THE INVENTION
为了解决上述技术问题,本发明提供了一种薄膜沉积方法,包括以下步骤:In order to solve the above-mentioned technical problems, the present invention provides a thin film deposition method, comprising the following steps:
S100对圆晶进行多个分步沉积;S100 performs multiple step-by-step depositions on wafers;
S200在分步沉积之间,进行多点的前步沉积厚度检测,得到多点的前步沉积厚度;S200 performs multi-point pre-deposition thickness detection between the step-by-step deposition, and obtains the multi-point pre-deposition thickness;
S300根据多点的前步沉积厚度分析前步沉积均匀度;S300 analyzes the pre-deposition uniformity according to the multi-point pre-deposition thickness;
S400判断前步沉积均匀度是否满足要求,若不满足则执行S500步骤;S400 judges whether the deposition uniformity of the previous step meets the requirements, and if not, executes step S500;
S500根据不均匀点分布情况,调整检测的后步沉积的各点局部沉积速率,在检测后继续进行的后步沉积中进行沉积厚度的均匀度补偿。S500 adjusts the local deposition rate of each point of the detected subsequent deposition according to the uneven point distribution, and performs uniformity compensation of the deposition thickness in the subsequent subsequent deposition after the detection.
可选的,在S200步骤中,沉积厚度检测采用光学测量方式,以光束照射各点,采集各点的表面反射率和折射率;Optionally, in step S200, the deposition thickness detection adopts an optical measurement method, irradiating each point with a light beam, and collecting the surface reflectivity and refractive index of each point;
在S300步骤中,根据各点的表面反射率和折射率计算得到各点的前步沉积厚度,再计算各点前步沉积厚度的标准方差,标准方差等于各点前步沉积厚度的最大值与最小值之差除以检测点数,标准方差越小则表示沉积越均匀。In step S300, the previous deposition thickness of each point is calculated according to the surface reflectivity and refractive index of each point, and then the standard deviation of the previous deposition thickness of each point is calculated, and the standard deviation is equal to the maximum value of the previous deposition thickness of each point and The difference between the minimum values is divided by the number of detection points. The smaller the standard deviation, the more uniform the deposition.
可选的,在S400步骤中,若计算得到的标准方差大于设定阈值,则表示前步沉积均匀度不满足要求。Optionally, in step S400, if the calculated standard deviation is greater than the set threshold, it means that the deposition uniformity of the previous step does not meet the requirements.
可选的,在S500步骤中,调整检测的后步沉积的各点局部沉积速率的方式包括气体流量调节、托盘的水平调节、靶材的高低调节以及传送装置的步进马达步数调节中的一种或者多种;Optionally, in step S500, the methods for adjusting the local deposition rate of each point of the detected subsequent deposition include gas flow adjustment, level adjustment of the tray, height adjustment of the target material, and adjustment of the number of steps of the stepping motor of the conveying device. one or more;
所述气体流量调节采用控制不同管路的气体流量方式改变局部沉积速率;The gas flow adjustment adopts the method of controlling the gas flow of different pipelines to change the local deposition rate;
所述托盘的水平调节通过调节托盘的水平度方式改变局部沉积速率;The level adjustment of the tray changes the local deposition rate by adjusting the level of the tray;
所述靶材的高低调节通过改变靶材悬挂高度方式改变局部沉积速率;The height adjustment of the target material changes the local deposition rate by changing the hanging height of the target material;
所述传送装置的步进马达步数调节,从而控制晶圆在托盘上的位置改变局部沉积速率。The number of steps of the stepper motor of the conveying device is adjusted, thereby controlling the position of the wafer on the tray to change the local deposition rate.
可选的,在S200步骤中,进行49点或者128点的前步沉积厚度检测,各点均匀分布为圆晶表面。Optionally, in step S200, 49 points or 128 points of the previous deposition thickness detection are performed, and each point is evenly distributed as the wafer surface.
可选的,在S300步骤中,通过设置圆晶检测点模型,根据检测点的对应关系,将实时检测的各点厚度数据导入圆晶检测点模型;Optionally, in step S300, by setting a wafer detection point model, and according to the corresponding relationship of the detection points, import the thickness data of each point detected in real time into the wafer detection point model;
在S500步骤中,依据各点厚度绘制形成圆晶表面形貌图,然后根据圆晶表面形貌图确定各点局部沉积速率,在检测后继续进行的后步沉积进行沉积厚度的均匀度补偿。In step S500, a topography map of the wafer surface is drawn according to the thickness of each point, and then the local deposition rate of each point is determined according to the topography map of the wafer surface, and the subsequent deposition after detection is performed to compensate for the uniformity of the deposition thickness.
本发明还提供了一种薄膜沉积设备,包括PVD沉积腔体、光学测试腔体和控制器;其中,The present invention also provides a thin film deposition equipment, comprising a PVD deposition chamber, an optical test chamber and a controller; wherein,
所述PVD沉积腔体用于对圆晶进行多个分步沉积;The PVD deposition chamber is used to perform multiple step-by-step depositions on the wafer;
所述光学测试腔体用于在分步沉积之间,进行多点的前步沉积厚度检测;The optical test cavity is used for multi-point pre-deposition thickness detection between the step-by-step deposition;
所述控制器分别与PVD沉积腔体与光学测试腔体连接,所述控制器用于控制分步沉积和在分步沉积之间进行多点的前步沉积厚度检测,根据多点的前步沉积厚度分析前步沉积均匀度;判断前步沉积均匀度是否满足要求,若不满足则根据不均匀点分布情况,调整检测的后步沉积的各点局部沉积速率,在检测后继续进行的后步沉积中进行沉积厚度的均匀度补偿。The controller is respectively connected with the PVD deposition chamber and the optical test chamber, and the controller is used to control the step-by-step deposition and perform multi-point pre-step deposition thickness detection between the step-by-step depositions. According to the multi-point pre-step deposition Thickness analysis of the deposition uniformity of the previous step; to judge whether the deposition uniformity of the previous step meets the requirements, if not, adjust the local deposition rate of each point of the detection of the subsequent deposition according to the distribution of uneven points, and continue the subsequent step after the detection The uniformity compensation of the deposition thickness is performed during deposition.
可选的,所述PVD沉积腔体包括旋转永磁体、金属靶材、托盘和多个气体出口;Optionally, the PVD deposition chamber includes a rotating permanent magnet, a metal target, a tray and multiple gas outlets;
所述托盘用于承载圆晶;the tray is used for carrying wafers;
所述金属靶材设置于托盘上方且与托盘间隔第一距离;The metal target is arranged above the tray and is spaced from the tray by a first distance;
所述旋转永磁体设置于金属靶材上方且与金属靶材间隔第二距离;The rotating permanent magnet is disposed above the metal target and is spaced from the metal target by a second distance;
所述多个气体出口分别设置于托盘下部以及金属靶材与托盘间隔空间处的侧面,每个气体出口与不同管路连接。The plurality of gas outlets are respectively arranged on the lower part of the tray and the side of the space between the metal target and the tray, and each gas outlet is connected with a different pipeline.
可选的,所述托盘配置有调节基座,所述调节基座与控制器连接,所述调节基座在控制器的控制下能够改变托盘的水平度。Optionally, the tray is provided with an adjustment base, the adjustment base is connected to the controller, and the adjustment base can change the levelness of the tray under the control of the controller.
可选的,所述多个气体出口连接的不同管路都设有流量调节阀,所述流量调节阀与控制器连接,所述流量调节阀在控制器的控制下能够改变对应气体出口管路的气体流量。Optionally, different pipelines connected to the multiple gas outlets are provided with flow regulating valves, the flow regulating valves are connected to the controller, and the flow regulating valves can change the corresponding gas outlet pipelines under the control of the controller. gas flow.
可选的,所述控制器包括主控芯片,所述主控芯片内置圆晶检测点模型,根据检测点的对应关系,将实时检测的各点厚度数据导入圆晶检测点模型;依据各点厚度绘制形成圆晶表面形貌图,然后根据圆晶表面形貌图确定各点局部沉积速率,在检测后继续进行的后步沉积进行沉积厚度的均匀度补偿。Optionally, the controller includes a main control chip, the main control chip has a built-in wafer detection point model, and according to the corresponding relationship of the detection points, the thickness data of each point detected in real time is imported into the wafer detection point model; The thickness is drawn to form a topography map of the wafer surface, and then the local deposition rate of each point is determined according to the topography map of the wafer surface, and the subsequent deposition after the detection is performed to compensate for the uniformity of the deposition thickness.
可选的,所述金属靶材设有高度调节器,所述高度调节器与控制器连接,所述高度调节器在控制器的控制下能够改变金属靶材与托盘间隔的第一距离。Optionally, the metal target is provided with a height adjuster, the height adjuster is connected to the controller, and the height adjuster can change the first distance between the metal target and the tray under the control of the controller.
本发明的薄膜沉积方法及设备,通过将同一沉积层薄膜的沉积工艺分为多个分步沉积,在分步沉积之间,进行多点的前步沉积厚度检测,根据检测若存在厚度不均匀情况,则根据不均匀点分布,相应地调整检测的后步沉积的各点局部沉积速率,在检测后继续进行的后步沉积进行沉积厚度的均匀度补偿,使得沉积后的沉积层薄膜厚度均匀,不需要在后续工艺中增加圆晶的表面修复或者补偿工序,简化了后续生产流程,提高了生产效率,降低了生产成本。The film deposition method and device of the present invention divide the deposition process of the same deposition layer film into a plurality of step-by-step depositions, and between the step-by-step depositions, perform multi-point pre-deposition thickness detection, and if there is uneven thickness according to the detection According to the uneven point distribution, the local deposition rate of each point of the subsequent deposition of the detection is adjusted accordingly, and the subsequent deposition that continues after the detection is performed to compensate for the uniformity of the deposition thickness, so that the thickness of the deposited layer after deposition is uniform. , there is no need to increase the surface repair or compensation process of the wafer in the subsequent process, which simplifies the subsequent production process, improves the production efficiency, and reduces the production cost.
本发明的其它特征和优点将在随后的说明书中阐述,并且,部分地从说明书中变得显而易见,或者通过实施本发明而了解。本发明的目的和其他优点可通过在所写的说明书、权利要求书、以及附图中所特别指出的结构来实现和获得。Other features and advantages of the present invention will be set forth in the description which follows, and in part will be apparent from the description, or may be learned by practice of the invention. The objectives and other advantages of the invention may be realized and attained by the structure particularly pointed out in the written description, claims, and drawings.
下面通过附图和实施例,对本发明的技术方案做进一步的详细描述。The technical solutions of the present invention will be further described in detail below through the accompanying drawings and embodiments.
附图说明Description of drawings
附图用来提供对本发明的进一步理解,并且构成说明书的一部分,与本发明的实施例一起用于解释本发明,并不构成对本发明的限制。在附图中:The accompanying drawings are used to provide a further understanding of the present invention, and constitute a part of the specification, and are used to explain the present invention together with the embodiments of the present invention, and do not constitute a limitation to the present invention. In the attached image:
图1为现有的薄膜沉积设备立体图;1 is a perspective view of an existing thin film deposition equipment;
图2为本发明实施例中一种薄膜沉积方法流程图;2 is a flow chart of a thin film deposition method according to an embodiment of the present invention;
图3为本发明实施例中一种薄膜沉积设备示意图;3 is a schematic diagram of a thin film deposition apparatus in an embodiment of the present invention;
图4为本发明的薄膜沉积设备实施例采用的PVD沉积腔体示意图;4 is a schematic diagram of a PVD deposition chamber used in an embodiment of the thin film deposition apparatus of the present invention;
图5为本发明采用9点进行前步沉积厚度检测的取点布置示意图;FIG. 5 is a schematic diagram of the arrangement of the points of the present invention using 9 points to detect the thickness of the previous step;
图6为本发明采用多点进行前步沉积厚度检测的取点布置以及根据各点检测数据得出的晶圆表面形貌及均匀度情况示意图。FIG. 6 is a schematic diagram showing the arrangement of the points of the present invention for detecting the thickness of the previous deposition by using multiple points, and the surface morphology and uniformity of the wafer obtained according to the detection data of each point.
具体实施方式Detailed ways
以下结合附图对本发明的优选实施例进行说明,应当理解,此处所描述的优选实施例仅用于说明和解释本发明,并不用于限定本发明。The preferred embodiments of the present invention will be described below with reference to the accompanying drawings. It should be understood that the preferred embodiments described herein are only used to illustrate and explain the present invention, but not to limit the present invention.
如图2所示,本发明实施例提供了一种薄膜沉积方法,包括以下步骤:As shown in FIG. 2, an embodiment of the present invention provides a thin film deposition method, comprising the following steps:
S100对圆晶进行多个分步沉积;S100 performs multiple step-by-step depositions on wafers;
S200在分步沉积之间,进行多点的前步沉积厚度检测,得到多点的前步沉积厚度;S200 performs multi-point pre-deposition thickness detection between the step-by-step deposition, and obtains the multi-point pre-deposition thickness;
S300根据多点的前步沉积厚度分析前步沉积均匀度;S300 analyzes the pre-deposition uniformity according to the multi-point pre-deposition thickness;
S400判断前步沉积均匀度是否满足要求,若不满足则执行S500步骤;S400 judges whether the deposition uniformity of the previous step meets the requirements, and if not, executes step S500;
S500根据不均匀点分布情况,调整检测的后步沉积的各点局部沉积速率,在检测后继续进行的后步沉积中进行沉积厚度的均匀度补偿。S500 adjusts the local deposition rate of each point of the detected subsequent deposition according to the uneven point distribution, and performs uniformity compensation of the deposition thickness in the subsequent subsequent deposition after the detection.
上述技术方案的工作原理为:本方案对圆晶进行多个分步沉积,可以采用2-5个分步沉积,例如采用3个或者4个分步沉积;对于分3个分步沉积的,可以在第一个分步沉积和第二个分步沉积之间和/或第二个分步沉积和第三个分步沉积之间对前步沉积的沉积厚度进行多点检测,根据检测进行均匀度情况判断,以确定是否需要调整局部沉积速率;若调整局部沉积速率,调整原则是提高沉积厚度偏薄的局部区域的局部沉积速率,降低沉积厚度偏厚的局部区域的局部沉积速率;后步沉积采用调整后的沉积速率对沉积厚度均匀性进行补偿,以控制成膜后的薄膜厚度均匀度。前步沉积是指当前检测之前的所有分步沉积,后步沉积是指当前检测之后的所有分步沉积;例如分3个分步沉积,对于第一分步沉积和第二分步沉积之间的检测,则其前步沉积指第一分步沉积,后步沉积是指第二分步沉积和第三分步沉积;对于第二分步沉积和第三分步沉积之间的检测,则其前步沉积指第一分步沉积和第二分步沉积,后步沉积是指第三分步沉积。所有分步沉积的时间总长为该沉积层需要的总沉积时长,各分步沉积的分时长可以相同也可以不同;例如若沉积层需要的总沉积时长为60秒,分3个分步沉积,可以是每个分步沉积的分时长为20秒,也可以第一分步沉积的分时长为10秒,第二分步沉积的分时长为20秒,而第三分步沉积的分时长为30秒。The working principle of the above technical solution is as follows: in this solution, the wafer is deposited in multiple steps, and 2-5 step-by-step depositions can be used, for example, 3 or 4 step-by-step depositions; A multi-point inspection of the deposition thickness of the previous step deposition can be performed between the first step deposition and the second step deposition and/or between the second step deposition and the third step deposition, according to the inspection. The uniformity is judged to determine whether the local deposition rate needs to be adjusted; if the local deposition rate is adjusted, the adjustment principle is to increase the local deposition rate in the local area with thin deposition thickness and reduce the local deposition rate in the local area with thick deposition thickness; The step deposition uses an adjusted deposition rate to compensate for the deposition thickness uniformity to control the film thickness uniformity after film formation. Pre-step deposition refers to all step depositions before the current detection, and post-step deposition refers to all step depositions after the current detection; for example, 3 step depositions, for the time between the first step deposition and the second step deposition detection, the previous deposition refers to the first deposition, the latter deposition refers to the second deposition and the third deposition; for the detection between the second deposition and the third deposition, then The previous step deposition refers to the first step deposition and the second step deposition, and the latter step deposition refers to the third step deposition. The total deposition time of all the sub-layers is the total deposition time required for the deposition layer, and the sub-deposition time of each sub-deposition can be the same or different; It can be that each sub-step deposition is 20 seconds long, or the first sub-step deposition is 10 seconds, the second sub-step deposition is 20 seconds, and the third sub-step deposition sub-time is 30 seconds.
上述技术方案的有益效果为:本方案通过将同一沉积层薄膜的沉积工艺分为多个分步沉积,在分步沉积之间,进行多点的前步沉积厚度检测,根据检测若存在厚度不均匀情况,则根据不均匀点分布,相应地调整检测的后步沉积的各点局部沉积速率,在检测后继续进行的后步沉积进行沉积厚度的均匀度补偿,使得沉积后的沉积层薄膜厚度均匀,不需要在后续工艺中增加圆晶的表面修复或者补偿工序,简化了后续生产流程,提高了生产效率,降低了生产成本。The beneficial effects of the above technical solutions are: in this solution, the deposition process of the same deposition layer film is divided into multiple step-by-step depositions, and between the step-by-step depositions, multi-point pre-deposition thickness detection is performed. In the case of uniformity, according to the uneven point distribution, the local deposition rate of each point of the subsequent deposition of the detection is adjusted accordingly, and the subsequent deposition after the detection is performed to compensate for the uniformity of the deposition thickness, so that the thickness of the deposited layer after deposition is It is uniform and does not need to increase the surface repair or compensation process of the wafer in the subsequent process, which simplifies the subsequent production process, improves the production efficiency, and reduces the production cost.
在一个实施例中,在S200步骤中,沉积厚度检测采用光学测量方式,以光束照射各点,采集各点的表面反射率和折射率;In one embodiment, in step S200, the deposition thickness detection adopts an optical measurement method, irradiates each point with a light beam, and collects the surface reflectivity and refractive index of each point;
在S300步骤中,根据各点的表面反射率和折射率计算得到各点的前步沉积厚度,再计算各点前步沉积厚度的标准方差,标准方差等于各点前步沉积厚度的最大值与最小值之差除以检测点数,标准方差越小则表示沉积越均匀。In step S300, the previous deposition thickness of each point is calculated according to the surface reflectivity and refractive index of each point, and then the standard deviation of the previous deposition thickness of each point is calculated, and the standard deviation is equal to the maximum value of the previous deposition thickness of each point and The difference between the minimum values is divided by the number of detection points. The smaller the standard deviation, the more uniform the deposition.
上述技术方案的工作原理和有益效果为:本方案采用光学测量方式进行沉积厚度检测,通过光束照射各点,采集各点的表面反射率和折射率,同一点的反射率和折射率反应了沉积的厚度,可以设定反射率和折射率与沉积的厚度数量关系的公式,用来计算各点的沉积厚度;本方案还引入标准方差来对沉积的厚度均匀性进行评价,标准方差等于各点前步沉积厚度的最大值与最小值之差除以检测点数,标准方差越小则表示沉积越均匀,标准方差越大则表示沉积越不均匀,以数值量化评价,更利于进行厚度均匀性判断,提高了判断的客观性和准确性。The working principle and beneficial effects of the above technical solution are as follows: this solution adopts an optical measurement method to detect the deposition thickness, irradiates each point with a light beam, and collects the surface reflectivity and refractive index of each point, and the reflectivity and refractive index of the same point reflect the deposition. The thickness of the deposit can be set by the formula of the quantitative relationship between the reflectivity and the refractive index and the thickness of the deposition, which can be used to calculate the deposition thickness of each point; this scheme also introduces the standard deviation to evaluate the thickness uniformity of the deposition, and the standard deviation is equal to the thickness of each point. The difference between the maximum value and the minimum value of the deposition thickness in the previous step is divided by the number of detection points. The smaller the standard deviation is, the more uniform the deposition is, and the larger the standard deviation is, the more uneven the deposition is. Numerical quantitative evaluation is more conducive to the determination of thickness uniformity. , improve the objectivity and accuracy of judgment.
在一个实施例中,在S400步骤中,若计算得到的标准方差大于设定阈值,则表示前步沉积均匀度不满足要求。In one embodiment, in step S400, if the calculated standard deviation is greater than the set threshold, it means that the deposition uniformity of the previous step does not meet the requirements.
上述技术方案的工作原理和有益效果为:本方案在前述引入标准方差对厚度均匀性以数值量化评价的基础上,采用设定阈值与标准方差的对比来进行厚度均匀性判断,若计算得到的标准方差大于设定阈值,则表示前步沉积均匀度不满足要求,提高了判断的客观性和准确性。The working principle and beneficial effects of the above technical solutions are as follows: in this solution, on the basis of numerically quantifying the thickness uniformity by introducing the standard deviation, the comparison between the set threshold and the standard deviation is used to judge the thickness uniformity. If the standard deviation is greater than the set threshold, it means that the deposition uniformity of the previous step does not meet the requirements, which improves the objectivity and accuracy of judgment.
在一个实施例中,在S500步骤中,调整检测的后步沉积的各点局部沉积速率的方式包括气体流量调节、托盘的水平调节、靶材的高低调节以及传送装置的步进马达步数调节中的一种或者多种;In one embodiment, in step S500, the method of adjusting the local deposition rate of each point of the detected subsequent deposition includes gas flow adjustment, level adjustment of the tray, height adjustment of the target material, and adjustment of the number of steps of the stepping motor of the conveying device one or more of;
所述气体流量调节采用控制不同管路的气体流量方式改变局部沉积速率;The gas flow adjustment adopts the method of controlling the gas flow of different pipelines to change the local deposition rate;
所述托盘的水平调节通过调节托盘的水平度方式改变局部沉积速率;The level adjustment of the tray changes the local deposition rate by adjusting the level of the tray;
所述靶材的高低调节通过改变靶材悬挂高度方式改变局部沉积速率;The height adjustment of the target material changes the local deposition rate by changing the hanging height of the target material;
所述传送装置的步进马达步数调节,从而控制晶圆在托盘上的位置改变局部沉积速率。The number of steps of the stepper motor of the conveying device is adjusted, thereby controlling the position of the wafer on the tray to change the local deposition rate.
上述技术方案的工作原理和有益效果为:本方案提供了对后步沉积的各点局部沉积速率调整的方式,可以采用气体流量调节、托盘的水平调节、靶材的高低调节或者传送装置的步进马达步数调节,也可以采用前述调节方式中的多种进行组合调节,以达到改变局部沉积速率的目的,实现工艺补偿,提高沉积厚度均匀性。The working principle and beneficial effects of the above technical solutions are as follows: this solution provides a method for adjusting the local deposition rate of each point of the subsequent deposition, which can be adjusted by gas flow adjustment, level adjustment of the tray, height adjustment of the target material or step of the conveying device. For the adjustment of the number of motor steps, various of the aforementioned adjustment methods can also be used for combined adjustment, so as to achieve the purpose of changing the local deposition rate, realize process compensation, and improve the uniformity of deposition thickness.
在一个实施例中,在S200步骤中,进行49点或者128点的前步沉积厚度检测,各点均匀分布为圆晶表面。In one embodiment, in step S200, 49 points or 128 points of previous deposition thickness detection are performed, and each point is evenly distributed as the wafer surface.
上述技术方案的工作原理和有益效果为:检测点布置可以根据需要,结合精度要求确定检测点的数量,为了分析简便,一般检测点采用均匀分布为圆晶表面,如图5所示为在圆晶4的表面布置有9个检测点5的布局方式;本方案限定检测点的数量为49点或者128点,检测点布置越密集,对圆晶表面的形貌描述会更细致,更能够精确反应沉积厚度分布情况,但检测点太多,各局部区域面积越小,检测及处理的数据量增加,影响检测的实时性和效率,因此选择49点~128点范围为宜,也可以采用64点或者96点等。The working principle and beneficial effects of the above technical solutions are as follows: the number of detection points can be determined according to the needs and in combination with the accuracy requirements. In order to simplify the analysis, the detection points are generally uniformly distributed on the surface of the wafer, as shown in Figure 5. There are 9
如图3所示,本发明实施例提供了一种薄膜沉积设备,包括PVD沉积腔体1、光学测试腔体2和控制器(图中未示出);其中,As shown in FIG. 3, an embodiment of the present invention provides a thin film deposition apparatus, including a
所述PVD沉积腔体1用于对圆晶进行多个分步沉积;The
所述光学测试腔体2用于在分步沉积之间,进行多点的前步沉积厚度检测;The
所述控制器分别与PVD沉积腔体与光学测试腔体连接,所述控制器用于控制分步沉积和在分步沉积之间进行多点的前步沉积厚度检测,根据多点的前步沉积厚度分析前步沉积均匀度;判断前步沉积均匀度是否满足要求,若不满足则根据不均匀点分布情况,调整检测的后步沉积的各点局部沉积速率,在检测后继续进行的后步沉积中进行沉积厚度的均匀度补偿。The controller is respectively connected with the PVD deposition chamber and the optical test chamber, and the controller is used to control the step-by-step deposition and perform multi-point pre-step deposition thickness detection between the step-by-step depositions. According to the multi-point pre-step deposition Thickness analysis of the deposition uniformity of the previous step; to judge whether the deposition uniformity of the previous step meets the requirements, if not, adjust the local deposition rate of each point of the detection of the subsequent deposition according to the distribution of uneven points, and continue the subsequent step after the detection The uniformity compensation of the deposition thickness is performed during deposition.
上述技术方案的工作原理和有益效果为:本方案通过在薄膜沉积设备中设置光学测试腔体,通过控制器进行沉积控制,在PVD沉积腔体中将同一沉积层薄膜的沉积工艺分为多个分步沉积,在分步沉积之间,将圆晶放入光学测试腔体进行多点的前步沉积厚度检测,根据检测若存在厚度不均匀情况,则根据不均匀点分布,相应地调整检测的后步沉积的各点局部沉积速率,在检测后继续进行的后步沉积进行沉积厚度的均匀度补偿,使得沉积后的沉积层薄膜厚度均匀,不需要在后续工艺中增加圆晶的表面修复或者补偿工序,简化了后续生产流程,提高了生产效率,降低了生产成本。The working principle and beneficial effects of the above technical solutions are as follows: in this solution, an optical test cavity is set in the film deposition equipment, and the deposition control is performed by a controller, and the deposition process of the same deposition layer film is divided into multiple layers in the PVD deposition cavity. Step-by-step deposition, between the step-by-step deposition, put the wafer into the optical test chamber for multi-point pre-deposition thickness detection, if there is uneven thickness according to the detection, adjust the detection accordingly according to the uneven point distribution The local deposition rate of each point of the subsequent deposition, after the detection, the subsequent deposition that continues to perform the uniformity compensation of the deposition thickness, so that the thickness of the deposited layer after deposition is uniform, and there is no need to increase the surface repair of the wafer in the subsequent process. Or the compensation process simplifies the subsequent production process, improves the production efficiency, and reduces the production cost.
在一个实施例中,如图4所示,所述PVD沉积腔体1包括旋转永磁体11、金属靶材12、托盘13和多个气体出口14;In one embodiment, as shown in FIG. 4 , the
所述托盘13用于承载圆晶4;The
所述金属靶材12设置于托盘13上方且与托盘13间隔第一距离;The
所述旋转永磁体11设置于金属靶材12上方且与金属靶材12间隔第二距离;The rotating
所述多个气体出口14分别设置于托盘13下部以及金属靶材12与托盘13间隔空间处的侧面,每个气体出口14与不同管路连接。The plurality of
上述技术方案的工作原理和有益效果为:本方案提供了PVD沉积腔体采用的结构形式,其中,第一距离指金属靶材与托盘在高度方向的间隔距离,第二距离指旋转永磁体与金属靶材在高度方向的间隔距离;生产中,通过传送装置将圆晶送至托盘,以管路连接供应气体出口向PVD沉积腔体内提供相应的工艺气体,旋转永磁体产生高速荷能粒子磁控溅射,通过高速荷能粒子轰击金属靶材,实现对圆晶表面进行镀膜。The working principle and beneficial effects of the above technical solutions are as follows: this solution provides the structural form adopted by the PVD deposition cavity, wherein the first distance refers to the distance between the metal target and the tray in the height direction, and the second distance refers to the rotating permanent magnet and the tray. The spacing distance of metal targets in the height direction; during production, the wafer is sent to the tray through the conveyor, and the corresponding process gas is supplied to the PVD deposition chamber by connecting the supply gas outlet with the pipeline, and the rotating permanent magnet generates high-speed charged particle magnetism. Controlled sputtering, by bombarding the metal target with high-speed charged particles, realizes the coating on the surface of the wafer.
在一个实施例中,所述托盘配置有调节基座,所述调节基座与控制器连接,所述调节基座在控制器的控制下能够改变托盘的水平度。In one embodiment, the tray is provided with an adjustment base, the adjustment base is connected with the controller, and the adjustment base can change the levelness of the tray under the control of the controller.
上述技术方案的工作原理和有益效果为:本方案通过给托盘配置有调节基座,用于调整托盘的水平度,改变了圆晶各点与金属靶材的间隔距离,从而引起圆晶各点沉积速率的差异,在圆晶表面各点形成不同的沉积速率,实现对沉积均匀性的补偿。The working principle and beneficial effects of the above technical solutions are as follows: in this solution, the tray is provided with an adjustment base to adjust the levelness of the tray, and the distance between each point of the wafer and the metal target is changed, thereby causing various points of the wafer to be separated. The difference in deposition rate results in different deposition rates at each point on the wafer surface, realizing compensation for deposition uniformity.
在一个实施例中,所述多个气体出口连接的不同管路都设有流量调节阀,所述流量调节阀与控制器连接,所述流量调节阀在控制器的控制下能够改变对应气体出口管路的气体流量。In one embodiment, different pipelines connected to the multiple gas outlets are provided with flow regulating valves, the flow regulating valves are connected to the controller, and the flow regulating valves can change the corresponding gas outlets under the control of the controller Gas flow in the pipeline.
上述技术方案的工作原理和有益效果为:本方案通过给气体出口连接不同管路,调节不同管路设置的流量调节阀,改变对应气体出口管路的气体流量,从而引起圆晶各点沉积速率的差异,在圆晶表面各点形成不同的沉积速率,实现对沉积均匀性的补偿。The working principle and beneficial effects of the above technical solution are as follows: this solution connects different pipelines to the gas outlet, adjusts the flow control valves set in the different pipelines, and changes the gas flow rate of the corresponding gas outlet pipeline, thereby causing the deposition rate of each point of the wafer. Different deposition rates are formed at each point on the wafer surface to achieve compensation for deposition uniformity.
在一个实施例中,所述金属靶材设有高度调节器,所述高度调节器与控制器连接,所述高度调节器在控制器的控制下能够改变金属靶材与托盘间隔的第一距离,旋转永磁体与金属靶材的第二距离也发生变化。In one embodiment, the metal target is provided with a height adjuster, the height adjuster is connected to the controller, and the height adjuster can change the first distance between the metal target and the tray under the control of the controller , the second distance between the rotating permanent magnet and the metal target also changes.
上述技术方案的工作原理和有益效果为:本方案通过给金属靶材设高度调节器,用于调整金属靶材与托盘间隔的第一距离,旋转永磁体与金属靶材的第二距离也发生变化,从而影响高速荷能粒子对金属靶材的轰击,引起圆晶各点沉积速率的差异,在圆晶表面各点形成不同的沉积速率,实现对沉积均匀性的补偿。The working principle and beneficial effects of the above technical solutions are as follows: in this solution, a height adjuster is provided for the metal target to adjust the first distance between the metal target and the tray, and the second distance between the rotating permanent magnet and the metal target also occurs. Changes, thereby affecting the bombardment of high-speed charged particles on the metal target, causing the difference in the deposition rate of each point of the wafer, forming different deposition rates at each point on the wafer surface, and realizing the compensation of deposition uniformity.
在一个实施例中,所述圆晶采用传送装置送至托盘,所述传送装置采用步进马达驱动,所述步进马达与控制器连接。In one embodiment, the wafers are delivered to the tray by a conveying device, and the conveying device is driven by a stepping motor, and the stepping motor is connected with the controller.
上述技术方案的工作原理和有益效果为:本方案采用传送装置将圆晶送至托盘,以步进马达驱动传送装置,改变步进马达的步进量,可以控制晶圆在托盘上的位置,可以造成局部沉积厚度不同,实现对沉积均匀性的补偿。The working principle and beneficial effects of the above technical solution are as follows: this solution adopts a conveying device to send the wafer to the tray, drives the conveying device with a stepping motor, changes the stepping amount of the stepping motor, and can control the position of the wafer on the tray, The local deposition thickness can be caused to be different, and the compensation for the deposition uniformity can be realized.
在一个实施例中,所述控制器包括主控芯片,所述主控芯片内置圆晶检测点模型,根据检测点的对应关系,将实时检测的各点厚度数据导入圆晶检测点模型,依据各点厚度绘制形成圆晶表面形貌图,然后根据圆晶表面形貌图确定各点局部沉积速率,在检测后继续进行的后步沉积进行沉积厚度的均匀度补偿。In one embodiment, the controller includes a main control chip, and the main control chip has a built-in wafer detection point model. According to the corresponding relationship of the detection points, the thickness data of each point detected in real time is imported into the wafer detection point model. The thickness of each point is drawn to form a topography map of the wafer surface, and then the local deposition rate of each point is determined according to the topography map of the wafer surface, and the subsequent deposition after detection is performed to compensate for the uniformity of the deposition thickness.
上述技术方案的工作原理和有益效果为:本方案将实时检测的各点厚度数据导入圆晶检测点模型,如图6所示,依据各点厚度绘制形成圆晶表面形貌图,图中各点标示有导入的检测厚度数据,检测点布置越密集,对圆晶表面的形貌描述会更细致,更能够精确反应沉积厚度分布情况,但检测点太多,各局部区域面积越小,检测及处理的数据量增加,影响检测的实时性和效率,因此宜选择适当数量的检测点进行布置;本方案通过绘制形成圆晶表面形貌图,例如采用不同颜色代表不同的沉积厚度,从而可以直观地了解圆晶表面平整情况,甚至可以引入类似地图海拔分析的图像方式进行沉积厚度均匀性评价,拓宽了评价手段与方式。The working principle and beneficial effects of the above technical solutions are as follows: In this solution, the real-time detected thickness data of each point is imported into the wafer detection point model, as shown in FIG. The points are marked with the imported inspection thickness data. The denser the inspection points are, the more detailed the topography of the wafer surface will be, and the more accurate the deposition thickness distribution will be. However, if there are too many inspection points, the smaller the area of each local area, the more And the increase in the amount of data processed will affect the real-time performance and efficiency of detection, so it is appropriate to select an appropriate number of detection points for layout; this scheme forms a wafer surface topography map by drawing, for example, using different colors to represent different deposition thicknesses, so that it can be Intuitively understand the flatness of the wafer surface, and even introduce an image method similar to map elevation analysis to evaluate the uniformity of deposition thickness, which broadens the evaluation methods and methods.
在一个实施例中,所述控制器采用以下公式计算后步沉积的各点局部沉积速率的调整值:In one embodiment, the controller uses the following formula to calculate the adjustment value of the local deposition rate at each point of the subsequent deposition:
上式中,V′i表示第i点局部沉积速率的调整值;D表示沉积层的总沉积厚度,设计值;di前表示检测得到的第i点前步沉积的沉积厚度;t前表示前步沉积的di前时长,若前步沉积有多个分步沉积,则t前为前步沉积所有分步沉积的总时长;t后表示后步沉积的时长,若后步沉积有多个分步沉积,则t后为后步沉积所有分步沉积的总时长;Vi表示前步沉积的第i点局部沉积速率,若前步沉积有多个分步沉积且各分步沉积采用的局部沉积速率不同,则Vi取各分步沉积采用的局部沉积速率的时长加权均值;In the above formula, V′ i represents the adjustment value of the local deposition rate at the ith point; D represents the total deposition thickness of the deposited layer, the design value; before d i represents the detected deposition thickness of the previous step at the ith point; before t represents The time before d i of the previous step deposition, if there are multiple step depositions in the previous step, then before t is the total time of all step depositions in the previous step; After t is the total time of all the step depositions of the subsequent step; Vi represents the local deposition rate of the i-th point of the previous step. If there are multiple step depositions in the previous step, and If the local deposition rates are different, V i takes the time-weighted average of the local deposition rates used for each step deposition;
根据计算结果,调整各点的局部沉积速率。According to the calculation results, adjust the local deposition rate of each point.
上述技术方案的工作原理和有益效果为:本方案的控制器采用上述计算公式计算后步沉积的各点局部沉积速率的调整值,实现了各点局部沉积速率的调整的量化精确计算与控制,形成各点的局部沉积速率的相对独立控制,从而对沉积均匀性进行补偿。The working principle and beneficial effects of the above technical scheme are as follows: the controller of this scheme uses the above calculation formula to calculate the adjustment value of the local deposition rate of each point deposited in the subsequent step, and realizes the quantitative and accurate calculation and control of the adjustment of the local deposition rate of each point, Relatively independent control of the local deposition rate at each point is created, compensating for deposition uniformity.
目前所有半导体溅射设备中都没有光学测试设备,本发明在光学薄膜沉积机台中,本身带有(光学)测试设备,本发明将光学测试功能与现有半导体工艺进行整合。At present, there is no optical testing equipment in all semiconductor sputtering equipment. The present invention has (optical) testing equipment in the optical thin film deposition machine. The present invention integrates the optical testing function with the existing semiconductor process.
当一片晶圆在沉积结束之后,在传送过程中,利用光学测试设备跟现有机台整合(分步沉积:例如原沉积菜单一次沉积所需沉积时间为60秒,分步沉积可以将沉积菜单60秒分为若干次,如分3次沉积,则每次沉积时间就为20秒。分步沉积在本发明中的必要性体现:由于一次沉积无法对最后成膜的表面均匀度进行补偿及修正,而分步进行可以使每次沉积根据光学测试的反馈结果进行表面均匀度的补偿及修正),对晶圆的表面进行厚度监控,即使用光学测试设备,针对已经部分薄膜(每个分步沉积后的薄膜)进行沉积后实时光学测量,光学测量包括表面反射率和折射率的采集。且可以由使用者定义测试点(检测点)于晶圆表面的分布,分布取点方式越细致(密集),则量测效果越细节化。通过反馈机制至沉积腔体,反馈机制详述为:进行薄膜表面形貌测试,一般为多点测试(检测),例如49点或者128点测试,测试点(检测点)位均匀分布于整个晶圆,测试后形成薄膜表面形貌图及均匀度——测试后薄膜表面形貌图传输至晶圆表面平整度修复机台——晶圆表面平整度修复机台依据形貌图对薄膜不同区域形貌进行平整度修复。After a wafer is deposited, during the transfer process, the optical testing equipment is used to integrate with the existing machine (step deposition: for example, the deposition time required for one deposition in the original deposition menu is 60 seconds, and the step deposition can make the deposition menu 60 seconds) The second is divided into several times, such as 3 times of deposition, then the deposition time is 20 seconds each time. The necessity of the step-by-step deposition in the present invention is reflected: because one deposition cannot compensate and correct the surface uniformity of the final film formation , and the step-by-step process enables each deposition to be compensated and corrected for the surface uniformity according to the feedback results of the optical test), and the thickness of the wafer surface is monitored, that is, using optical test equipment, for some thin films (each step post-deposition film) for post-deposition real-time optical measurements, including the acquisition of surface reflectance and refractive index. Moreover, the user can define the distribution of test points (detection points) on the wafer surface. The more detailed (intensive) point distribution method is, the more detailed the measurement effect will be. Through the feedback mechanism to the deposition chamber, the feedback mechanism is described in detail as follows: test the surface morphology of the film, generally a multi-point test (detection), such as a 49-point or 128-point test, the test points (detection points) are evenly distributed throughout the crystal. After the test, the film surface topography and uniformity are formed. After the test, the film surface topography is transmitted to the wafer surface flatness repair machine. The wafer surface flatness repair machine determines the different areas of the film according to the topography. The shape is repaired for flatness.
显然,本领域的技术人员可以对本发明进行各种改动和变型而不脱离本发明的精神和范围。这样,倘若本发明的这些修改和变型属于本发明权利要求及其等同技术的范围之内,则本发明也意图包含这些改动和变型在内。It will be apparent to those skilled in the art that various modifications and variations can be made in the present invention without departing from the spirit and scope of the invention. Thus, provided that these modifications and variations of the present invention fall within the scope of the claims of the present invention and their equivalents, the present invention is also intended to include these modifications and variations.
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