[go: up one dir, main page]

CN114000202B - Crystalline silicon solar cell variable temperature diffusion furnace - Google Patents

Crystalline silicon solar cell variable temperature diffusion furnace Download PDF

Info

Publication number
CN114000202B
CN114000202B CN202111165033.8A CN202111165033A CN114000202B CN 114000202 B CN114000202 B CN 114000202B CN 202111165033 A CN202111165033 A CN 202111165033A CN 114000202 B CN114000202 B CN 114000202B
Authority
CN
China
Prior art keywords
furnace
ring
furnace door
block
door
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202111165033.8A
Other languages
Chinese (zh)
Other versions
CN114000202A (en
Inventor
庄洋
魏秀平
王福强
张楠
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangsu Longheng New Energy Co ltd
Original Assignee
Jiangsu Longheng New Energy Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiangsu Longheng New Energy Co ltd filed Critical Jiangsu Longheng New Energy Co ltd
Priority to CN202111165033.8A priority Critical patent/CN114000202B/en
Publication of CN114000202A publication Critical patent/CN114000202A/en
Application granted granted Critical
Publication of CN114000202B publication Critical patent/CN114000202B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B31/00Diffusion or doping processes for single crystals or homogeneous polycrystalline material with defined structure; Apparatus therefor
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/02Elements
    • C30B29/06Silicon
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10FINORGANIC SEMICONDUCTOR DEVICES SENSITIVE TO INFRARED RADIATION, LIGHT, ELECTROMAGNETIC RADIATION OF SHORTER WAVELENGTH OR CORPUSCULAR RADIATION
    • H10F10/00Individual photovoltaic cells, e.g. solar cells
    • H10F10/10Individual photovoltaic cells, e.g. solar cells having potential barriers
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10FINORGANIC SEMICONDUCTOR DEVICES SENSITIVE TO INFRARED RADIATION, LIGHT, ELECTROMAGNETIC RADIATION OF SHORTER WAVELENGTH OR CORPUSCULAR RADIATION
    • H10F71/00Manufacture or treatment of devices covered by this subclass
    • H10F71/137Batch treatment of the devices
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E10/00Energy generation through renewable energy sources
    • Y02E10/50Photovoltaic [PV] energy
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50Manufacturing or production processes characterised by the final manufactured product

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Furnace Details (AREA)
  • Furnace Housings, Linings, Walls, And Ceilings (AREA)

Abstract

The invention discloses a variable-temperature diffusion furnace for a crystalline silicon solar cell, and relates to the technical field of diffusion furnaces. The invention discloses a crystalline silicon solar cell variable-temperature diffusion furnace, which comprises a furnace body, wherein a furnace mouth is formed in the furnace body, a furnace door for closing the furnace mouth is hinged to the furnace body on one side of the furnace mouth, the furnace mouth is arranged in a circular shape, a sealing piece, an auxiliary isolating piece and a locking piece are arranged on the furnace door, the sealing piece comprises a fixed ring formed on the furnace door, the outer side of the fixed ring is connected with a sealing ring with the same shape as the furnace mouth in a sliding manner, and the sealing ring is used for being in sliding connection outside the furnace mouth and sealing the furnace mouth when the furnace door is closed.

Description

晶硅太阳能电池变温扩散炉Crystalline silicon solar cell variable temperature diffusion furnace

技术领域technical field

本发明涉及及扩散炉技术领域,特别是涉及一种晶硅太阳能电池变温扩散炉。The invention relates to the technical field of diffusion furnaces, in particular to a temperature-variable diffusion furnace for crystalline silicon solar cells.

背景技术Background technique

扩散炉是半导体生产线前工序的重要工艺设备之一,用于大规模集成电路、分立器件、电力电子、光电器件和光导纤维等行业的扩散、氧化、退火、合金及烧结等工艺。它的主要用途是对半导体进行掺杂,即在高温条件下将掺杂材料扩散入硅片,从而改变和控制半导体内杂质的类型、浓度和分布,以便建立起不同的电特性区域。Diffusion furnace is one of the important process equipment in the pre-process of semiconductor production line. It is used for diffusion, oxidation, annealing, alloying and sintering in industries such as large-scale integrated circuits, discrete devices, power electronics, optoelectronic devices and optical fibers. Its main purpose is to dope semiconductors, that is, to diffuse dopant materials into silicon wafers under high temperature conditions, so as to change and control the type, concentration and distribution of impurities in semiconductors, so as to establish regions with different electrical characteristics.

虽然某些工艺可以使用离子注入的方法进行掺杂,但是热扩散仍是最主要、最普遍的掺杂方法。硅的热氧化作用是使硅片表面在高温下与氧化剂发生反应,生长一层二氧化硅膜。氧化方法有干氧氧化和水汽氧化(含氢氧合成)两种,扩散炉是用这两种氧化方法制备氧化层的必备设备。扩散炉是半导体集成电路工艺的基础设备,它与半导体工艺互相依存、互相促进、共同发展。Although some processes can be doped by ion implantation, thermal diffusion is still the most important and common doping method. The thermal oxidation of silicon is to make the surface of silicon wafer react with oxidant at high temperature to grow a layer of silicon dioxide film. Oxidation methods include dry oxygen oxidation and water vapor oxidation (hydrogen-oxygen synthesis), and the diffusion furnace is an essential equipment for preparing oxide layers with these two oxidation methods. Diffusion furnace is the basic equipment of semiconductor integrated circuit technology, which is interdependent, mutually promoted and developed together with semiconductor technology.

扩散炉有垂直扩散炉和水平扩散炉两种类型。垂直扩散炉是石英舟垂直于水平面,更加有利于机械手传送硅片,片内工艺参数一致性更好。水平扩散炉是石英舟平行于水平面,一台可以4个或4个以上的工艺炉管,平均炉管的占地面积更小,片间的工艺参数较垂直扩散炉更好。There are two types of diffusion furnaces: vertical diffusion furnace and horizontal diffusion furnace. In the vertical diffusion furnace, the quartz boat is perpendicular to the horizontal plane, which is more conducive to the transfer of silicon wafers by the manipulator, and the consistency of the process parameters within the wafer is better. The horizontal diffusion furnace is a quartz boat parallel to the horizontal plane. One can have 4 or more process furnace tubes. The average area of the furnace tube is smaller, and the process parameters between the plates are better than the vertical diffusion furnace.

目前,公开号为CN107604444A的中国专利公开了一种硅片加热扩散炉,包括炉体和设置于炉体内的多根炉管,炉体上设有控制柜,炉管相互间隔的横向装设于炉体内,且炉管的两端设为炉口和炉尾,且炉口和炉尾于炉体上设有炉门。炉管的炉口、炉尾和炉管的中部分别设有加热元件,炉管内设有石英层,且炉管的炉口和炉尾的外表面分别套设有石棉垫和石棉圈,控制柜实时监控和控制炉体内的温度。At present, the Chinese patent with the publication number CN107604444A discloses a silicon wafer heating diffusion furnace, which includes a furnace body and a plurality of furnace tubes arranged in the furnace body. In the furnace body, the two ends of the furnace tube are set as a furnace mouth and a furnace tail, and the furnace mouth and the furnace tail are provided with a furnace door on the furnace body. The furnace mouth, the furnace tail and the middle part of the furnace tube are respectively provided with heating elements, the furnace pipe is provided with a quartz layer, and the outer surfaces of the furnace mouth and the furnace tail of the furnace pipe are respectively covered with asbestos pads and asbestos rings, and the control cabinet Real-time monitoring and control of the temperature in the furnace body.

这种硅片加热扩散炉虽然可达到对炉口和炉尾保温的作用,防止其散热导致炉口,但这种扩散炉在使用时,其炉口由于炉门的存在,封闭不够良好,在生产过程中容易造成热量的逸散,同时由于高温条件,硅片容易产生有害气体,并从炉门位置泄露,从而对操作人员的身体健康造成一定损伤。Although this silicon wafer heating diffusion furnace can achieve the effect of heat preservation on the furnace mouth and the furnace tail, preventing its heat dissipation from causing the furnace mouth, but when this diffusion furnace is in use, the furnace mouth is not closed well enough due to the existence of the furnace door. It is easy to cause heat dissipation during the production process. At the same time, due to high temperature conditions, silicon wafers are prone to generate harmful gases and leak from the furnace door, which will cause certain damage to the health of operators.

发明内容Contents of the invention

本发明针对上述技术问题,克服现有技术的缺点,提供一种晶硅太阳能电池变温扩散炉。The present invention aims at the above technical problems, overcomes the shortcomings of the prior art, and provides a temperature-variable diffusion furnace for crystalline silicon solar cells.

为了解决以上技术问题,本发明提供一种晶硅太阳能电池变温扩散炉。In order to solve the above technical problems, the present invention provides a variable temperature diffusion furnace for crystalline silicon solar cells.

技术效果:能够在关闭扩散炉的炉门时,通过联动件带动封闭机构同步对其炉口进行封闭,一方面增加对炉口封闭时的隔热性,避免发生热量逸散,保证炉体内温度快速增长并维持平衡,另一方面能够提升炉口位置的气密性,从而防止炉体内经过高温后硅片或其他元件产生的有害气体泄露,以保证操作人员的身体健康。Technical effect: When closing the furnace door of the diffusion furnace, the closing mechanism can be driven by the linkage to simultaneously seal the furnace mouth. On the one hand, it increases the heat insulation when the furnace mouth is closed, avoids heat dissipation, and ensures the temperature in the furnace body. Rapid growth and maintenance of balance, on the other hand, can improve the airtightness of the furnace mouth, so as to prevent the leakage of harmful gases generated by silicon wafers or other components after high temperature in the furnace, so as to ensure the health of operators.

本发明进一步限定的技术方案是:一种晶硅太阳能电池变温扩散炉,包括炉体,炉体上开设有炉口,炉口一侧的炉体上铰接设有用于封闭炉口的炉门,炉口呈圆形状设置,炉门上设有The technical solution further defined in the present invention is: a temperature-variable diffusion furnace for crystalline silicon solar cells, including a furnace body, a furnace mouth is opened on the furnace body, and a furnace door for closing the furnace mouth is hinged on the furnace body on one side of the furnace mouth. The furnace mouth is set in a circular shape, and the furnace door is provided with

封闭件,包括形成于炉门上的固定环,固定环外滑移连接有形状与炉口相同的封闭环,用于在炉门封闭时滑移卡接在炉口外并封闭炉口,炉口上设有形状与固定环匹配的连接环,炉门封闭时固定环嵌设于连接环内,且封闭环套设于连接环外;The closure includes a fixed ring formed on the furnace door, and a closed ring with the same shape as the furnace mouth is slidably connected to the outside of the fixed ring, which is used to slide and clamp outside the furnace mouth and close the furnace mouth when the furnace door is closed. There is a connecting ring whose shape matches the fixing ring. When the furnace door is closed, the fixing ring is embedded in the connecting ring, and the closing ring is sleeved outside the connecting ring;

辅助隔离件,包括两块关于固定环对称设置并滑移连接在炉门上的隔离块,隔离块呈半环形设置,其形状与封闭环贴合,炉门上设有联动件,包括转轮,用于通过旋转的方式带动两块隔离块相对或相背方向滑移,以辅助隔离或放开封闭环;Auxiliary spacer, including two spacers arranged symmetrically with respect to the fixed ring and slidingly connected to the furnace door. The spacer is arranged in a semi-circular shape, and its shape fits the closed ring. There is a linkage on the furnace door, including the runner , which is used to drive the two isolation blocks to slide in opposite or opposite directions by rotating, so as to assist in isolating or releasing the closed ring;

锁紧件,包括固定在炉体上的嵌槽以及滑移连接在炉门上的连接块,连接块通过连动杆与联动件连接,转轮旋转时通过连动杆带动连接块嵌设于嵌槽内或拉出嵌槽,以实现炉门的锁紧。The locking piece includes a slot fixed on the furnace body and a connecting block slidingly connected to the furnace door. The connecting block is connected to the connecting piece through a linkage rod. When the runner rotates, the linkage rod drives the connection block to be embedded in the Insert or pull out the caulking groove to realize the locking of the furnace door.

进一步的,炉体上设有用于容纳炉门的容纳槽,炉口位于容纳槽中间位置,封闭件包括活动杆,活动杆中间位置铰接在炉门上,活动杆一端铰接在封闭环侧面,另一端与炉门之间通过固定弹簧连接,容纳槽内对应活动杆末端设有压块。Further, the furnace body is provided with an accommodating groove for accommodating the furnace door, the furnace mouth is located in the middle of the accommodating groove, the closure includes a movable rod, the middle position of the movable rod is hinged on the furnace door, one end of the movable rod is hinged on the side of the closed ring, and the other One end is connected to the furnace door through a fixed spring, and a pressure block is provided at the end of the corresponding movable rod in the receiving tank.

前所述的晶硅太阳能电池变温扩散炉,固定环底部设有限位凸环,封闭环末端形成有内凸环,内凸环在炉门与限位凸环之间滑移,炉门封闭时内凸环顶面与限位凸环相互贴合,封闭环整体由钢化玻璃材料制成,其包括两层,中间位置设置真空隔热层。In the variable temperature diffusion furnace for crystalline silicon solar cells mentioned above, the bottom of the fixed ring is provided with a limiting convex ring, and the end of the closed ring is formed with an inner convex ring. The inner convex ring slides between the furnace door and the limiting convex ring. When the furnace door is closed, The top surface of the inner convex ring and the limit convex ring are attached to each other, and the closed ring is made of toughened glass material as a whole, which includes two layers, and a vacuum heat insulation layer is arranged in the middle.

前所述的晶硅太阳能电池变温扩散炉,嵌槽设于容纳槽内侧面顶部和底部位置,炉门上滑移连接有活动块,活动块与连接块之间通过连动杆固定,炉门内设有主动齿轮,活动块一侧设有与主动齿轮相互啮合的活动齿条,用于驱动活动块和连动杆滑移。In the temperature-variable diffusion furnace for crystalline silicon solar cells mentioned above, the embedded grooves are arranged at the top and bottom of the inner side of the containing tank, and the furnace door is slidably connected with a movable block, and the movable block and the connecting block are fixed by a linkage rod, and the furnace door A drive gear is provided inside, and a movable rack intermeshing with the drive gear is provided on one side of the movable block for driving the movable block and the linkage rod to slide.

前所述的晶硅太阳能电池变温扩散炉,转轮通过转轴转动连接在炉门上,转轴穿透炉门设置,主动齿轮同轴心固定在转轴上,辅助隔离件包括驱动块,驱动块滑移连接在炉门上,驱动块末端通过驱动杆与隔离块固定。In the above-mentioned variable temperature diffusion furnace for crystalline silicon solar cells, the runner is connected to the furnace door through the rotating shaft, and the rotating shaft penetrates through the furnace door to set, and the driving gear is fixed on the rotating shaft with the coaxial center. The shifter is connected to the furnace door, and the end of the drive block is fixed with the isolation block through the drive rod.

前所述的晶硅太阳能电池变温扩散炉,驱动块上一体形成有驱动齿条,驱动齿条与主动齿轮相互啮合,用于带动驱动块滑移,驱动齿条与活动齿条相互错位,驱动块位于主动齿轮上下两侧,活动块位于主动齿轮的左右两侧。In the variable temperature diffusion furnace for crystalline silicon solar cells mentioned above, a driving rack is integrally formed on the driving block, and the driving rack and the driving gear mesh with each other to drive the sliding of the driving block, and the driving rack and the movable rack are misaligned to drive The block is positioned at the upper and lower sides of the driving gear, and the movable block is positioned at the left and right sides of the driving gear.

前所述的晶硅太阳能电池变温扩散炉,隔离块内设有贴合在封闭环上的石棉垫,炉门包括内层和外层,内层与外层之间真空设置,炉门和炉体的对应设有钢化玻璃形成的视窗,用于观测炉体内工作情况。In the above-mentioned variable temperature diffusion furnace for crystalline silicon solar cells, an asbestos pad attached to the closed ring is arranged in the isolation block, the furnace door includes an inner layer and an outer layer, and a vacuum is set between the inner layer and the outer layer. Corresponding to the body, there is a window formed by tempered glass, which is used to observe the working conditions in the furnace body.

本发明的有益效果是:The beneficial effects of the present invention are:

(1)本发明中,在关闭炉门时,操作人员先将炉门闭合至容纳槽,此时固定环与连接环配合,固定环嵌设于连接环内,继续封闭炉门,通过两侧的压块将活动杆末端向外顶出,由于活动杆中间铰接在炉门上,活动杆另一端能够带动封闭环在固定环上滑移,从而使封闭环套设在连接环外形成封闭,由于封闭环中间真空设置,能够提升整个炉门的封闭性能,而辅助隔离件能够在炉门关闭时,在封闭环外实现两块隔离块的合并,从而将整个封闭环包容在内,进一步提升炉门的隔热性能和气密性,最后配合锁紧件,能够将整个炉门锁紧在容纳槽内,从而实现炉门的牢固封闭;(1) In the present invention, when closing the furnace door, the operator first closes the furnace door to the receiving groove. At this time, the fixing ring cooperates with the connecting ring, and the fixing ring is embedded in the connecting ring, and continues to close the furnace door. The pressing block pushes the end of the movable rod outward. Since the middle of the movable rod is hinged on the furnace door, the other end of the movable rod can drive the closed ring to slide on the fixed ring, so that the closed ring is sleeved outside the connecting ring to form a seal. Due to the vacuum setting in the middle of the closed ring, the sealing performance of the entire furnace door can be improved, and the auxiliary spacer can realize the merging of two spacers outside the closed ring when the furnace door is closed, so as to contain the entire closed ring and further improve The heat insulation performance and air tightness of the furnace door, and finally with the locking piece, can lock the entire furnace door in the containing groove, so as to realize the firm closure of the furnace door;

(2)本发明中,固定环底部设置限位凸环,而封闭环末端形成内凸环,因此在封闭环卡设在连接环外时,内凸环顶面能够抵接在封闭凸环上,从而提升整体的密封性,钢化玻璃材料制成的封闭环具有良好的气密性,而真空隔热层的设置也能够使整个密封环具有良好的保温性能,从而保证整个炉口的温度不发生逸散,同时炉体内气体不易发生泄露;(2) In the present invention, a limiting convex ring is provided at the bottom of the fixed ring, and an inner convex ring is formed at the end of the closed ring, so when the closed ring is clamped outside the connecting ring, the top surface of the inner convex ring can abut against the closed convex ring , so as to improve the overall airtightness, the closed ring made of tempered glass material has good airtightness, and the setting of the vacuum insulation layer can also make the whole sealing ring have good heat preservation performance, so as to ensure that the temperature of the entire furnace mouth is not high. Dissipation occurs, and the gas in the furnace is not easy to leak;

(3)本发明中,在炉门封闭后,操作人员可以通过旋转转轮,带动内部的主动齿轮旋转,由于主动齿轮左右两侧与活动齿条啮合,能够带动活动齿条上下滑移,从而联动活动块和连动杆,驱使连动杆末端的连接块滑移,使连接块嵌设在嵌槽内或从嵌槽中拉出,达到锁紧整个炉门的效果,同样的,通过主动齿轮能够带动齿轮上下侧的驱动齿条滑移,实现对隔离块的拉动;(3) In the present invention, after the furnace door is closed, the operator can drive the internal driving gear to rotate by rotating the runner. Since the left and right sides of the driving gear mesh with the movable rack, the movable rack can be driven to slide up and down, thereby Link the movable block and the connecting rod to drive the connecting block at the end of the connecting rod to slide, so that the connecting block is embedded in the slot or pulled out from the slot to achieve the effect of locking the entire furnace door. Similarly, through the active The gear can drive the driving rack on the upper and lower sides of the gear to slide, so as to realize the pulling of the isolation block;

(4)本发明中,驱动齿条能够带动两个隔离块相互贴合或相互分离,在需要时能够完成对封闭环外的贴紧,而操作人员只需要转动转轮就能够实现对炉门的锁紧和对隔离块的驱动,整体较为方便,另外隔离块内设有贴合在封闭环上的石棉垫,能够对封闭环进行隔热和气密性能的辅助提升,达到更好的封闭效果;(4) In the present invention, the drive rack can drive the two isolation blocks to fit or separate from each other, and when necessary, the tight fit to the outside of the closed ring can be completed, and the operator only needs to turn the runner to realize the alignment of the furnace door. The locking of the isolation block and the driving of the isolation block are more convenient overall. In addition, there is an asbestos pad attached to the closed ring in the isolation block, which can assist in improving the heat insulation and airtight performance of the closed ring to achieve a better sealing effect. ;

(5)本发明中,能够在关闭扩散炉的炉门时,通过联动件带动封闭机构同步对其炉口进行封闭,一方面增加对炉口封闭时的隔热性,避免发生热量逸散,保证炉体内温度快速增长并维持平衡,另一方面能够提升炉口位置的气密性,从而防止炉体内经过高温后硅片或其他元件产生的有害气体泄露,以保证操作人员的身体健康。(5) In the present invention, when the furnace door of the diffusion furnace is closed, the closing mechanism is driven by the linkage to simultaneously seal the furnace mouth, on the one hand, the heat insulation when the furnace mouth is closed is increased, and heat dissipation is avoided. Ensure the temperature in the furnace increases rapidly and maintain balance. On the other hand, it can improve the airtightness of the furnace mouth, thereby preventing the leakage of harmful gases generated by silicon wafers or other components after high temperature in the furnace, so as to ensure the health of operators.

附图说明Description of drawings

图1为实施例1的结构图;Fig. 1 is the structural diagram of embodiment 1;

图2为实施例1的连接示意图;Fig. 2 is the connection schematic diagram of embodiment 1;

图3为实施例1中封闭环与固定环的结构图;Fig. 3 is the structural diagram of closed ring and fixed ring in embodiment 1;

图4为实施例1中封闭环的连接示意图;Fig. 4 is the connection schematic diagram of closed loop in embodiment 1;

图5为实施例1中辅助隔离件的结构图。FIG. 5 is a structural diagram of the auxiliary spacer in Embodiment 1. FIG.

其中:1、炉体;11、炉口;12、炉门;121、内层;122、外层;123、视窗;13、容纳槽;2、封闭件;21、固定环;211、限位凸环;22、封闭环;221、内凸环;23、连接环;24、活动杆;25、压块;3、辅助隔离件;31、隔离块;311、石棉垫;32、驱动块;33、驱动杆;34、驱动齿条;4、锁紧件;41、嵌槽;42、连接块;43、活动块;44、连动杆;45、活动齿条;5、联动件;51、转轮;52、转轴;53、主动齿轮。Among them: 1. Furnace body; 11. Furnace mouth; 12. Furnace door; 121. Inner layer; 122. Outer layer; 123. Viewing window; 13. Accommodating groove; Convex ring; 22, closed ring; 221, inner convex ring; 23, connecting ring; 24, movable rod; 25, pressure block; 3, auxiliary isolation piece; 31, isolation block; 33. Drive rod; 34. Drive rack; 4. Locking piece; 41. Insert groove; 42. Connecting block; 43. Movable block; 44. Linkage rod; 45. Movable rack; 5. Linkage piece; 51 , runner; 52, rotating shaft; 53, driving gear.

具体实施方式Detailed ways

本实施例提供的一种晶硅太阳能电池变温扩散炉,结构如图1-3所示,包括炉体1,炉体1上开设有炉口11,炉口11一侧的炉体1上铰接设有用于封闭炉口11的炉门12,炉口11呈圆形状设置,炉门12上设有封闭件2、辅助隔离件3和锁紧件4。A temperature-variable diffusion furnace for crystalline silicon solar cells provided in this embodiment has a structure as shown in Figure 1-3, including a furnace body 1, a furnace mouth 11 is opened on the furnace body 1, and the furnace body 1 on the side of the furnace mouth 11 is hinged A furnace door 12 for closing the furnace mouth 11 is provided, the furnace mouth 11 is arranged in a circular shape, and the furnace door 12 is provided with a closing part 2 , an auxiliary insulating part 3 and a locking part 4 .

如图2-4所示,封闭件2,包括形成于炉门12上的固定环21,固定环21外滑移连接有形状与炉口11相同的封闭环22,用于在炉门12封闭时滑移卡接在炉口11外并封闭炉口11,炉口11上设有形状与固定环21匹配的连接环23,炉门12封闭时固定环21嵌设于连接环23内,且封闭环22套设于连接环23外。As shown in Figures 2-4, the closure 2 includes a fixed ring 21 formed on the furnace door 12, and a closed ring 22 with the same shape as the furnace mouth 11 is slidably connected to the outside of the fixed ring 21 for closing the furnace door 12. When the furnace door 12 is closed, the fixed ring 21 is embedded in the connecting ring 23, and The closed ring 22 is sheathed outside the connecting ring 23 .

如图3-5所示,炉体1上设有用于容纳炉门12的容纳槽13,炉口11位于容纳槽13中间位置,封闭件2包括活动杆24,活动杆24中间位置铰接在炉门12上,活动杆24一端铰接在封闭环22侧面,另一端与炉门12之间通过固定弹簧连接,容纳槽13内对应活动杆24末端设有压块25。As shown in Fig. 3-5, the furnace body 1 is provided with an accommodation groove 13 for accommodating the furnace door 12, the furnace mouth 11 is located in the middle of the accommodation groove 13, and the closure 2 includes a movable rod 24, which is hinged at the middle position of the furnace. On the door 12, one end of the movable rod 24 is hinged on the side of the closed ring 22, and the other end is connected to the furnace door 12 by a fixed spring.

如图3-5所示,固定环21底部设有限位凸环211,封闭环22末端形成有内凸环221,内凸环221在炉门12与限位凸环211之间滑移,炉门12封闭时内凸环221顶面与限位凸环211相互贴合,封闭环22整体由钢化玻璃材料制成,其包括两层,中间位置设置真空隔热层。隔离块31内设有贴合在封闭环22上的石棉垫311,炉门12包括内层121和外层122,内层121与外层122之间真空设置,炉门12和炉体1的对应设有钢化玻璃形成的视窗123,用于观测炉体1内工作情况。As shown in Figure 3-5, the bottom of the fixed ring 21 is provided with a limiting convex ring 211, the end of the closed ring 22 is formed with an inner convex ring 221, and the inner convex ring 221 slides between the furnace door 12 and the limiting convex ring 211. When the door 12 is closed, the top surface of the inner convex ring 221 and the limiting convex ring 211 are attached to each other, and the closed ring 22 is made of toughened glass material as a whole, which includes two layers, and a vacuum insulation layer is arranged in the middle. The spacer 31 is provided with an asbestos mat 311 attached to the closed ring 22. The furnace door 12 includes an inner layer 121 and an outer layer 122. A vacuum is set between the inner layer 121 and the outer layer 122. The furnace door 12 and the furnace body 1 Correspondingly, a window 123 formed of toughened glass is provided for observing the working conditions in the furnace body 1 .

如图3-5所示,辅助隔离件3包括两块关于固定环21对称设置并滑移连接在炉门12上的隔离块31,隔离块31呈半环形设置,其形状与封闭环22贴合,炉门12上设有联动件5,包括转轮51,用于通过旋转的方式带动两块隔离块31相对或相背方向滑移,以辅助隔离或放开封闭环22。As shown in Figures 3-5, the auxiliary spacer 3 includes two spacers 31 that are arranged symmetrically with respect to the fixed ring 21 and are slidably connected to the furnace door 12. Closed, the furnace door 12 is provided with a linkage 5, including a runner 51, which is used to drive the two isolation blocks 31 to slide in opposite or opposite directions through rotation, so as to assist in isolating or releasing the closed ring 22.

如图3-5所示,还设有锁紧件4,包括固定在炉体1上的嵌槽41以及滑移连接在炉门12上的连接块42,连接块42通过连动杆44与联动件5连接,转轮51旋转时通过连动杆44带动连接块42嵌设于嵌槽41内或拉出嵌槽41,以实现炉门12的锁紧。As shown in Figures 3-5, a locking piece 4 is also provided, including a slot 41 fixed on the furnace body 1 and a connecting block 42 slidably connected to the furnace door 12. The connecting block 42 connects with the connecting rod 44 The linkage 5 is connected, and when the runner 51 rotates, the linkage rod 44 drives the connection block 42 to be embedded in the insertion groove 41 or pulled out of the insertion groove 41 to realize the locking of the furnace door 12 .

如图3-5所示,嵌槽41设于容纳槽13内侧面顶部和底部位置,炉门12上滑移连接有活动块43,活动块43与连接块42之间通过连动杆44固定,炉门12内设有主动齿轮53,活动块43一侧设有与主动齿轮53相互啮合的活动齿条45,用于驱动活动块43和连动杆44滑移。转轮51通过转轴52转动连接在炉门12上,转轴52穿透炉门12设置,主动齿轮53同轴心固定在转轴52上,辅助隔离件3包括驱动块32,驱动块32滑移连接在炉门12上,驱动块32末端通过驱动杆33与隔离块31固定。As shown in Figure 3-5, the embedded groove 41 is located at the top and bottom of the inner surface of the receiving groove 13, and the movable block 43 is slidably connected to the furnace door 12, and the movable block 43 and the connecting block 42 are fixed by a linkage rod 44 , The furnace door 12 is provided with a drive gear 53, and one side of the movable block 43 is provided with a movable rack 45 meshing with the drive gear 53 for driving the movable block 43 and the linkage rod 44 to slide. The rotating wheel 51 is rotatably connected to the furnace door 12 through the rotating shaft 52, the rotating shaft 52 is set through the furnace door 12, the driving gear 53 is coaxially fixed on the rotating shaft 52, the auxiliary spacer 3 includes a driving block 32, and the driving block 32 is slidably connected On the furnace door 12 , the end of the driving block 32 is fixed to the isolation block 31 through the driving rod 33 .

如图3-5所示,驱动块32上一体形成有驱动齿条34,驱动齿条34与主动齿轮53相互啮合,用于带动驱动块32滑移,驱动齿条34与活动齿条45相互错位,驱动块32位于主动齿轮53上下两侧,活动块43位于主动齿轮53的左右两侧。As shown in Figures 3-5, a driving rack 34 is integrally formed on the driving block 32, and the driving rack 34 meshes with the driving gear 53 to drive the driving block 32 to slide, and the driving rack 34 and the movable rack 45 interact with each other. Misaligned, the driving block 32 is located at the upper and lower sides of the driving gear 53 , and the movable block 43 is located at the left and right sides of the driving gear 53 .

在关闭炉门12时,操作人员先将炉门12闭合至容纳槽13,此时固定环21与连接环23配合,固定环21嵌设于连接环23内,继续封闭炉门12,通过两侧的压块25将活动杆24末端向外顶出,由于活动杆24中间铰接在炉门12上,活动杆24另一端能够带动封闭环22在固定环21上滑移,从而使封闭环22套设在连接环23外形成封闭,由于封闭环22中间真空设置,能够提升整个炉门12的封闭性能,而辅助隔离件3能够在炉门12关闭时,在封闭环22外实现两块隔离块31的合并,从而将整个封闭环22包容在内,进一步提升炉门12的隔热性能和气密性,最后配合锁紧件4,能够将整个炉门12锁紧在容纳槽13内,从而实现炉门12的牢固封闭。When closing the furnace door 12, the operator first closes the furnace door 12 to the receiving groove 13. At this time, the fixing ring 21 cooperates with the connecting ring 23, and the fixing ring 21 is embedded in the connecting ring 23, and continues to close the furnace door 12. The briquetting block 25 on the side pushes the end of the movable rod 24 outward. Since the middle of the movable rod 24 is hinged on the furnace door 12, the other end of the movable rod 24 can drive the closed ring 22 to slide on the fixed ring 21, so that the closed ring 22 It is sleeved outside the connection ring 23 to form a seal. Due to the vacuum setting in the middle of the seal ring 22, the sealing performance of the entire furnace door 12 can be improved, and the auxiliary spacer 3 can realize two pieces of isolation outside the seal ring 22 when the furnace door 12 is closed. Blocks 31 are merged to contain the entire closed ring 22, further improving the heat insulation performance and airtightness of the furnace door 12, and finally with the locking piece 4, the entire furnace door 12 can be locked in the receiving groove 13, thereby A firm closure of the furnace door 12 is achieved.

本发明能够在关闭扩散炉的炉门12时,通过联动件5带动封闭机构同步对其炉口11进行封闭,一方面增加对炉口11封闭时的隔热性,避免发生热量逸散,保证炉体1内温度快速增长并维持平衡,另一方面能够提升炉口11位置的气密性,从而防止炉体1内经过高温后硅片或其他元件产生的有害气体泄露,以保证操作人员的身体健康。The present invention can drive the closing mechanism through the linkage 5 to simultaneously seal the furnace mouth 11 when closing the furnace door 12 of the diffusion furnace. The temperature in the furnace body 1 increases rapidly and maintains a balance. On the other hand, it can improve the airtightness of the furnace mouth 11, thereby preventing the leakage of harmful gases generated by silicon wafers or other components after high temperature in the furnace body 1, so as to ensure the safety of operators. In good health.

除上述实施例外,本发明还可以有其他实施方式。凡采用等同替换或等效变换形成的技术方案,均落在本发明要求的保护范围。In addition to the above-mentioned embodiments, the present invention can also have other implementations. All technical solutions formed by equivalent replacement or equivalent transformation fall within the scope of protection required by the present invention.

Claims (3)

1.一种晶硅太阳能电池变温扩散炉,包括炉体(1),炉体(1)上开设有炉口(11),炉口(11)一侧的炉体(1)上铰接设有用于封闭炉口(11)的炉门(12),其特征在于:所述炉口(11)呈圆形状设置,炉门(12)上设有1. A variable temperature diffusion furnace for crystalline silicon solar cells, comprising a body of furnace (1), the body of furnace (1) is provided with a furnace mouth (11), and the body of furnace (1) on the side of the furnace mouth (11) is hingedly provided with a furnace body (1). The furnace door (12) for closing the furnace mouth (11) is characterized in that: the furnace mouth (11) is arranged in a circular shape, and the furnace door (12) is provided with 封闭件(2),包括形成于炉门(12)上的固定环(21),固定环(21)外滑移连接有形状与炉口(11)相同的封闭环(22),用于在炉门(12)封闭时滑移卡接在炉口(11)外并封闭炉口(11),炉口(11)上设有形状与固定环(21)匹配的连接环(23),炉门(12)封闭时固定环(21)嵌设于连接环(23)内,且封闭环(22)套设于连接环(23)外;The closure (2) comprises a fixed ring (21) formed on the furnace door (12), and a closed ring (22) with the same shape as the furnace mouth (11) is slidably connected to the outside of the fixed ring (21). When the furnace door (12) is closed, it slides and clamps outside the furnace mouth (11) and closes the furnace mouth (11). The furnace mouth (11) is provided with a connecting ring (23) whose shape matches the fixed ring (21). When the door (12) is closed, the fixed ring (21) is embedded in the connecting ring (23), and the closed ring (22) is sleeved outside the connecting ring (23); 辅助隔离件(3),包括两块关于固定环(21)对称设置并滑移连接在炉门(12)上的隔离块(31),隔离块(31)呈半环形设置,其形状与封闭环(22)贴合,炉门(12)上设有联动件(5),包括转轮(51),用于通过旋转的方式带动两块隔离块(31)相对或相背方向滑移,以辅助隔离或放开封闭环(22);The auxiliary spacer (3) includes two spacers (31) that are arranged symmetrically about the fixed ring (21) and are slidably connected to the furnace door (12). The ring (22) fits together, and the furnace door (12) is provided with a linkage (5), including a runner (51), which is used to drive the two spacers (31) to slide in opposite or opposite directions through rotation. To assist in isolating or releasing the closed loop (22); 锁紧件(4),包括固定在炉体(1)上的嵌槽(41)以及滑移连接在炉门(12)上的连接块(42),连接块(42)通过连动杆(44)与联动件(5)连接,转轮(51)旋转时通过连动杆(44)带动连接块(42)嵌设于嵌槽(41)内或拉出嵌槽(41),以实现炉门(12)的锁紧,所述固定环(21)底部设有限位凸环(211),封闭环(22)末端形成有内凸环(221),内凸环(221)在炉门(12)与限位凸环(211)之间滑移,炉门(12)封闭时内凸环(221)顶面与限位凸环(211)相互贴合,封闭环(22)整体由钢化玻璃材料制成,其包括两层,中间位置设置真空隔热层,所述嵌槽(41)设于容纳槽(13)内侧面顶部和底部位置,炉门(12)上滑移连接有活动块(43),活动块(43)与连接块(42)之间通过连动杆(44)固定,炉门(12)内设有主动齿轮(53),活动块(43)一侧设有与主动齿轮(53)相互啮合的活动齿条(45),用于驱动活动块(43)和连动杆(44)滑移,所述转轮(51)通过转轴(52)转动连接在炉门(12)上,转轴(52)穿透炉门(12)设置,主动齿轮(53)同轴心固定在转轴(52)上,辅助隔离件(3)包括驱动块(32),驱动块(32)滑移连接在炉门(12)上,驱动块(32)末端通过驱动杆(33)与隔离块(31)固定,所述驱动块(32)上一体形成有驱动齿条(34),驱动齿条(34)与主动齿轮(53)相互啮合,用于带动驱动块(32)滑移,驱动齿条(34)与活动齿条(45)相互错位,驱动块(32)位于主动齿轮(53)上下两侧,活动块(43)位于主动齿轮(53)的左右两侧。The locking piece (4) comprises a slot (41) fixed on the furnace body (1) and a connecting block (42) slidingly connected to the furnace door (12), and the connecting block (42) passes through the linkage rod ( 44) Connected with the linkage (5), when the runner (51) rotates, the linkage rod (44) drives the connection block (42) to be embedded in the slot (41) or pulled out of the slot (41) to realize The locking of the furnace door (12), the bottom of the fixed ring (21) is provided with a limiting convex ring (211), and the end of the closed ring (22) is formed with an inner convex ring (221), and the inner convex ring (221) is on the furnace door. (12) slips between the limiting convex ring (211), when the furnace door (12) is closed, the top surface of the inner convex ring (221) and the limiting convex ring (211) are attached to each other, and the closed ring (22) is integrally formed by Made of toughened glass material, it consists of two layers, the middle position is provided with a vacuum heat insulation layer, and the embedding groove (41) is arranged at the top and bottom positions of the inner side of the containing groove (13), and the furnace door (12) is slidably connected with Movable block (43), is fixed by linkage rod (44) between movable block (43) and connecting block (42), is provided with driving gear (53) in the furnace door (12), and movable block (43) one side is provided with There is a movable rack (45) meshing with the driving gear (53), which is used to drive the movable block (43) and the linkage rod (44) to slide, and the runner (51) is connected to the On the furnace door (12), the rotating shaft (52) penetrates the furnace door (12) and is set, and the driving gear (53) is fixed on the rotating shaft (52) concentrically, and the auxiliary spacer (3) includes a driving block (32), which drives The block (32) is slidingly connected on the furnace door (12), and the end of the drive block (32) is fixed with the spacer block (31) by the drive rod (33), and a drive rack ( 34), the driving rack (34) and the driving gear (53) mesh with each other, and are used to drive the driving block (32) to slide, and the driving rack (34) and the movable rack (45) are misaligned with each other, and the driving block (32) Be located at the upper and lower sides of the driving gear (53), and the movable block (43) is located at the left and right sides of the driving gear (53). 2.根据权利要求1所述的晶硅太阳能电池变温扩散炉,其特征在于:所述炉体(1)上设有用于容纳炉门(12)的容纳槽(13),炉口(11)位于容纳槽(13)中间位置,封闭件(2)包括活动杆(24),活动杆(24)中间位置铰接在炉门(12)上,活动杆(24)一端铰接在封闭环(22)侧面,另一端与炉门(12)之间通过固定弹簧连接,容纳槽(13)内对应活动杆(24)末端设有压块(25)。2. The temperature-variable diffusion furnace for crystalline silicon solar cells according to claim 1, characterized in that: the furnace body (1) is provided with an accommodating groove (13) for accommodating the furnace door (12), and the furnace mouth (11) Located in the middle of the receiving tank (13), the closure (2) includes a movable rod (24), the middle position of the movable rod (24) is hinged on the furnace door (12), and one end of the movable rod (24) is hinged on the closed ring (22) On the side, the other end is connected with the furnace door (12) by a fixed spring, and a pressing block (25) is provided at the end of the corresponding movable rod (24) in the accommodation groove (13). 3.根据权利要求1所述的晶硅太阳能电池变温扩散炉,其特征在于:所述隔离块(31)内设有贴合在封闭环(22)上的石棉垫(311),炉门(12)包括内层(121)和外层(122),内层(121)与外层(122)之间真空设置,炉门(12)和炉体(1)的对应设有钢化玻璃形成的视窗(123),用于观测炉体(1)内工作情况。3. The temperature-variable diffusion furnace for crystalline silicon solar cells according to claim 1, characterized in that: an asbestos pad (311) attached to the closed ring (22) is provided in the spacer block (31), and the furnace door ( 12) Including the inner layer (121) and the outer layer (122), the vacuum is set between the inner layer (121) and the outer layer (122), and the corresponding furnace door (12) and the furnace body (1) are provided with tempered glass Window (123) is used to observe the working conditions in the body of furnace (1).
CN202111165033.8A 2021-09-30 2021-09-30 Crystalline silicon solar cell variable temperature diffusion furnace Active CN114000202B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111165033.8A CN114000202B (en) 2021-09-30 2021-09-30 Crystalline silicon solar cell variable temperature diffusion furnace

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202111165033.8A CN114000202B (en) 2021-09-30 2021-09-30 Crystalline silicon solar cell variable temperature diffusion furnace

Publications (2)

Publication Number Publication Date
CN114000202A CN114000202A (en) 2022-02-01
CN114000202B true CN114000202B (en) 2023-06-02

Family

ID=79922231

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202111165033.8A Active CN114000202B (en) 2021-09-30 2021-09-30 Crystalline silicon solar cell variable temperature diffusion furnace

Country Status (1)

Country Link
CN (1) CN114000202B (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB191121195A (en) * 1911-09-26 1912-10-28 Edwin Ramsbottom Improvements in Furnaces for Steam Boilers.
FR2451004A1 (en) * 1979-03-09 1980-10-03 Pruines Iseco Sa De Metal door for microwave oven - is manoeuvred in closing position by electric motor and lever system
CN203432348U (en) * 2013-07-11 2014-02-12 上海大学 Automatic furnace door sealing device for diffusion furnace

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN209819584U (en) * 2019-04-17 2019-12-20 刘秋娜 A kind of stove

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB191121195A (en) * 1911-09-26 1912-10-28 Edwin Ramsbottom Improvements in Furnaces for Steam Boilers.
FR2451004A1 (en) * 1979-03-09 1980-10-03 Pruines Iseco Sa De Metal door for microwave oven - is manoeuvred in closing position by electric motor and lever system
CN203432348U (en) * 2013-07-11 2014-02-12 上海大学 Automatic furnace door sealing device for diffusion furnace

Also Published As

Publication number Publication date
CN114000202A (en) 2022-02-01

Similar Documents

Publication Publication Date Title
KR101193169B1 (en) Apparatus and method for drying electrode plate
CN204570081U (en) A kind of device for growing large-size high-purity silicon carbide monocrystalline
CN114000202B (en) Crystalline silicon solar cell variable temperature diffusion furnace
CN108707966A (en) A kind of low nitrogen content SiC single crystal grower and its application
JP2015530478A (en) System and method for processing a substrate
CN102877116B (en) Closed single crystal growth furnace for crystal growth by molten salt method
WO2018103763A1 (en) Preparation method for low oxygen content semiconductor core composite material optical fibre preform
CN102169810B (en) Laser processing apparatus using vacuum cavity and processing method thereof
CN207418920U (en) A kind of long-life graphite crucible single crystal growing furnace
CN213977814U (en) Vacuum heat treatment furnace for hydrogen storage material
CN111778559B (en) Graphite disc turnover type GaN single crystal substrate laser pre-stripping integrated cavity
CN217063679U (en) Photovoltaic module light infiltration device
CN217239394U (en) a furnace tube
CN102618935B (en) Annealing method for infrared nonlinear single crystal of multi-component compound containing easily volatile components
CN213327937U (en) Graphite plate turnover type GaN single crystal substrate laser pre-stripping integrated cavity
CN102169827A (en) Method of manufacturing a semiconductor device
CN113351146B (en) A special rotary high-temperature vulcanization device for the synthesis of rare earth sulfides
CN214060634U (en) Cold pump activating machine of molecular beam epitaxy equipment
CN221861598U (en) A high temperature rapid annealing device for semiconductor materials
CN111926391A (en) Quartz tube high-vacuum exhaust system and method
CN221460578U (en) High flux perovskite film vacuum heating crystallization device
JP3240180B2 (en) Heat treatment equipment
CN221201194U (en) Device for preparing silicon dioxide film layer and solar cell production equipment
CN100472719C (en) Box Zinc Diffusion Method for Fabrication of InGaAs Photodetector Chips
CN109943884A (en) A kind of zinc selenide raw material high temperature purification method

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant