CN113698254A - Multi-organic-matter polymerized fertilizer and preparation process thereof - Google Patents
Multi-organic-matter polymerized fertilizer and preparation process thereof Download PDFInfo
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- CN113698254A CN113698254A CN202010378889.2A CN202010378889A CN113698254A CN 113698254 A CN113698254 A CN 113698254A CN 202010378889 A CN202010378889 A CN 202010378889A CN 113698254 A CN113698254 A CN 113698254A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
- C05D9/02—Other inorganic fertilisers containing trace elements
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
Abstract
本发明公开了一种多有机物聚合肥，其特征在于，包括：以下重量份数的原料:主料，所述主料包括高活性酯基粉11‑15份和碳酶多肽74‑81份；辅料，沙棘总黄酮粉5‑7份和农业有机硅3‑4份。本发明提供的一种有机物聚合肥的肥料效果：抗寒抗旱、平衡土壤酸碱值，疏松土壤，延长肥效，提高肥料利用率，提高作物抗逆性，耐存储运输，改善作物品质，可以增加果实糖度、蔬菜叶片肥厚。对葡萄的大小粒、樱桃的畸形果、辣椒炭疽病、马铃薯晚疫病，红薯根腐病，黄瓜霜霉病、果树腐烂病，苦痘病、棉花黄萎病等有显著的抑制作用。The invention discloses a multi-organic polymer fertilizer, which is characterized by comprising: the following raw materials in parts by weight: a main material, wherein the main material includes 11-15 parts of high-activity ester base powder and 74-81 parts of carbon enzyme polypeptide; The accessories are 5-7 parts of sea buckthorn total flavonoid powder and 3-4 parts of agricultural organic silicon. The fertilizer effect of the organic polymer fertilizer provided by the invention: cold resistance and drought resistance, balance soil pH value, loosen soil, prolong fertilizer efficiency, improve fertilizer utilization rate, improve crop stress resistance, storage and transportation resistance, improve crop quality, and can increase Fruit sugar content, vegetable leaf hypertrophy. It has a significant inhibitory effect on the size of grapes, deformed fruit of cherries, pepper anthracnose, potato late blight, sweet potato root rot, cucumber downy mildew, fruit tree rot, bitter pox, cotton verticillium wilt, etc.
Description
Technical Field
The invention relates to the technical field of polymeric fertilizers, in particular to a multi-organic polymeric fertilizer and a preparation process thereof.
Background
The global chemical fertilizer is the largest material input in agricultural production, and the statistical data of the food and agriculture organization of the united nations show that the effect of the chemical fertilizer on the yield increase accounts for 40-60% in the process of increasing the yield per unit. However, production practices show that the utilization rate of the chemical fertilizer is low due to the comprehensive influences of the properties of the chemical fertilizer, soil environmental conditions, agricultural measures and the like. The nutrient resource waste caused by low utilization rate of the fertilizer nutrient in China is quite remarkable. The latest authoritative data show that the direct economic loss of farmers caused by blind excessive fertilization per year in China is 650 yuan per hectare on average, the cost of environment is about 730 million yuan, and the fertilizer is lost by over 1100 million yuan per year. How to improve the utilization rate of chemical fertilizers and reduce the problem of environmental pollution caused by improper fertilization has become a common concern of all countries in the world for sustainable development of high-efficiency agriculture.
Disclosure of Invention
An object of the present invention is to solve at least the above problems and to provide at least the advantages described later.
The invention also aims to provide the multi-organic-matter polymerized fertilizer which has simple process and low cost.
In order to achieve the above object, the present invention provides a multi-organic polymeric fertilizer, comprising: the following raw materials in parts by weight:
the main material comprises 11-15 parts of high-activity ester-based powder and 74-81 parts of carbohydrase polypeptide;
5-7 parts of total seabuckthorn flavone powder and 3-4 parts of agricultural organic silicon.
The invention discloses a preparation process of the multi-organic-matter polymerized fertilizer, which is characterized by comprising the following process steps:
s1: mixing the vinasse with an organic fertilizer starter according to the ratio of 7000:1, and fermenting the vinasse mixture in a fermentation chamber for 12-15 h;
s2: steaming the fermented distiller 'S grains mixture in the S1 in boiling water for 20-25min to obtain distiller' S grains solution;
s3: carrying out filter pressing on the vinasse solution obtained in the step S2 to remove filter residues to obtain a pure vinasse solution;
s4: pumping the filtered pure vinasse solution in the S3 into a preheating system for preheating for 9 hours;
s5: pumping the preheated pure distiller' S grains solution of S4 into an evaporator for evaporation and concentration until high-activity ester base powder is separated out for later use;
s6: taking carbohydrase polypeptide according to the mass part, dissolving the carbohydrase polypeptide in purified water at 40 ℃ to obtain carbohydrase polypeptide solution, keeping the concentration at 45 percent for 10-15min, taking the high-activity ester group powder obtained in S5 according to the mass part, and adding the high-activity ester group powder into the carbohydrase polypeptide solution to obtain primary carbohydrase polypeptide-high-activity ester group solution;
s7: stirring the primary carbohydrase polypeptide-high activity ester group solution obtained in the step S6 for 30min by a high shear stirrer, and simultaneously keeping the primary carbohydrase polypeptide-high activity ester group solution at 50 ℃;
s8: taking the total seabuckthorn flavone powder and the agricultural organic silicon in parts by mass, and adding the total seabuckthorn flavone powder and the agricultural organic silicon into the carbohydrase polypeptide-high activity ester group solution obtained in the step S7 to obtain a secondary carbohydrase polypeptide-high activity ester group solution;
s9: carrying out mean value treatment on the secondary carbohydrase polypeptide-high activity ester group solution obtained in the step S8 for 40min by a homogenizer, wherein the pressure of the homogenizer is adjusted to 25mpa within 1-30min, the pressure of the homogenizer is adjusted to 22mpa within 30-40min, and meanwhile, the secondary carbohydrase polypeptide-high activity ester group solution is kept at 50 ℃;
s10: pumping the second-level carbohydrase polypeptide-high activity ester-based solution after the S9 homogenization treatment into an evaporator for evaporation and concentration until multi-organic-matter polymer fertilizer with high activity ester-based powder, carbohydrase polypeptide, sea buckthorn total flavonoid powder and agricultural organosilicon is separated out.
The preferable scheme of the multi-organic-matter polymer fertilizer provided by the invention is characterized by comprising the following raw materials in parts by weight:
the main material comprises 12-14 parts of high-activity ester-based powder and 75-80 parts of carbohydrase polypeptide;
auxiliary materials, 6 parts of seabuckthorn total flavone powder and 3 parts of agricultural organic silicon.
The preferable scheme of the multi-organic-matter polymer fertilizer provided by the invention is characterized by comprising the following raw materials in parts by weight:
the main material comprises 13 parts of high-activity ester-based powder and 78 parts of carbohydrase polypeptide;
auxiliary materials, 6 parts of seabuckthorn total flavone powder and 3 parts of agricultural organic silicon.
The preferable scheme of the multi-organic-matter polymer fertilizer provided by the invention is characterized by comprising the following raw materials in parts by weight:
the main material comprises 12 parts of high-activity ester-based powder and 76 parts of carbohydrase polypeptide;
auxiliary materials, 6 parts of seabuckthorn total flavone powder and 4 parts of agricultural organic silicon.
High active ester group: the vinasse vinegar residue is processed and purified again, and then the catalyst is added, so that the main components are subjected to esterification reaction, high-activity ester groups are generated and purified, and the vinasse vinegar residue is rich in beneficial factors such as crude protein, trace elements, vitamins, zymogen and crude fiber and has the effect of balancing the acid-base property of soil.
Seabuckthorn total flavonoids: the sea buckthorn fertilizer is extracted from sea buckthorn, has the characteristics of cold and drought resistance, barren resistance, no toxicity, no moisture absorption and strong adaptability, has the biological ecological characteristics of root nodules and the like, has high growth speed, developed root systems and strong tillering property, can effectively improve the corrosion resistance and impact resistance of soil, and further plays roles of keeping water and soil, conserving water sources, preventing wind and fixing sand and the like.
Agricultural organic silicon: the agricultural organic silicon is a high-molecular high-activity polymer active auxiliary agent, has the effects of improving the granular structure of soil, improving hardened soil, loosening soil, maintaining fertilizer and improving fertilizer efficiency, and particularly has a reinforcing effect on the lodging resistance and stress resistance of gramineous crops.
Carbohydrase polypeptide: the fertilizer is mainly extracted from peat and lignite before coal formation, provides sufficient organic carbon for crops, contains various functional groups such as methoxy, phenolic hydroxyl, alcoholic hydroxyl and aldehyde groups, and small molecular organic acid fragments as efficient transportation and activation carriers, and is combined with enzymatic reaction of biological enzyme, so that the fertilizer efficiency is greatly improved, and the effectiveness of comprehensive fertilizer nutrients is improved by over 35 percent.
The carbohydrase polypeptide in the main material mainly has the following functions:
soil improvement
The carbohydrase polypeptide has a loose and porous structure and is hydrophilic colloid, and the adhesive force is half smaller than that of the clay, so that loose granules are easily formed after the clay is coated, and the soil becomes loose and is not agglomerated into hard blocks. The carbohydrase polypeptide can make sandy soil compact and clay loose. Can absorb a large amount of water, thereby greatly improving the water retention capacity of the soil
The carbohydrase polypeptide is weak acid containing polyacid functional groups, and salts of the carbohydrase polypeptide have the effect of amphoteric colloid, so that the carbohydrase polypeptide has strong capacity of buffering acid-base change, the mass fraction of the carbohydrase polypeptide in soil is improved, the acid-base buffering performance of the soil can be enhanced, and the over-acid or over-base condition of the soil can be relieved.
Second, synergistic fertilizer
Reduce the volatilization of nitrogen fertilizer and promote the absorption of nitrogen. The carbohydrase polypeptide can inhibit the fixation of water-soluble phosphorus by soil, convert ineffective phosphorus into effective phosphorus, increase the moving distance of phosphorus in the soil, stimulate the development of root systems and promote the absorption of the phosphorus by the root systems. The functional group of the carbohydrase polypeptide can absorb and store potassium ions, and the quantity of potassium lost with water in soil is reduced. The carbohydrase polypeptide can prevent the fixation of the potassium by the cohesive soil and increase the number of exchangeable potassium. The carbohydrase polypeptide has the function of corroding potassium-containing minerals, slowly increases the release of potassium and improves the quick-acting potassium content of soil. Promote the absorption of trace element fertilizer and effectively solve the nutrient deficiency.
Third, stimulating growth
1. After the carbohydrase polypeptide is applied to the root promoting agent, the root system is developed on crops, the number and the length of the root system are improved, and secondary roots are obviously increased.
2. Enhancing photosynthesis can promote chlorophyll formation and increase photosynthetic efficiency.
Fourthly, the stress resistance of the plants is enhanced
1. Enhancing cold resistance. After the carbohydrase polypeptide is applied, the cold-resistant substance free proline, protein and soluble sugar in the plant nutritive organ are obviously improved compared with the lighting, and the permeability of the leaf cell membrane is reduced to 12.4 percent from 20.7 percent of the control, so that the cold resistance of the plant is improved.
2. And (4) drought resistance is enhanced. The mineral source fulvic acid can reduce the opening strength of pores of plant leaves and reduce transpiration of the leaf surfaces, thereby reducing water consumption, improving the water condition in the plants, ensuring the normal growth and development of crops under drought conditions and enhancing the drought resistance.
3. Improve the capability of resisting plant diseases and insect pests of crops. The salicylic acid and phenol structures in the carbohydrase polypeptide are antibacterial agent structures, and the carbohydrase polypeptide is applied to improve the metabolism function of plants and improve the activity and the immunity of certain cytoprotective enzymes (POD and IAA).
The invention at least comprises the following beneficial effects:
the fertilizer effect of the organic matter polymerized fertilizer is as follows: cold and drought resistance, soil pH value balance, soil loosening, fertilizer efficiency prolonging, fertilizer utilization rate improving, crop stress resistance improving, storage and transportation resisting, crop quality improving, fruit sugar degree increasing, and vegetable leaf thickness increasing. Has obvious inhibiting effect on grape granules, cherry malformed fruits, pepper anthracnose, potato late blight, sweet potato root rot, cucumber downy mildew, fruit tree rot, bitter pox, cotton verticillium wilt and the like.
Detailed Description
It will be understood that terms such as "having," "including," and "comprising," when used herein, do not preclude the presence or addition of one or more other elements or groups thereof.
Example 1:
the invention discloses a multi-organic-matter polymerized fertilizer which is characterized by comprising the following components: the following raw materials in parts by weight:
the main material comprises 13 parts of high-activity ester-based powder and 78 parts of carbohydrase polypeptide;
auxiliary materials, 6 parts of seabuckthorn total flavone powder and 3 parts of agricultural organic silicon.
The invention discloses a preparation process of the multi-organic-matter polymerized fertilizer, which is characterized by comprising the following process steps:
s1: mixing the vinasse with an organic fertilizer starter according to the ratio of 7000:1, and fermenting the vinasse mixture in a fermentation chamber for 12-15 h;
s2: steaming the fermented distiller 'S grains mixture in the S1 in boiling water for 20-25min to obtain distiller' S grains solution;
s3: carrying out filter pressing on the vinasse solution obtained in the step S2 to remove filter residues to obtain a pure vinasse solution;
s4: pumping the filtered pure vinasse solution in the S3 into a preheating system for preheating for 9 hours;
s5: pumping the preheated pure distiller' S grains solution of S4 into an evaporator for evaporation and concentration until high-activity ester base powder is separated out for later use;
s6: taking carbohydrase polypeptide according to the mass part, dissolving the carbohydrase polypeptide in purified water at 40 ℃ to obtain carbohydrase polypeptide solution, keeping the concentration at 45 percent for 10-15min, taking the high-activity ester group powder obtained in S5 according to the mass part, and adding the high-activity ester group powder into the carbohydrase polypeptide solution to obtain primary carbohydrase polypeptide-high-activity ester group solution;
s7: stirring the primary carbohydrase polypeptide-high activity ester group solution obtained in the step S6 for 30min by a high shear stirrer, and simultaneously keeping the primary carbohydrase polypeptide-high activity ester group solution at 50 ℃;
s8: taking the total seabuckthorn flavone powder and the agricultural organic silicon in parts by mass, and adding the total seabuckthorn flavone powder and the agricultural organic silicon into the carbohydrase polypeptide-high activity ester group solution obtained in the step S7 to obtain a secondary carbohydrase polypeptide-high activity ester group solution;
s9: carrying out mean value treatment on the secondary carbohydrase polypeptide-high activity ester group solution obtained in the step S8 for 40min by a homogenizer, wherein the pressure of the homogenizer is adjusted to 25mpa within 1-30min, the pressure of the homogenizer is adjusted to 22mpa within 30-40min, and meanwhile, the secondary carbohydrase polypeptide-high activity ester group solution is kept at 50 ℃;
s10: pumping the second-level carbohydrase polypeptide-high activity ester-based solution after the S9 homogenization treatment into an evaporator for evaporation and concentration until multi-organic-matter polymer fertilizer with high activity ester-based powder, carbohydrase polypeptide, sea buckthorn total flavonoid powder and agricultural organosilicon is separated out.
Example 2:
a multi-organic matter polymerized fertilizer is characterized by comprising: the following raw materials in parts by weight:
the main material comprises 12 parts of high-activity ester-based powder and 76 parts of carbohydrase polypeptide;
auxiliary materials, 6 parts of seabuckthorn total flavone powder and 4 parts of agricultural organic silicon.
The invention discloses a preparation process of the multi-organic-matter polymerized fertilizer, which is characterized by comprising the following process steps:
s1: mixing the vinasse with an organic fertilizer starter according to the ratio of 7000:1, and fermenting the vinasse mixture in a fermentation chamber for 12-15 h;
s2: steaming the fermented distiller 'S grains mixture in the S1 in boiling water for 20-25min to obtain distiller' S grains solution;
s3: carrying out filter pressing on the vinasse solution obtained in the step S2 to remove filter residues to obtain a pure vinasse solution;
s4: pumping the filtered pure vinasse solution in the S3 into a preheating system for preheating for 9 hours;
s5: pumping the preheated pure distiller' S grains solution of S4 into an evaporator for evaporation and concentration until high-activity ester base powder is separated out for later use;
s6: taking carbohydrase polypeptide according to the mass part, dissolving the carbohydrase polypeptide in purified water at 40 ℃ to obtain carbohydrase polypeptide solution, keeping the concentration at 45 percent for 10-15min, taking the high-activity ester group powder obtained in S5 according to the mass part, and adding the high-activity ester group powder into the carbohydrase polypeptide solution to obtain primary carbohydrase polypeptide-high-activity ester group solution;
s7: stirring the primary carbohydrase polypeptide-high activity ester group solution obtained in the step S6 for 30min by a high shear stirrer, and simultaneously keeping the primary carbohydrase polypeptide-high activity ester group solution at 50 ℃;
s8: taking the total seabuckthorn flavone powder and the agricultural organic silicon in parts by mass, and adding the total seabuckthorn flavone powder and the agricultural organic silicon into the carbohydrase polypeptide-high activity ester group solution obtained in the step S7 to obtain a secondary carbohydrase polypeptide-high activity ester group solution;
s9: carrying out mean value treatment on the secondary carbohydrase polypeptide-high activity ester group solution obtained in the step S8 for 40min by a homogenizer, wherein the pressure of the homogenizer is adjusted to 25mpa within 1-30min, the pressure of the homogenizer is adjusted to 22mpa within 30-40min, and meanwhile, the secondary carbohydrase polypeptide-high activity ester group solution is kept at 50 ℃;
s10: pumping the second-level carbohydrase polypeptide-high activity ester-based solution after the S9 homogenization treatment into an evaporator for evaporation and concentration until multi-organic-matter polymer fertilizer with high activity ester-based powder, carbohydrase polypeptide, sea buckthorn total flavonoid powder and agricultural organosilicon is separated out.
While embodiments of the invention have been disclosed above, it is not limited to the applications listed in the description and the embodiments, which are fully applicable in all kinds of fields of application of the invention, and further modifications may readily be effected by those skilled in the art, so that the invention is not limited to the specific details without departing from the general concept defined by the claims and the scope of equivalents.
Claims (5)
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|---|---|---|---|---|
| CN1611464A (en) * | 2003-12-16 | 2005-05-04 | 山东日照酒业有限公司 | Organic fertilizer using distillers' grains as raw material and its production process |
| CN103113160A (en) * | 2013-02-22 | 2013-05-22 | 西北师范大学 | Plant cold-resistant agent and preparation method and application thereof |
| US20130312471A1 (en) * | 2010-11-22 | 2013-11-28 | Hpd Process Engineering, S.A. | Method for obtaining a solid fertilizer and biofuel product from sugarcane vinasses and solid fertilizer and biofuel product obtained by means of said method |
| CN105693429A (en) * | 2016-02-25 | 2016-06-22 | 中节能绿碳环保有限公司 | Clear liquid type distiller's grain fermentation liquid fertilizer and preparation method thereof |
| CN105948831A (en) * | 2016-06-07 | 2016-09-21 | 齐鲁工业大学 | Method for producing biocontrol fertilizer by means of brewer's grain |
| CN106747729A (en) * | 2016-12-05 | 2017-05-31 | 安徽爱能洁生物科技有限公司 | A kind of grape special fertilizer preparation method for improving fruiting rate |
| CN107056537A (en) * | 2017-04-05 | 2017-08-18 | 宝鸡文理学院 | A kind of Agro-ecology fertilizer |
| CN108530181A (en) * | 2018-05-31 | 2018-09-14 | 贵州盈丰农业发展有限公司 | A kind of production method for the vinasse fermentation Liquid Fertilizer being exclusively used in Rosa roxburghii Tratt |
-
2020
- 2020-05-07 CN CN202010378889.2A patent/CN113698254A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1611464A (en) * | 2003-12-16 | 2005-05-04 | 山东日照酒业有限公司 | Organic fertilizer using distillers' grains as raw material and its production process |
| US20130312471A1 (en) * | 2010-11-22 | 2013-11-28 | Hpd Process Engineering, S.A. | Method for obtaining a solid fertilizer and biofuel product from sugarcane vinasses and solid fertilizer and biofuel product obtained by means of said method |
| CN103113160A (en) * | 2013-02-22 | 2013-05-22 | 西北师范大学 | Plant cold-resistant agent and preparation method and application thereof |
| CN105693429A (en) * | 2016-02-25 | 2016-06-22 | 中节能绿碳环保有限公司 | Clear liquid type distiller's grain fermentation liquid fertilizer and preparation method thereof |
| CN105948831A (en) * | 2016-06-07 | 2016-09-21 | 齐鲁工业大学 | Method for producing biocontrol fertilizer by means of brewer's grain |
| CN106747729A (en) * | 2016-12-05 | 2017-05-31 | 安徽爱能洁生物科技有限公司 | A kind of grape special fertilizer preparation method for improving fruiting rate |
| CN107056537A (en) * | 2017-04-05 | 2017-08-18 | 宝鸡文理学院 | A kind of Agro-ecology fertilizer |
| CN108530181A (en) * | 2018-05-31 | 2018-09-14 | 贵州盈丰农业发展有限公司 | A kind of production method for the vinasse fermentation Liquid Fertilizer being exclusively used in Rosa roxburghii Tratt |
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Application publication date: 20211126 |