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CN113080206A - Aromatic essential oil air disinfectant and preparation method thereof - Google Patents

Aromatic essential oil air disinfectant and preparation method thereof Download PDF

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Publication number
CN113080206A
CN113080206A CN202110394562.9A CN202110394562A CN113080206A CN 113080206 A CN113080206 A CN 113080206A CN 202110394562 A CN202110394562 A CN 202110394562A CN 113080206 A CN113080206 A CN 113080206A
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essential oil
oil
water
rosemary
cinnamon
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梁新丽
徐希强
董伟
汪新娌
赵国魏
周爱鲜
黄小英
杨明
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Jiangxi University of Traditional Chinese Medicine
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Jiangxi University of Traditional Chinese Medicine
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Priority to CN202110394562.9A priority Critical patent/CN113080206A/en
Publication of CN113080206A publication Critical patent/CN113080206A/en
Priority to CN202210051185.3A priority patent/CN114532368A/en
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/06—Coniferophyta [gymnosperms], e.g. cypress
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
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  • Agronomy & Crop Science (AREA)
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  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Botany (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Fats And Perfumes (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

The invention discloses an aromatic essential oil air disinfectant and a preparation method thereof. The aromatic essential oil air disinfectant comprises the following components in percentage by weight: 0.01-1% of folium artemisiae argyi essential oil, 0.01-1% of cinnamon essential oil, 0.01-1% of rosemary essential oil, 0.01-1% of cedar essential oil, 0.01-1% of sweet orange essential oil, 0.01-1% of mint essential oil, 0.1-2% of organic solvent and the balance of water. The air disinfectant provided by the invention has the characteristics of remarkable use effect, mild performance, no stimulation and no side effect; the production process is simple, the cost is low, the safety and the environmental protection are realized, and the economic value is extremely high; the raw materials used by the invention comprise folium artemisiae argyi essential oil, cinnamon essential oil, rosemary essential oil, cedar essential oil, sweet orange essential oil and mint essential oil, so that the traditional Chinese medicine resources are fully utilized, and greater economic and social benefits are generated.

Description

Aromatic essential oil air disinfectant and preparation method thereof
Technical Field
The invention relates to the technical field of air purification, in particular to an aromatic essential oil air disinfectant and a preparation method thereof.
Background
People's awareness of preventing germs and viruses will be significantly enhanced. Methods for cutting off the virus transmission path include physical isolation methods (such as ultraviolet irradiation, household isolation, and wearing a mask when going out), chemical blocking of transmission (such as use of a disinfectant), and the like. Air disinfection is adopted in families and other public places such as shopping malls, which is the most effective method for blocking pathogen transmission through air and preventing virus transmission at present. However, the traditional household disinfectant mainly comprises chlorine-containing disinfectant, peroxide disinfectant, alcohol disinfectant and the like, and the preparations are very easy to generate health safety hidden troubles in the production and use processes. Therefore, more and more people favor the disinfectant which is purely natural, has no pollution, mild performance, no stimulation and no side effect.
Disclosure of Invention
The invention aims to provide an aromatic essential oil air disinfectant and a preparation method thereof, so as to solve the technical problems.
In order to achieve the purpose, the technical scheme of the invention is as follows:
in a first aspect, the invention provides an aromatic essential oil air disinfectant, which comprises the following components in percentage by weight: 0.01-1% of folium artemisiae argyi essential oil, 0.01-1% of cinnamon essential oil, 0.01-1% of rosemary essential oil, 0.01-1% of cedar essential oil, 0.01-1% of sweet orange essential oil, 0.01-1% of mint essential oil, 0.1-2% of organic solvent and the balance of water.
Preferably, the organic solvent is at least one selected from ethanol and glycerol.
Further preferably, the organic solvent is ethanol.
Preferably, the aromatic essential oil air disinfectant comprises the following components in percentage by weight: 0.05-0.2% of argy wormwood leaf essential oil, 0.05-0.2% of cinnamon essential oil, 0.1-0.3% of rosemary essential oil, 0.05-0.2% of cedar essential oil, 0.05-0.2% of sweet orange essential oil, 0.05-0.2% of mint essential oil, 0.3-1% of organic solvent and the balance of water.
Further preferably, the aromatic essential oil air disinfectant comprises the following components in percentage by weight: 0.1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of organic solvent and the balance of water.
Preferably, the folium artemisiae argyi essential oil, the cinnamon essential oil, the rosemary essential oil, the cedar essential oil, the sweet orange essential oil and the mint essential oil are all obtained by sequentially cleaning, extracting and concentrating folium artemisiae argyi, cinnamon bark, rosemary leaf, cedar pine needle, orange and mint leaf raw materials.
Further preferably, the argyi leaf essential oil is prepared by the following method: cleaning fresh folium artemisiae argyi, putting the cleaned fresh folium artemisiae argyi into a steam distillation extraction instrument, adding saturated salt water with the mass being 5-15 times of that of the fresh folium artemisiae argyi, performing reflux extraction at the temperature of 100-120 ℃ for 3-5 hours, collecting distillate, cooling the distillate to room temperature, transferring the distillate into an oil-water separator for oil-water separation, and drying and separating an oil layer by anhydrous sodium sulfate to obtain the essential oil of the folium artemisiae argyi.
Further preferably, the cinnamon essential oil is prepared by the following method: cleaning, drying and crushing fresh cinnamon bark, adding 60-90% by mass of ethanol solution, refluxing for 2-4 hours at 100-120 ℃, performing solid-liquid separation to obtain crude extract, performing vacuum concentration on the crude extract, performing freeze-drying treatment to obtain crude extract, dispersing the crude extract with water, loading the crude extract to a macroporous resin gel column, sequentially eluting with water and 30-95% by mass of ethanol solution for 0.5-2 hours each time, collecting eluates respectively, mixing the eluates, stirring uniformly, and concentrating to 1/5 of the original volume to obtain the cinnamon essential oil.
Further preferably, the rosemary essential oil is prepared by adopting the following method: cleaning fresh rosemary, putting the cleaned rosemary into a steam distillation extraction instrument, adding saturated salt water with the mass being 5-15 times of that of the rosemary, performing reflux extraction at 100-120 ℃ for 3-5 hours, collecting distillate, cooling the distillate to room temperature, transferring the distillate into an oil-water separator for oil-water separation, and drying and separating an oil layer by anhydrous sodium sulfate to obtain rosemary essential oil.
Further preferably, the cedar essential oil is prepared by the following method: cleaning, drying and crushing fresh cedar pine needles, adding the crushed cedar pine needles into an ethanol solution with the mass fraction of 70-95%, refluxing for 2-4 hours at 100-120 ℃, performing solid-liquid separation to obtain a crude extract, performing vacuum concentration on the crude extract, performing freeze-drying treatment to obtain a crude extract, dispersing the crude extract with water, loading the crude extract to a macroporous resin gel column, sequentially eluting with water and an ethanol solution with the mass fraction of 50-95% for 0.5-2 hours each time, collecting eluates respectively, mixing the eluates, stirring uniformly, and concentrating to 1/5 of the original volume to obtain cedar essential oil.
Further preferably, the sweet orange essential oil is prepared by the following method: soaking fresh sweet orange peel in saturated calcium hydroxide water solution, taking out, cleaning and crushing; taking an ethanol solution with the mass fraction of 80-95% as a solvent, carrying out ultrasonic extraction for 2-6 h under the conditions that the ratio of the mass of the crushed sweet orange peels to the volume of the ethanol solution is 1: 10-20 g/mL and the temperature is 60-80 ℃, filtering to obtain a filtrate, re-extracting filter residues twice according to the steps, combining the obtained extracting solutions, carrying out vacuum concentration, carrying out freeze-drying treatment to obtain a crude extract, dispersing the crude extract with water, loading the crude extract onto a macroporous resin gel column, sequentially eluting with water and the ethanol solution with the mass fraction of 30-95%, wherein the elution time is 0.5-2 h each time, respectively collecting eluents, combining the eluents, uniformly stirring, and concentrating to 1/5 of the original volume to obtain the sweet orange essential oil.
Further preferably, the mint leaf essential oil is prepared by adopting the following method: putting fresh mint leaves into a steam distillation extraction instrument, adding saturated salt water with the mass of 5-15 times of that of the mint leaves, performing reflux extraction at 100-120 ℃ for 3-5 h, collecting distillate, cooling to room temperature, transferring into an oil-water separator for oil-water separation, and drying and separating an oil layer by anhydrous sodium sulfate to obtain mint leaf essential oil.
In a second aspect, the present invention provides a method for preparing an essential oil air disinfectant, which comprises the following steps:
(1) mixing folium artemisiae argyi essential oil, cinnamon essential oil, rosemary essential oil, cedar essential oil, sweet orange essential oil, mint essential oil and an organic solvent, and stirring and mixing at the rotating speed of 2000-8000 r/min for 5-15 min at the temperature of 20-45 ℃ to obtain plant mixed essential oil;
(2) adding the prepared plant mixed essential oil into water, stirring and mixing at the rotating speed of 2000-8000 r/min for 5-15 min at the temperature of 20-35 ℃, and then irradiating and sterilizing for 0.5-1 h by using an ultraviolet lamp to obtain the aromatic essential oil air disinfectant.
Compared with the prior art, the invention has the beneficial effects that:
(1) the air disinfectant provided by the invention has the characteristics of remarkable use effect, mild performance, no stimulation and no side effect;
(2) the air disinfectant provided by the invention can be added with other traditional Chinese medicine essential oil with similar efficacy, and has extremely wide application value;
(3) the air disinfectant provided by the invention has the advantages of simple production process, low cost, safety, environmental protection and extremely high economic value.
(4) The air disinfectant provided by the invention uses raw materials including folium artemisiae argyi essential oil, cinnamon essential oil, rosemary essential oil, cedar essential oil, sweet orange essential oil and mint essential oil, fully utilizes traditional Chinese medicine resources, and generates greater economic and social benefits.
Detailed Description
The following further describes the embodiments of the present invention. It should be noted that the description of the embodiments is provided to help understanding of the present invention, but the present invention is not limited thereto. In addition, the technical features involved in the embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
The argy wormwood leaf essential oil in the following examples is prepared by the following method: cleaning fresh folium Artemisiae Argyi, placing into a steam distillation extraction instrument, adding 10 times of saturated salt solution, reflux extracting at 120 deg.C for 4 hr, collecting distillate, cooling to room temperature, separating oil and water in an oil-water separator, drying the oil layer with anhydrous sodium sulfate, and separating to obtain folium Artemisiae Argyi essential oil.
The cinnamon essential oil in the following examples is prepared by the following method: cleaning fresh cinnamon bark, drying in the sun, crushing, adding into an ethanol solution with the mass fraction of 80%, refluxing for 3 hours at 120 ℃, performing solid-liquid separation to obtain a crude extract, performing vacuum concentration on the crude extract, performing freeze-drying treatment to obtain a crude extract, dispersing the crude extract with water, loading into a macroporous resin gel column, sequentially eluting with water, an ethanol solution with the mass fraction of 30%, an ethanol solution with the mass fraction of 70% and an ethanol solution with the mass fraction of 95% for four times, wherein the elution time is 1 hour each time, respectively collecting eluents, mixing the eluents, uniformly stirring, and concentrating to 1/5 of the original volume to obtain the cinnamon essential oil.
The rosemary essential oil in the following examples is prepared by the following method: cleaning fresh rosemary, putting into a steam distillation extraction instrument, adding saturated salt water with the mass being 8 times of that of the rosemary, carrying out reflux extraction at 100 ℃ for 4 hours, collecting distillate, cooling to room temperature, transferring into an oil-water separator for oil-water separation, drying and separating an oil layer by anhydrous sodium sulfate to obtain rosemary essential oil.
The cedar essential oil in the following examples is prepared by the following method: cleaning, drying and crushing fresh cedar pine needles, adding the crushed cedar pine needles into an ethanol solution with the mass fraction of 90%, refluxing for 4 hours at 120 ℃, performing solid-liquid separation to obtain a crude extract, performing vacuum concentration on the crude extract, performing freeze-drying treatment to obtain a crude extract, dispersing the crude extract with water, loading the crude extract into a macroporous resin gel column, sequentially eluting with water, an ethanol solution with the mass fraction of 50%, an ethanol solution with the mass fraction of 75% and an ethanol solution with the mass fraction of 90% for four times, wherein the elution time is 1 hour each time, respectively collecting eluents, combining the eluents, uniformly stirring, and concentrating to 1/5 of the original volume to obtain cedar essential oil.
The sweet orange essential oil in the following examples is prepared by the following method: the sweet orange essential oil is prepared by adopting the following method: soaking fresh sweet orange peel in saturated calcium hydroxide water solution for 30min, taking out, cleaning, and crushing; taking an ethanol solution with the mass fraction of 85% as a solvent, carrying out ultrasonic extraction for 4 hours under the conditions that the ratio of the mass of the crushed material of the sweet orange peels to the volume of the ethanol solution is 1:15g/mL and the temperature is 75 ℃, filtering to obtain a filtrate, re-extracting filter residues twice according to the steps, combining the obtained extracting solutions, carrying out vacuum concentration, carrying out freeze-drying treatment to obtain a crude extract, dispersing the crude extract with water, loading the crude extract to a macroporous resin gel column, sequentially eluting with water, an ethanol solution with the mass fraction of 40%, an ethanol solution with the mass fraction of 70% and an ethanol solution with the mass fraction of 90%, wherein the elution time is 1 hour each time, respectively collecting eluents, combining the eluents, uniformly stirring, and concentrating to 1/5 of the original volume to obtain the sweet orange essential oil.
The mint leaf essential oil in the following examples is prepared by the following method: putting fresh mint leaves into a steam distillation extraction instrument, adding 10 times of saturated salt water, extracting for 3 hours at 100 ℃ under reflux, collecting distillate, cooling to room temperature, transferring into an oil-water separator for oil-water separation, drying an oil layer by anhydrous sodium sulfate, and separating to obtain the mint leaf essential oil.
And (3) argy wormwood leaf essential oil: has antibacterial, antifungal, antiviral, and mycoplasma resisting effects;
cinnamon essential oil: the bactericidal effect is extremely strong, and most of bacteria can be killed in a small amount;
rosemary essential oil: antibacterial activity is often used as an antimicrobial;
cedar essential oil: has antibacterial activity and remarkable antioxidant activity;
sweet orange essential oil: can inhibit growth of Aspergillus niger and Aspergillus flavus, and the inhibiting effect is enhanced with increase of essential oil concentration; meanwhile, the compound has certain antibacterial capacity on staphylococcus aureus, escherichia coli, candida albicans and the like, has sweet orange fragrance, and can be used for flavoring;
mint essential oil: has broad antibacterial spectrum and elegant fragrance, and can be used as correctant.
Example 1
Weighing the following raw materials in percentage by weight: 0.05% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.1% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. Adding folium Artemisiae Argyi essential oil, cortex Cinnamomi essential oil, herba Rosmarini officinalis essential oil, cedar essential oil, fructus Citri sinensis essential oil, herba Menthae essential oil and ethanol into high speed dispersing emulsifying machine, mixing, and stirring at 35 deg.C and 5000r/min for 112min to obtain plant mixed essential oil; sequentially adding purified water and the prepared plant mixed essential oil into a high-speed dispersion emulsifying machine, stirring and mixing at 25 ℃ at the rotating speed of 5000r/min for 12min, and irradiating and sterilizing by using an ultraviolet lamp for 45min to obtain the aromatic essential oil air disinfectant.
Example 2
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 3
Weighing the following raw materials in percentage by weight: 0.01% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 4
Weighing the following raw materials in percentage by weight: 0.2% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 5
Weighing the following raw materials in percentage by weight: 1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 6
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.01% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 7
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.05% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 8
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.2% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 9
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.3% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 10
Weighing the following raw materials in percentage by weight: 0.05% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.01% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 11
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.01% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 12
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.2% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 13
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.01% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 14
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.05% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 15
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.2% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 16
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.01% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 17
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.05% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 18
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.2% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Example 19
Weighing the following raw materials in percentage by weight: the aromatic essential oil air disinfectant is prepared by the method of example 1, wherein the aromatic essential oil air disinfectant comprises 1% of argy wormwood leaf essential oil, 1% of cinnamon essential oil, 1% of rosemary essential oil, 1% of cedar essential oil, 1% of sweet orange essential oil, 1% of mint essential oil, 2% of ethanol and the balance of water.
Comparative example 1
The essential oils are prepared by the method of the above example, and the following raw materials are weighed according to the weight percentage: rosemary essential oil 0.2%, cedar essential oil 0.1%, sweet orange essential oil 0.1%, mint essential oil 0.1%, ethanol 0.5%, and water in balance. An essential oil air sanitizer was prepared as in example 1.
Comparative example 2
The essential oils are prepared by the method of the above example, and the following raw materials are weighed according to the weight percentage: 0.1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
Comparative example 3
Cleaning fresh folium Artemisiae Argyi, placing into a steam distillation extraction instrument, adding 10 times of saturated salt solution, reflux extracting at 120 deg.C for 4 hr, collecting distillate, cooling to room temperature, separating oil and water in an oil-water separator, drying the oil layer with anhydrous sodium sulfate, and separating to obtain folium Artemisiae Argyi essential oil.
Cleaning fresh cinnamon bark, putting into a steam distillation extraction instrument, adding 10 times of saturated salt water, extracting at 120 ℃ under reflux for 4h, collecting distillate, cooling to room temperature, transferring into an oil-water separator for oil-water separation, drying the oil layer with anhydrous sodium sulfate, and separating to obtain the cinnamon essential oil.
Cleaning fresh rosemary, putting into a steam distillation extraction instrument, adding saturated salt water with the mass being 8 times of that of the rosemary, carrying out reflux extraction at 100 ℃ for 4 hours, collecting distillate, cooling to room temperature, transferring into an oil-water separator for oil-water separation, drying and separating an oil layer by anhydrous sodium sulfate to obtain rosemary essential oil.
Putting fresh cedar pine needles into a steam distillation extraction instrument, adding 10 times of saturated salt water, carrying out reflux extraction at 120 ℃ for 4 hours, collecting distillate, cooling to room temperature, transferring into an oil-water separator for oil-water separation, drying an oil layer by anhydrous sodium sulfate, and separating to obtain cedar essential oil.
Cleaning fresh sweet oranges, putting the fresh sweet oranges into a steam distillation extraction instrument, adding 10 times of saturated salt water by mass, carrying out reflux extraction at 120 ℃ for 4 hours, collecting distillate, cooling to room temperature, transferring the distillate into an oil-water separator for oil-water separation, drying an oil layer by anhydrous sodium sulfate, and separating to obtain the sweet orange essential oil.
Weighing the following raw materials in percentage by weight: 0.1% of argyi leaf essential oil, 0.1% of cinnamon essential oil, 0.2% of rosemary essential oil, 0.1% of cedar essential oil, 0.1% of sweet orange essential oil, 0.1% of mint essential oil, 0.5% of ethanol and the balance of water. An essential oil air sanitizer was prepared as in example 1.
The mint leaf essential oil in the following examples is prepared by the following method: putting fresh mint leaves into a steam distillation extraction instrument, adding 10 times of saturated salt water, extracting for 3 hours at 100 ℃ under reflux, collecting distillate, cooling to room temperature, transferring into an oil-water separator for oil-water separation, drying an oil layer by anhydrous sodium sulfate, and separating to obtain the mint leaf essential oil.
The air disinfectant and the commercially available Sansei air disinfectant provided by the above examples and comparative examples are respectively subjected to bacteriostasis experiments according to relevant regulations of GB 15979-2002 hygienic Standard for Disposable sanitary articles, and the bactericidal rates after 6h, 12h and 24h of the disinfectant are respectively detected and calculated, and the experimental results are shown in the following table 1.
TABLE 1
Figure BDA0003018042060000081
Figure BDA0003018042060000091
And (3) analyzing a test result:
comparing and analyzing the detection results of the air sterilizer obtained in the example 1, the comparative example 1 and the comparative example 2 in the table 1, it can be seen that the sterilization effect of the air sterilizer of the example 1 is obviously better than that of the air sterilizer of the comparative examples 1-2, which shows that the argyi leaf essential oil, the cinnamon essential oil, the rosemary essential oil, the cedar essential oil, the sweet orange essential oil and the mint essential oil selected by the invention have synergistic sterilization effects. The sterilizing rate of the air sterilizer in the embodiment 1 reaches 92.4% after 6 hours, and the sterilizing rate of the air sterilizer in the embodiment 1 reaches 98.1% after 24 hours, which fully shows that the air sterilizer provided by the invention has the advantages of high sterilizing efficiency and long duration.
Comparing and analyzing the detection results of the air disinfectant and the commercially available Sansei air disinfectant obtained in example 1 and comparative example 3 in Table 1, it is known that the present invention can effectively extract the bactericidal components in the cinnamon bark and cedar pine needles through the extraction process of 'reflux extraction → solid-liquid separation → concentration → freeze-drying → column filling → water, ethanol solution elution → concentration', and can effectively extract the bactericidal components in the sweet orange peel Chinese through the extraction process of 'soaking → ultrasonic extraction → concentration → freeze-drying → column filling → elution → concentration', while the steam distillation method cannot sufficiently extract the bactericidal components in the cinnamon bark, cedar pine needles and sweet orange peel, thereby affecting the bactericidal effect of the air disinfectant.
The comparative analysis of the detection results of the air sterilizer in examples 1 to 5 in table 1 shows that when the amount of the argy wormwood leaf essential oil is in the range of 0.01 to 0.1% and the sterilization time is the same, the sterilization rate of the product increases with the increase of the amount of the argy wormwood leaf essential oil, and when the amount of the argy wormwood leaf essential oil is in the range of 0.1 to 1% and the sterilization time is the same, the sterilization rate of the sterilizer does not change significantly, the comprehensive cost and the sterilization effect are good, and the preferable amount of the argy wormwood leaf essential oil is 0.1%.
The comparative analysis of the detection results of the air sterilizer in examples 1 and 6 to 8 in table 1 shows that when the dosage of the cinnamon essential oil is in the range of 0.01 to 0.1% and the sterilization time is the same, the sterilization rate of the product increases with the increase of the dosage of the cinnamon essential oil, and when the dosage of the cinnamon essential oil is in the range of 0.1 to 0.2% and the sterilization time is the same, the sterilization rate of the sterilizer has no obvious change, the comprehensive cost and the sterilization effect are good, and the cinnamon essential oil of the present invention is preferably 0.1%.
The comparative analysis of the detection results of the air sterilizer in examples 1, 2, 9 and 10 in table 1 shows that when the usage amount of rosemary essential oil is in the range of 0.2-0.3% and the sterilization time is the same, the sterilization rate of the sterilizer has no obvious change, the comprehensive cost and the sterilization effect are good, and the rosemary essential oil of the present invention is preferably 0.2%.
The comparative analysis of the detection results of the air disinfectants in the examples 1 and 11 to 12 in the table 1 shows that when the dosage of the cedar essential oil is in the range of 0.1 to 0.2 percent and the sterilization time is the same, the sterilization rate of the disinfectants has no obvious change, the comprehensive cost and the sterilization effect are good, and the cedar essential oil of the invention is preferably 0.1 percent.
Comparing and analyzing the detection results of the air disinfectants in examples 1 and 13-15 in table 1, it can be seen that when the dosage of the sweet orange essential oil is in the range of 0.01-0.1% and the sterilization time is the same, the sterilization rate of the product increases with the increase of the dosage of the sweet orange essential oil, and when the dosage of the sweet orange essential oil is in the range of 0.1-0.2% and the sterilization time is the same, the sterilization rate of the disinfectants has no obvious change, the comprehensive cost and the sterilization effect are good, and the sweet orange essential oil of the present invention is preferably 0.1%.
Comparing and analyzing the results of the tests of the air sterilizer in examples 1 and 16 to 18 in table 1, it can be seen that the sterilization rate of the product increases with the increase of the amount of the mint essential oil when the amount of the mint essential oil is in the range of 0.01 to 0.1% and the sterilization time is the same, and the sterilization rate of the sterilizer slightly decreases when the amount of the mint essential oil is in the range of 0.1 to 0.2%, and the mint essential oil of the present invention is preferably 0.1%.
The embodiments of the present invention have been described in detail, but the present invention is not limited to the described embodiments. It will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, and the scope of protection is still within the scope of the invention.

Claims (10)

1.一种芳香精油空气消杀剂，其特征在于，按重量百分比计，包括：艾叶精油0.01～1％、肉桂精油0.01～1％、迷迭香精油0.01～1％、雪松精油0.01～1％、甜橙精油0.01～1％、薄荷精油0.01～1％、有机溶剂0.1～2％、水余量。1. an aromatic essential oil air disinfectant, is characterized in that, by weight percentage, comprises: wormwood essential oil 0.01～1%, cinnamon essential oil 0.01～1%, rosemary essential oil 0.01～1%, cedar essential oil 0.01～1% %, sweet orange essential oil 0.01-1%, peppermint essential oil 0.01-1%, organic solvent 0.1-2%, water balance. 2.根据权利要求1所述的芳香精油空气消杀剂，其特征在于，所述有机溶剂选自乙醇、丙三醇中的至少一种。2. aromatic essential oil air disinfectant according to claim 1, is characterized in that, described organic solvent is selected from at least one in ethanol, glycerol. 3.根据权利要求1所述的芳香精油空气消杀剂，其特征在于，所述芳香精油空气消杀剂，按重量百分比计，包括：艾叶精油0.05～0.2％、肉桂精油0.05～0.2％、迷迭香精油0.1～0.3％、雪松精油0.05～0.2％、甜橙精油0.05～0.2％、薄荷精油0.05～0.2％、有机溶剂0.3～1％、水余量。3. The aromatic essential oil air sterilizer according to claim 1, wherein the aromatic essential oil air sterilizer, by weight percentage, comprises: 0.05-0.2% of argyi essential oil, 0.05-0.2% of cinnamon essential oil, Rosemary essential oil 0.1-0.3%, cedar essential oil 0.05-0.2%, sweet orange essential oil 0.05-0.2%, peppermint essential oil 0.05-0.2%, organic solvent 0.3-1%, water balance. 4.根据权利要求3所述的芳香精油空气消杀剂，其特征在于，所述芳香精油空气消杀剂，按重量百分比计，包括：艾叶精油0.1％、肉桂精油0.1％、迷迭香精油0.2％、雪松精油0.1％、甜橙精油0.1％、薄荷精油0.1％、有机溶剂0.5％、水余量。4. aromatic essential oil air sterilizer according to claim 3, is characterized in that, described aromatic essential oil air sterilizer, by weight percentage, comprises: Artemisia argyi essential oil 0.1%, cinnamon essential oil 0.1%, rosemary essential oil 0.2%, cedarwood essential oil 0.1%, sweet orange essential oil 0.1%, peppermint essential oil 0.1%, organic solvent 0.5%, water balance. 5.根据权利要求1所述的芳香精油空气消杀剂，其特征在于，所述艾叶精油、肉桂精油、迷迭香精油、雪松精油、甜橙精油、薄荷精油均是选用艾叶、肉桂树皮、迷迭香叶、雪松松针、香橙和薄荷叶原料依次洗净、提取、浓缩而得到的。5. aromatic essential oil air disinfectant according to claim 1, is characterized in that, described wormwood essential oil, cinnamon essential oil, rosemary essential oil, cedarwood essential oil, sweet orange essential oil, peppermint essential oil are all selected from argyi leaf, cinnamon bark , rosemary leaves, cedar pine needles, orange and mint leaves raw materials are washed, extracted and concentrated in turn. 6.根据权利要求5所述的芳香精油空气消杀剂，其特征在于，所述艾叶精油为采用下述方法制得：将新鲜的艾叶洗净后放入水蒸气蒸馏提取仪器中，加入5～15倍质量的饱和食盐水，100～120℃回流提取3～5h，收集蒸馏液，冷却至室温后，转入油水分离器中进行油水分离，油层经无水硫酸钠干燥、分离得到艾叶精油；6. aromatic essential oil air disinfectant according to claim 5, is characterized in that, described argyi leaf essential oil is to adopt the following method to make: put into steam distillation extraction apparatus after fresh argyi leaf is cleaned, add 5 ～15 times the mass of saturated brine, reflux extraction at 100～120℃ for 3～5h, collect the distillate, cool to room temperature, transfer to the oil-water separator for oil-water separation, dry the oil layer with anhydrous sodium sulfate, and separate to obtain the essential oil of Artemisia argyi ; 所述迷迭香精油为采用下述方法制得：将新鲜的迷迭香洗净后放入水蒸气蒸馏提取仪器中，加入5～15倍质量的饱和食盐水，100～120℃回流提取3～5h，收集蒸馏液，冷却至室温后，转入油水分离器中进行油水分离，油层经无水硫酸钠干燥、分离得到迷迭香精油。The rosemary essential oil is prepared by adopting the following method: after washing fresh rosemary, put it into a steam distillation extraction apparatus, add 5-15 times the mass of saturated saline, and reflux at 100-120 DEG C to extract 3 After ~5h, the distillate was collected, cooled to room temperature, transferred to an oil-water separator for oil-water separation, and the oil layer was dried over anhydrous sodium sulfate and separated to obtain rosemary essential oil. 7.根据权利要求5所述的芳香精油空气消杀剂，其特征在于，所述肉桂精油为采用下述方法制得：将新鲜的肉桂树皮洗净、晒干、粉碎后，加入质量分数为60～90％的乙醇溶液中，在100～120℃下回流2～4h，固液分离得到粗提液，将粗提液减压浓缩后冻干处理得到粗提取物，将粗提取物用水分散后，上样到大孔树脂凝胶柱，依次用水和质量分数为30～95％的乙醇溶液进行洗脱，每次洗脱时间为0.5～2h，分别收集洗脱液，将各洗脱液合并后搅拌均匀，再浓缩至原体积的1/5即得肉桂精油；7. aromatic essential oil air disinfectant according to claim 5, is characterized in that, described cinnamon essential oil is to adopt following method to make: after fresh cinnamon bark is cleaned, dried, pulverized, add mass fraction 60～90% ethanol solution, reflux at 100～120℃ for 2～4h, solid-liquid separation to obtain a crude extract, the crude extract is concentrated under reduced pressure and then freeze-dried to obtain a crude extract, and the crude extract is washed with water After dispersion, load the sample onto the macroporous resin gel column, and elute with water and ethanol solution with a mass fraction of 30-95% in sequence. After the liquids are combined, stir evenly, and then concentrate to 1/5 of the original volume to obtain cinnamon essential oil; 所述雪松精油为采用下述方法制得：将新鲜的雪松松针洗净、晒干、粉碎后，加入质量分数为70～95％的乙醇溶液中，在100～120℃下回流2～4h，固液分离得到粗提液，将粗提液减压浓缩后冻干处理得到粗提取物，将粗提取物用水分散后，上样到大孔树脂凝胶柱，依次用水和质量分数为50～95％的乙醇溶液进行洗脱，每次洗脱时间为0.5～2h，分别收集洗脱液，将各洗脱液合并后搅拌均匀，再浓缩至原体积的1/5即得雪松精油。The cedar essential oil is prepared by adopting the following method: after washing, drying and pulverizing fresh cedar pine needles, adding it into an ethanol solution with a mass fraction of 70-95%, and refluxing at 100-120 DEG C for 2-4 hours, The crude extract is obtained by solid-liquid separation, the crude extract is concentrated under reduced pressure and then freeze-dried to obtain a crude extract, after the crude extract is dispersed with water, the sample is loaded onto a macroporous resin gel column, followed by water and a mass fraction of 50- 95% ethanol solution for elution, each elution time is 0.5 to 2h, the eluents are collected separately, the eluents are combined, stirred evenly, and then concentrated to 1/5 of the original volume to obtain cedarwood essential oil. 8.根据权利要求5所述的芳香精油空气消杀剂，其特征在于，所述甜橙精油为采用下述方法制得：将新鲜的甜橙果皮放入饱和氢氧化钙水溶液中浸泡后取出并洗净后破碎；以质量分数为80～95％的乙醇溶液为溶剂，在甜橙皮破碎料的质量与乙醇溶液的体积的比为1:10～20g/mL、温度为60～80℃的条件下超声提取2～6h，过滤取滤液，滤渣按上述步骤重提两次，再将所得的提取液合并后减压浓缩后冻干处理得当粗提取物，将粗提取物用水分散后，上样到大孔树脂凝胶柱，依次用水和质量分数为30～95％的乙醇溶液进行洗脱，每次洗脱时间为0.5～2h，分别收集洗脱液，将各洗脱液合并后搅拌均匀，再浓缩至原体积的1/5即得甜橙精油。8. aromatic essential oil air disinfectant according to claim 5, is characterized in that, described sweet orange essential oil is for adopting the following method to make: fresh sweet orange peel is put into saturated calcium hydroxide aqueous solution and takes out after soaking And washed and crushed; using ethanol solution with a mass fraction of 80-95% as a solvent, the ratio of the mass of the crushed orange peel to the volume of the ethanol solution is 1:10-20g/mL, and the temperature is 60-80 ℃ Ultrasonic extraction was carried out for 2 to 6 h under the conditions of 100 ℃, filtrate was collected by filtration, and the filtrate was re-extracted twice according to the above steps. Then, the obtained extracts were combined, concentrated under reduced pressure, and lyophilized to prepare the crude extract. After dispersing the crude extract with water, Load the sample onto a macroporous resin gel column, and elute with water and 30-95% ethanol solution in sequence, each elution time is 0.5-2 h, collect the eluents separately, and combine the eluents. Stir well, and then concentrate to 1/5 of the original volume to obtain sweet orange essential oil. 9.根据权利要求5所述的芳香精油空气消杀剂，其特征在于，所述薄荷叶精油为采用下述方法制得：将新鲜的薄荷叶后放入水蒸气蒸馏提取仪器中，加入5～15倍质量的饱和食盐水，100～120℃回流提取3～5h，收集蒸馏液，冷却至室温后，转入油水分离器中进行油水分离，油层经无水硫酸钠干燥、分离即得薄荷叶精油。9. aromatic essential oil air disinfectant according to claim 5, is characterized in that, described peppermint leaf essential oil is to adopt the following method to make: put into steam distillation extraction apparatus after fresh peppermint leaf, add 5 ～15 times the mass of saturated brine, reflux extraction at 100～120℃ for 3～5h, collect the distillate, cool to room temperature, transfer to oil-water separator for oil-water separation, dry the oil layer with anhydrous sodium sulfate and separate to obtain mint Leaf essential oil. 10.一种如权利要求1～9中任一项所述的芳香精油空气消杀剂的制备方法，包括如下步骤：10. a preparation method of an aromatic essential oil air disinfectant as described in any one of claims 1 to 9, comprising the steps: (1)将艾叶精油、肉桂精油、迷迭香精油、雪松精油、甜橙精油、薄荷精油和有机溶剂混合后，在20～45℃下，以2000～8000r/min转速搅拌混合5～15min，制得植物混合精油；(1) After mixing Artemisia argyi essential oil, cinnamon essential oil, rosemary essential oil, cedar essential oil, sweet orange essential oil, peppermint essential oil and an organic solvent, at 20-45°C, stir and mix at 2000-8000 r/min for 5-15 minutes, Preparation of plant mixed essential oils; (2)将制得的植物混合精油加入水中，在20～35℃下，以2000～8000r/min转速搅拌混合5～15min，再用紫外灯照射杀菌0.5～1h即得芳香精油空气消杀剂。(2) Add the prepared plant mixed essential oil into water, stir and mix at 2000 to 8000 r/min for 5 to 15 minutes at 20 to 35°C, and then sterilize it with an ultraviolet lamp for 0.5 to 1 h to obtain an air disinfectant for aromatic essential oils. .
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113729038A (en) * 2021-07-13 2021-12-03 江西省科学院微生物研究所 Traditional Chinese medicine air disinfectant
CN114532368A (en) * 2021-04-13 2022-05-27 江西中医药大学 Aromatic essential oil air disinfectant and preparation method thereof

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103947686A (en) * 2014-04-24 2014-07-30 广东药学院 Traditional Chinese medicine air disinfectant, preparation method and application of traditional Chinese medicine air disinfectant
CN106310323A (en) * 2016-08-01 2017-01-11 淄博林森生物制品有限公司 Plant essential oil air freshener
CN106359472A (en) * 2016-08-26 2017-02-01 成都维恒医药科技有限公司 Bactericidal compound essential oil and preparation method of same
CN108371191A (en) * 2018-04-24 2018-08-07 纯美生物医药科技（上海）有限公司 A kind of air antiseptic and its preparation method and application
CN108902204A (en) * 2018-07-12 2018-11-30 佛山市汇汾化妆品科技有限公司 A kind of natural air freshener and preparation method thereof
CN111567575A (en) * 2020-05-16 2020-08-25 无锡市伙伴日化科技有限公司 Environment-friendly sterilizing and mite-killing agent and preparation method thereof
CN111887264A (en) * 2020-07-15 2020-11-06 上海驰纺材料科技有限公司 Natural plant essential oil microemulsion antibacterial spray and preparation method thereof
EP3771725A1 (en) * 2019-07-31 2021-02-03 Plastisac S.r.l. Masterbatch with antibacterial and / or antimicrobial properties

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105999341A (en) * 2016-06-02 2016-10-12 杨凌盈科中药现代化研究中心 Preparation method and application of pure natural antibacterial resuscitation-inducing air fresher
CN110859872A (en) * 2019-12-04 2020-03-06 湖北创界生物科技有限公司 Anti-inflammatory and bactericidal essential oil composition, and preparation method and application thereof
CN113080206A (en) * 2021-04-13 2021-07-09 江西中医药大学 Aromatic essential oil air disinfectant and preparation method thereof

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103947686A (en) * 2014-04-24 2014-07-30 广东药学院 Traditional Chinese medicine air disinfectant, preparation method and application of traditional Chinese medicine air disinfectant
CN106310323A (en) * 2016-08-01 2017-01-11 淄博林森生物制品有限公司 Plant essential oil air freshener
CN106359472A (en) * 2016-08-26 2017-02-01 成都维恒医药科技有限公司 Bactericidal compound essential oil and preparation method of same
CN108371191A (en) * 2018-04-24 2018-08-07 纯美生物医药科技（上海）有限公司 A kind of air antiseptic and its preparation method and application
CN108902204A (en) * 2018-07-12 2018-11-30 佛山市汇汾化妆品科技有限公司 A kind of natural air freshener and preparation method thereof
EP3771725A1 (en) * 2019-07-31 2021-02-03 Plastisac S.r.l. Masterbatch with antibacterial and / or antimicrobial properties
CN111567575A (en) * 2020-05-16 2020-08-25 无锡市伙伴日化科技有限公司 Environment-friendly sterilizing and mite-killing agent and preparation method thereof
CN111887264A (en) * 2020-07-15 2020-11-06 上海驰纺材料科技有限公司 Natural plant essential oil microemulsion antibacterial spray and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
吕飞: "天然植物精油的抑菌活性及其作用机理研究", 《中国优秀硕士学位论文全文数据库，医药卫生科技辑》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114532368A (en) * 2021-04-13 2022-05-27 江西中医药大学 Aromatic essential oil air disinfectant and preparation method thereof
CN113729038A (en) * 2021-07-13 2021-12-03 江西省科学院微生物研究所 Traditional Chinese medicine air disinfectant

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