CN112979165A - Method and process for preparing ceramic glaze - Google Patents
Method and process for preparing ceramic glaze Download PDFInfo
- Publication number
- CN112979165A CN112979165A CN202110407318.1A CN202110407318A CN112979165A CN 112979165 A CN112979165 A CN 112979165A CN 202110407318 A CN202110407318 A CN 202110407318A CN 112979165 A CN112979165 A CN 112979165A
- Authority
- CN
- China
- Prior art keywords
- parts
- mixture
- activated carbon
- ceramic particles
- zinc oxide
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- 239000000919 ceramic Substances 0.000 title claims abstract description 47
- 238000000034 method Methods 0.000 title claims abstract description 10
- 238000004519 manufacturing process Methods 0.000 title description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 36
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 36
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 32
- 238000003756 stirring Methods 0.000 claims abstract description 31
- 239000000203 mixture Substances 0.000 claims abstract description 28
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 24
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000002245 particle Substances 0.000 claims abstract description 24
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 18
- 239000011787 zinc oxide Substances 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 14
- 102000004316 Oxidoreductases Human genes 0.000 claims abstract description 12
- 108090000854 Oxidoreductases Proteins 0.000 claims abstract description 12
- DLHONNLASJQAHX-UHFFFAOYSA-N aluminum;potassium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Al+3].[Si+4].[Si+4].[Si+4].[K+] DLHONNLASJQAHX-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910021538 borax Inorganic materials 0.000 claims abstract description 12
- 229910052742 iron Inorganic materials 0.000 claims abstract description 12
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims abstract description 12
- 235000012239 silicon dioxide Nutrition 0.000 claims abstract description 12
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 12
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 12
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 12
- 238000002360 preparation method Methods 0.000 claims abstract description 10
- 239000011362 coarse particle Substances 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000011148 porous material Substances 0.000 claims description 5
- 239000002002 slurry Substances 0.000 claims description 5
- 238000007873 sieving Methods 0.000 abstract description 10
- 238000000746 purification Methods 0.000 abstract description 9
- 238000000227 grinding Methods 0.000 abstract description 5
- 238000002156 mixing Methods 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract 1
- 230000009286 beneficial effect Effects 0.000 description 2
- 229910010293 ceramic material Inorganic materials 0.000 description 2
- 238000005034 decoration Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
The invention discloses a method for preparing ceramic glaze, which consists of the following raw materials in parts by mass: 40-50 parts of silicon dioxide, 10-20 parts of potassium feldspar, 10-20 parts of titanium dioxide, 10-20 parts of aluminum oxide, 5-10 parts of zinc oxide, 1-2 parts of borax, 1-2 parts of oxidase, 3-5 parts of nano activated carbon and 50-80 parts of microporous ceramic particles; the preparation method comprises the following steps: placing silicon dioxide, potassium feldspar, titanium dioxide, aluminum oxide, zinc oxide, borax and oxidase into a ball mill for grinding and sieving, removing coarse particles, then using a high-strength iron remover for removing iron, and sieving to obtain a mixture A; mixing the nano activated carbon and the microporous ceramic particles, adding a proper amount of water, and uniformly stirring to obtain a mixture B; and finally, adding the obtained mixture A and B into a glaze slip pool and stirring. According to the invention, the raw materials are added with the microporous ceramic particles, the nano activated carbon, the titanium dioxide, the zinc oxide and other purification substance components, so that the environment purification effect is further improved.
Description
Technical Field
The invention relates to the technical field of ceramic materials, in particular to a method and a process for preparing ceramic glaze.
Background
Ceramic materials are one of the important materials used for interior decoration. The ceramic glaze is mainly used for floor and wall decoration, and some ceramic glazes used in the existing ceramics have an environment purification function, but the purification effect is not ideal and needs to be further optimized.
Disclosure of Invention
The invention aims to solve the problems that: the method and the process for preparing the ceramic glaze can increase the environmental purification function of the ceramic glaze.
The invention is realized by the following technical scheme:
the preparation method of the ceramic glaze is characterized by comprising the following raw materials in parts by mass: 40-50 parts of silicon dioxide, 10-20 parts of potassium feldspar, 10-20 parts of titanium dioxide, 10-20 parts of aluminum oxide, 5-10 parts of zinc oxide, 1-2 parts of borax, 1-2 parts of oxidase, 3-5 parts of nano activated carbon and 50-80 parts of microporous ceramic particles.
The preparation method comprises the following steps: putting silicon dioxide, potassium feldspar, titanium dioxide, aluminum oxide, zinc oxide, borax and oxidase into a ball mill for grinding for 8-10h, sieving by using a vibrating screen of 80-120 meshes, removing iron by using a high-strength iron remover after removing coarse particles, and sieving by using a vibrating screen of 200 meshes to obtain a mixture A; mixing the nano activated carbon and the microporous ceramic particles, adding a proper amount of water, and uniformly stirring to obtain a mixture B; and finally, adding the obtained mixture A and the obtained mixture B into a glaze slurry pool and stirring for 30-60min to obtain the environment-friendly ceramic glaze.
Further, the pore diameter of the microporous ceramic particle is 200-800nm, and the diameter is 10-100 μm.
Furthermore, the raw material components of the microporous ceramic particles contain at least one of titanium dioxide and zinc oxide.
Further, the stirring device after the nano activated carbon and the microporous ceramic particles are mixed is a plastic blade stirring device, the speed is 100-300 r/min, and the stirring time is 1-2 h.
Further, the stirring rate of the mixture A and the obtained mixture B was 100-300 rpm.
The invention has the beneficial effects that: according to the invention, the microporous ceramic particles are added into the raw materials, so that a microporous purification space can be added on the surface of the glaze, and the environment purification effect is improved; nano activated carbon permeates into the microporous ceramic particles, which is beneficial to improving the purification effect; the raw material itself contains the purification material components such as titanium dioxide and zinc oxide.
Detailed Description
The technical scheme of the invention is further illustrated by combining the specific examples.
Example 1: the preparation method of the ceramic glaze comprises the following raw materials in parts by mass: 40 parts of silicon dioxide, 10 parts of potassium feldspar, 10 parts of titanium dioxide, 10 parts of aluminum oxide, 5 parts of zinc oxide, 1 part of borax, 1 part of oxidase, 3 parts of nano activated carbon and 50 parts of microporous ceramic particles. The pore diameter of the microporous ceramic particles is 200-800nm, the diameter is 10-100 mu m, and the raw material components contain titanium dioxide and zinc oxide.
The preparation method comprises the following steps: putting silicon dioxide, potassium feldspar, titanium dioxide, aluminum oxide, zinc oxide, borax and oxidase into a ball mill for grinding for 8 hours, sieving by using a 80-mesh vibrating screen, removing iron by using a high-strength iron remover after removing coarse particles, and sieving by using a 200-mesh vibrating screen to obtain a mixture A; mixing the nano activated carbon and the microporous ceramic particles, adding a proper amount of water, and stirring, wherein the stirring device is a plastic blade stirring device, the speed is 100 revolutions per minute, and the stirring time is 2 hours, so as to obtain a mixture B; and finally, adding the obtained mixture A and the obtained mixture B into a glaze slurry pool, and stirring for 30min at the stirring speed of 300 revolutions per minute to obtain the environment-friendly ceramic glaze.
Example 2: the preparation method of the ceramic glaze comprises the following raw materials in parts by mass: 50 parts of silicon dioxide, 20 parts of potassium feldspar, 20 parts of titanium dioxide, 20 parts of aluminum oxide, 10 parts of zinc oxide, 2 parts of borax, 2 parts of oxidase, 5 parts of nano activated carbon and 80 parts of microporous ceramic particles. The pore diameter of the microporous ceramic particle is 200-800nm, the diameter is 10-100 μm, and the raw material components contain zinc oxide.
The preparation method comprises the following steps: placing silicon dioxide, potassium feldspar, titanium dioxide, aluminum oxide, zinc oxide, borax and oxidase into a ball mill for grinding for 10 hours, sieving by using a 120-mesh vibrating screen, removing iron by using a high-strength iron remover after removing coarse particles, and sieving by using a 200-mesh vibrating screen to obtain a mixture A; mixing the nano activated carbon and the microporous ceramic particles, adding a proper amount of water, and stirring, wherein the stirring device is a plastic blade stirring device, the speed is 300 revolutions per minute, and the stirring time is 1 hour, so as to obtain a mixture B; and finally, adding the obtained mixture A and the obtained mixture B into a glaze slurry pool, and stirring for 60min at the stirring speed of 100 revolutions per minute to obtain the environment-friendly ceramic glaze.
Example 3: the preparation method of the ceramic glaze comprises the following raw materials in parts by mass: 45 parts of silicon dioxide, 15 parts of potassium feldspar, 15 parts of titanium dioxide, 15 parts of aluminum oxide, 7.5 parts of zinc oxide, 1.5 parts of borax, 1.5 parts of oxidase, 4 parts of nano activated carbon and 65 parts of microporous ceramic particles. The pore diameter of the microporous ceramic particles is 200-800nm, the diameter is 10-100 mu m, and the raw material components contain titanium dioxide.
The preparation method comprises the following steps: putting silicon dioxide, potassium feldspar, titanium dioxide, aluminum oxide, zinc oxide, borax and oxidase into a ball mill for grinding for 9 hours, sieving by using a 100-mesh vibrating screen, removing iron by using a high-strength iron remover after coarse particles are removed, and sieving by using a 200-mesh vibrating screen to obtain a mixture A; mixing the nano activated carbon and the microporous ceramic particles, adding a proper amount of water, and stirring, wherein the stirring device is a plastic blade stirring device, the speed is 200 revolutions per minute, and the stirring time is 1.5 hours, so as to obtain a mixture B; and finally, adding the obtained mixture A and the obtained mixture B into a glaze slurry pool, and stirring for 45min at the stirring speed of 200 revolutions per minute to obtain the environment-friendly ceramic glaze.
The above embodiments are merely preferred embodiments of the present invention, which are intended to be illustrative and not limiting, and any changes, substitutions, combinations, simplifications, modifications, etc. made by those skilled in the art without departing from the spirit and principle of the present invention shall be included in the scope of the present invention.
Claims (5)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110407318.1A CN112979165A (en) | 2021-04-15 | 2021-04-15 | Method and process for preparing ceramic glaze |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110407318.1A CN112979165A (en) | 2021-04-15 | 2021-04-15 | Method and process for preparing ceramic glaze |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112979165A true CN112979165A (en) | 2021-06-18 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202110407318.1A Pending CN112979165A (en) | 2021-04-15 | 2021-04-15 | Method and process for preparing ceramic glaze |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112979165A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103408327A (en) * | 2013-08-08 | 2013-11-27 | 李涛 | Building decoration material and production method thereof |
| CN103524146A (en) * | 2013-10-26 | 2014-01-22 | 刘芳圃 | Preparation method of environment-friendly ceramic glaze capable of absorbing air pollutants |
| CN105736093A (en) * | 2016-03-02 | 2016-07-06 | 吴振华 | Multi-element nanometer rare earth catalyst motor vehicle exhaust purifier and manufacturing method thereof |
| CN106418694A (en) * | 2016-11-16 | 2017-02-22 | 广西大学 | Multifunctional ashtray |
| CN108316586A (en) * | 2018-01-30 | 2018-07-24 | 郝恩奇 | A kind of anti-pollution Ceramic Tiles and preparation method thereof having both sound absorption/adsorption function |
| CN112142329A (en) * | 2020-10-16 | 2020-12-29 | 广东永盛科技发展有限公司 | Preparation method of antibacterial self-cleaning ceramic glaze material convenient to operate |
| CN112321270A (en) * | 2020-10-26 | 2021-02-05 | 佛山市东鹏陶瓷有限公司 | Photocatalytic anion ceramic tile containing modified porous material and preparation process thereof |
-
2021
- 2021-04-15 CN CN202110407318.1A patent/CN112979165A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103408327A (en) * | 2013-08-08 | 2013-11-27 | 李涛 | Building decoration material and production method thereof |
| CN103524146A (en) * | 2013-10-26 | 2014-01-22 | 刘芳圃 | Preparation method of environment-friendly ceramic glaze capable of absorbing air pollutants |
| CN105736093A (en) * | 2016-03-02 | 2016-07-06 | 吴振华 | Multi-element nanometer rare earth catalyst motor vehicle exhaust purifier and manufacturing method thereof |
| CN106418694A (en) * | 2016-11-16 | 2017-02-22 | 广西大学 | Multifunctional ashtray |
| CN108316586A (en) * | 2018-01-30 | 2018-07-24 | 郝恩奇 | A kind of anti-pollution Ceramic Tiles and preparation method thereof having both sound absorption/adsorption function |
| CN112142329A (en) * | 2020-10-16 | 2020-12-29 | 广东永盛科技发展有限公司 | Preparation method of antibacterial self-cleaning ceramic glaze material convenient to operate |
| CN112321270A (en) * | 2020-10-26 | 2021-02-05 | 佛山市东鹏陶瓷有限公司 | Photocatalytic anion ceramic tile containing modified porous material and preparation process thereof |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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| WD01 | Invention patent application deemed withdrawn after publication | ||
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Application publication date: 20210618 |