CN111494250A - Plant lip balm and preparation method thereof - Google Patents
Plant lip balm and preparation method thereof Download PDFInfo
- Publication number
- CN111494250A CN111494250A CN202010494956.7A CN202010494956A CN111494250A CN 111494250 A CN111494250 A CN 111494250A CN 202010494956 A CN202010494956 A CN 202010494956A CN 111494250 A CN111494250 A CN 111494250A
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- China
- Prior art keywords
- oil
- parts
- wax
- esters
- lip balm
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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Classifications
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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Abstract
The application belongs to the technical field of daily chemicals, and particularly relates to a pure natural plant moisturizing lip balm and a preparation method thereof. The plant lip balm comprises the following raw materials in percentage by weight: 6-25% of natural plant wax base; 60-85% of natural vegetable oil; the balance of vegetable oil derivatives; wherein the natural plant wax base is selected from at least one of beeswax, jojoba esters, candelilla wax, carnauba wax, short myrica rubra fruit wax, and rice chaff wax. The lip balm is prepared from pure natural plant components, has outstanding moisturizing performance and good stability, and is natural and free of corrosion.
Description
Technical Field
The application belongs to the technical field of daily chemicals, and particularly relates to a plant lip balm and a preparation method thereof.
Background
The lip skin has different components with the tissues of the face, is between the skin of the body surface and the mucous membrane of the body, is a special tissue, has rich capillaries, no hair follicles and no pores, and is almost the thinnest part of the skin cuticle of the human body. Due to the special and fragile tissue structure of the lips, the lips lose moisture on their surfaces relatively quickly and are prone to dryness, chapping, etc., which requires a lip balm to provide a barrier to lock moisture and moisturize and repair the lips.
The lip balm mainly comprises a wax base and grease, most of the raw materials of the lip balm sold on the market at present contain mineral oil petrolatum, synthetic wax and synthetic grease, such as white mineral oil, vaseline, high molecular wax, microcrystalline wax, ozokerite, polyethylene wax, lanolin, phenyl trimethicone, tridecanol trimellitate and the like, and because the lip balm is frequently used every day, the raw materials containing the chemical components inevitably enter the body along with saliva or food, and generate certain irritation and sensitization on the human body.
The lip balm which is prepared by taking pure natural plant components as raw materials does not contain any colorant, essence and preservative, so that the harm to the health of a human body caused by the lip balm raw materials in the using process is reduced to the maximum extent; the lipstick has the effects of effectively fading lip wrinkles and lightening lip color, and makes the skin of the lips finer and more elastic; the product has the effects of moistening, retaining moisture, reducing moisture loss, keeping the lips moist all the time, and having beautiful color; the plant material has a natural, fresh and pleasant taste, and can give people a comfortable and refreshing feeling, and will not be disliked even after long-term use.
Disclosure of Invention
In order to solve the technical problems, the invention provides a plant lip balm, which comprises the following raw materials in percentage by weight: 6-25% of natural plant wax base; 60-85% of natural vegetable oil; the balance of vegetable oil derivatives; wherein the natural plant wax base is selected from at least one of beeswax, jojoba esters, candelilla wax, carnauba wax, short myrica rubra fruit wax, and rice chaff wax.
Preferably, the natural vegetable oil is at least one selected from the group consisting of meadowfoam seed oil, winged seed moringa seed oil, argan tree kernel oil, jojoba seed oil, Korean pine seed oil, brazil nut oil, macadamia ternifolia nut oil, walnut seed oil, shea butter, and squalane.
As a preferred technical scheme, the natural plant wax base comprises the following components in parts by weight: 2-8 parts of beeswax, 2-5 parts of jojoba esters, 1-3 parts of candelilla wax and 1-3 parts of carnauba wax.
As a preferred technical scheme, the natural vegetable oil comprises the following components in parts by weight: 10-20 parts of chinquapin seed oil, 20-30 parts of winged seed moringa seed oil, 10-15 parts of argania spinosa kernel oil and 10-15 parts of jojoba seed oil.
As a preferable technical scheme, the natural vegetable oil further comprises 1-3 parts of shea butter and 10-15 parts of squalane by weight.
As a preferable technical scheme, the melting point of the vegetable fat and oil derivative is 50-110 ℃.
As a preferable technical scheme, the vegetable oil and fat derivatives comprise 1-3 parts of hydrogenated olive oil alcohol esters and 8-12 parts of hydrogenated castor oil dimer acid esters.
As a preferable technical proposal, the hydrogenated castor oil dimer acid ester has the refractive index of more than or equal to 1.460, the hydroxyl value of 40-70(mgKOH/g) and the viscosity of 1000-1500(MPa.s/60 ℃).
As a preferred technical scheme, the melting point of the hydrogenated olive oil alcohol ester is 54-60 ℃; (ii) a Preferably, the hydrogenated olive oil alcohol esters are selected from hydrogenated olive oil lauryl alcohol esters; hydrogenated olive oil myristyl esters; at least one of hydrogenated olive oil stearyl esters.
The second aspect of the invention provides a preparation method of the lip balm, which comprises the following steps:
1) putting jojoba esters, candelilla wax, beeswax, carnauba wax and hydrogenated olive oil alcohol esters into a stirring pot, setting the temperature of the stirring pot to be 100-105 ℃, the stirring speed to be 20-30 Hz, stirring and heating to 100-105 ℃, stirring at constant temperature until the materials are completely dissolved, and then reducing the temperature to 85-90 ℃;
2) putting hydrogenated castor oil dimer acid ester, white pond flower seed oil, winged seed moringa seed oil, shea butter, squalane, argan tree kernel oil and jojoba seed oil into the stirring pot in the step 1), stirring at constant temperature until the materials are completely dissolved, cooling to 65-70 ℃, and discharging;
3) pouring into corresponding mould, filling and demoulding.
Has the advantages that: the lip balm is prepared from pure natural plant components, has outstanding moisturizing performance and good stability, and is natural and free of corrosion.
Detailed Description
In order to solve the problems, the invention provides a plant lip balm which comprises the following raw materials in percentage by weight: 6-25% of natural plant wax base; 60-85% of natural vegetable oil; the balance of vegetable oil derivatives.
Preferably, the raw materials comprise, by weight: 8-20% of natural plant wax base; 70-85% of natural vegetable oil; the balance of vegetable oil derivatives.
Wherein the natural plant wax base is selected from at least one of beeswax, jojoba esters, candelilla wax, carnauba wax, short myrica rubra fruit wax, and rice chaff wax; the natural vegetable oil is at least one selected from white Potentilla seed oil, winged seed Moringa seed oil, Aralia mandshurica Kerr kernel oil, Hoodia mexicana seed oil, Korean pine seed oil, Brazil nut oil, macadamia ternifolia oil, walnut seed oil, shea butter and squalane.
Natural plant wax base
The beeswax is a fatty substance secreted by abdominal wax glands of worker bees about two weeks old in bee colony, and the beeswax for the lipstick is obtained by removing impurities, decoloring, deodorizing and the like through a special process on the basis of original wax. The main chemical components comprise: esters (70% -72%) formed from alkanol and alkanoic acid, free fatty acid (14% -15%), hydrocarbons (12%) mainly containing saturated hydrocarbon, and also partial free fatty alcohols, water and minerals, and small amount of flavonoids, vitamins and pigments. The beeswax has good compatibility and almost has compatibility with all natural waxes and natural grease. Meanwhile, the lipstick has the characteristics of good plasticity, film forming property, adhesiveness, permeability, smoothness and the like, provides a lipstick wax base structure in the lipstick, can nourish and soften the skin and enhance the durability of products, and the purchase manufacturer of the beeswax comprises but is not limited to Guangzhou Ye male chemical engineering technology company.
The carnauba wax is a natural plant wax extracted from the leaves of the palm tree growing in northeast of the south american brazil, mainly palmitic acid, bee esters and cerotic acid. The palm wax is thin and has small viscosity, low resin content, uniform coating, good fluidity, good glossiness, high smoothness, no greasy feeling on the surface, certain softening and lubricating functions, and good emulsibility, adhesiveness, friction property, release property, smoothness and viscosity hardness adjustability. The carnauba wax vendor includes, but is not limited to, Qingdao Runkao Jiahe.
The candelilla wax is also known as candelilla wax, has a glossy waxy solid with light yellow corners, has aromatic flavor, and is a brittle and hard plant wax extracted from the bark of the candelilla shrub, which is a specialty product in northern mexico, southern texas, california, and the like. The candelilla wax contains special resin components and has strong temperature variability and the like. The lipstick mainly comprises alkyl ester, free alcohol, hydrocarbon compound, free acid and the like, and is used in a lipstick formula system, so that the heat resistance stability of a product can be improved, the overall quality of the product such as ductility, dispersibility, falling resistance and the like can be improved, meanwhile, the lipstick is endowed with bright luster and natural luster, and the lip feeling is very soft. The purchase of candelilla wax includes, but is not limited to, Wuhan Hua Bifuxiang Jieming Co.
The jojoba esters are ester products obtained by esterification of jojoba oil, have narrow melting point range, do not contain trans-fat, have high antioxidant stability, low odor and light color, and can be used as viscosity regulators in lipsticks. The purchase of jojoba esters includes, but is not limited to, Hangzhou Tuotu technologies, Inc.
As a preferred embodiment, the natural vegetable wax base comprises, in parts by weight: 2-8 parts of beeswax, 2-5 parts of jojoba esters, 1-3 parts of candelilla wax and 1-3 parts of carnauba wax.
The natural plant wax base takes beeswax as a main component, the melting point of the natural plant wax base is 62-66 ℃, and the natural plant wax base is soft in texture; and the hardness of the wax base is adjusted by matching with carnauba wax, candelilla wax and jojoba esters which have higher melting points and harder textures, so that the wax base still has proper hardness under different temperature conditions.
Natural vegetable oil
The winged seed moringa seed oil is derived from winged seed moringa seeds; the moringa seeds originate in India, are the oldest medicinal and edible plants in India, have been applied in India traditional medicine for more than 4000 years and are called as 'miracle trees'. Due to the extremely high health-preserving and medicinal values of the moringa seeds, the moringa seed oil is slowly applied to different types of cosmetics in the modern cosmetic industry. The moringa seed oil has extremely high oleic acid content and saturated fatty acid content, wherein the behenic acid is the typical saturated fatty acid of the moringa seed oil, so that the moringa seed oil without wax has excellent stability and aromatic fixity and is not easy to rancidity. In a lipstick formula system, the lipstick is endowed with the effects of softening epidermal cells, smoothing and moistening lips, removing melanin, inhibiting the generation of tyrosines and the like, and can moisten and moisturize the skin of the lips, and has the effects of sterilizing, cleaning the skin and the like.
The meadowfoam seed oil is extracted from meadowfoam, also called meadowfoam seed oil, meadowfoam seed oil and floret cauliflower extract oil, is obtained by squeezing seeds of meadowfoam, is produced from northern California, southern Oregon, Winghua and Columbia of the English genus, the meadowfoam seed oil is used in cosmetics in large quantities, particularly in a full oil system like lipstick, more than 98% of the meadowfoam seed oil structure is long chain fatty acid, does not contain easily oxidized polyunsaturated fatty acid commonly contained in other vegetable oils, dienoic acid in the meadowfoam contains non-methylene groups with interrupted double bonds at C-5 and C-13 positions, and has a special molecular structure, which gives the meadowfoam seed oil unique product performance, ① has very good antioxidant performance, is one of the most stable vegetable oils known at present, can be used as a high-efficiency natural antioxidant, gives lasting quality, can synergistically improve the performance of other vegetable oils in a lipstick formula system, increases the product performance of the formula, prolongs the product performance, locks the abundant water absorption of the skin, improves the moisture absorption rate of the skin, and helps to restore skin quality, and moisture recovery of skin, and helps to form a moisturizing skin tissue regeneration-promoting skin-repairing compound under high-temperature conditions.
The argania spinosa kernel oil is obtained by squeezing or low-temperature extraction of nuts growing on argania spinosa in Morocco, is recognized as 'liquid gold' worldwide, and is a reliable pure natural skin care raw material. Argania spinosa kernel oil is produced only in the south region of morocco, and is one of the three treasures of morocco. The argania spinosa kernel oil contains a large amount of fatty acids, sterols, vitamin E and phenolic compounds, which include a large amount of essential fatty acids, linoleic acid, unsaturated fatty acids and the like, the fatty acids maintain the hydration level of human health, the linoleic acid has obvious effects on inflammation resistance, acne reduction and moisturizing, and the lack of the unsaturated fatty acids can cause premature aging of the skin. The Aralia mandshurica kernel oil also contains rare phytosterol, the phytosterol can help to soften the skin, has high permeability on the skin, can keep the moisture on the surface of the skin, moisten and moisturize the skin, promote the metabolism of the skin, inhibit the skin inflammation, and can prevent sunburn, erythema and skin aging.
The squalane is derived from olive oil, is a natural skin-moistening oil with clear and transparent appearance, and has good oxidation resistance and thermal stability. Squalane is the main component of human sebum and sebum layer, has natural affinity with skin, is a kind of lipid closest to human sebum, can be integrated with human sebum membrane, forms a layer of natural barrier on the skin surface, can inhibit the peroxidation of skin lipid, can effectively permeate into skin, promotes the proliferation of skin basal cells, and has obvious physiological effects of delaying skin aging, improving and eliminating chloasma. Squalane can also open skin pores, promote blood circulation, promote cell metabolism, and help repair damaged cells. High purity squalane, free of any skin irritating ingredients.
Jojoba seed oil, also known as jojoba oil, is a liquid wax extracted from jojoba fruit native to mexico, which is currently grown in many countries and mainly grows in desert zones. The oil is in the form of unsaturated liquid, yellowish, stable, and high purity, and can not deteriorate and volatilize under high temperature of 285 deg.C for several times, and the jojoba seed oil component is similar to the oil on skin surface, so that it can be quickly absorbed by penetration after contacting skin, and soften stratum corneum to make skin soft and elastic.
The shea butter is a natural grease extracted from African shea butter, the appearance of the shea butter is light yellow grease, the refined shea butter is white, and the shea butter is a soft solid at normal temperature. The oil is rich in vitamin A, vitamin E, vitamin B6, protein and other elements, is relatively close to each index of sebum secretion oil of a human body, contains rich non-saponification components, is easy to be absorbed by the human body, supplements the oil lacking in epidermal cells of the human body, has the functions of moisturizing and moisturizing in cosmetics and has the function of delaying skin aging.
As a preferred embodiment, the natural vegetable oil or fat comprises, in parts by weight: 10-20 parts of chinquapin seed oil, 20-30 parts of winged seed moringa seed oil, 10-15 parts of argania spinosa kernel oil and 10-15 parts of jojoba seed oil.
More preferably, the natural vegetable oil further comprises 1-3 parts by weight of shea butter and 10-15 parts by weight of squalane.
The application effectively improves the smearing softness, spreadability, moistening degree and durability of the lip balm by reasonably selecting and matching natural vegetable oil.
Vegetable fat and oil derivatives
In a preferred embodiment, the vegetable fat and oil derivative has a melting point of 50 to 110 ℃;
preferably, the vegetable oil and fat derivatives comprise 1-3 parts by weight of hydrogenated olive oil alcohol esters and 8-12 parts by weight of hydrogenated castor oil dimer acid esters.
More preferably, the refractive index of the hydrogenated castor oil dimer acid ester is more than or equal to 1.460, the hydroxyl value is 40-70(mgKOH/g), and the viscosity is 1000-1500(MPa.s/60 ℃); more preferably, the hydrogenated castor oil dimer acid ester has a refractive index of 1.464, a hydroxyl value of 40-70mgKOH/g, and a viscosity of 1300-1500(MPa.s/60 ℃); still more preferably, the hydrogenated castor oil dimer acid ester is hydrogenated castor oil dimer linoleate, wherein the refractive index of the hydrogenated castor oil dimer acid ester is the refractive index at 20 ℃; "MPa.s/60 ℃ C" means viscosity at 60 ℃.
Still more preferably, the hydrogenated olive oil alcohol esters have a melting point of 54 to 60 ℃; the hydrogenated olive oil alcohol esters are selected from hydrogenated olive oil lauryl alcohol esters; hydrogenated olive oil myristyl esters; at least one of hydrogenated olive oil stearyl esters.
The hydrogenated olive oil stearyl alcohol ester has excellent emulsifying, dispersing and lubricating capabilities, brings silky feeling to the lipstick, and improves the texture and skin feeling of the formula; the hydrogenated castor oil dimer linoleate is a plant-derived oligomer with high viscosity and oligoester, has high glossiness and good moisturizing capability, can prevent dehydration and shrinkage, enhance the toughness of the lipstick, prevent the lipstick from breaking and sweating, and prevent solid raw materials from softening in a lipstick formula.
The stability of the lip balm can be effectively ensured by adding the vegetable oil derivative with specific components.
The natural vegetable wax base, the natural vegetable oil and the vegetable oil derivative are matched according to a proper proportion, so that the ductility and the smearing performance of the lipstick are enhanced while the hardness of the lipstick is stable, the lipstick is made of a pure natural plant source, and the lipstick has the advantages of good stability, smooth smearing, outstanding moisturizing performance and high durability.
A second aspect of the present application provides a method for preparing the plant lip gloss, comprising the steps of:
1) putting jojoba esters, candelilla wax, beeswax, carnauba wax and hydrogenated olive oil alcohol esters into a stirring pot, setting the temperature of the stirring pot to be 100-105 ℃, the stirring speed to be 20-30 Hz, stirring and heating to 100-105 ℃, stirring at constant temperature until the materials are completely dissolved, and then reducing the temperature to 85-90 ℃;
2) putting hydrogenated castor oil dimer acid ester, white pond flower seed oil, winged seed moringa seed oil, shea butter, squalane, argan tree kernel oil and jojoba seed oil into the stirring pot in the step 1), stirring at constant temperature until the materials are completely dissolved, cooling to 65-70 ℃, and discharging;
3) pouring into corresponding mould, filling and demoulding.
The present invention will be specifically described below by way of examples. It should be noted that the following examples are only for illustrating the present invention and should not be construed as limiting the scope of the present invention, and that the insubstantial modifications and adaptations of the present invention by those skilled in the art based on the above disclosure are still within the scope of the present invention.
In addition, the starting materials used are all commercially available, unless otherwise specified.
Examples
Example 1
The plant lip balm comprises the following raw materials in percentage by weight: 13% of natural plant wax base; 75% of natural vegetable oil; the balance of vegetable oil derivatives.
The natural plant wax base comprises the following components in parts by weight: 7 parts of beeswax, 4 parts of jojoba esters, 3 parts of candelilla wax and 3 parts of carnauba wax. The natural vegetable oil comprises: 20 parts of white Potentilla seed oil, 30 parts of winged seed moringa seed oil, 15 parts of Aralia mandshurica Kernel oil, 15 parts of jojoba seed oil, 2 parts of shea butter and 15 parts of squalane. The vegetable oil and fat derivative comprises 3 parts of hydrogenated olive oil stearyl alcohol esters and 12 parts of hydrogenated castor oil dilinoleate.
The beeswax is purchased from Xinya chemical Co., Ltd, Guangzhou city;
the jojoba esters are purchased from Guangzhou Sanjiya Biotechnology GmbH;
the candelilla wax is purchased from Xinya chemical industry Co., Ltd, Guangzhou city;
the carnauba wax is purchased from Xian Baichuan biological Co., Ltd;
the white Poissa seed oil is purchased from Guangzhou Sanjiya Biotechnology GmbH; the moringa oleifera seed oil is purchased from Guangzhou Sanjiya Biotechnology GmbH;
the argania spinosa kernel oil is purchased from Guangzhou Aibittrade, Inc.;
the jojoba seed oil is purchased from Guangzhou Sanjiya Biotechnology GmbH;
the shea butter is bought from Xian Baichuan biological Limited;
the squalane is purchased from Weixi Biotech, Inc., Guangzhou;
the hydrogenated olive oil stearyl esters were purchased from bomo chemical ltd, guangzhou;
the hydrogenated castor oil dimer linoleate was purchased from bomo chemical co.ltd, guangzhou;
the preparation method of the plant lip balm comprises the following steps:
1) putting jojoba esters, candelilla wax, beeswax, carnauba wax and hydrogenated olive oil stearyl alcohol esters into a stirring pot, setting the temperature of the stirring pot at 100-105 ℃, the stirring speed at 20Hz, stirring and heating to 100-105 ℃, stirring at constant temperature until the materials are completely dissolved, and then reducing the temperature to 85-90 ℃;
2) putting hydrogenated castor oil dimer linoleate, white pond flower seed oil, winged seed moringa oleifera seed oil, shea butter, squalane, argania spinosa kernel oil and jojoba seed oil into the stirring pot in the step 1), stirring at constant temperature until the materials are completely dissolved, cooling to 65-70 ℃, and discharging;
3) pouring into corresponding mould, filling and demoulding.
Example 2
The specific implementation mode of the plant lip balm is the same as that of the embodiment 1, and the difference is that the plant lip balm comprises the following raw materials in percentage by weight: 8% of natural plant wax base; 80% of natural vegetable oil; the balance of vegetable oil derivatives.
The natural plant wax base comprises the following components in parts by weight: 2 parts of beeswax, 2 parts of jojoba esters, 1 part of candelilla wax and 1 part of carnauba wax. The natural vegetable oil comprises: 10 parts of white Potentilla seed oil, 20 parts of winged seed moringa seed oil, 10 parts of Aralia mandshurica Kernel oil, 10 parts of jojoba seed oil, 1 part of shea butter and 10 parts of squalane. The vegetable oil and fat derivative comprises 1 part of hydrogenated olive oil stearyl alcohol ester and 8 parts of hydrogenated castor oil dilinoleate.
Example 3
The specific implementation mode of the plant lip balm is the same as that of the embodiment 1, and the difference is that the natural plant wax base accounts for 15 percent; 71% of natural vegetable oil; the balance of vegetable oil derivatives.
The natural plant wax base comprises the following components in parts by weight: 7 parts of beeswax, 4 parts of jojoba esters, 3 parts of candelilla wax and 3 parts of carnauba wax. The natural vegetable oil comprises: 20 parts of chinquapin seed oil, 30 parts of winged seed moringa seed oil, 15 parts of argania spinosa kernel oil and 15 parts of jojoba seed oil. The vegetable oil and fat derivative comprises 3 parts of hydrogenated olive oil stearyl alcohol esters and 12 parts of hydrogenated castor oil dilinoleate.
Comparative example 1
The specific implementation mode of the plant lip balm is the same as that in example 1, and the difference is that the plant oil and fat derivative is 15 parts by weight of hydrogenated castor oil dilinoleate.
The preparation method of the plant lip balm comprises the following steps:
1) putting jojoba esters, candelilla wax, beeswax, carnauba wax and 3 parts of hydrogenated castor oil dimer linoleate into a stirring pot, setting the temperature of the stirring pot to be 100-105 ℃, the stirring speed to be 20Hz, stirring and heating to 100-105 ℃, stirring at constant temperature until the materials are completely dissolved, and then reducing the temperature to 85-90 ℃;
2) putting 12 parts of hydrogenated castor oil dimer linoleate, white pond flower seed oil, winged seed moringa seed oil, shea butter, squalane, argan tree kernel oil and jojoba seed oil into the stirring pot in the step 1), stirring at constant temperature until the materials are completely dissolved, cooling to 65-70 ℃, and discharging;
3) pouring into corresponding mould, filling and demoulding.
Comparative example 2
The plant lip balm is similar to the embodiment 1, and is different from the embodiment 1,
the vegetable oil and fat derivative comprises 15 parts by weight of hydrogenated olive oil stearyl alcohol esters.
The preparation method of the plant lip balm comprises the following steps:
1) putting jojoba esters, candelilla wax, beeswax, carnauba wax and 3 parts of hydrogenated olive oil stearyl alcohol esters into a stirring pot, setting the temperature of the stirring pot at 100-105 ℃, the stirring speed at 20Hz, stirring and heating to 100-105 ℃, stirring at constant temperature until the materials are completely dissolved, and then reducing the temperature to 85-90 ℃;
2) putting 12 parts of hydrogenated olive oil stearyl alcohol esters, white chinquapin seed oil, winged seed moringa seed oil, shea butter, squalane, argan tree kernel oil and jojoba seed oil into the stirring pot in the step 1), stirring at constant temperature until the materials are completely dissolved, cooling to 65-70 ℃, and discharging;
3) pouring into corresponding mould, filling and demoulding.
Comparative example 3
A plant lip balm, according to the same embodiment as that of example 1, is different in that hydrogenated olive oil stearyl esters are replaced with hydrogenated olive oil hexyl esters.
Comparative example 4
The specific implementation mode of the plant lip balm is the same as that of the embodiment 1, and the difference is that the raw materials comprise: 17% of natural plant wax base; 68% of natural vegetable oil; the balance of vegetable oil derivatives.
The natural plant wax base comprises the following components in parts by weight: 7 parts of beeswax, 4 parts of jojoba esters, 3 parts of candelilla wax and 3 parts of carnauba wax. The natural vegetable oil comprises: 20 parts of white Potentilla seed oil, 0 part of winged seed moringa seed oil, 15 parts of Aralia mandshurica Kernel oil, 15 parts of jojoba seed oil, 2 parts of shea butter and 15 parts of squalane. The vegetable oil and fat derivative comprises 3 parts of hydrogenated olive oil stearyl alcohol esters and 12 parts of hydrogenated castor oil dilinoleate.
Comparative example 5
The specific implementation mode of the plant lip balm is the same as that of the embodiment 1, and the difference is that the raw materials comprise: 17% of natural plant wax base; 68% of natural vegetable oil; the balance of vegetable oil derivatives.
The vegetable oil and fat derivative comprises 8 parts of hydrogenated olive oil stearyl alcohol esters and 12 parts of hydrogenated castor oil dilinoleate.
Performance testing
1. Product stability evaluation
The conventional physicochemical index tests were performed on the lip balms of the examples and comparative examples to evaluate the stability of the products in general. Wherein the detection period of cold resistance, normal temperature, heat resistance and circulation is 30 days, and the observation is carried out once every 48 hours; the detection period of illumination is 3 days, observation is carried out once every 24 hours, and table 1 shows the physicochemical detection results. Table 2 shows the results of the peroxide number test of example 1.
TABLE 1
TABLE 2
As can be seen from the data in tables 1 and 2, the cold resistance, heat resistance, circulation, illumination and peroxide value of the lipstick prepared by the invention all meet the requirements of the national standard GB/T25613-2011, the test conditions are more severe than the national standard, and the test result is still qualified.
2. Sensory index testing
① test materials lipstick made according to the invention.
② test subjects, 240 healthy adults 18-45 years old with no history of lip skin allergy, were divided into 8 groups of 30 individuals each, meeting the test volunteer enrollment criteria.
③ trial method lips were cleaned after getting up in the morning, coated with test lipstick, observed and recorded in Table 3.
TABLE 3
As can be seen from the data in Table 3, the lipstick of the invention has higher acceptance of the indicators of moistening degree, durability, spreadability and the like of the product for the volunteers, and the skin feel is more watery.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in other forms, and any person skilled in the art may modify or change the technical content of the above disclosure into equivalent embodiments with equivalent changes, but all those simple modifications, equivalent changes and modifications made to the above embodiments according to the technical spirit of the present invention still belong to the protection scope of the present invention.
Claims (10)
1. The plant lip balm is characterized by comprising the following raw materials in percentage by weight: 6-25% of natural plant wax base; 60-85% of natural vegetable oil; the balance of vegetable oil derivatives;
wherein the natural plant wax base is selected from at least one of beeswax, jojoba esters, candelilla wax, carnauba wax, short myrica rubra fruit wax, and rice chaff wax.
2. The vegetable lip balm according to claim 1, wherein the natural vegetable oil is at least one selected from the group consisting of meadowfoam seed oil, winged seed moringa seed oil, argan nut oil, jojoba seed oil, Korean pine seed oil, brazil nut oil, macadamia ternifolia nut oil, walnut seed oil, shea butter, and squalane.
3. The botanical lip balm according to claim 1 or 2, wherein the natural botanical wax base comprises, in parts by weight: 2-8 parts of beeswax, 2-5 parts of jojoba esters, 1-3 parts of candelilla wax and 1-3 parts of carnauba wax.
4. The plant lip balm according to claim 1 or 2, wherein the natural vegetable oil comprises, in parts by weight: 10-20 parts of chinquapin seed oil, 20-30 parts of winged seed moringa seed oil, 10-15 parts of argania spinosa kernel oil and 10-15 parts of jojoba seed oil.
5. The vegetable lip balm according to claim 4, wherein the natural vegetable oil further comprises 1-3 parts by weight of shea butter and 10-15 parts by weight of squalane.
6. The vegetable lip balm according to claim 5, wherein the vegetable oil and fat derivative comprises 1 to 3 parts by weight of hydrogenated olive oil alcohol esters and 8 to 12 parts by weight of hydrogenated castor oil dimer acid esters.
7. The botanical lip gloss as in claim 6, wherein the hydrogenated castor oil dimer acid esters have a refractive index of 1.460 or more, a hydroxyl number of 40-70(mgKOH/g), and a viscosity of 1000-.
8. The botanical lip balm of claim 7, wherein the hydrogenated castor oil dimer acid ester is hydrogenated castor oil dimer linoleate.
9. The botanical lip gloss of claim 7, wherein said hydrogenated olive oil alcohol esters have a melting point of 54-60 ℃; preferably, the hydrogenated olive oil alcohol esters are selected from hydrogenated olive oil lauryl alcohol esters; hydrogenated olive oil myristyl esters; at least one of hydrogenated olive oil stearyl esters.
10. A method of preparing a lip balm according to any one of claims 6-9, comprising the steps of:
1) putting jojoba esters, candelilla wax, beeswax, carnauba wax and hydrogenated olive oil alcohol esters into a stirring pot, setting the temperature of the stirring pot to be 100-105 ℃, the stirring speed to be 20-30 Hz, stirring and heating to 100-105 ℃, stirring at constant temperature until the materials are completely dissolved, and then reducing the temperature to 85-90 ℃;
2) putting hydrogenated castor oil dimer acid ester, white pond flower seed oil, winged seed moringa seed oil, shea butter, squalane, argan tree kernel oil and jojoba seed oil into the stirring pot in the step 1), stirring at constant temperature until the materials are completely dissolved, cooling to 65-70 ℃, and discharging;
3) pouring into corresponding mould, filling and demoulding.
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| CN115957155A (en) * | 2021-10-12 | 2023-04-14 | 科丝美诗株式会社 | Non-aqueous ointment cosmetic composition containing plant-derived component |
| CN116211749A (en) * | 2023-03-10 | 2023-06-06 | 上海创美研化妆品科技有限公司 | Anti-pollution lip balm and preparation method thereof |
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| CN111494250B (en) | 2022-07-01 |
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