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CN110702148B - Preparation method and application of optical fiber sensing device capable of simultaneously distinguishing and measuring three parameters - Google Patents

Preparation method and application of optical fiber sensing device capable of simultaneously distinguishing and measuring three parameters Download PDF

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CN110702148B
CN110702148B CN201910726315.7A CN201910726315A CN110702148B CN 110702148 B CN110702148 B CN 110702148B CN 201910726315 A CN201910726315 A CN 201910726315A CN 110702148 B CN110702148 B CN 110702148B
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optical fiber
efpi
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刘颖刚
杨丹青
王钰玺
张庭
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Heze New Century Electronic Technology Co ltd
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Xian Shiyou University
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    • G01MEASURING; TESTING
    • G01DMEASURING NOT SPECIALLY ADAPTED FOR A SPECIFIC VARIABLE; ARRANGEMENTS FOR MEASURING TWO OR MORE VARIABLES NOT COVERED IN A SINGLE OTHER SUBCLASS; TARIFF METERING APPARATUS; MEASURING OR TESTING NOT OTHERWISE PROVIDED FOR
    • G01D5/00Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable
    • G01D5/26Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light
    • G01D5/268Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light using optical fibres

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Abstract

A three-parameter simultaneous differential measurement optical fiber sensor preparation method and application, a section of standard single mode fiber Bragg grating with the total length of a grid region about 15mm, which is inscribed by 193nm excimer laser, is cut into two small sections in the grid region by an optical fiber cutter, so that the grating with uniform refractive index modulation is damaged; respectively fixing two small sections of gratings on a left optical fiber fixing clamp and a right optical fiber fixing clamp of a fusion splicer, and aligning the two sections of gratings in a manual adjusting mode of the fusion splicer and adjusting the two sections of gratings to a proper interval; another section of optical fiber is taken, the tail end of the optical fiber is stripped off a distance coating layer and cleaned by alcohol, and then a small drop of photosensitive glue is dipped and dropped into the gap between the two fixed sections of optical gratings; and irradiating the photosensitive glue by using an ultraviolet curing lamp to cure the photosensitive glue to form a photosensitive glue cavity, thereby introducing structural phase shift. The invention can effectively realize the distinguishing measurement of temperature, pressure and refractive index according to the spectral characteristics of the structural phase shift, and the method has simple operation process and lower cost.

Description

一种三参量同时区分测量光纤传感器件的制备方法及应用A preparation method and application of a three-parameter simultaneous differential measurement optical fiber sensor device

技术领域technical field

本发明涉及光纤传感器件技术领域,特别涉及一种三参量同时区分测量光纤传感器制备方法及应用。The invention relates to the technical field of optical fiber sensor devices, in particular to a preparation method and application of a three-parameter simultaneous differential measurement optical fiber sensor.

背景技术Background technique

将光纤用作传感器件时,它可以直接或间接的测量多个物理量,譬如拉力、压 强、温度、折射率、湿度等等。但是,随着周围环境的日益复杂多变,对单一物理 量的变化的检测已经不能满足人们的测量需求。因此,设计并制作一种可以实现多 参量、多功能的传感器件已经成为光纤传感技术的研究热点。When an optical fiber is used as a sensing device, it can directly or indirectly measure several physical quantities, such as tension, pressure, temperature, refractive index, humidity, and so on. However, with the increasingly complex and changeable surrounding environment, the detection of changes in a single physical quantity can no longer meet people's measurement needs. Therefore, designing and fabricating a sensor device that can realize multi-parameter and multi-function has become a research hotspot of optical fiber sensing technology.

基于光学干涉原理制作的干涉型光纤传感器,特别是光纤法布里-珀罗干涉仪(FPI),因其结构灵活多样、高反射率、低损耗等优点被广泛的应用于光纤传感检 测等领域。制作光纤干涉型法布里-珀罗结构的方式类型可分为:全光纤F-P腔结构 的本征型干涉仪(IFPI)和借助其他材料或物体(如毛细管、陶瓷套芯等)构成F-P 腔结构的非本征型干涉仪(EFPI)。目前,利用基于全光纤的FPI和光纤光栅的集 成结构传感器来实现温度与压强、温度与折射率、温度与位移、温度与湿度等的双 参量同时区分测量的技术已经非常成熟,但是其响应灵敏度也仅限于光纤水平,且 制作成本较高。以上这些双参量区分测量的原理多是采用温度补偿法,即集成传感 器中的结构——光纤光栅,对压强、折射率等不敏感,在测量时可以用作温度补偿。 同时,双或多参量区分测量,交叉敏感效应又是一个本征问题。Interferometric fiber optic sensors based on the principle of optical interference, especially fiber Fabry-Perot interferometers (FPI), are widely used in fiber optic sensing and detection due to their flexible and diverse structures, high reflectivity, and low loss. field. The methods of fabricating optical fiber interference Fabry-Perot structures can be divided into: Intrinsic Interferometer (IFPI) with all-fiber F-P cavity structure and F-P cavity with the help of other materials or objects (such as capillaries, ceramic cores, etc.) Structural Extrinsic Interferometer (EFPI). At present, the technology of using the integrated structure sensor based on all-fiber FPI and fiber grating to realize the simultaneous differential measurement of temperature and pressure, temperature and refractive index, temperature and displacement, temperature and humidity is very mature, but its response sensitivity It is also limited to the optical fiber level, and the production cost is high. The principle of the above two-parameter differential measurement is mostly the temperature compensation method, that is, the structure in the integrated sensor, the fiber grating, is not sensitive to pressure, refractive index, etc., and can be used as temperature compensation during measurement. At the same time, dual or multi-parameter discriminating measurement, cross-sensitivity effect is an intrinsic problem.

发明内容SUMMARY OF THE INVENTION

为了解决以上技术问题,本发明的目的在于提供一种三参量同时区分测量光纤传感器制备方法及应用,通过在光纤光栅中间位置使用感光胶制作F-P腔,引入结 构相移,根据结构相移的光谱特点可有效实现温度、压强和折射率的区分测量,此 方法操作工艺简单、成本较低。In order to solve the above technical problems, the purpose of the present invention is to provide a preparation method and application of a three-parameter simultaneous differential measurement optical fiber sensor, by using photoreceptor in the middle position of the fiber grating to make an F-P cavity, introducing a structural phase shift, according to the spectrum of the structural phase shift The characteristics can effectively realize the differential measurement of temperature, pressure and refractive index, and the method is simple in operation and low in cost.

为了实现上述目的,本发明采用的技术方案是:In order to achieve the above object, the technical scheme adopted in the present invention is:

一种三参量同时区分测量光纤传感器的制备方法,包括以下步骤;A preparation method of a three-parameter simultaneous differential measurement optical fiber sensor, comprising the following steps;

步骤一:将一段采用193nm准分子激光器刻写的栅区总长度为15mm的标准单模 光纤布拉格光栅以光纤切刀在栅区切断分为两小段,导致均匀折射率调制的光栅被 破坏;Step 1: a standard single-mode fiber Bragg grating with a grating region total length of 15mm written by a 193nm excimer laser is cut into two small sections with a fiber cutter in the grating region, resulting in the destruction of the grating with uniform refractive index modulation;

步骤二:将两小段光栅分别固定在熔接机的左右两个光纤固定夹上,然后通过 熔接机手动调节模式对齐两段光栅,并调整间距为50到100um以便得到较好的干涉 谱图;Step 2: Fix the two small sections of gratings on the left and right optical fiber clamps of the fusion splicer respectively, then align the two sections of gratings through the manual adjustment mode of the fusion splicer, and adjust the spacing to be 50 to 100um in order to obtain a better interference spectrum;

步骤三:另取一段光纤,将其末端剥去一段距离涂覆层并用酒精擦洗干净,然 后蘸取一小滴感光胶使其滴在固定好的两段光栅(如步骤二所述)的缝隙中;Step 3: Take another piece of optical fiber, strip the end of the coating for a distance and clean it with alcohol, and then dip a small drop of photosensitive glue into the gap between the two fixed gratings (as described in step 2) middle;

步骤四:使用紫外固化灯照射感光胶,使感光胶固化形成感光胶腔,从而引入 结构相移,得到了一种基于非本征FPI和相移光栅的集成传感器。Step 4: Irradiate the photoresist with an ultraviolet curing lamp to cure the photoresist to form a photoresist cavity, thereby introducing a structural phase shift, and obtaining an integrated sensor based on extrinsic FPI and phase shift grating.

所述的紫外固化灯照射感光胶5分钟,以提高感光胶腔的强度。The ultraviolet curing lamp irradiates the photosensitive adhesive for 5 minutes, so as to improve the strength of the photosensitive adhesive cavity.

所述的光纤切刀在栅区大约中间位置被切断分为两小段。The fiber cutter is cut into two small sections at about the middle of the grid region.

一种三参量同时区分测量光纤传感器的应用,本装置应用于对温度、压强和折 射率这三个参量的同时区分测量;An application of a three-parameter simultaneous differential measurement of an optical fiber sensor, the device is applied to the simultaneous differential measurement of the three parameters of temperature, pressure and refractive index;

所述的光纤传感器有两个反射面,分别为反射面1与反射面2,都是光纤与感光 胶的交界面,入射光经过光纤光栅被部分反射,剩余的光继续向前传播,到达反射面1再次被反射部分,剩余的光继续向前传播然后通过折射率约为1.5、长度约为57um 的感光胶腔被反射面2反射部分光,剩余光继续向前传播而在此被光纤光栅部分反 射,光经过密闭EFPI两个反射面反射后,由于不同光程差引起的相位延迟不同,在 输出端产生干涉图样,由于反射面反射率较低,可以忽略多光束反射,因此,输出 光强近似为在这两个腔中形成的干涉,输出光强度为:The optical fiber sensor has two reflective surfaces, namely reflective surface 1 and reflective surface 2, which are the interface between the optical fiber and the photosensitive adhesive. The incident light is partially reflected by the fiber grating, and the remaining light continues to propagate forward, reaching the reflection. The surface 1 is reflected again, and the remaining light continues to propagate forward, and then passes through the photosensitive glue cavity with a refractive index of about 1.5 and a length of about 57um. Part of the light is reflected by the reflective surface 2, and the remaining light continues to propagate forward and is captured by the fiber grating here. Partial reflection, after the light is reflected by the two reflective surfaces of the airtight EFPI, the phase delay caused by different optical path differences is different, and an interference pattern is generated at the output end. Due to the low reflectivity of the reflective surface, multi-beam reflection can be ignored. Therefore, the output light The strong approximation is the interference formed in these two cavities, and the output light intensity is:

Figure BDA0002159061030000031
Figure BDA0002159061030000031

其中,I为输出光强;I1和I2分别为入射光在密闭EFPI腔体端面处的反射光强;

Figure BDA0002159061030000032
为干涉的初始相位;n为密闭EFPI腔的折射率;λ为光学波长;L为密闭EFPI的腔 长,因此,腔体的光学长度可以计算为:Among them, I is the output light intensity; I 1 and I 2 are the reflected light intensity of the incident light at the end face of the closed EFPI cavity, respectively;
Figure BDA0002159061030000032
is the initial phase of interference; n is the refractive index of the sealed EFPI cavity; λ is the optical wavelength; L is the cavity length of the sealed EFPI, so the optical length of the cavity can be calculated as:

Figure BDA0002159061030000033
Figure BDA0002159061030000033

式中,λ1和λ2为密闭EFPI干涉光谱中相邻两个波谷的波长,密闭EFPI谱中的自 由光谱范围(FSR)可以表示为:where λ 1 and λ 2 are the wavelengths of two adjacent valleys in the sealed EFPI interference spectrum, and the free spectral range (FSR) in the sealed EFPI spectrum can be expressed as:

Figure BDA0002159061030000034
Figure BDA0002159061030000034

传输矩阵法被广泛应用于相移光纤光栅等非均匀光纤光栅的光波场计算,因此采用该方法对通过在栅区制作密闭EFPI而引入的结构相移的过程中的光谱特性进行 分析.由于引入结构相移时,相位相对延迟,需在光栅相移前加入负号,相移矩阵为:The transmission matrix method is widely used in the calculation of the optical wave field of non-uniform fiber gratings such as phase-shifted fiber gratings. Therefore, this method is used to analyze the spectral characteristics of the phase shift of the structure introduced by making a closed EFPI in the grating region. When the structure is phase shifted, the phase is relatively delayed, and a negative sign needs to be added before the phase shift of the grating. The phase shift matrix is:

Figure BDA0002159061030000035
Figure BDA0002159061030000035

式中

Figure BDA0002159061030000036
表示相移量的大小;in the formula
Figure BDA0002159061030000036
Indicates the magnitude of the phase shift;

通过测量密闭EFPI光谱的波长漂移(ΔλEFPI)、结构相移光谱的功率变化(ΔKPS)和波长漂移(ΔλPS),可以利用灵敏度系数矩阵实现对温度、压强和折射率这三个参 量的同时区分测量,设温度、压强和折射率的变化量为ΔT,ΔP和Δn,则其灵敏度 矩阵可表示为:By measuring the wavelength shift (Δλ EFPI ), the power change (ΔK PS ), and the wavelength shift (Δλ PS ) of the structural phase-shift spectrum in the confinement EFPI spectrum, the sensitivity coefficient matrix can be used to realize the three parameters of temperature, pressure and refractive index. At the same time, the measurement is distinguished, and the changes of temperature, pressure and refractive index are set as ΔT, ΔP and Δn, then the sensitivity matrix can be expressed as:

Figure BDA0002159061030000041
Figure BDA0002159061030000041

式中,S1n、S1T和S1P为密闭EFPI波长漂移随折射率、温度、压力变化的灵敏 度;S2n、S2T和S2P为结构相移波长漂移随被测量变化的灵敏度;,S3n、S3T和S3P为 结构相移功率漂移随测量值变化的灵敏度。通过矩阵的逆运算可以得到被测量的三 个物理量的变化量为:In the formula, S 1n , S 1T and S 1P are the sensitivities of the sealed EFPI wavelength drift with the change of refractive index, temperature and pressure; S 2n , S 2T and S 2P are the sensitivities of the structural phase shift wavelength drift with the measured change; , S 3n , S 3T and S 3P are the sensitivities of the structural phase shift power drift to the measured value. Through the inverse operation of the matrix, the changes of the three physical quantities to be measured can be obtained as:

Figure BDA0002159061030000042
Figure BDA0002159061030000042

式中

Figure BDA0002159061030000043
in the formula
Figure BDA0002159061030000043

是灵敏度系数矩阵的行列式;is the determinant of the sensitivity coefficient matrix;

将以上实验测量结果代入式(6),可以得到:Substituting the above experimental measurement results into formula (6), we can get:

Figure BDA0002159061030000044
Figure BDA0002159061030000044

至此,可以有效实现对温度、压强和折射率这三个参量的同时区分测量。So far, the simultaneous differential measurement of the three parameters of temperature, pressure and refractive index can be effectively achieved.

本发明的有益效果:Beneficial effects of the present invention:

第一,本发明制作的密闭EFPI是使用感光胶固化形成的,突破了光纤传感器灵 敏度仅局限于光纤的问题;第二,通过在栅区制备EFPI结构而引入结构相移,为相 移光栅的制作提出了一种新思路;第三,F-P腔长是通过调整固定在熔接机固定夹左 右两端的两小段光栅之间的缝隙确定的,所以其腔体长度可灵活、精确的控制。第 四,可以实现温度、压强和折射率三参量的同时区分测量并且灵敏度高、成本低廉, 在光纤传感检测领域具有很重要的研究意义。First, the airtight EFPI made by the present invention is formed by curing with photosensitive glue, which breaks through the problem that the sensitivity of the optical fiber sensor is limited to the optical fiber; A new idea is proposed for production; thirdly, the length of the F-P cavity is determined by adjusting the gap between the two small gratings fixed at the left and right ends of the welding machine clamp, so the cavity length can be flexibly and precisely controlled. Fourth, it can realize the simultaneous differential measurement of the three parameters of temperature, pressure and refractive index, with high sensitivity and low cost, which has very important research significance in the field of optical fiber sensing and detection.

附图说明Description of drawings

图1是一根标准单模光纤光栅大约在栅区中间位置被切断示意图。Figure 1 is a schematic diagram of a standard single-mode fiber grating cut at about the middle of the grating region.

图2是将被切断的两段光栅固定在熔接机的光纤固定夹上的示意图。Fig. 2 is a schematic diagram of fixing the cut-off two-segment grating on the optical fiber fixing clip of the fusion splicer.

图3是另取一根单模光纤并蘸取感光胶滴在两段光栅缝隙的示意图。Figure 3 is a schematic diagram of taking another single-mode optical fiber and dipping the photosensitive glue into the gap of two gratings.

图4是使用紫外固化灯照射固化两段光栅缝隙的感光胶的示意图。FIG. 4 is a schematic diagram of a photosensitive adhesive for curing two grating gaps by irradiation with an ultraviolet curing lamp.

图5是集成传感器的显微图像。Figure 5 is a microscopic image of the integrated sensor.

图6是集成传感器测量实验装置的示意图。Figure 6 is a schematic diagram of the integrated sensor measurement experimental setup.

图7是集成传感器对温度的响应光谱图。Figure 7 is a spectral graph of the response of the integrated sensor to temperature.

图8是25℃时放大的结构相移光栅的反射光谱图。Figure 8 is an enlarged reflection spectrum of the structured phase-shift grating at 25°C.

图9是40℃时放大的结构相移光栅的反射光谱图。Figure 9 is an enlarged reflection spectrum of the structured phase-shift grating at 40°C.

图10是50℃时放大的结构相移光栅的反射光谱图。Figure 10 is an enlarged reflection spectrum of the structured phase-shift grating at 50°C.

图11是密闭EFPI波长漂移随温度变化的线性拟合曲线图。Figure 11 is a linear fit plot of the wavelength drift of a sealed EFPI as a function of temperature.

图12是结构相移波长漂移随温度变化的线性拟合曲线图。FIG. 12 is a linear fitting graph of the wavelength shift of the structural phase shift as a function of temperature.

图13是结构相移功率漂移随温度变化的线性拟合曲线图。FIG. 13 is a linear fit curve of structural phase shift power drift as a function of temperature.

图14是集成传感器对压强的响应光谱图。Figure 14 is a spectral graph of the response of the integrated sensor to pressure.

图15是增加压强时放大的结构相移光栅的反射光谱图。Figure 15 is an enlarged reflection spectrum of a structured phase-shift grating with increasing pressure.

图16是密闭EFPI波长漂移随压强变化的线性拟合曲线图。Figure 16 is a linear fit plot of the wavelength drift of a sealed EFPI as a function of pressure.

图17是集成传感器对折射率的响应光谱图。Figure 17 is a spectral graph of the response of the integrated sensor to the refractive index.

图18是折射率为1.3342时放大的结构相移光栅的反射光谱图。Figure 18 is an enlarged reflection spectrum of a structured phase-shift grating with a refractive index of 1.3342.

图19是折射率为1.3388时放大的结构相移光栅的反射光谱图。Figure 19 is a magnified reflection spectrum of a structured phase-shift grating with a refractive index of 1.3388.

图20是折射率为1.3478时放大的结构相移光栅的反射光谱图。Figure 20 is a magnified reflection spectrum of a structured phase-shift grating at a refractive index of 1.3478.

图21是密闭EFPI波长漂移随折射率变化的线性拟合曲线图。Figure 21 is a linear fit plot of the wavelength shift of a sealed EFPI as a function of refractive index.

图22是结构相移光栅功率漂移随折射率变化的线性拟合曲线图。FIG. 22 is a linear fitting graph of the power drift of a structured phase-shift grating as a function of refractive index.

具体实施方式Detailed ways

下面结合附图对本发明作进一步详细说明。The present invention will be further described in detail below in conjunction with the accompanying drawings.

传感器制备的技术方案包括以下四个步骤:The technical scheme of sensor preparation includes the following four steps:

步骤一:一段采用193nm准分子激光器刻写的栅区总长度约为15mm的标准单模 光纤布拉格光栅被光纤切刀(FITEL S326)在栅区大约中间位置被切断分为两小段, 导致均匀折射率调制的光栅被破坏,如图1所示。;Step 1: A standard single-mode fiber Bragg grating with a total length of about 15mm in the gate region written by a 193nm excimer laser is cut into two small sections by a fiber cutter (FITEL S326) at about the middle of the gate region, resulting in a uniform refractive index The modulated grating is destroyed, as shown in Figure 1. ;

步骤二:将两小段光栅分别固定在熔接机(古河FITELS177)的左右两个光纤 固定夹上,然后通过熔接机手动调节模式对齐两段光栅并调整至合适间距。因为FPI 自由普范围与腔长成反比,所以较小的腔体长度约为L=57um被调节确定,如图2所 示;Step 2: Fix the two small gratings on the left and right optical fiber clips of the fusion splicer (Furukawa FITELS177), then align the two gratings with the manual adjustment mode of the fusion splicer and adjust the distance to a suitable distance. Because the free general range of FPI is inversely proportional to the cavity length, the smaller cavity length is adjusted to be about L=57um, as shown in Figure 2;

步骤三:另取一段光纤,将其末端剥去一段距离涂覆层并用酒精擦洗干净,然 后蘸取一小滴感光胶(AUSBONDA332)使其滴在固定好的两段光栅(如步骤二所述)的 缝隙中,如图3所示;Step 3: Take another piece of optical fiber, strip the end of the coating for a distance and clean it with alcohol, then dip a small drop of photosensitive glue (AUSBONDA332) on the two fixed gratings (as described in step 2). ) in the gap, as shown in Figure 3;

步骤四:使用紫外固化灯照射感光胶约5分钟,使感光胶固化形成感光胶腔, 而引入结构相移,如图4所示。图8所示为在光学显微镜下看到的集成传感器的显 微图,在图中结构相移图像是不可见的。Step 4: Irradiate the photosensitive adhesive with a UV curing lamp for about 5 minutes, so that the photosensitive adhesive is cured to form a photosensitive adhesive cavity, and a structural phase shift is introduced, as shown in FIG. 4 . Figure 8 shows a micrograph of the integrated sensor seen under an optical microscope, where the structural phase-shift image is not visible.

本发明提出一种三参量同时区分测量光纤传感器制备方法。所用的光纤为普通标准单模光纤;写栅设备为193nm准分子激光器;熔接机的作用是对齐被切断的两 小段光栅以及调整确定F-P腔体长度,起微位移调节平台的作用而不做熔接光纤光 栅使用;实验中制作密闭EFPI的是高透明、高强度的感光胶AUSBONDA332;实验中解 调设备是SM125解调仪,是微米光学国际公司生产。The invention provides a preparation method of a three-parameter simultaneous differential measurement optical fiber sensor. The optical fiber used is an ordinary standard single-mode fiber; the writing grating device is a 193nm excimer laser; the function of the fusion splicer is to align the two small sections of grating that are cut off and adjust the length of the F-P cavity, which acts as a micro-displacement adjustment platform without welding. The fiber grating is used; in the experiment, the airtight EFPI is made of high-transparency and high-strength photosensitive adhesive AUSBONDA332; the demodulation equipment in the experiment is SM125 demodulator, which is produced by Micron Optics International Company.

全光纤型FPI的灵敏度局限于光纤水平,因此,本发明通过固化感光胶形成EFPI,可以有效提高光纤F-P腔的测量灵敏度;本发明中的EFPI是在折射率均匀调制的光 纤光栅的栅区大约中间位置制作的,打破了光栅的均匀折射率调制而引入结构相移, 这对相移光栅的研究制作具有一定的意义;本发明制备的光纤传感器成本低廉,但 制作出的传感光谱质量高,与标准F-P腔光谱相当;发明给出了栅区制作EFPI集成 光纤传感器制备技术,并初步对温度、压强和折射率进行的较高灵敏度测试,进而 实现对这三个物理量的同时区分测量,这对较高灵敏度的可实现三参量同时区分测 量的光纤传感器件的研制提供一定的技术支持。The sensitivity of the all-fiber type FPI is limited to the level of the optical fiber. Therefore, the invention can effectively improve the measurement sensitivity of the fiber F-P cavity by curing the photosensitive adhesive to form the EFPI; It is made in the middle position, which breaks the uniform refractive index modulation of the grating and introduces the structural phase shift, which has certain significance for the research and manufacture of the phase-shift grating; the fiber sensor prepared by the invention has low cost, but the produced sensing spectrum has high quality , which is equivalent to the standard F-P cavity spectrum; the invention provides the preparation technology of EFPI integrated optical fiber sensor in the gate area, and conducts a preliminary high sensitivity test on temperature, pressure and refractive index, and then realizes the simultaneous differential measurement of these three physical quantities, This provides a certain technical support for the development of a fiber-optic sensor device with high sensitivity that can realize the simultaneous differential measurement of three parameters.

本发明提出的集成传感器的制备过程中特别需要注意的是:①感光胶具有高透明度,即较高的反射率,因此为了成功的引入较好的结构相移光谱,光栅应在栅区 大约中间位置被切断制作感光胶腔;②感光胶尽管可快速固化,但是为了提高其固 化强度,可适当增加固化时间,约5分钟左右;③通过熔接机手动调节模式调节被 切断的两段光栅间的缝隙距离即腔体长度时,在可获得F-P干涉谱的前提下,间距 不宜过长,以免损坏感光胶腔;In the preparation process of the integrated sensor proposed by the present invention, special attention should be paid to: (1) The photoresist has high transparency, that is, high reflectivity. Therefore, in order to successfully introduce a better structural phase shift spectrum, the grating should be about the middle of the gate area. The position is cut off to make the photosensitive glue cavity; ②The photosensitive glue can be cured quickly, but in order to improve its curing strength, the curing time can be appropriately increased, about 5 minutes; When the gap distance is the length of the cavity, on the premise that the F-P interference spectrum can be obtained, the spacing should not be too long, so as not to damage the photosensitive glue cavity;

传感原理与区分测量:Sensing principle and discriminating measurement:

传感器工作基本原理是由于外界环境参数变化,譬如温度、压强和折射率等物 理参量的改变,促使密闭EFPI腔长发生改变,进而影响结构相移的相移点位置或相 移量的大小发生变化,最后结果如实验光谱所反应的密闭EFPI的反射光谱产生漂移, 且结构相移的波长和功率也产生一定的线性变化,达到传感作用并实现三参量区分 测量。The basic working principle of the sensor is that due to changes in external environmental parameters, such as changes in physical parameters such as temperature, pressure and refractive index, the length of the sealed EFPI cavity changes, which in turn affects the position of the phase shift point or the magnitude of the phase shift of the structure. , the final result is that the reflection spectrum of the closed EFPI reflected by the experimental spectrum drifts, and the wavelength and power of the structural phase shift also produce a certain linear change, which achieves the sensing effect and realizes the three-parameter discrimination measurement.

本发明制备出的集成光纤传感器,是将一段完整的光纤光栅在栅区大约中间位置被切断分为两小段光栅后,被固定在熔接机上且通过手动调节模式可方便控制两 小段光栅之间的缝隙即腔长,从而实现实验所需要的自由谱个数,用感光胶填充此 缝隙固化后形成了密闭EFPI。The integrated optical fiber sensor prepared by the invention is that after a complete optical fiber grating is cut into two small gratings at about the middle position of the grating area, it is fixed on the fusion splicer, and the mode between the two small gratings can be easily controlled by manually adjusting the mode. The gap is the length of the cavity, so as to achieve the number of free spectra required for the experiment, and the gap is filled with photosensitive adhesive to form a closed EFPI after curing.

以下实验室数据全部建立在如图5所示的传感器之上,The following laboratory data are all based on the sensor shown in Figure 5,

该光纤传感器有两个反射面,都是光纤与感光胶的交界面。入射光经过光纤光 栅被部分反射,剩余的光继续向前传播,到达反射面1再次被反射部分,剩余的光继 续向前传播然后通过折射率约为1.5、长度约为57um的感光胶腔被反射面2反射部 分光,剩余光继续向前传播而在此被光纤光栅部分反射。光经过密闭EFPI两个反射 面反射后,由于不同光程差引起的相位延迟不同,在输出端产生干涉图样。由于反 射面反射率较低,可以忽略多光束反射。因此,输出光强近似为在这两个腔中形成的 干涉,输出光强度为:The optical fiber sensor has two reflective surfaces, both of which are the interface between the optical fiber and the photosensitive glue. The incident light is partially reflected by the fiber grating, the remaining light continues to propagate forward, reaches the reflecting surface 1 and is reflected again, the remaining light continues to propagate forward and then passes through the photosensitive glue cavity with a refractive index of about 1.5 and a length of about 57um. The reflection surface 2 reflects part of the light, and the remaining light continues to propagate forward and is partially reflected by the fiber grating. After the light is reflected by the two reflective surfaces of the sealed EFPI, the phase delay caused by different optical path differences is different, and an interference pattern is generated at the output end. Due to the low reflectivity of the reflective surface, multi-beam reflections can be ignored. Therefore, the output light intensity is approximated by the interference formed in these two cavities, and the output light intensity is:

Figure BDA0002159061030000081
Figure BDA0002159061030000081

其中,I为输出光强;I1和I2分别为入射光在密闭EFPI腔体端面处的反射光强;

Figure BDA0002159061030000082
为干涉的初始相位;n为密闭EFPI腔的折射率;λ为光学波长;L为密闭EFPI的腔 长。因此,腔体的光学长度可以计算为:Among them, I is the output light intensity; I 1 and I 2 are the reflected light intensity of the incident light at the end face of the closed EFPI cavity, respectively;
Figure BDA0002159061030000082
is the initial phase of interference; n is the refractive index of the sealed EFPI cavity; λ is the optical wavelength; L is the cavity length of the sealed EFPI. Therefore, the optical length of the cavity can be calculated as:

Figure BDA0002159061030000083
Figure BDA0002159061030000083

式中,λ1和λ2为密闭EFPI干涉光谱中相邻两个波谷的波长。密闭EFPI谱中的自 由光谱范围(FSR)可以表示为:In the formula, λ 1 and λ 2 are the wavelengths of two adjacent valleys in the closed EFPI interference spectrum. The free spectral range (FSR) in a confined EFPI spectrum can be expressed as:

Figure BDA0002159061030000084
Figure BDA0002159061030000084

传输矩阵法被广泛应用于相移光纤光栅等非均匀光纤光栅的光波场计算,因此采用该方法对通过在栅区制作密闭EFPI而引入的结构相移的过程中的光谱特性进行 分析.由于引入结构相移时,相位相对延迟,需在光栅相移前加入负号,相移矩阵为:The transmission matrix method is widely used in the calculation of the optical wave field of non-uniform fiber gratings such as phase-shifted fiber gratings. Therefore, this method is used to analyze the spectral characteristics of the phase shift of the structure introduced by making a closed EFPI in the grating region. When the structure is phase shifted, the phase is relatively delayed, and a negative sign needs to be added before the phase shift of the grating. The phase shift matrix is:

Figure BDA0002159061030000091
Figure BDA0002159061030000091

式中

Figure BDA0002159061030000092
表示相移量的大小。in the formula
Figure BDA0002159061030000092
Indicates the magnitude of the phase shift.

集成传感器测量装置如图6所示,测量精度为1pm的SM125解调仪一端连接计 算机,另一端连接传感器。当将传感器置于不同的测量环境时,其光谱变化可通过 计算机获取。The integrated sensor measurement device is shown in Figure 6. One end of the SM125 demodulator with a measurement accuracy of 1pm is connected to the computer, and the other end is connected to the sensor. When the sensor is placed in different measurement environments, its spectral changes can be acquired by a computer.

图10是传感器在常压下,温度变化为25℃、30℃、35℃、40℃、45℃和50℃ 的反射谱,其中密闭EFPI光谱的红移可以明显的看到。为了明显观察温度变化对结 构相移的影响,选取了在25℃、40℃和50℃下具有代表性的几个光谱并将其放大, 如图11、12和13所示,可以看到结构相移的透射窗口的波长右移、功率减小。如 图14、15和16所示,是对不同温度下的光谱漂移量进行线性拟合,得到了密闭EFPI 光谱波长漂移对温度响应灵敏度为0.3076nm/℃,相比于裸光纤F-P的温度响应灵 敏度提高了30多倍,同时结构相移的波长漂移和功率变化对温度也表现出6.2pm/℃ 和-0.2299dB/℃的响应灵敏度。Figure 10 shows the reflectance spectra of the sensor under normal pressure with temperature changes of 25°C, 30°C, 35°C, 40°C, 45°C and 50°C, where the red shift of the closed EFPI spectrum can be clearly seen. In order to clearly observe the effect of temperature change on the phase shift of the structure, several representative spectra at 25 °C, 40 °C and 50 °C were selected and enlarged, as shown in Figures 11, 12 and 13, the structure can be seen The wavelength of the phase-shifted transmission window is shifted to the right and the power is reduced. As shown in Figures 14, 15 and 16, the spectral drift at different temperatures is linearly fitted, and the sensitivity of the spectral wavelength drift of the sealed EFPI to temperature response is 0.3076nm/℃, compared with the temperature response of the bare fiber F-P The sensitivity is improved by more than 30 times, and the wavelength shift and power change of the structural phase shift also show a response sensitivity of 6.2pm/℃ and -0.2299dB/℃ to temperature.

如图17所示,是传感器在压强从0MPa-1.2MPa变化时的反射谱。插图是放大 的密闭EFPI的光谱,其中可以看到光谱逐渐向长波方向移动,证明传感器在高压环 境下也可以正常工作。图18是传感器应用于压强后,放大了的结构相移的光谱。可 以看出,对传感器施加压强,结构相移光谱几乎没有变化,这是因为施加压强产生 的折射率变化并没有引起相移量的变化。对施加不同压强下密闭EFPI光谱的波长漂 移进行线性拟合,得到了其对压强的响应灵敏度为0.81nm/MPa,如图19所示。As shown in Figure 17, it is the reflectance spectrum of the sensor when the pressure varies from 0 MPa to 1.2 MPa. The inset is a zoomed-in spectrum of the confined EFPI, where the spectrum can be seen to gradually shift towards longer wavelengths, proving that the sensor works well under high pressure. Figure 18 is an amplified spectrum of the structural phase shift after the sensor is applied to pressure. It can be seen that when pressure is applied to the sensor, the phase shift spectrum of the structure has almost no change, because the change in the refractive index caused by the applied pressure does not cause a change in the amount of phase shift. The wavelength shift of the sealed EFPI spectrum under different pressures was linearly fitted, and the response sensitivity to pressure was obtained as 0.81 nm/MPa, as shown in Figure 19.

结构相移发生的变化归根结底是因为折射率的变化,因此对该集成传感器又进行折射率试验。将传感器置于一系列折射率值分别为1.3342,1.3360,1.3373, 1.3388,1.3408,1.3418,1.3438,1.3438,1.3450,1.3466,1.3478的蔗 糖溶液中,得到的传感器的响应光谱如图20所示。插图是放大了的密闭EFPI的光 谱,可以看到其反射谱亦是往长波方向漂移。此外,为了明显观察不同浓度的蔗糖 溶液对结构相移光谱的影响,选取了在折射率为1.3342、1.3388和1.3478时具有 代表性的结构相移的光谱,并将其放大,如图21、22所示。可以看到结构相移光谱 的功率逐渐减小,但其波长几乎没有移动。对不同折射率溶液变化时密闭EFPI光谱 的波长漂移进行线性拟合,得到了其对折射率溶液的响应灵敏度为355.03nm/RIU。 此外,结构相移的功率变化对折射率的响应灵敏度为319.82dB/nm。The change in the structural phase shift is ultimately due to the change in the refractive index, so the integrated sensor was again subjected to refractive index experiments. The sensor was placed in a series of sucrose solutions with refractive index values of 1.3342, 1.3360, 1.3373, 1.3388, 1.3408, 1.3418, 1.3438, 1.3438, 1.3450, 1.3466, and 1.3478, respectively. The response spectrum of the sensor obtained is shown in Figure 20. The inset is the magnified spectrum of the confined EFPI, and it can be seen that its reflection spectrum also shifts to the longer wavelength. In addition, in order to clearly observe the effect of different concentrations of sucrose solution on the structural phase shift spectra, the representative structural phase shift spectra at refractive indices of 1.3342, 1.3388 and 1.3478 were selected and enlarged, as shown in Figures 21 and 22 shown. It can be seen that the power of the structural phase-shift spectrum gradually decreases, but its wavelength hardly shifts. The wavelength shift of the sealed EFPI spectrum when the solution with different refractive index changes was linearly fitted, and the response sensitivity to the solution with different refractive index was obtained as 355.03 nm/RIU. In addition, the response sensitivity of the power change of the structural phase shift to the refractive index is 319.82 dB/nm.

通过测量密闭EFPI光谱的波长漂移(ΔλEFPI)、结构相移光谱的功率变化(ΔKPS)和波长漂移(ΔλPS),可以利用灵敏度系数矩阵实现对温度、压强和折射率这三个参 量的同时区分测量。设温度、压强和折射率的变化量为ΔT,ΔP和Δn,则其灵敏度 矩阵可表示为:By measuring the wavelength shift (Δλ EFPI ), the power change (ΔK PS ), and the wavelength shift (Δλ PS ) of the structural phase-shift spectrum in the confinement EFPI spectrum, the sensitivity coefficient matrix can be used to realize the three parameters of temperature, pressure and refractive index. Also differentiate measurements. Assuming that the changes of temperature, pressure and refractive index are ΔT, ΔP and Δn, the sensitivity matrix can be expressed as:

Figure BDA0002159061030000101
Figure BDA0002159061030000101

式中,S1n、S1T和S1P为密闭EFPI波长漂移随折射率、温度、压力变化的灵敏 度;S2n、S2T和S2P为结构相移波长漂移随被测量变化的灵敏度;,S3n、S3T和S3P为 结构相移功率漂移随测量值变化的灵敏度。通过矩阵的逆运算可以得到被测量的三 个物理量的变化量为:In the formula, S 1n , S 1T and S 1P are the sensitivities of the sealed EFPI wavelength drift with the change of refractive index, temperature and pressure; S 2n , S 2T and S 2P are the sensitivities of the structural phase shift wavelength drift with the measured change; , S 3n , S 3T and S 3P are the sensitivities of the structural phase shift power drift to the measured value. Through the inverse operation of the matrix, the changes of the three physical quantities to be measured can be obtained as:

Figure BDA0002159061030000111
Figure BDA0002159061030000111

式中

Figure BDA0002159061030000112
in the formula
Figure BDA0002159061030000112

是灵敏度系数矩阵的行列式。is the determinant of the sensitivity coefficient matrix.

将以上实验测量结果代入式(6),可以得到:Substituting the above experimental measurement results into equation (6), we can get:

Figure BDA0002159061030000113
Figure BDA0002159061030000113

至此,可以有效实现对温度、压强和折射率这三个参量的同时区分测量。So far, the simultaneous differential measurement of the three parameters of temperature, pressure and refractive index can be effectively achieved.

本发明在以往的双参量测量传感器的制作方法的基础上,在一根光纤光栅的大约中间位置使用感光胶制作密闭F-P腔。因此,具有均匀折射率调制的光纤光栅被 破坏,而引入一结构相移。实验验证该集成传感器对温度、压强和折射率的响应特 性。结果表明,与全光纤FPI相比,由感光胶制作的密闭FPI的灵敏度显著提高。 更重要的是,在实验过程中,结构相移对温度、压强和折射率也表现出一定的规律 的响应特点,因此可以有效解决交叉敏感问题,实现三参量的同时区分测量。On the basis of the conventional manufacturing method of the dual-parameter measuring sensor, the invention uses photosensitive glue to manufacture a closed F-P cavity at about the middle position of an optical fiber grating. Thus, the fiber grating with uniform index modulation is destroyed, introducing a structural phase shift. Experiments verify the response characteristics of the integrated sensor to temperature, pressure and refractive index. The results show that the sensitivity of the hermetic FPI fabricated from photoresist is significantly improved compared to the all-fiber FPI. More importantly, during the experiment, the structural phase shift also showed a certain regular response characteristics to temperature, pressure and refractive index, so it can effectively solve the problem of cross-sensitivity and realize the simultaneous and differentiated measurement of three parameters.

Claims (1)

1.一种三参量同时区分测量光纤传感器制备方法,其特征在于,包括以下步骤;1. A method for preparing a three-parameter measurement optical fiber sensor is characterized in that, comprising the following steps; 步骤一:将一段采用193nm准分子激光器刻写的栅区总长度为15mm的标准单模光纤布拉格光栅以光纤切刀在栅区切断分为两小段,导致均匀折射率调制的光栅被破坏;Step 1: Divide a standard single-mode fiber Bragg grating with a total length of 15mm in the grating region written by a 193nm excimer laser into two small sections with a fiber cutter in the grating region, resulting in the destruction of the grating with uniform refractive index modulation; 步骤二:将两小段光栅分别固定在熔接机的左右两个光纤固定夹上,然后通过熔接机手动调节模式对齐两段光栅并调整至间距为50到100um;Step 2: Fix the two small sections of grating on the left and right optical fiber fixing clips of the fusion splicer respectively, and then align the two sections of the grating through the manual adjustment mode of the fusion splicer and adjust the distance to a distance of 50 to 100um; 步骤三:另取一段光纤,将其末端剥去一段距离涂覆层并用酒精擦洗干净,然后蘸取一小滴感光胶使其滴在固定好的两段光栅(如步骤二所述)的缝隙中;Step 3: Take another piece of optical fiber, strip the end of the coating for a distance and clean it with alcohol, and then dip a small drop of photosensitive glue into the gap between the two fixed gratings (as described in step 2) middle; 步骤四:使用紫外固化灯照射感光胶,使感光胶固化形成感光胶腔,而引入结构相移;Step 4: Irradiate the photosensitive adhesive with a UV curing lamp, so that the photosensitive adhesive is cured to form a photosensitive adhesive cavity, and a structural phase shift is introduced; 所述的紫外固化灯照射感光胶5分钟,以提高感光胶腔的强度;The ultraviolet curing lamp irradiates the photosensitive glue for 5 minutes, so as to improve the strength of the photosensitive glue cavity; 所述的光纤切刀在栅区大约中间位置被切断分为两小段;The optical fiber cutter is cut into two small sections at about the middle position of the gate area; 通过本方法制备的装置应用于对温度、压强和折射率这三个参量的同时区分测量;The device prepared by this method is applied to the simultaneous differential measurement of the three parameters of temperature, pressure and refractive index; 所述的光纤传感器有两个反射面,分别为第一反射面(1)与第二反射面(2),都是光纤与感光胶的交界面,入射光经过光纤光栅被部分反射,剩余的光继续向前传播,到达第一反射面(1)再次被反射部分,剩余的光继续向前传播然后通过折射率约为1.5、长度约为57um的感光胶腔被第二反射面(2)反射部分光,剩余光继续向前传播而在此被光纤光栅部分反射,光经过密闭EFPI两个反射面反射后,由于不同光程差引起的相位延迟不同,在输出端产生干涉图样,由于反射面反射率较低,可以忽略多光束反射,因此,输出光强近似为在这两个腔中形成的干涉,输出光强度为:The optical fiber sensor has two reflection surfaces, namely a first reflection surface (1) and a second reflection surface (2), both of which are the interface between the optical fiber and the photosensitive adhesive. The incident light is partially reflected by the fiber grating, and the remaining The light continues to propagate forward and reaches the first reflecting surface (1) to be reflected again. The remaining light continues to propagate forward and then passes through the photosensitive glue cavity with a refractive index of about 1.5 and a length of about 57um and is reflected by the second reflecting surface (2). Part of the light is reflected, and the remaining light continues to propagate forward and is partially reflected by the fiber grating. After the light is reflected by the two reflecting surfaces of the sealed EFPI, the phase delay caused by different optical path differences is different, and an interference pattern is generated at the output end. The surface reflectivity is low, and multi-beam reflections can be ignored, so the output light intensity is approximated by the interference formed in these two cavities, and the output light intensity is:
Figure FDA0003536100610000021
Figure FDA0003536100610000021
其中,I为输出光强;I1和I2分别为入射光在密闭EFPI腔体端面处的反射光强;
Figure FDA0003536100610000022
为干涉的初始相位;n为密闭EFPI腔的折射率;λ为光学波长;L为密闭EFPI的腔长,因此,腔体的光学长度可以计算为:
Among them, I is the output light intensity; I 1 and I 2 are the reflected light intensity of the incident light at the end face of the closed EFPI cavity, respectively;
Figure FDA0003536100610000022
is the initial phase of interference; n is the refractive index of the sealed EFPI cavity; λ is the optical wavelength; L is the cavity length of the sealed EFPI, so the optical length of the cavity can be calculated as:
Figure FDA0003536100610000023
Figure FDA0003536100610000023
式中,λ1和λ2为密闭EFPI干涉光谱中相邻两个波谷的波长,密闭EFPI谱中的自由光谱范围(FSR)可以表示为:where λ 1 and λ 2 are the wavelengths of two adjacent valleys in the sealed EFPI interference spectrum, and the free spectral range (FSR) in the sealed EFPI spectrum can be expressed as:
Figure FDA0003536100610000024
Figure FDA0003536100610000024
传输矩阵法被广泛应用于相移光纤光栅等非均匀光纤光栅的光波场计算,因此采用该方法对通过在栅区制作密闭EFPI而引入的结构相移的过程中的光谱特性进行分析,由于引入结构相移时,相位相对延迟,需在光栅相移前加入负号,相移矩阵为:The transmission matrix method is widely used in the calculation of the optical wave field of non-uniform fiber gratings such as phase-shifted fiber gratings. Therefore, this method is used to analyze the spectral characteristics of the structural phase shift introduced by making a closed EFPI in the grating region. When the structure is phase shifted, the phase is relatively delayed, and a negative sign needs to be added before the phase shift of the grating. The phase shift matrix is:
Figure FDA0003536100610000025
Figure FDA0003536100610000025
式中
Figure FDA0003536100610000026
表示相移量的大小;
in the formula
Figure FDA0003536100610000026
Indicates the magnitude of the phase shift;
通过测量密闭EFPI光谱的波长漂移(ΔλEFPI)、结构相移光谱的功率变化(ΔKPS)和波长漂移(ΔλPS),可以利用灵敏度系数矩阵实现对温度、压强和折射率这三个参量的同时区分测量,设温度、压强和折射率的变化量为ΔT,ΔP和Δn,则其灵敏度矩阵可表示为:By measuring the wavelength shift (Δλ EFPI ), the power change (ΔK PS ), and the wavelength shift (Δλ PS ) of the structural phase-shift spectrum in the confinement EFPI spectrum, the sensitivity coefficient matrix can be used to realize the three parameters of temperature, pressure and refractive index. At the same time, the measurement is distinguished, and the changes of temperature, pressure and refractive index are set as ΔT, ΔP and Δn, then the sensitivity matrix can be expressed as:
Figure FDA0003536100610000031
Figure FDA0003536100610000031
式中,S1n、S1T和S1P为密闭EFPI波长漂移随折射率、温度、压力变化的灵敏度;S2n、S2T和S2P为结构相移波长漂移随被测量变化的灵敏度;S3n、S3T和S3P为结构相移功率漂移随测量值变化的灵敏度,通过矩阵的逆运算可以得到被测量的三个物理量的变化量为:In the formula, S 1n , S 1T and S 1P are the sensitivities of the sealed EFPI wavelength drift with the change of refractive index, temperature and pressure; S 2n , S 2T and S 2P are the sensitivities of the structural phase shift wavelength drift with the measured change; S 3n , S 3T and S 3P are the sensitivities of the structural phase shift power drift with the change of the measured value. Through the inverse operation of the matrix, the changes of the three measured physical quantities can be obtained as follows:
Figure FDA0003536100610000032
Figure FDA0003536100610000032
式中
Figure FDA0003536100610000033
in the formula
Figure FDA0003536100610000033
是灵敏度系数矩阵的行列式;is the determinant of the sensitivity coefficient matrix; 将以上实验测量结果代入式(6),可以得到:Substituting the above experimental measurement results into formula (6), we can get:
Figure FDA0003536100610000034
Figure FDA0003536100610000034
实现对温度、压强和折射率这三个参量的同时区分测量。Simultaneous and differentiated measurement of the three parameters of temperature, pressure and refractive index is achieved.
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