CN110302094A - A kind of non-sticky cup lip glaze of high glaze and preparation method thereof - Google Patents
A kind of non-sticky cup lip glaze of high glaze and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/895—Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The present invention provides non-sticky cup lip glaze of a kind of high glaze and preparation method thereof, belong to cosmetic field.The non-sticky cup lip glaze of high glaze of the present invention is oil-in-water system, include following components in percentage by weight: the ethyl cellulose A of 0.1-10%, the ethyl cellulose B of 0.1-10%, and 0.1-30% dimethyl silicone polymer and Dimethicone/Vinyl Dimethicone cross-linked polymer mixture, it can be formed uniformly in lip, lightweight, it is smooth, it is soft, it moistens, glossiness is high, the film of good water-proof effect, and there is excellent non-sticky cup performance, again by being used in compounding the oil-soluble colorant of water-soluble colorant and discoloration, make lip glaze that there is excellent colouring persistence, furthermore, the non-sticky cup lip glaze preparation process of high glaze of the present invention is simple, it is easy to industrialized production.
Description
Technical field
The invention belongs to cosmetic technical fields, and in particular to a kind of non-sticky cup lip glaze of high glaze and preparation method thereof.
Background technique
By making up to lip, can make one complexion becomes ruddy glossy, but lip Cosmetics product is mostly oily wax body at present
System, there is a problem of following aspects:
(1) it moistens glossiness lipstick or the generally existing easily de- adornment of lip glaze, adornment imitates unabiding problem, and persistently non-sticky cup
Lipstick or lip glaze be generally dumb light cloudy surface, moisten degree it is poor；
(2) lipstick or lip glaze of oily wax body system can form closure oil film in lip, easily bring greasy and heavy feeling, and
Seldom it can give lip real moisturizing by moisture absorption；
(3) currently on the market almost without not only with high glaze, but also the lip product of the lasting non-sticky cup of energy.
In view of the above technical problems, applicant tests and tests by a large amount of, has developed and not only moistens degree height, gloss
Degree is high, and the lip product of the lasting non-sticky cup of energy.
Summary of the invention
It is an object of the invention to overcome drawbacks described above in the prior art, provide a kind of high glaze non-sticky cup lip glaze and
Preparation method.
To achieve the above object, the technical solution adopted by the present invention are as follows:
In a first aspect, being oil-in-water system the present invention provides a kind of non-sticky cup lip glaze of high glaze, comprising following heavy
Measure the component of percentage: poly- the two of the ethyl cellulose B and 0.1-30% of ethyl cellulose A, 0.1-10% of 0.1-10%
The mixture of methylsiloxane and Dimethicone/Vinyl Dimethicone cross-linked polymer, the ethyl are fine
Dimension element A, ethyl cellulose B use the solution that the Compound mixed solution of toluene and ethyl alcohol is 5% at mass fraction respectively, measure at 25 DEG C
Viscosity is respectively 3-5.5mPas, 90-110mPas, and the mass ratio of toluene and ethyl alcohol is 4 in the mixed liquor of toluene and ethyl alcohol:
1, in the mixture of the dimethyl silicone polymer and Dimethicone/Vinyl Dimethicone cross-linked polymer
The mass ratio of dimethyl silicone polymer and Dimethicone/Vinyl Dimethicone cross-linked polymer is 80-90:
10-20；Preferably, it is calculated on the basis of the total weight of the lip glaze, ethyl cellulose A accounts for 3%, and ethyl cellulose B is accounted for
1.5%, the mixture of dimethyl silicone polymer and Dimethicone/Vinyl Dimethicone cross-linked polymer accounts for
15%.Ethyl cellulose A can make to give skin moisturizing, provide long-acting moistening effect；Ethyl cellulose A and ethyl cellulose B is multiple
With use, it is possible to provide uniform, lightweight, smooth, waterproofness and all good film of persistence can be used as barrier, slow down lip
Moisture evaporation be formed by film compared with traditional film forming agent trimethyl silicane alkoxy esters of silicon acis or hydrogenated polycyclopentadiene
It is soft more preferable；The mixing of dimethyl silicone polymer and Dimethicone/Vinyl Dimethicone cross-linked polymer
Object glossiness is high, there is certain film-formation result, can provide good silk sliding skin sense；When lip glaze be oil-in-water system, and contain weight
Percentage is respectively the poly- diformazan of the ethyl cellulose B and 0.1-30% of ethyl cellulose A, 0.1-10% of 0.1-10%
When the mixture of radical siloxane and Dimethicone/Vinyl Dimethicone cross-linked polymer, because of poly dimethyl
The mixture of siloxanes and Dimethicone/Vinyl Dimethicone cross-linked polymer and ethyl cellulose A, second
Base cellulose B is incompatible, lip glaze can be made to generate extraordinary non-sticky cup effect, especially when on the basis of the total weight of the lip glaze
It calculates, ethyl cellulose A accounts for 3%, and ethyl cellulose B accounts for 1.5%, dimethyl silicone polymer and dimethyl silicone polymer/ethylene
When the mixture of base Dimethicone Crosspolymer accounts for 15%, the non-sticky cup effect of lip glaze is more preferable.
Preferably, the lip glaze also includes water-soluble colorant, oil-soluble colorant, emulsifier and water, water-soluble coloring
Agent includes the mixture of CI 45410, CI 15510 and CI 77891 and sodium alginate, and oil-soluble colorant includes CI
45380；It is calculated on the basis of the total weight of the lip glaze, CI 45410 accounts for 0.01-3%, and CI 15510 accounts for 0.01-3%, CI
77891 and the mixture of sodium alginate account for 0.01-10%, CI 45380 accounts for 0.01-2%, and emulsifier accounts for 0.11-20%, and water accounts for
20-60%, wherein the weight ratio of CI 77891 and sodium alginate is 97:3.Opposite oil-based system and water-in-oil system, lip glaze are adopted
With oil-in-water system, when smearing, can be more frivolous and salubrious；CI 45410, CI 15510 and CI 77891 and sodium alginate
Mixture is water-soluble colorant, is added to water phase, and compared to the colorant in oily phase, tinting strength, tinting power is not only strong but also lasting；CI 45380
For the oil-soluble colorant that changes colour, it is added in oily phase, certain color changeable effect can be provided；By CI 45410, the CI in water phase
The mixture of 15510 and CI 77891 and sodium alginate is compounded with the CI 45380 in oily phase, can be effectively improved on product
The persistence of color.Wherein, CI 45410 is acid red 92, and CI 15510 is acid orange 7, and CI 77891 is titanium dioxide, CI
45380 be acid red 87.
Preferably, it being calculated on the basis of the total weight of the lip glaze, CI 45410 accounts for 0.6%, CI 15510 and accounts for 0.6%,
The mixture of CI 77891 and sodium alginate accounts for 0.4%, CI 45380 altogether and accounts for 1%.
Preferably, the emulsifier includes laruyl alcohol sodium sulfovinate, the smooth stearate of sorb and sucrose cocounut oil acid esters；With institute
It states and calculates on the basis of the total weight of lip glaze, laruyl alcohol sodium sulfovinate accounts for 0.01-5%, the smooth stearate of sorb and sucrose coconut oil
Ester accounts for 0.1-15% altogether；It is further preferred that laruyl alcohol sodium sulfovinate accounts for 0.3-5%, the smooth stearate of sorb and sucrose cocounut oil
Acid esters accounts for 3-15% altogether.Applicant has found the dimethyl silicone polymer and dimethyl silicone polymer/second by a large amount of test
The mixture and laruyl alcohol sodium sulfovinate, the smooth stearate of sorb, sucrose cocounut oil of alkenyl Dimethicone Crosspolymer
Acid esters is incompatible, when the lip glaze makees emulsifier with laruyl alcohol sodium sulfovinate, the smooth stearate of sorb and sucrose cocounut oil acid esters
When, the non-sticky cup effect of lip glaze can be further promoted, is especially calculated when on the basis of the total weight of the lip glaze, laruyl alcohol sulfuric acid
Ester sodium accounts for 0.3-5%, and when the smooth stearate of sorb and sucrose cocounut oil acid esters account for 3-15% altogether, the non-sticky cup effect of lip glaze is obtained greatly
It is promoted to amplitude, non-sticky cup testing evaluation is at 9 points or more.
Preferably, the lip glaze also includes moisturizer, and moisturizer includes the glycerol for accounting for lip glaze weight 1-15%.Glycerol can be with
Moisture in product or air combines, and keeps the skin wet directly to lip；It will not pass through as the traditional pure oily wax body system of lip glaze
Closure oil film keeps adornment sense greasy thick and heavy to be retained.
Preferably, the lip glaze also includes thickener, and thickener includes the hydroxypropyl melon for accounting for lip glaze weight 0.1-2%
Glue.Hydroxypropyl melon rubber can not only thicken, and improve the viscosity of product, there are also certain film forming and moisture retention, can with product or
Moisture in air combines, and keeps the skin wet directly to lip.
Preferably, the lip glaze also includes emollient and preservative, and emollient includes to account for lip glaze weight 5-60%'s respectively
The cetanol of octyl dodecanol and 0.01-10%, preservative include account for respectively the glycerol caprylate of lip glaze weight 0.05-1% with
And 0.05-1% Phenoxyethanol and Sensiva SC50 mixture.
Preferably, the lip glaze also includes following components in percentage by weight: the CI of 0.6% CI 45410,0.6%
15510, the mixture of 0.4% CI 77891 and sodium alginate, 1% CI 45380,0.3% laruyl alcohol sodium sulfovinate,
The smooth stearate of 3% sorb and the mixture of sucrose cocounut oil acid esters, 4% glycerol, 0.2% hydroxypropyl melon rubber, 31%
Octyl dodecanol, 1% cetanol, 0.3% glycerol caprylate, 0.3% Phenoxyethanol and Sensiva SC50 it is mixed
The water of object and 37.8% is closed, wherein the weight ratio of the smooth stearate of sorb and sucrose cocounut oil acid esters is 82.5:17.5, benzene oxygen second
The weight ratio of pure and mild Sensiva SC50 is 9:1.The lip glaze water content is up to 37.8%, is tied to form this more than traditional oily wax body
It is low.
Second aspect, the present invention provides a kind of preparation methods of above-mentioned lip glaze comprising following steps:
(1) ethyl cellulose A, ethyl cellulose B, CI 45380 and part octyl dodecanol are mixed, is heated to 90-95
DEG C, until being completely dissolved and being uniformly mixed, heat preservation obtains A phase materials for stirring；By laruyl alcohol sodium sulfovinate, cetanol and part
Water mixing, is heated to 90-95 DEG C, stirs to after being completely dissolved, and is slowly added to the A phase materials while stirring, and stirring is until mixed
It closes uniformly, obtains B phase materials；The smooth stearate of sorb, sucrose cocounut oil acid esters and remaining octyl dodecanol have been heated to again
After fully dissolved, under the conditions of 90-95 DEG C, it is added in the B phase materials while stirring, then sequentially adds poly dimethyl silicon
The mixture and glycerol caprylate of oxygen alkane and Dimethicone/Vinyl Dimethicone cross-linked polymer, stirring
Uniformly obtain C phase materials；
(2) the mixture stirring and dissolving of remaining water, CI 45410, CI 15510 and CI77891 and mosanom is complete
Entirely, glycerol and hydroxypropyl melon rubber are added later, under 1000-3000rpm revolving speed homogeneous to no particle, be completely dispersed it is uniform,
Obtain D phase materials；
(3) under 300-800rpm revolving speed, while stirring by the mixed of D phase materials and Phenoxyethanol and Sensiva SC50
It closes object to be added in the C phase materials, later the homogeneous uniform under 1000-3000rpm revolving speed again, be filled after then cooling to room temperature
Dress is to get the lip glaze.
Compared with prior art, the present invention has the following advantages and beneficial effects:
(1) the non-sticky cup lip glaze of high glaze of the present invention can form uniform, lightweight, smooth, soft, moist, gloss in lip
The film of degree height, good water-proof effect, and there is excellent non-sticky cup performance, good usage experience can be brought to user.
(2) the non-sticky cup lip glaze of high glaze of the present invention makes water-soluble colorant and the oil-soluble colorant of discoloration compounding
With effectively improving the colouring ability of lip glaze and the persistence of colouring.
(3) the non-sticky cup lip glaze of high glaze of the present invention has effects that moisture absorption by addition glycerol, hydroxypropyl melon rubber etc.
Ingredient can keep the skin wet directly to lip, and dressing is salubriouser.
(4) the non-sticky cup lip glaze water content of high glaze of the present invention can substantially reduce formulation cost up to 37.8% or more,
Keep lip glaze cost performance higher, there is better application prospect.
(5) the preparation method simple process of the non-sticky cup lip glaze of high glaze of the present invention, condition is controllable, is easy to industrial metaplasia
It produces.
Detailed description of the invention
Fig. 1 is that the non-sticky cup of lip glaze in embodiment 2 tests photo；
Fig. 2 is that the non-sticky cup of lipstick in comparative example 5 tests photo；
Fig. 3 is that the non-sticky cup of lip glaze in comparative example 6 tests photo.
Specific embodiment
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention
It is described further.
Embodiment 1-8
Embodiment 1-8 is a kind of embodiment of the non-sticky cup lip glaze of high glaze of the present invention, the composition of these lip glaze such as table 1
Shown, wherein ethyl cellulose A is the ETHOCEL purchased from Dow ChemicalTMStd 4Premium, ethyl cellulose B are
ETHOCEL purchased from Dow ChemicalTMEthyl cellulose A, ethyl cellulose B are used first by Std 100Premium respectively
The solution that the Compound mixed solution of benzene and ethyl alcohol is 5% at mass fraction, measuring viscosity at 25 DEG C is respectively 3-5.5mPas, 90-
The mass ratio of toluene and ethyl alcohol is 4:1 in the mixed liquor of 110mPas, toluene and ethyl alcohol；Dimethyl silicone polymer and poly- diformazan
Dimethyl silicone polymer and polydimethylsiloxanes in radical siloxane/vinyl dimethicone cross polymer mixture
Alkane/vinyl dimethicone cross polymer mass ratio is 80-90:10-20；CI 77891 and sodium alginate it is mixed
Closing the weight ratio of CI 77891 and sodium alginate in object is 97:3, in the mixture of the smooth stearate of sorb and sucrose cocounut oil acid esters
The weight ratio of the smooth stearate of sorb and sucrose cocounut oil acid esters is 82.5:17.5, the mixing of Phenoxyethanol and Sensiva SC50
The weight ratio of Phenoxyethanol and Sensiva SC50 is 9:1 in object.
Composition/% of lip glaze in 1 embodiment 1-8 of table
Lip glaze in embodiment 1-8 is made by the steps:
(1) ethyl cellulose A, ethyl cellulose B, CI 45380 and part octyl dodecanol are mixed, is heated to 90-95
DEG C, until being completely dissolved and being uniformly mixed, heat preservation obtains A phase materials for stirring；By laruyl alcohol sodium sulfovinate, cetanol and part
Water mixing, is heated to 90-95 DEG C, stirs to after being completely dissolved, and is slowly added to the A phase materials while stirring, and stirring is until mixed
It closes uniformly, obtains B phase materials；Again by the smooth stearate of sorb, sucrose cocounut oil acid esters and remaining octyl dodecanol Hybrid Heating
It to 75 DEG C, waits after being completely dissolved, under the conditions of 90-95 DEG C, is added in the B phase materials while stirring, then successively added again
Enter the mixture and glycerol of dimethyl silicone polymer and Dimethicone/Vinyl Dimethicone cross-linked polymer
Caprylate is uniformly mixing to obtain C phase materials；
(2) the mixture stirring and dissolving of remaining water, CI 45410, CI 15510 and CI77891 and mosanom is complete
Entirely, glycerol and hydroxypropyl melon rubber are added later, under 1000-3000rpm revolving speed homogeneous to no particle, be completely dispersed it is uniform,
Obtain D phase materials；
(3) under 300-800rpm revolving speed, while stirring by the mixed of D phase materials and Phenoxyethanol and Sensiva SC50
It closes object to be added in the C phase materials, later the homogeneous uniform under 1000-3000rpm revolving speed again, be filled after then cooling to room temperature
Dress is to get the lip glaze.
Comparative example 1-4
Comparative example 1-4 is a kind of lip glaze, and the composition of these lip glaze is as shown in table 2, wherein CI 77891 and sodium alginate
Mixture, the smooth stearate of sorb and sucrose cocounut oil acid esters mixture and Phenoxyethanol and Sensiva SC50 mixing
Object is identical as in embodiment 1-8.
Composition/% of lip glaze in 2 comparative example 1-4 of table
Comparative example 5-6
Comparative example 5-6 is a kind of commercially available lip glaze or lipstick, and wherein comparative example 5 is that the flower of Estee Lauder ripples and adores mouth
Red, comparative example 6 is that Armani (ARMANI) attains cause velvet dumb light lip glaze.
The effect of the non-sticky cup lip glaze of the application high glaze is tested applicant carried out following test:
(1) color glossiness is tested
Lip glaze in comparative example 5-6 has high glaze to declare, by the lip in the lip glaze and comparative example 5-6 in embodiment 1-8
Glaze is applied to lip respectively, then observes the gloss of lip after makeup, it is found that the lip glaze in embodiment 1-8 has Qi Guang, gloss
Degree just looks at Geng Shuirun no less than the lip glaze in comparative example 5-6.
(2) non-sticky cup effect and smear test
Test sample: lip glaze or lipstick in embodiment 1-8, comparative example 1-2 and comparative example 5-6.
Test method: after lip uniformly smears lip glaze or lipstick, scoring with regard to smear, and range 0-10 points of scoring,
Score is higher to illustrate that smear is better, easier uniformly to smear drawout in lip.Then phase is used on identical cup respectively
Same power presses lip print, then is just stained with a glass situation and scores, and the range that scores is 0-10 points, and score is higher, represents non-sticky cup feelings
Condition is better, and concrete outcome is shown in Table 3.
3 non-sticky glasss of effects of table and smear appraisal result
| Sample | Smear scoring | Non-sticky cup scoring |
| Embodiment 1 | 6 | 2 |
| Embodiment 2 | 9 | 9 |
| Embodiment 3 | 3 | 10 |
| Embodiment 4 | 3 | 9 |
| Embodiment 5 | 9 | 9 |
| Embodiment 6 | 7 | 6 |
| Embodiment 7 | 5 | 4 |
| Embodiment 8 | 4 | 9 |
| Comparative example 1 | 8 | 3 |
| Comparative example 2 | 4 | 4 |
| Comparative example 5 | 8 | 3 |
| Comparative example 6 | 6 | 5 |
In addition, Fig. 1-3 is compared, it can also be seen that the non-sticky cup effect of the lip glaze in embodiment 2 is more preferable.
(3) color durability is tested
Test sample: lip glaze or lipstick in embodiment 1-8, comparative example 3-6.
Test method: lip lip glaze or lipstick are measured after lip uniformly smears lip glaze or lipstick, after certain time
Residual quantity the results are shown in Table 4.
4 color durability test result of table/%
Note: the "/" representative in table 4 is not tested.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than protects to the present invention
The limitation of range is protected, although the invention is described in detail with reference to the preferred embodiments, those skilled in the art should
Understand, it can be with modification or equivalent replacement of the technical solution of the present invention are made, without departing from the essence of technical solution of the present invention
And range.
Claims (10)
1. a kind of non-sticky cup lip glaze of high glaze, it is characterised in that: the lip glaze is oil-in-water system, includes following weight percent
The component of ratio: the poly dimethyl silicon of the ethyl cellulose B and 0.1-30% of ethyl cellulose A, 0.1-10% of 0.1-10%
The mixture of oxygen alkane and Dimethicone/Vinyl Dimethicone cross-linked polymer, the ethyl cellulose A,
Ethyl cellulose B uses the solution that the Compound mixed solution of toluene and ethyl alcohol is 5% at mass fraction respectively, and viscosity point is measured at 25 DEG C
Not Wei 3-5.5mPas, 90-110mPas, the mass ratio of toluene and ethyl alcohol is 4:1 in the mixed liquor of toluene and ethyl alcohol；It is described
Poly- diformazan in the mixture of dimethyl silicone polymer and Dimethicone/Vinyl Dimethicone cross-linked polymer
The mass ratio of radical siloxane and Dimethicone/Vinyl Dimethicone cross-linked polymer is 80-90:10-20.
2. lip glaze according to claim 1, it is characterised in that: the lip glaze includes following components in percentage by weight: 3%
Ethyl cellulose A, 1.5% ethyl cellulose B and 15% dimethyl silicone polymer and dimethyl silicone polymer/second
The mixture of alkenyl Dimethicone Crosspolymer.
3. lip glaze according to claim 1 or 2, it is characterised in that: the lip glaze also includes water-soluble colorant, oil-soluble
Colorant, emulsifier and water, the water-soluble colorant include acid red 92, acid orange 7 and titanium dioxide and sodium alginate
Mixture, the oil-soluble colorant include acid red 87；It is calculated on the basis of the total weight of the lip glaze, acid red 92 accounts for
0.01-3%, acid orange 7 account for 0.01-3%, and the mixture of titanium dioxide and sodium alginate accounts for 0.01-10%, and acid red 87 accounts for
0.01-2%, emulsifier account for 0.11-20%, and water accounts for 20-60%, and wherein the weight ratio of titanium dioxide and sodium alginate is 97:3.
4. lip glaze according to claim 3, it is characterised in that: calculated on the basis of the total weight of the lip glaze, acid red
92 account for 0.6%, and acid orange 7 accounts for 0.6%, and the mixture of titanium dioxide and sodium alginate accounts for 0.4% altogether, and acid red 87 accounts for 1%.
5. lip glaze according to claim 3, it is characterised in that: the emulsifier is smooth comprising laruyl alcohol sodium sulfovinate, sorb
Stearate and sucrose cocounut oil acid esters；It being calculated on the basis of the total weight of the lip glaze, laruyl alcohol sodium sulfovinate accounts for 0.01-5%,
The smooth stearate of sorb and sucrose cocounut oil acid esters account for 0.1-15% altogether.
6. lip glaze according to claim 3, it is characterised in that: the lip glaze also includes moisturizer, and the moisturizer includes
Account for the glycerol of the lip glaze weight 1-15%.
7. lip glaze according to claim 3, it is characterised in that: the lip glaze also includes thickener, and the thickener includes
Account for the hydroxypropyl melon rubber of the lip glaze weight 0.1-2%.
8. lip glaze according to claim 3, it is characterised in that: the lip glaze also includes emollient and preservative, the profit
Skin agent includes the cetanol of the octyl dodecanol and 0.01-10% that account for the lip glaze weight 5-60% respectively, the preservative packet
Phenoxyethanol and Sensiva SC50 containing the glycerol caprylate and 0.05-1% for accounting for the lip glaze weight 0.05-1% respectively
Mixture.
9. lip glaze according to claim 3, it is characterised in that: the lip glaze also includes following components in percentage by weight:
0.6% acid red 92,0.6% acid orange 7, the mixture of 0.4% titanium dioxide and sodium alginate, 1% acid red
87,0.3% laruyl alcohol sodium sulfovinate, 3% the smooth stearate of sorb and sucrose cocounut oil acid esters mixture, 4% glycerol,
0.2% hydroxypropyl melon rubber, 31% octyl dodecanol, 1% cetanol, 0.3% glycerol caprylate, 0.3% benzene
The mixture of oxyethanol and Sensiva SC50 and 37.8% water, the wherein smooth stearate of sorb and sucrose cocounut oil acid esters
Weight ratio is 82.5:17.5, and the weight ratio of Phenoxyethanol and Sensiva SC50 is 9:1.
10. a kind of preparation method of lip glaze as claimed in any one of claims 1-9 wherein, it is characterised in that: the preparation method
The following steps are included:
(1) ethyl cellulose A, ethyl cellulose B, acid red 87 and part octyl dodecanol are mixed, are heated to 90-95 DEG C,
Until being completely dissolved and being uniformly mixed, heat preservation obtains A phase materials for stirring；Laruyl alcohol sodium sulfovinate, cetanol and part water are mixed
It closes, is heated to 90-95 DEG C, stir to after being completely dissolved, be slowly added to the A phase materials while stirring, stirring is until mixing is equal
It is even, obtain B phase materials；The smooth stearate of sorb, sucrose cocounut oil acid esters and remaining octyl dodecanol have been mixed and heated to again
After fully dissolved, under the conditions of 90-95 DEG C, it is added in the B phase materials while stirring, then sequentially adds poly dimethyl silicon
The mixture and glycerol caprylate of oxygen alkane and Dimethicone/Vinyl Dimethicone cross-linked polymer, stirring
Uniformly obtain C phase materials；
It is (2) the mixture stirring and dissolving of remaining water, acid red 92, acid orange 7 and titanium dioxide and mosanom is complete,
Glycerol and hydroxypropyl melon rubber are added later, homogeneous is completely dispersed uniformly, obtains to no particle under 1000-3000rpm revolving speed
D phase materials；
(3) under 300-800rpm revolving speed, while stirring by D phase materials and the mixture of Phenoxyethanol and Sensiva SC50
Be added in the C phase materials, later the homogeneous uniform under 1000-3000rpm revolving speed again, then cool to room temperature it is rear filling, i.e.,
Obtain the lip glaze.
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|---|---|---|---|---|
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2765799A1 (en) * | 1997-07-08 | 1999-01-15 | Oreal | GLOSSY COMPOSITION CONTAINING AROMATIC OILS THICKENED BY A POLYSACCHARIDE ALKYLETHER |
| FR2964873A1 (en) * | 2010-09-20 | 2012-03-23 | Oreal | Cosmetic process for care of lips, comprises applying composition comprising water, alkylcellulose, preferably ethylcellulose, active agent e.g. moisturizing agents, non-volatile oil and non-volatile hydrocarbon oil, on lips |
| CN104198336A (en) * | 2014-09-10 | 2014-12-10 | 天津爱勒易医药材料有限公司 | Method for detecting kinetic viscosity of ethylcellulose aqueous dispersion |
| CN107320766A (en) * | 2016-12-08 | 2017-11-07 | 沈阳圣劳伦斯医疗器械有限公司 | A kind of composition for skin superficial protecting wound surface |
| CN107349136A (en) * | 2017-05-27 | 2017-11-17 | 清远初曲智能科技有限公司 | A kind of anti-dizzy dye and it is long when keep discoloration lip glaze of bright-coloured colour generation and preparation method thereof |
| CN107661231A (en) * | 2017-12-06 | 2018-02-06 | 佛山微赢电子商务有限公司 | Lip glaze that a kind of moist and non-sticky cup does not fade and preparation method thereof |
| CN107997992A (en) * | 2017-12-29 | 2018-05-08 | 广州慈康生物科技有限公司 | A kind of velvet lipstick of plentiful lip and preparation method thereof |
| CN109330905A (en) * | 2018-11-28 | 2019-02-15 | 广州艾蓓生物科技有限公司 | A kind of velvet dumb light lip glaze and preparation method thereof |
-
2019
- 2019-07-16 CN CN201910642996.9A patent/CN110302094B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2765799A1 (en) * | 1997-07-08 | 1999-01-15 | Oreal | GLOSSY COMPOSITION CONTAINING AROMATIC OILS THICKENED BY A POLYSACCHARIDE ALKYLETHER |
| FR2964873A1 (en) * | 2010-09-20 | 2012-03-23 | Oreal | Cosmetic process for care of lips, comprises applying composition comprising water, alkylcellulose, preferably ethylcellulose, active agent e.g. moisturizing agents, non-volatile oil and non-volatile hydrocarbon oil, on lips |
| CN104198336A (en) * | 2014-09-10 | 2014-12-10 | 天津爱勒易医药材料有限公司 | Method for detecting kinetic viscosity of ethylcellulose aqueous dispersion |
| CN107320766A (en) * | 2016-12-08 | 2017-11-07 | 沈阳圣劳伦斯医疗器械有限公司 | A kind of composition for skin superficial protecting wound surface |
| CN107349136A (en) * | 2017-05-27 | 2017-11-17 | 清远初曲智能科技有限公司 | A kind of anti-dizzy dye and it is long when keep discoloration lip glaze of bright-coloured colour generation and preparation method thereof |
| CN107661231A (en) * | 2017-12-06 | 2018-02-06 | 佛山微赢电子商务有限公司 | Lip glaze that a kind of moist and non-sticky cup does not fade and preparation method thereof |
| CN107997992A (en) * | 2017-12-29 | 2018-05-08 | 广州慈康生物科技有限公司 | A kind of velvet lipstick of plentiful lip and preparation method thereof |
| CN109330905A (en) * | 2018-11-28 | 2019-02-15 | 广州艾蓓生物科技有限公司 | A kind of velvet dumb light lip glaze and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 广州碧美化妆品有限公司: "凯迪雅邂逅甜蜜红酒唇釉", 《HTTP://FTBA.NMPA.GOV.CN:8181/FTBAN/ITOWNET/HZP_BA/FW/PZ.JSP?PROCESSID=20160629223513SB9OW&NID=20160629223513SB9OW》 * |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110638691A (en) * | 2019-11-14 | 2020-01-03 | 广州那比昂生物科技有限公司 | Paint light mirror color-holding lip glaze and preparation method thereof |
| CN110638691B (en) * | 2019-11-14 | 2022-07-08 | 广州那比昂生物科技有限公司 | Paint mirror surface color-holding lip glaze and preparation method thereof |
| CN110711153B (en) * | 2019-11-28 | 2022-05-17 | 广州那比昂生物科技有限公司 | Lip composition with plumping and moisturizing effects and preparation method and application thereof |
| CN110711153A (en) * | 2019-11-28 | 2020-01-21 | 广州那比昂生物科技有限公司 | Lip composition with plumping and moisturizing effects and preparation method and application thereof |
| CN111084732B (en) * | 2020-01-08 | 2022-08-23 | 安焱 | Moisture-preserving and color-protecting lip glaze and preparation method thereof |
| CN111084732A (en) * | 2020-01-08 | 2020-05-01 | 安焱 | Moisture-preserving and color-protecting lip glaze and preparation method thereof |
| CN111728899A (en) * | 2020-08-10 | 2020-10-02 | 丽鑫生技化妆品（上海）有限公司 | Three-layer lip glaze and preparation method thereof |
| CN111728899B (en) * | 2020-08-10 | 2023-01-17 | 丽鑫生技化妆品（上海）有限公司 | Three-layer lip glaze and preparation method thereof |
| CN112120968A (en) * | 2020-09-15 | 2020-12-25 | 铂臻(广州)生物科技有限公司 | Velvet matte lip glaze and preparation method thereof |
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| CN114588080A (en) * | 2022-04-08 | 2022-06-07 | 广州卡洛莱化妆品有限公司 | Light and smooth lip glaze and preparation method thereof |
| CN115670979A (en) * | 2022-11-11 | 2023-02-03 | 广州正千生物科技有限公司 | Preparation method of silicon elastomer |
| CN116098820A (en) * | 2023-02-28 | 2023-05-12 | 广州多多化妆品有限公司 | Tear-type water-based lip-rounding moisturizing lip glaze capable of preventing cup from being stained and preparation method thereof |
| CN118477000A (en) * | 2024-03-04 | 2024-08-13 | 广州莱倩化妆品有限公司 | Mirror-surface color-holding lip glaze and preparation method thereof |
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