CN109439020A - The preparation method of brown color color material on a kind of glaze - Google Patents
The preparation method of brown color color material on a kind of glaze Download PDFInfo
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- CN109439020A CN109439020A CN201811262077.0A CN201811262077A CN109439020A CN 109439020 A CN109439020 A CN 109439020A CN 201811262077 A CN201811262077 A CN 201811262077A CN 109439020 A CN109439020 A CN 109439020A
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- glaze
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- 239000000463 material Substances 0.000 title claims abstract description 58
- 238000002360 preparation method Methods 0.000 title claims description 12
- 238000000498 ball milling Methods 0.000 claims abstract description 24
- 238000001035 drying Methods 0.000 claims abstract description 13
- 238000010304 firing Methods 0.000 claims abstract description 13
- 239000000843 powder Substances 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 229910021532 Calcite Inorganic materials 0.000 claims abstract description 11
- 239000011521 glass Substances 0.000 claims abstract description 11
- 238000000034 method Methods 0.000 claims abstract description 11
- 238000001354 calcination Methods 0.000 claims abstract description 10
- 229910021538 borax Inorganic materials 0.000 claims abstract description 8
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 8
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 8
- 238000010298 pulverizing process Methods 0.000 claims abstract description 5
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 4
- 239000011707 mineral Substances 0.000 claims abstract description 4
- 238000007873 sieving Methods 0.000 claims abstract description 4
- 239000003973 paint Substances 0.000 claims abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 230000001590 oxidative effect Effects 0.000 claims description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 5
- 239000000049 pigment Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 abstract description 6
- 229910052573 porcelain Inorganic materials 0.000 abstract description 5
- 238000010422 painting Methods 0.000 abstract 2
- 238000004040 coloring Methods 0.000 abstract 1
- 239000003086 colorant Substances 0.000 description 21
- 238000005034 decoration Methods 0.000 description 9
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 8
- YOBAEOGBNPPUQV-UHFFFAOYSA-N iron;trihydrate Chemical compound O.O.O.[Fe].[Fe] YOBAEOGBNPPUQV-UHFFFAOYSA-N 0.000 description 8
- 238000001816 cooling Methods 0.000 description 7
- 239000000919 ceramic Substances 0.000 description 6
- 239000000126 substance Substances 0.000 description 5
- 238000000227 grinding Methods 0.000 description 4
- 238000010792 warming Methods 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 208000002173 dizziness Diseases 0.000 description 3
- 239000000155 melt Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 238000003786 synthesis reaction Methods 0.000 description 3
- 238000005303 weighing Methods 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000009412 basement excavation Methods 0.000 description 1
- 235000015895 biscuits Nutrition 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000003760 hair shine Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/0009—Pigments for ceramics
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Organic Chemistry (AREA)
- Glass Compositions (AREA)
Abstract
本发明涉及一种釉上褐彩彩料的制备方法，以天然矿物为主要原料，所述彩料的重量百分比组成为：赭石40～70％、玻璃粉10～30％、方解石10～30％、硼砂0～40％，然后经配料、球磨、干燥、煅烧、粉碎、漂洗、干燥、过筛后制成褐彩彩料。本发明通过调整配方组成，既可适用于高温釉上彩绘后一次烧成，也可适用于高温烧后的白釉瓷上釉上彩绘后二次烧成，还不受烧成气氛的影响，具有极佳的呈色稳定性，色泽深沉、古朴大方，所绘图案淳厚古朴、线条清晰细腻、不易晕散，彩绘色料与深入釉层，彩釉结合良好，不易磨损，具有极佳的艺术表现性。此外，也填补了传统彩绘色料缺乏釉上褐彩彩料的空白，具有广阔的应用前景。The invention relates to a method for preparing an on-glaze brown color material. Natural minerals are used as main raw materials. The weight percentage of the color material is composed of: ocher 40-70%, glass powder 10-30%, calcite 10-30% , 0-40% borax, and then through batching, ball milling, drying, calcining, pulverizing, rinsing, drying and sieving to make brown color material. By adjusting the composition of the formula, the present invention can be applied to one-time firing after high-temperature on-glaze painting, and can also be applied to secondary firing of white-glazed porcelain after high-temperature firing after on-glaze painting, and is not affected by the firing atmosphere. It has excellent color stability, deep color, simple and elegant, simple and simple pattern, clear and delicate lines, not easy to smear, color paint and deep glaze layer, good combination of color glaze, not easy to wear, with excellent art expressiveness. In addition, it also fills the blank of the lack of on-glaze brown color materials in traditional coloring materials, and has broad application prospects.
Description
Technical field
The invention belongs to inorganic non-metallic material (ceramics) fields, and in particular to the preparation method of brown color color material on a kind of glaze.
Background technique
It is to occur a kind of painted decoration skill and technique earlier, Zao Dong in China's ancient pottery and porcelain that brown color-dotted ornament is applied on ceramics
Just occur before the Chinese, has just had Eastern Han Dynasty's celadon glaze with brown colour device, Wu Zhouyao in the unearthed ware in Hunan Xiangyin County ruins Qing Zhu Si Yao
It has also been found that crossing entire body applies greenish yellow glaze, body adorns double raised line designs, Eastern Han Dynasty's blueness glaze stippling tripodia small jar of brown dot coloured silk is equidistantly adornd at raised line design.
To the Western Jin Dynasty this green glaze brown point faience from the Changjiang river areas to the south, gradually development is dispersed throughout southern each department, in Fengcheng
Big vast state kiln finds that the Western Jin Dynasty blueness glaze point faience of the equidistant decorations brown stippling of opening's edge.Enter this brown color-dotted ornament of Song Yihou to exist
Jiangxi Gu kiln has become a kind of pandemic decorative technique, and in Jing Dezhen land reclaimed from a lake, kiln, Ji'an Chien ware etc. have largely
Such implements are unearthed.It is shown according to Jing Dezhen land reclaimed from a lake kiln report on the excavation, the Jing Dezhen land reclaimed from a lake benevolence ancestor period in the Northern Song Dynasty (1023-1063) kiln
Beginning newly sees brown color-dotted ornament, and brown coloured picture case is mostly based on dot, or arbitrarily distribution or in quincunx distribution, and color development brown is pure
Just, go deep into tire bone.
The emergence and development of brown point faience provide not only a kind of new ceramic decoration skill and technique, also to fire glaze later
Upper color and underglaze colour provides good basis.The iron that a kind of class blue and white porcelain just occurs on this basis in the Yuan Dynasty in Jing Dezhen is drawn
Underglaze colour porcelain has high artistry, but its colored drawing pattern is easily dizzy scattered, it is difficult to which expression is as in the blue and white similar hachure of member
Hold, in article " chemical composition and technology characteristics that the Jing Dezhen land reclaimed from a lake kiln Northern Song Dynasty brown faience is rested the head on ", the sample that author is shown shines
Piece limits its further development and application to a certain extent.In addition, being also difficult to find brown coloured silk in overglaze color colored drawing colorant
Draw content.In consideration of it, the present invention attempts to fill up this technological gap, innovatively develop one kind can be used for high temperature on glaze it is primary or
The brown color color material of low temperature twice firing, enriches China's ceramic decoration color and content.
Summary of the invention
That the technical problem to be solved in the present invention is to provide a kind of preparation processes is simple, low in cost, glaze color development is stable
The preparation method of brown coloured silk color material on glaze.
The present invention is achieved by the following technical programs: the preparation method of brown color color material on a kind of glaze, with natural minerals
For primary raw material, it is characterised in that: the weight percent of the color material forms are as follows: ochre 40~70%, glass powder 10~30%,
Calcite 10~30%, borax 0~40%, then make after ingredient, ball milling, drying, calcining, crushing, rinsing, drying, sieving
At brown color color material, wherein calcination temperature is 1150~1350 DEG C.
The material of the ball milling process: ball: the weight ratio of water is 1:2:0.8~1.0, and Ball-milling Time is 20~40 minutes.
The system of the calcination process are as follows: first in high-temperature electric resistance furnace, heated up with 1.5~3 hours slow fires, make furnace Nei Wenda
To 400~550 DEG C, moisture contained in product is sufficiently excluded；1150~1350 DEG C were warming up to 3~5 hours again, and keeps the temperature 1
It~2 hours, melts raw material sufficiently, be effectively synthesized required colorant；Finally with furnace natural cooling.
The pulverizing process are as follows: the color material that will be cooled down after calcining, with material: ball: water weight ratio is the loading of 1:2:0.8~1.0
Ball-grinding machine, ball milling 10~20 hours, the color material fineness after ball milling reached 10000-hole sieve and tails over less than 0.05%.
The rinsing process are as follows: will be anti-in 40~60 DEG C of warm water with 5~15% dilute hydrochloric acid after the drying of smashed color material
It rinses 3~6 times again, until color material color does not change.
The application mode of the brown color color material are as follows: brown color color material is plotted on temperature resistant transparent glaze, is being restored after drying
The product that brown color equipment decorations on glaze are made is burnt under atmosphere or oxidizing atmosphere in 800~1310 DEG C.
The present invention is primary raw material using ochre, glass powder, calcite, borax etc., through ingredient, ball milling, drying, calcining,
Brown coloured silk color material on the glaze is made after crushing, rinsing, dry, sieving to be both applicable on high-temperature glaze by adjusting formula composition
Once-firing after colored drawing is equally applicable on the white glaze porcelain after high temperature is burnt twice firing after over-glaze decoration, also not by firing atmosphere
Influence, can both fire, can also be fired under oxidizing atmosphere under reducing atmosphere, there is splendid colour stability, color is deep
It is heavy, simple and unsophisticated generous, institute's drawing case it is pure and honest it is simple and unsophisticated, svelteness is fine and smooth, be not easy it is dizzy dissipate, colored drawing colorant and go deep into glaze layer, colored glaze knot
It closes well, it is not easy to wear, there is splendid artistic expression.In addition, also having filled up traditional colored drawing colorant lacks brown coloured silk coloured silk on glaze
The blank of material, has broad application prospects.
Specific embodiment
For further illustrate the present invention, to reach the technical means and efficacy that predetermined goal of the invention is taken, tie below
Preferred embodiment is closed, the present invention is described in detail, raw mineral materials ochre, glass powder, calcite used in embodiment,
Its chemical component is as follows:
Embodiment 1
Step 1: the weight percent of brown coloured silk color material formula are as follows: ochre 65%, glass powder 25%, calcite 10%；It is described reddish brown
Stone, glass powder, the chemical composition weight percent of calcite are as shown above.
Step 2: weighing raw material by colorant formulas requirement and mixing, with material: ball: water weight ratio is that 1:2:0.8 is packed into ball milling
Equipment ball milling 20 minutes.
Step 3: being heated up with 1.5 hours slow fires in high-temperature electric resistance furnace, temperature in furnace being made to reach 400 DEG C, sufficiently exclude institute in product
The moisture contained；It is warming up within 5 hours 1350 DEG C again, and keeps the temperature 2 hours, melts raw material sufficiently, be effectively synthesized required colorant；Finally
With furnace natural cooling.
Step 4: with material: ball: water weight ratio is that 1:2:0.8 is packed into ball-grinding machine ball after colored drawing colorant after synthesis is cooling
Mill 20 hours, the colorant fineness after ball milling reaches 10000-hole sieve and tails over less than 0.05%.
Step 5: need to be rinsed repeatedly in 60 DEG C of warm water 3 times using 15% dilute hydrochloric acid after the colorant after ball milling is dried, until
Pigment color does not change, then is dried for standby.
Step 6: treated brown color color material is plotted on temperature resistant transparent glaze, in reducing atmosphere after then drying
Under in 1310 DEG C of high temperature once-firings be made glaze on brown faience product.
Brown coloured silk color material color development is pure and honest simple and unsophisticated on the glaze of the present embodiment resulting product, is applicable to high temperature oxidative atmosphere or reduction
Over-glaze decoration once-firing uses under atmosphere, and the drawn pattern line of color material is fine and smooth, color development is uniform, be not easy it is dizzy scattered, color material it is deep in
Glaze layer is tightly combined, simple and unsophisticated wear-resisting, has splendid artistic expression.
Embodiment 2
Step 1: the weight percent of brown coloured silk color material formula are as follows: ochre 40%, glass powder 10%, calcite 15%, borax
35%；The ochre, glass powder, the chemical composition weight percent of calcite are as shown above, and borax is technical pure.
Step 2: weighing raw material by colorant formulas requirement and mixing, with material: ball: water weight ratio is that 1:2:1.0 is packed into ball milling
Equipment ball milling 40 minutes.
Step 3: being heated up with 3 hours slow fires in high-temperature electric resistance furnace, temperature in furnace being made to reach 550 DEG C, sufficiently exclude contained in product
Moisture；1150 DEG C were warming up to 3 hours again, and keeps the temperature 1 hour, raw material is melted sufficiently, is effectively synthesized required colorant；Finally
With furnace natural cooling.
Step 4: with material: ball: water weight ratio is that 1:2:1.0 is packed into ball-grinding machine ball after colored drawing colorant after synthesis is cooling
Mill 10 hours, the colorant fineness after ball milling reaches 10000-hole sieve and tails over less than 0.05%.
Step 5: need to be rinsed repeatedly in 40 DEG C of warm water 6 times using 5% dilute hydrochloric acid after the colorant after ball milling is dried, until
Pigment color does not change, then is dried for standby.
Step 6: treated brown color color material after adding camphorated oil to modulate, is plotted in the white biscuit after high temperature is fired
On clear frit, it is burnt under oxidizing atmosphere in 800 DEG C after then drying and brown faience product on glaze is made.
Brown coloured silk color material is applicable to the overglaze colors such as the five colours, powder enamel ceramics on the glaze of the present embodiment resulting product, burns in high temperature
After white ceramic glaze color drawing for curved surface of body afterwards, dark brown pattern is presented in low temperature grilling, and institute's drawing case is well combined with glaze, and outline is clear
Clear exquisiteness, being not easy to swoon dissipates, and artistic expression excellent performance can greatly enrich the form of expression of over-glaze decoration pattern.
Embodiment 3
Step 1: the weight percent of brown coloured silk color material formula are as follows: ochre 50%, glass powder 15%, calcite 25%, borax
10%；The ochre, glass powder, the chemical composition weight percent of calcite are as shown above, and borax is technical pure.
Step 2: weighing raw material by colorant formulas requirement and mixing, with material: ball: water weight ratio is that 1:2:0.9 is packed into ball milling
Equipment ball milling 30 minutes.
Step 3: being heated up with 2 hours slow fires in high-temperature electric resistance furnace, temperature in furnace being made to reach 500 DEG C, sufficiently exclude contained in product
Moisture；It is warming up within 4 hours 1200 DEG C again, and keeps the temperature 1.5 hours, melts raw material sufficiently, be effectively synthesized required colorant；Finally
With furnace natural cooling.
Step 4: with material: ball: water weight ratio is that 1:2:0.9 is packed into ball-grinding machine ball after colored drawing colorant after synthesis is cooling
Mill 15 hours, the colorant fineness after ball milling reaches 10000-hole sieve and tails over less than 0.05%.
Step 5: need to be rinsed repeatedly in 50 DEG C of warm water 5 times using 10% dilute hydrochloric acid after the colorant after ball milling is dried, until
Pigment color does not change, then is dried for standby.
Step 6: treated brown color color material is plotted on temperature resistant transparent glaze, in oxidizing atmosphere after then drying
Under in 1200 DEG C of high temperature once-firings be made glaze on brown faience product.
Brown coloured silk color material color development is deep simple and honest on the glaze of the present embodiment resulting product, is applicable to medium temperature oxidizing atmosphere or reduction
Over-glaze decoration once-firing uses under atmosphere, and the drawn case svelteness of color material, which is not easy to swoon, to be dissipated, and color material is tightly combined with glaze layer, no
Only there is preferable artistic appreciation, go back wearable environment protection, it is practical.
Claims (6)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811262077.0A CN109439020A (en) | 2018-10-27 | 2018-10-27 | The preparation method of brown color color material on a kind of glaze |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811262077.0A CN109439020A (en) | 2018-10-27 | 2018-10-27 | The preparation method of brown color color material on a kind of glaze |
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| CN109439020A true CN109439020A (en) | 2019-03-08 |
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| CN201811262077.0A Pending CN109439020A (en) | 2018-10-27 | 2018-10-27 | The preparation method of brown color color material on a kind of glaze |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110963786A (en) * | 2019-11-19 | 2020-04-07 | 福建省德化县山花陶瓷有限公司 | Colored art porcelain based on Dehua white porcelain body and preparation process thereof |
| CN111302628A (en) * | 2020-04-03 | 2020-06-19 | 范平 | Cold-color jade-like crystal paste for ceramic jade bead colored drawing and preparation method and application thereof |
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| CN110963786A (en) * | 2019-11-19 | 2020-04-07 | 福建省德化县山花陶瓷有限公司 | Colored art porcelain based on Dehua white porcelain body and preparation process thereof |
| CN111302628A (en) * | 2020-04-03 | 2020-06-19 | 范平 | Cold-color jade-like crystal paste for ceramic jade bead colored drawing and preparation method and application thereof |
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