CN112374762A - Moon white glaze for jun porcelain and preparation method thereof - Google Patents
Moon white glaze for jun porcelain and preparation method thereof Download PDFInfo
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- CN112374762A CN112374762A CN202011375904.4A CN202011375904A CN112374762A CN 112374762 A CN112374762 A CN 112374762A CN 202011375904 A CN202011375904 A CN 202011375904A CN 112374762 A CN112374762 A CN 112374762A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/20—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
- C03C8/08—Frit compositions, i.e. in a powdered or comminuted form containing phosphorus
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2205/00—Compositions applicable for the manufacture of vitreous enamels or glazes
- C03C2205/02—Compositions applicable for the manufacture of vitreous enamels or glazes for opaque enamels or glazes
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Abstract
The invention relates to the technical field of jun porcelain glaze, in particular to a jun porcelain moon white glaze and a preparation method thereof, wherein the jun porcelain moon white glaze is prepared by mixing frit and glaze slurry, and the frit is prepared from the following raw materials in parts by weight: feldspar, quartz, fluorite, talc, phosphorus compounds; the glaze slip is prepared from the following raw materials in parts by weight: frit, clay, ferric oxide, barium carbonate, strontium carbonate, manganese oxide, titanium oxide and hydroxypropyl methyl cellulose; according to the invention, the quartz, fluorite, talc and phosphorus compounds are used for eliminating the pinhole defect of the glaze, increasing the gloss of the glaze, improving the quality of finished products and increasing the gloss of the glaze; reasonably configuring the amount of feldspar and quartz, and forming a good middle layer between the glaze layer and the green body to tightly combine the green body glaze; the heat stress among the blank glazes is promoted to be uniform, the stress among the blank glazes is weakened, and the mechanical strength of the jun porcelain is increased; the ceramic material is prepared by one-time firing of 1350-DEG high-temperature reducing flame, and has the advantages of simple operation, high yield, production cost reduction and good finished product effect.
Description
Technical Field
The invention relates to the technical field of jun porcelain glaze materials, in particular to a moon white glaze for jun porcelain and a preparation method thereof.
Background
Jun porcelain is from Tang and contained in Song, is one of five famous porcelain ancient China, and is miraculous and famous for the kiln transformation produced by the unique glaze and the firing method; the porcelain is an important symbol in the artistic history of Chinese Jun porcelain, plays an important role in the development history of world Jun porcelain, and has the saying that gold valuable Jun is not valuable and family is very popular, rather than Jun porcelain; the unique kiln-changing art is widely loved by Jun porcelain amateurs due to the artistic characteristics of 'one color in kiln and ten thousand colors out of kiln'.
The Jun porcelain glaze of the moon-white glaze is moon-white in color, elegant and noble; when the light is sufficient, the jade-like moist feeling and the greasy feeling are presented, and the light brightness is presented in the greasy feeling; when the light is weak, the moon looks like a treasure pearl in the dark, the moon color is very natural, and the moon color is slightly moist and glossy; really feel that the Ru kiln is 'blue as the day and romantic as jade'.
Glaze is a glassy thin layer covered on a ceramic body, but the composition of the glaze is more complex than that of glass, and the property and the microstructure of the glaze are also greatly different from that of the glass, for example, the high-temperature viscosity of the glaze is far greater than that of the glass; the composition and preparation process of the glass are close to those of a blank and different from those of glass; the glaze has the functions of: the surface performance of the ceramic product is improved, so that the surface of the product is smooth, and the product is impermeable to liquid and gas and is not easy to stain; secondly, the mechanical strength, the electrical property, the chemical stability and the thermal stability of the product can be improved; the glaze also has a decorative effect on the blank, it can cover the bad colour and rough surface of the blank; a plurality of glazes such as colored glaze, matt glaze, gold sand glaze, devitrified glaze and the like have unique decorative effects; however, in the firing process of the moon white glaze in the prior art, the moon white glaze mostly needs to be fired through the stages of oxidation period firing, reduction period firing and cooling to room temperature, the operation time is long, the difficulty is high, and the finished product quality is low and the qualified products are few, so that the cost of the jun porcelain is increased, and the popularization of the jun porcelain is not facilitated; therefore, how to overcome the above technical problems and disadvantages is a problem to be solved.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides the moon white glaze for the jun porcelain and the preparation method thereof, wherein the moon white glaze is fired once, has high yield and can effectively reduce the production cost of the jun porcelain.
In order to achieve the purpose, the technical scheme of the invention is as follows: the moon white glaze for Jun porcelain is prepared by mixing a frit and glaze slip, wherein the frit is prepared from the following raw materials in parts by weight: 30-40 parts of feldspar, 20-30 parts of quartz, 10-20 parts of fluorite, 10-16 parts of talcum and 9-15 parts of phosphorus compound; the glaze slip is prepared from the following raw materials in parts by weight: 70-90 parts of frit, 5-10 parts of clay, 2-6 parts of ferric oxide, 1-4 parts of barium carbonate, 1-4 parts of strontium carbonate, 1-4 parts of manganese oxide, 1-4 parts of titanium oxide and 1-3 parts of hydroxypropyl methyl cellulose.
Further, the moon white glaze for Jun porcelain is prepared by mixing a frit and glaze slurry, wherein the frit is prepared from the following raw materials in parts by weight: 32-38 parts of feldspar, 23-27 parts of quartz, 13-17 parts of fluorite, 12-14 parts of talcum and 11-13 parts of phosphorus compound; the glaze slip is prepared from the following raw materials in parts by weight: 75-85 parts of frit, 6-9 parts of clay, 3-5 parts of ferric oxide, 1-3 parts of barium carbonate, 1-3 parts of strontium carbonate, 1-3 parts of manganese oxide, 1-3 parts of titanium oxide and 1-2 parts of hydroxypropyl methyl cellulose.
Further, the moon white glaze for Jun porcelain is prepared by mixing a frit and glaze slurry, wherein the frit is prepared from the following raw materials in parts by weight: 35 parts of feldspar, 25 parts of quartz, 15 parts of fluorite, 13 parts of talcum and 12 parts of phosphorus compound; the glaze slip is prepared from the following raw materials in parts by weight: 80 parts of frit, 7 parts of clay, 4 parts of ferric oxide, 2 parts of barium carbonate, 2 parts of strontium carbonate, 2 parts of manganese oxide, 2 parts of titanium oxide and 1 part of hydroxypropyl methyl cellulose.
Further, the phosphorus compound is one or a mixture of more of calcium phosphate, bone ash and apatite; the phosphorus compound can be used as an opacifier in the glaze to make the glaze opaque; the refractive index of the glaze to light can be increased, and the luster of the glaze can be increased; the calcium phosphate, bone ash and apatite can make the glaze form good opacification and brightness effect.
In addition, the invention also discloses a preparation method of the moon white glaze for preparing Jun porcelain, which is characterized by comprising the following steps: the method comprises the following steps:
(1) preparing a frit: putting the feldspar, the quartz, the fluorite, the talc and the phosphorus compound in parts by weight into a ball mill for crushing, and sieving with a 160-sand 180-mesh sieve to obtain mixture powder; placing the mixture powder in a rotary furnace, calcining to 1200-1240 ℃, melting for 15-20min, and then quenching to obtain a fusion cake;
(2) preparing glaze slip: putting the frit, clay, ferric oxide, barium carbonate, strontium carbonate, manganese oxide, titanium oxide and hydroxypropyl methyl cellulose in parts by weight into a ball mill, adding water accounting for 50-60% of the mass of the raw materials, grinding for 70 hours, and finely grinding to 400 meshes to obtain glaze slurry;
(3) glazing, namely uniformly applying glaze slip on the raw blank body of the Jun porcelain, controlling the thickness of a glaze layer within the range of 0.9-1.2 mm, placing the Jun porcelain blank body in an electric furnace for firing, heating to 1350 ℃ in a reducing atmosphere, preserving the heat for 20-25 minutes under the temperature condition, and naturally cooling to room temperature to obtain the moon white glaze.
Further, placing the mixture powder in the step (1) in a crucible for calcining; the frit material is not contacted with flame, so that the volatilization is small, and the frit quality is good; different kinds of frits can be simultaneously melted in different crucibles, and the method is flexible.
Further, the density of the glaze slip in the step (2) is 1.3-1.5g/cm3If the density is too small, the glaze layer is too thin, and dry glaze is easy to generate; the excessive density of the glaze slurry can cause the glaze layer to be too thick and the glazing to be uneven, and the density of the glaze slurry is 1.3 to 1.5g/cm through tests3And the glazing effect is better.
The moon white glaze for Jun porcelain has the beneficial effects that:
the feldspar is added into the clinker, and the feldspar contains a large amount of Al2O3Widening the sintering range of the green body; quartz can eliminate pinhole defect of the glaze, increase glaze luster and enlarge melting range; fluorite can be made into glaze with complete vitrification and high melting degree; the talc contains magnesium oxide, which can promote opacification, improve whiteness, improve the suspension property of glaze slip, increase the firing range of glaze and overcome the defects of smoking, yellowing and the like; the phosphorus compound can be used as an opacifier in the glaze to make the glaze opaque; the refractive index of the glaze to light can be increased, and the luster of the glaze can be increased; the calcium phosphate, the bone ash and the apatite can make the glaze form good opacification and brightness effects; the clay is added into the glaze slip, so that the suspension property of the glaze slip can be improved; ferric oxide is a colorant, and iron can form light blue gray, green, blue or black when in a reducing flame atmosphere; the barium carbonate is introduced, so that the glaze is more white or the milky white feeling is increased; strontium carbonate is very effective in reducing bubbles in the glaze; the manganese oxide can generate light blue after being sintered at high temperature, so that the chroma of the moon white glaze is increased; will oxidizeWhen titanium is added into the glaze, high-grade white opaque glaze can be prepared, and hydroxypropyl methyl cellulose has thickening and bonding effects; as a thickening agent, the viscosity of the glaze slip can be increased, and glaze is not easy to flow during glazing, so that a thick glaze layer can be applied, and the phenomenon that dry glaze is easy to generate due to too thin glaze during glazing is avoided; as the binder, the speed of water evaporation from the glaze slip can be controlled, the movement of water entering the porous blank is also controlled, and the function of increasing the hardness of the dried glaze surface is achieved.
According to the invention, through calculation, the amount of feldspar and quartz is reasonably configured, so that a good middle layer can be formed between the glaze layer and the green body, and the blank glaze is tightly combined; the intermediate layer can promote the uniform thermal stress among the blank glazes, the well-developed intermediate layer can fill the gaps on the surface of the blank, weaken the stress among the blank glazes and increase the mechanical strength of the Jun porcelain.
The moon white glaze has high viscosity at high temperature, and glaze is not easy to flow at high temperature, so that a glaze layer can be thick; glaze hanging is carried out on the green body, the green body is placed into a kiln and is subjected to one-time firing through high-temperature reduction flame at 1350 ℃, and soft and elegant jade feeling is achieved through proper high temperature and reduction atmosphere; the method has the advantages of simple operation, high yield, production cost reduction and good finished product effect.
In conclusion, the invention has the advantages that the good intermediate layer is formed between the glaze layer and the green body by one-time firing, the stress between the glaze layers of the green bodies is weakened, and the mechanical strength of the Jun porcelain is increased; eliminating pinhole defect of glaze, increasing glaze luster and improving the quality of finished products.
Detailed Description
Example 1
The moon white glaze for the jun porcelain is prepared by mixing frit and glaze slip, wherein the frit is prepared from the following raw materials in parts by weight: 30 parts of feldspar, 20 parts of quartz, 10 parts of fluorite, 10 parts of talcum and 9 parts of phosphorus compound; the glaze slip is prepared from the following raw materials in parts by weight: 70 parts of frit, 5 parts of clay, 2 parts of ferric oxide, 1 part of barium carbonate, 1 part of strontium carbonate, 1 part of manganese oxide, 1 part of titanium oxide and 1 part of hydroxypropyl methyl cellulose.
A preparation method of a moon white glaze for Jun porcelain comprises the following steps:
(1) preparing a frit: putting the feldspar, the quartz, the fluorite, the talc and the phosphorus compound in parts by weight into a ball mill for crushing, and sieving with a 160-sand 180-mesh sieve to obtain mixture powder; placing the mixture powder in a rotary furnace, calcining to 1200-1240 ℃, melting for 15-20min, and then quenching to obtain a fusion cake;
(2) preparing glaze slip: putting the frit, clay, ferric oxide, barium carbonate, strontium carbonate, manganese oxide, titanium oxide and hydroxypropyl methyl cellulose in parts by weight into a ball mill, adding water accounting for 50-60% of the mass of the raw materials, grinding for 70 hours, and finely grinding to 400 meshes to obtain glaze slurry; the density of the glaze slip is 1.3-1.5g/cm3；
(3) Glazing, namely uniformly applying glaze slip on the raw blank body of the Jun porcelain, controlling the thickness of a glaze layer within the range of 0.9-1.2 mm, placing the Jun porcelain blank body in an electric furnace for firing, heating to 1350 ℃ in a reducing atmosphere, preserving the heat for 20-25 minutes under the temperature condition, and naturally cooling to room temperature to obtain the moon white glaze.
Example 2
The moon white glaze for the jun porcelain is prepared by mixing frit and glaze slip, wherein the frit is prepared from the following raw materials in parts by weight: 40 parts of feldspar, 30 parts of quartz, 20 parts of fluorite, 16 parts of talcum and 15 parts of phosphorus compound; the glaze slip is prepared from the following raw materials in parts by weight: 90 parts of clinker, 10 parts of clay, 6 parts of ferric oxide, 4 parts of barium carbonate, 4 parts of strontium carbonate, 4 parts of manganese oxide, 4 parts of titanium oxide and 2 parts of hydroxypropyl methyl cellulose.
The preparation method is the same as example 1.
Example 3
The moon white glaze for the Jun porcelain is prepared by mixing a frit and glaze slurry, wherein the frit is prepared from the following raw materials in parts by weight: 35 parts of feldspar, 25 parts of quartz, 15 parts of fluorite, 13 parts of talcum and 12 parts of phosphorus compound; the glaze slip is prepared from the following raw materials in parts by weight: 80 parts of frit, 7 parts of clay, 4 parts of ferric oxide, 2 parts of barium carbonate, 2 parts of strontium carbonate, 2 parts of manganese oxide, 2 parts of titanium oxide and 1 part of hydroxypropyl methyl cellulose.
The preparation method is the same as example 1.
The product detection method comprises the following steps:
the comparative tests of the glaze materials of example 1, example 2 and example 3 of the invention and the glaze materials in general on the market are carried out; taking 75 green bodies, dividing the green bodies into 3 groups, respectively coating the glaze materials of the embodiment 1, the embodiment 2 and the embodiment 3 on the surfaces of the green bodies, carrying out primary high-temperature glaze firing, and inspecting the glaze fired Jun porcelain; and glazing the surfaces of 25 green bodies, respectively coating commercial glaze materials on the surfaces of the green bodies, and then glazing and firing the green bodies according to a method of firing in an oxidation period, firing in a reduction period and cooling to room temperature.
Then glaze firing is carried out, the glaze fired Jun porcelain is tested, and the test result is shown in Table 1:
table 1: results of glaze firing test
As can be clearly seen from the table 1, compared with the prior art, the color development of the Jun porcelain moon white glaze is more natural by scientifically and reasonably mixing the raw materials and controlling the firing process and utilizing various color development substances contained in the ore, the color development of the prepared Jun porcelain moon white glaze is changed into a transition color, the effect of enough copper and iron is achieved, the jade texture and the opaqueness are strong, and the yield is high and can reach more than 95%; the moon white glaze for Jun porcelain has the advantages of increased blank whiteness, higher thermal stability, good glaze quality, strong glaze hardness and the like.
The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention, and various modifications and changes may be made by those skilled in the art. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (7)
1. The moon white glaze for Jun porcelain is characterized in that: the moon white glaze for Jun porcelain is prepared by mixing a frit and glaze slurry, wherein the frit is prepared from the following raw materials in parts by weight: 30-40 parts of feldspar, 20-30 parts of quartz, 10-20 parts of fluorite, 10-16 parts of talcum and 9-15 parts of phosphorus compound; the glaze slip is prepared from the following raw materials in parts by weight: 70-90 parts of frit, 5-10 parts of clay, 2-6 parts of ferric oxide, 1-4 parts of barium carbonate, 1-4 parts of strontium carbonate, 1-4 parts of manganese oxide, 1-4 parts of titanium oxide and 1-3 parts of hydroxypropyl methyl cellulose.
2. The moon white glaze for Jun porcelain according to claim 1, which is characterized in that: the moon white glaze for Jun porcelain is prepared by mixing a frit and glaze slurry, wherein the frit is prepared from the following raw materials in parts by weight: 32-38 parts of feldspar, 23-27 parts of quartz, 13-17 parts of fluorite, 12-14 parts of talcum and 11-13 parts of phosphorus compound; the glaze slip is prepared from the following raw materials in parts by weight: 75-85 parts of frit, 6-9 parts of clay, 3-5 parts of ferric oxide, 1-3 parts of barium carbonate, 1-3 parts of strontium carbonate, 1-3 parts of manganese oxide, 1-3 parts of titanium oxide and 1-2 parts of hydroxypropyl methyl cellulose.
3. The moon white glaze for Jun porcelain according to claim 1, which is characterized in that: the moon white glaze for Jun porcelain is prepared by mixing a frit and glaze slurry, wherein the frit is prepared from the following raw materials in parts by weight: 35 parts of feldspar, 25 parts of quartz, 15 parts of fluorite, 13 parts of talcum and 12 parts of phosphorus compound; the glaze slip is prepared from the following raw materials in parts by weight: 80 parts of frit, 7 parts of clay, 4 parts of ferric oxide, 2 parts of barium carbonate, 2 parts of strontium carbonate, 2 parts of manganese oxide, 2 parts of titanium oxide and 1 part of hydroxypropyl methyl cellulose.
4. The moon white glaze for Jun porcelain according to any one of claims 1 to 3, which is characterized in that: the phosphorus compound is one or more of calcium phosphate, bone ash and apatite.
5. A method for preparing the moon white glaze for Jun porcelain according to any one of claims 1 to 4, which is characterized by comprising the following steps: the method comprises the following steps:
preparing a frit: putting the feldspar, the quartz, the fluorite, the talc and the phosphorus compound in parts by weight into a ball mill for crushing, and sieving with a 160-sand 180-mesh sieve to obtain mixture powder; placing the mixture powder in a rotary furnace, calcining to 1200-1240 ℃, melting for 15-20min, and then quenching to obtain a fusion cake;
preparing glaze slip: putting the frit, clay, ferric oxide, barium carbonate, strontium carbonate, manganese oxide, titanium oxide and hydroxypropyl methyl cellulose in parts by weight into a ball mill, adding water accounting for 50-60% of the mass of the raw materials, grinding for 70 hours, and finely grinding to 400 meshes to obtain glaze slurry;
glazing, namely uniformly applying glaze slip on the raw blank body of the Jun porcelain, controlling the thickness of a glaze layer within the range of 0.9-1.2 mm, placing the ceramic blank body in an electric furnace for firing, heating to 1350 ℃ in a reducing atmosphere, preserving the heat for 20-25 minutes under the temperature condition, and then naturally cooling to room temperature to obtain the moon white glaze.
6. The method for preparing the moon white glaze for Jun porcelain as claimed in claim 5, wherein: and (2) placing the mixture powder in the step (1) into a crucible for calcining.
7. The method for preparing the moon white glaze for Jun porcelain as claimed in claim 5, wherein: the density of the glaze slip in the step (2) is 1.3-1.5g/cm3。
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113121202A (en) * | 2021-04-07 | 2021-07-16 | 福建省德化县宏泉工艺品有限公司 | Preparation process of split lard white glaze porcelain |
| CN113582547A (en) * | 2021-09-29 | 2021-11-02 | 佛山市三水区康立泰无机合成材料有限公司 | Metal glaze and preparation method and application method thereof |
| CN113845311A (en) * | 2021-08-03 | 2021-12-28 | 苏州市亿林玻璃加工制造有限公司 | Non-edge colored glazed glass |
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| CN113582547A (en) * | 2021-09-29 | 2021-11-02 | 佛山市三水区康立泰无机合成材料有限公司 | Metal glaze and preparation method and application method thereof |
| CN113582547B (en) * | 2021-09-29 | 2022-01-18 | 佛山市三水区康立泰无机合成材料有限公司 | Metal glaze and preparation method and application method thereof |
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