CN109380635A - A kind of inulin stachyose solid beverage - Google Patents
A kind of inulin stachyose solid beverage Download PDFInfo
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- CN109380635A CN109380635A CN201710679078.4A CN201710679078A CN109380635A CN 109380635 A CN109380635 A CN 109380635A CN 201710679078 A CN201710679078 A CN 201710679078A CN 109380635 A CN109380635 A CN 109380635A
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- inulin
- stachyose
- feed liquid
- preparation
- organic
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- 229920001202 Inulin Polymers 0.000 title claims abstract description 76
- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 title claims abstract description 76
- 229940029339 inulin Drugs 0.000 title claims abstract description 76
- UQZIYBXSHAGNOE-USOSMYMVSA-N Stachyose Natural products O(C[C@H]1[C@@H](O)[C@H](O)[C@H](O)[C@@H](O[C@@]2(CO)[C@H](O)[C@@H](O)[C@@H](CO)O2)O1)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@H](CO[C@@H]2[C@@H](O)[C@@H](O)[C@@H](O)[C@H](CO)O2)O1 UQZIYBXSHAGNOE-USOSMYMVSA-N 0.000 title claims abstract description 63
- UQZIYBXSHAGNOE-XNSRJBNMSA-N stachyose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO[C@@H]2[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO[C@@H]3[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO)O3)O)O2)O)O1 UQZIYBXSHAGNOE-XNSRJBNMSA-N 0.000 title claims abstract description 63
- 239000007787 solid Substances 0.000 title claims abstract description 18
- 235000013361 beverage Nutrition 0.000 title claims abstract description 17
- 238000002360 preparation method Methods 0.000 claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000002156 mixing Methods 0.000 claims abstract description 7
- 239000004615 ingredient Substances 0.000 claims abstract description 5
- 239000007788 liquid Substances 0.000 claims description 45
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- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 9
- 239000000843 powder Substances 0.000 claims description 9
- 239000011347 resin Substances 0.000 claims description 9
- 229920005989 resin Polymers 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 7
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- 235000005116 Stachys sieboldii Nutrition 0.000 claims description 6
- 244000057214 Stachys sieboldii Species 0.000 claims description 6
- 229910052742 iron Inorganic materials 0.000 claims description 6
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- 241000196324 Embryophyta Species 0.000 claims description 3
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- 102000004190 Enzymes Human genes 0.000 claims description 3
- 240000008892 Helianthus tuberosus Species 0.000 claims description 3
- 235000003230 Helianthus tuberosus Nutrition 0.000 claims description 3
- 229920000377 Sinistrin Polymers 0.000 claims description 3
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- 238000004042 decolorization Methods 0.000 claims description 3
- 238000011033 desalting Methods 0.000 claims description 3
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- 238000000909 electrodialysis Methods 0.000 claims description 3
- 239000000284 extract Substances 0.000 claims description 3
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- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 4
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- YTBSYETUWUMLBZ-QWWZWVQMSA-N D-threose Chemical compound OC[C@@H](O)[C@H](O)C=O YTBSYETUWUMLBZ-QWWZWVQMSA-N 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- 208000031226 Hyperlipidaemia Diseases 0.000 description 2
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- 235000019698 starch Nutrition 0.000 description 2
- ZGXJTSGNIOSYLO-UHFFFAOYSA-N 88755TAZ87 Chemical compound NCC(=O)CCC(O)=O ZGXJTSGNIOSYLO-UHFFFAOYSA-N 0.000 description 1
- 241000193830 Bacillus <bacterium> Species 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 108010023302 HDL Cholesterol Proteins 0.000 description 1
- 108010010234 HDL Lipoproteins Proteins 0.000 description 1
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- 102000007330 LDL Lipoproteins Human genes 0.000 description 1
- 206010034719 Personality change Diseases 0.000 description 1
- 241000270295 Serpentes Species 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
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- 210000002249 digestive system Anatomy 0.000 description 1
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- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 239000003623 enhancer Substances 0.000 description 1
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- 239000003337 fertilizer Substances 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000005417 food ingredient Substances 0.000 description 1
- 230000037406 food intake Effects 0.000 description 1
- 210000000245 forearm Anatomy 0.000 description 1
- 235000013376 functional food Nutrition 0.000 description 1
- 210000000232 gallbladder Anatomy 0.000 description 1
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- 230000003516 hyperlipidaemic effect Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 208000003243 intestinal obstruction Diseases 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 230000003907 kidney function Effects 0.000 description 1
- 210000002429 large intestine Anatomy 0.000 description 1
- 229940118199 levulan Drugs 0.000 description 1
- 108010022197 lipoprotein cholesterol Proteins 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 230000003908 liver function Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000001473 noxious effect Effects 0.000 description 1
- 229920001542 oligosaccharide Polymers 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000035755 proliferation Effects 0.000 description 1
- 238000003908 quality control method Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 235000014347 soups Nutrition 0.000 description 1
- 238000007619 statistical method Methods 0.000 description 1
- 238000000528 statistical test Methods 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 150000003538 tetroses Chemical class 0.000 description 1
- 238000012549 training Methods 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- 210000003462 vein Anatomy 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Polymers & Plastics (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Nutrition Science (AREA)
- Mycology (AREA)
- Botany (AREA)
- Molecular Biology (AREA)
- Medicines Containing Plant Substances (AREA)
- Non-Alcoholic Beverages (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses a kind of inulin stachyose solid beverages, it belongs to new resource food technical field.The inulin stachyose solid beverage includes following components in percentage by weight: organic inulin 86.67% and stachyose 13.34%.The preparation method of the inulin stachyose solid beverage is the preparation of organic inulin；The preparation of stachyose；The mixing of organic inulin and stachyose.Raw material is planted using Qinghai-xizang Plateau Region, and growth course is polluted without pesticide, soil etc.；The full physics mode of pure plant extracts, and does not add any chemical solvent, Chinese and Western medicine ingredient etc.；Good water solubility, mouthfeel is slightly sweet, and entrance is smooth fresh and sweet taste, is easy to be accepted and eat.Promote gastrointestinal peristalsis, adjusts enteron aisle PH, improve constipation, adjust intestinal beneficial bacterium group structure, promote mineral matter element to absorb, reduce blood lipid.
Description
Technical field:
The present invention relates to a kind of inulin stachyose solid beverages, belong to new resource food technical field.
Background technique:
Inulin is used widely in American-European countries, and processing technology also relative maturity, is gradually formed to market
Monopolization.China's inulin industry starts to walk relatively late, and uses for reference sucrose processing process, generally existing technical level mostly
The situations such as low, factory automation, the not high, unstable product quality of continuous production degree.The product of processing can only go out as raw material
Mouthful, rather than a kind of high value added product, and it is external by purification processing, and export China back.Therefore for China, optimize inulin
The new separation and refining method of production technology, exploitation, raising added value of product are particularly important.
Inulin is the mixture of a kind of natural levulan, and inulin can reduce serum total cholesterol and low-density lipoprotein gallbladder is solid
Alcohol improves high-density lipoprotein/ldl ratio rate, improves status of blood lipid.Therefore inulin has heat low, prevention fertilizer
It is fat；Blood glucose is adjusted, blood glucose fluctuation is not caused；Reducing blood lipid prevents the functional characteristic of cardiovascular and cerebrovascular disease, can greatly improve Ca2+,
The absorption of the minerals such as Mg2+, Zn2+, Cu2+, Fe2+, promotes the absorption of minerals, and inulin is not digested absorption and is directly entered
Large intestine is preferentially utilized by Bifidobacterium, to inhibit the growth of harmful bacteria, establishes healthy gut flora.
Stachyose is a kind of naturally occurring tetrose, to beneficial bacteriums such as Bifidobacterium, Bacillus acidi lacticis in human gastrointestinal tract
Group has apparent proliferation function, can improve environment in human body alimentary canal, adsorbable gastrointestinal tract noxious material and pathogen rapidly, into
And it enhances human immunity, the physiological function of lowering blood pressure etc..Stachyose property is stablized, and stachyose is emerging function
Property oligosaccharide, be a kind of excellent functional food ingredient.But limitation is also compared for the research of stachyose and inulin at present.
Summary of the invention:
In view of the above-mentioned problems, the technical problem to be solved in the present invention is to provide a kind of inulin stachyose solid beverages.
Inulin stachyose solid beverage of the invention includes following components in percentage by weight: organic 86.67% He of inulin
Stachyose 13.34%.
The preparation method of inulin stachyose solid beverage of the invention is divided into three steps, the preparation of a, organic inulin；b,
The preparation of stachyose；C, the mixing of organic inulin and stachyose；Organic inulin the preparation method comprises the following steps: a1, jerusalem artichoke be sent into
Iron remover is first crossed before beet washer, except de-iron is miscellaneous, is then cleaned, and it is miscellaneous to reduce silt, weeds, iron-stone carried secretly in raw material etc.
Object, the raw material after over cleaning are crushed into pulverizer, and grain diameter is less than 5mm, then will be added in the raw material of crushing appropriate
Hot water, be stirred ingredient, material liquid mixture, which is sent into, extracts heating extraction in kettle, and in due course is passed through steam heating, temperature
Degree keeps the temperature 10min to 80 DEG C；Then be separated by solid-liquid separation: stirring feed liquid enters band filter, sleeping spiral shell, carries out in disk machine
It is separated by solid-liquid separation, the raw material that extracting solution is handled as subsequent handling；
A2, the concentration of extracting solution, decoloration and desalting processing, the extracting solution after being separated by solid-liquid separation are evaporated dense with evaporator
Contracting, until brix >=70%, the syrup feed liquid after concentration is put into storage tank: the syrup feed liquid in storage tank being heated, uses material after dilution
Pump squeezes into next process and carries out decolorization, and feed liquid crosses resin process, carries out macroporous resin adsorption decoloration；It is taken off after decoloration
Salt treatment: feed liquid crosses electrodialysis, is clarified after removing ionic impurity, use microorganism in micro-filtration removal feed liquid and impurity for
Clarify feed liquid；
The filtering and impurity removing of a3, feed liquid, feed liquid are filtered by film, and removal impurity sugar is simultaneously classified product, pass through film point
From feed liquid can be classified to inulin, oligofructose, the polyfructosan product solution of different size, then inulin feed liquid carries out
It being concentrated by evaporation, concentrate passes through spray drying after being sterilized by high-temperature instantaneous, and forming white powder finished product is inulin,
Then inulin finished product can be used after ultraviolet lamp sterilizes 30min；
The stachyose the preparation method comprises the following steps: Chinese artichoke dry product is soaked in water 1-2h, then go out at 80-100 DEG C
After enzyme 3-8 minutes, the water of 10-15 times of volume of Chinese artichoke weight is added, defibrination is carried out using fiberizer, by grinding slurry in 30-50
1-2h is extracted at DEG C, supernatant is collected by centrifugation, by supernatant through Bag filter, macroreticular resin decoloration, ultrafiltration purification and reverse osmosis
Spray drying obtains high purity stachyose powder after enrichment process.
C, the mixing of organic inulin and stachyose；Organic inulin of preparation and stachyose powder are mixed according to weight percent
Conjunction stirs evenly.
Beneficial effects of the present invention: 1, raw material is planted using Qinghai-xizang Plateau Region, and growth course is without dirts such as pesticide, soil
Dye；
2, the full physics mode of pure plant extracts, and does not add any chemical solvent, Chinese and Western medicine ingredient etc.；
3, effective component property is stablized, convenient, saves without particular forms such as refrigerations, can drink after being dissolved in water
With can also mix feed, such as soup, congee, milk, soya-bean milk with other foods, it is both effectiveness all to will not influence its；
4, good water solubility, mouthfeel is slightly sweet, and entrance is smooth fresh and sweet taste, is easy to be accepted and eat.
5, promote gastrointestinal peristalsis, adjust enteron aisle PH, improve constipation, adjust intestinal beneficial bacterium group structure, promote minerals member
Element absorbs, reduces blood lipid.
Detailed description of the invention
Fig. 1 is that prize-winning of embodiment of the present invention inulin stachyose is applied to real in the effect of hyperlipidemia patient effect for reducing fat
Test datagram；
Fig. 2 is that inulin of embodiment of the present invention stachyose improves the group that preceding constipation degree is tested in the research of elderly constipation effect
Between compare referring to figure；
Fig. 3 is the group that inulin of embodiment of the present invention stachyose improves constipation degree after test in the research of elderly constipation effect
Between compare referring to figure；
Fig. 4 is that inulin of embodiment of the present invention stachyose improves constipation before and after test-meal group test-meal in the research of elderly constipation effect
The comparison figure of degree；
Fig. 5 is that biochemistry refer to before and after two groups of test-meals in the research of inulin of embodiment of the present invention stachyose improvement elderly constipation effect
Target compares referring to figure.
Specific embodiment:
Present embodiment is described in further detail invention using following technical scheme and embodiment.
Inulin stachyose solid beverage includes following components in percentage by weight in present embodiment: organic inulin
86.67% and stachyose 13.34%.
The preparation method of the inulin stachyose solid beverage of this specific implementation is divided into three steps, the system of a, organic inulin
It is standby；B, the preparation of stachyose；C, the mixing of organic inulin and stachyose；Organic inulin the preparation method comprises the following steps: a1, jerusalem artichoke
It is sent into before beet washer and first crosses iron remover, except de-iron is miscellaneous, then cleaned, reduce silt, weeds, the iron-stone etc. carried secretly in raw material
Sundries, the raw material after over cleaning are crushed into pulverizer, and grain diameter is less than 5mm, then will be added in the raw material of crushing suitable
The hot water of amount is stirred ingredient, and material liquid mixture, which is sent into, extracts heating extraction in kettle, and the in due course steam that is passed through heats,
Temperature keeps the temperature 10min to 80 DEG C；Then be separated by solid-liquid separation: stirring feed liquid enter band filter, sleeping spiral shell, in disk machine into
Row is separated by solid-liquid separation, the raw material that extracting solution is handled as subsequent handling；
A2, the concentration of extracting solution, decoloration and desalting processing, the extracting solution after being separated by solid-liquid separation are evaporated dense with evaporator
Contracting, until brix >=70%, the syrup feed liquid after concentration is put into storage tank: the syrup feed liquid in storage tank being heated, uses material after dilution
Pump squeezes into next process and carries out decolorization, and feed liquid crosses resin process, carries out macroporous resin adsorption decoloration；It is taken off after decoloration
Salt treatment: feed liquid crosses electrodialysis, is clarified after removing ionic impurity, use microorganism in micro-filtration removal feed liquid and impurity for
Clarify feed liquid；
The filtering and impurity removing of a3, feed liquid, feed liquid are filtered by film, and removal impurity sugar is simultaneously classified product, pass through film point
From feed liquid can be classified to inulin, oligofructose, the polyfructosan product solution of different size, then inulin feed liquid carries out
It being concentrated by evaporation, concentrate passes through spray drying after being sterilized by high-temperature instantaneous, and forming white powder finished product is inulin,
Then inulin finished product can be used after ultraviolet lamp sterilizes 30min；
The stachyose the preparation method comprises the following steps: Chinese artichoke dry product is soaked in water 1-2h, then go out at 80-100 DEG C
After enzyme 3-8 minutes, the water of 10-15 times of volume of Chinese artichoke weight is added, defibrination is carried out using fiberizer, by grinding slurry in 30-50
1-2h is extracted at DEG C, supernatant is collected by centrifugation, by supernatant through Bag filter, macroreticular resin decoloration, ultrafiltration purification and reverse osmosis
Spray drying obtains high purity stachyose powder after enrichment process.
C, the mixing of organic inulin and stachyose；Organic inulin of preparation and stachyose powder are mixed according to weight percent
Conjunction stirs evenly.
Embodiment inulin stachyose solid beverage includes following components in percentage by weight: organic inulin 86.67% and water
Threose 13.34%.
The inulin stachyose of embodiment is applied to the observation of curative effect to hyperlipidemia patient effect for reducing fat, test is using double
Blind.After the test, A group is test group, takes stachyose；B group is control group, takes placebo (starch).Work as in taking
It and after taking 8 weeks, take forearm vein hematometry blood lipid on an empty stomach.TC, TG and HDL-C use enzymatic assays, and LDL-C is used
Friedwald formula calculates (in terms of mmol/L).Hepatic and renal function is measured simultaneously.Experimental data is as shown in Figure 1, experiment conclusion: water
Threose has an obvious effect for reducing fat to hyperlipemic patients, experiment show A group after 8 weeks total cholesterol density of serum than more significant drop
It is low, there is conspicuousness (P < 0.05) through statistical test difference.Concentration of low density lipoprotein cholesterol also has significant decrease, decline
Amplitude is statistically significant (P < 0.05).A group triglyceride concentration before take compared with also have reduction, but statistically difference
Without conspicuousness (P > 0.05).Test front and back is compared, and the indices of control group are showed no statistical difference.
Inulin stachyose improves the research of elderly constipation effect
Object and method, object collect elderly constipation patient by anal intestine section hospital, screen 120 volunteers, male
48, women 70 (has 8 male participants to be on home leave to other places, another 8 male participants do not take test-meal product as required halfway
And cause lost to follow-up)；It is the oldest=75 years old, minimum 60 years old, average age (64.7 ± 3.3) year；The course of disease is most 1 year short, longest 12
Year.Standard is included in referring to pertinent literature and standard
It is included in standard are as follows: be less than 9 persons within defecation one week；" defecation frequency reduces and stool hardness enhancer；Without it is organic just
Secret person；Habitual constipation person.Exclude by Grade III Class A hospital's physical examination have intestinal obstruction, severe digestive system and the heart, liver, brain,
The patient of the complication such as kidney.Defecation condition is divided into 4 grades: I grade (0 point) according to difficult defecation degree: defecation is normal.II grades (1
Point): only bearing down, sense of discomfort.' III level (2 points): bearing down, sense of discomfort are obvious or have just frequency but difficult defecation and a small amount of,
It is less abdominal pain or anus burn feeling occur.IV grades (3 points): abdominal pain or anus burn feeling often occur, influence defecation.Defecation character
Divide 3 grades: I grade (0 point): smooth and soft as sausage or snake；As sausage, but there is slight crack on its surface.II grades (1 point): sausage shaped
Shape, but have agglomerate；Loose bulk, edge roughness, as slimy excrement.III level (2 points): the hard group of separation, as fruit stone
(being not easy to be discharged).
Test method
Volunteer is divided into equal two groups of number of cases by the method for completely randomized design.30 days amounts are provided by double-blind study
Inulin stachyose (13+2) product or placebo, everyone 1 bag/d；Amount of drinking water guarantees to be not less than 1500ml/d；Clothes are provided simultaneously
With specification, points for attention, consulting telephone and take situation record.Fibre and placebo are by certain food production unit
It provides.Inulin stachyose (13+2) product weight 15g, every bag of 13g containing inulin, stachyose 2g；Placebo is purified starch.
Record sheet is collected, all subjects carry out the 2nd comprehensive physical examination in Grade III Class A hospital, to confirm the test to healthy nothing
Evil.
Investigation method questionnaire survey:
All subjects are respectively completed continuous 7 days defecations record (defecation frequency, defecation condition, excrement before and after test-meal
Just character) and daily ingestion of inulin stachyose (13+2) or the case where placebo (including adverse reaction).
Quality control
The training for carrying out inulin stachyose (13+2) relevant knowledge to volunteer before test-meal, makes it fully understand this experiment
Meaning and safety, dispel misgivings.To guarantee that volunteer has sufficient amount of drinking water (1500ml), the graduated drink of mark has been provided
Cup, and remind volunteer that test-meal product and water glass are placed on obvious place together.It is required that volunteer conscientiously fills in during test-meal
Every application form, including 7 days defecation records, edible time record, edible rear physical condition record.Regular telephone is reminded, every 2
It carries out telephone questionnaire to all volunteers, includes whether edible daily, if guarantee enough amounts of drinking water, if having adverse reaction
Deng.Conscientiously check application form, checked whether null term, logic error and distortion phenomenon, if discovery the above problem in time with aspiration
Person, which contacts, to be verified.
Statistical method test data is that measurement data, defecation condition and fecal character are assigned by grade scale (Bristol)
Different score values are given, adduction is added up.Test-meal group itself cross-reference uses paired t-test, it is edible after two groups of means compare using at
Group t is examined.Statistical software is spss17.The comparison among groups of constipation degree are referring to shown in Fig. 2 before testing, referring to shown in Fig. 2, it is seen that
The t that test-meal group is included in index with control group 3 is examined, and difference is not statistically significant, the equal > 0.05 of P.Illustrate that the research runs through
Random principle ensure that two groups of equilibrium.
The comparison among groups of constipation degree are referring to shown in Fig. 3 after test, the comparison among groups of constipation degree after test-meal,.Test-meal group
After test-meal compared with the control group, defecation frequency, defecation condition and fecal character difference are statistically significant (P < 0.01).
The comparison of constipation degree before and after test-meal group test-meal, referring to shown in Fig. 4, the paired t-test before and after test-meal is shown, defecation
Number, defecation condition, fecal character difference are statistically significant (P < 0.01).Investigation result is shown, increases inulin stachyose
The intake of (13+2) can be effectively improved constipation.
The comparison of two groups of test-meals front and back biochemical indicators is referring to Figure 5, it is seen that blood biochemistry index difference before and after two groups of test-meals
Not statistically significant (the equal > 0.05 of P).Illustrate that the intake for increasing inulin stachyose (13+2) in right amount will not influence normally
Blood biochemistry index.
Experiment conclusion: inulin stachyose (13+2) can improve the effect of constipation of old people, be tried using Double-blind randomized controlled
It tests, carries out the quantitative intervention for increasing inulin stachyose (13+2) in test group, control group eats placebo.It is soft using spss 17
Part analyzes the improvement of constipation degree between itself front and back and group.As a result the defecation frequency before and after test group itself, defecation condition, excrement
Character changes (P < 0.01)；Defecation frequency, defecation condition, fecal character after test-meal between group also statistically significant (P
< 0.01).Conclusion: by the intake of inulin stachyose (13+2), it can achieve the effect for improving constipation of old people.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (3)
1. a kind of inulin stachyose solid beverage, it is characterised in that: the inulin stachyose solid beverage includes following weight
The component of percentage: organic inulin 86.67% and stachyose 13.34%.
2. a kind of inulin stachyose solid beverage according to claim 1, it is characterised in that: the inulin stachyose is solid
The preparation method of body beverage is divided into three steps, the preparation of (a), organic inulin；(b), the preparation of stachyose；(c), organic inulin
With the mixing of stachyose.
3. a kind of inulin stachyose solid beverage according to claim 2, it is characterised in that: the system of organic inulin
Preparation Method are as follows: (a1), jerusalem artichoke, which are sent into before beet washer, first crosses iron remover, except de-iron is miscellaneous, is then cleaned, reduces and carry secretly in raw material
The sundries such as silt, weeds, iron-stone, the raw material after over cleaning crushes into pulverizer, and grain diameter is less than 5mm, then will
Suitable hot water is added in the raw material of crushing, is stirred ingredient, material liquid mixture, which is sent into, extracts heating extraction in kettle, and fits
When be passed through steam heating, temperature to 80 DEG C, keep the temperature 10min；Then be separated by solid-liquid separation: stirring feed liquid enters belt type filter
Machine, sleeping spiral shell are separated by solid-liquid separation in disk machine, the raw material that extracting solution is handled as subsequent handling；
(a2), the concentration, decoloration and desalting processing of extracting solution, the extracting solution after being separated by solid-liquid separation are evaporated dense with evaporator
Contracting, until brix >=70%, the syrup feed liquid after concentration is put into storage tank: the syrup feed liquid in storage tank being heated, uses material after dilution
Pump squeezes into next process and carries out decolorization, and feed liquid crosses resin process, carries out macroporous resin adsorption decoloration；It is taken off after decoloration
Salt treatment: feed liquid crosses electrodialysis, is clarified after removing ionic impurity, use microorganism in micro-filtration removal feed liquid and impurity for
Clarify feed liquid；
(a3), the filtering and impurity removing of feed liquid, feed liquid are filtered by film, and removal impurity sugar is simultaneously classified product, pass through UF membrane
Feed liquid can be classified to inulin, oligofructose, the polyfructosan product solution of different size, then inulin feed liquid is steamed
Hair concentration, concentrate pass through spray drying after being sterilized by high-temperature instantaneous, and forming white powder finished product is inulin, so
Inulin finished product can be used after ultraviolet lamp sterilizes 30min afterwards；
(b), the stachyose the preparation method comprises the following steps: Chinese artichoke dry product is soaked in water 1-2h, then go out at 80-100 DEG C
After enzyme 3-8 minutes, the water of 10-15 times of volume of Chinese artichoke weight is added, defibrination is carried out using fiberizer, by grinding slurry in 30-50
1-2h is extracted at DEG C, supernatant is collected by centrifugation, by supernatant through Bag filter, macroreticular resin decoloration, ultrafiltration purification and reverse osmosis
Spray drying obtains high purity stachyose powder after enrichment process；
(c), the mixing of organic inulin and stachyose；Organic inulin of preparation and stachyose powder are mixed according to weight percent
It stirs evenly.
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| CN104844733A (en) * | 2015-05-04 | 2015-08-19 | 武汉英纽林生物科技有限公司 | Production technique for extracting high-purity pure natural inulin from Jerusalem artichoke |
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| US20070042992A1 (en) * | 2000-02-15 | 2007-02-22 | Anne Frippiat | Inulin products with improved nutritional properties |
| CN101037480A (en) * | 2006-03-15 | 2007-09-19 | 中国科学院大连化学物理研究所 | Method for producing high-quality inulin by using jerusalem artichoke as raw material |
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