CN109354928A - A kind of organic mat special-used colour starch and preparation method thereof - Google Patents
A kind of organic mat special-used colour starch and preparation method thereof Download PDFInfo
- Publication number
- CN109354928A CN109354928A CN201810818644.XA CN201810818644A CN109354928A CN 109354928 A CN109354928 A CN 109354928A CN 201810818644 A CN201810818644 A CN 201810818644A CN 109354928 A CN109354928 A CN 109354928A
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- Prior art keywords
- parts
- revolving speed
- sanded
- deionized water
- 25rpm
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 229920002472 Starch Polymers 0.000 title claims abstract description 15
- 235000019698 starch Nutrition 0.000 title claims abstract description 15
- 239000008107 starch Substances 0.000 title claims abstract description 15
- 238000002360 preparation method Methods 0.000 title abstract description 5
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000008367 deionised water Substances 0.000 claims abstract description 19
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 19
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 18
- -1 hydramine ethers Chemical class 0.000 claims abstract description 14
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 11
- 239000002562 thickening agent Substances 0.000 claims abstract description 10
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 8
- 229920000142 Sodium polycarboxylate Polymers 0.000 claims abstract description 7
- 239000003139 biocide Substances 0.000 claims abstract description 7
- 239000000470 constituent Substances 0.000 claims abstract description 7
- MGIYRDNGCNKGJU-UHFFFAOYSA-N isothiazolinone Chemical compound O=C1C=CSN1 MGIYRDNGCNKGJU-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004576 sand Substances 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 11
- 239000000843 powder Substances 0.000 claims description 10
- 239000006185 dispersion Substances 0.000 claims description 9
- 238000000227 grinding Methods 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 7
- 239000002002 slurry Substances 0.000 claims description 7
- 238000004140 cleaning Methods 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 5
- 230000000855 fungicidal effect Effects 0.000 claims description 4
- 239000000417 fungicide Substances 0.000 claims description 4
- 238000012790 confirmation Methods 0.000 claims description 3
- 238000001514 detection method Methods 0.000 claims description 3
- 239000002270 dispersing agent Substances 0.000 claims description 3
- 239000001034 iron oxide pigment Substances 0.000 claims description 3
- 238000003801 milling Methods 0.000 claims description 3
- 239000003960 organic solvent Substances 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 239000002699 waste material Substances 0.000 claims description 3
- 239000000080 wetting agent Substances 0.000 claims description 3
- 229910002012 Aerosil® Inorganic materials 0.000 claims 1
- 229910021485 fumed silica Inorganic materials 0.000 abstract description 6
- 239000005416 organic matter Substances 0.000 abstract description 6
- 241000894006 Bacteria Species 0.000 abstract description 3
- 238000000855 fermentation Methods 0.000 abstract description 2
- 230000004151 fermentation Effects 0.000 abstract description 2
- 238000005507 spraying Methods 0.000 abstract description 2
- 238000000576 coating method Methods 0.000 description 5
- 239000011248 coating agent Substances 0.000 description 4
- 239000002689 soil Substances 0.000 description 3
- 238000004040 coloring Methods 0.000 description 2
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 150000003077 polyols Chemical class 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/001—Pigment pastes, e.g. for mixing in paints in aqueous medium
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/002—Pigment pastes, e.g. for mixing in paints in organic medium
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/004—Pigment pastes, e.g. for mixing in paints containing an inorganic pigment
- C09D17/007—Metal oxide
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of organic mat special-used colour starch, component including following parts by weight: 150 ~ 180 parts of deionized water, 20 ~ 40 parts of sodium polycarboxylate dipersant, 1 ~ 5 part of the nonionic surfactant of 95% active constituent, 1 ~ 5 part of hydramine ethers organic matter, 1 ~ 5 part of Lauryl Alcohol ester coalescing agent, 0.1 ~ 2 part of isothiazolinone biocide agent, 70 ~ 85 parts of propylene glycol and 0.5 ~ 2 part of fumed silica thickener.Meanwhile the invention also discloses the preparation methods of above-mentioned special-used colour starch.The mill base that the present invention produces perfect can be applied to organic mat, after spraying is dried, nearly all mill base can not be smeared with hand with paper, directly being rushed with water also can not rinse, stack in fermentation process will not because of bacterium colony growth and rotten fall off that generates mill base is faded.
Description
Technical field
The invention belongs to chemical fields, and in particular to a kind of organic mat special-used colour starch and preparation method thereof.
Background technique
The especially U.S. of most of American-European countries, has popularized the use of organic mat, organic mat be with
A kind of covering for being layered on soil ground that recycling branch timber etc. produces, the covering can improve soil quality, Ke Nengqi
To the effect of beautification.Common business mill base is released both for coatings enterprises, and it is to put that coating manufacturer, which buys back mill base later,
Just paint what the inside was used to mix colours in base, it usually needs what is considered is storage and color etc., is also to see coating manufacturer
The coating of production is used in what field, the opposite requirement for having some this aspects, and film forming coloring is typically all that coating needs to consider
, mill base is without consideration.
Mill base on the market at present, can seldom be directly used in coloring, be painted on dielectric surface, it is easy to be smeared down
Come, can not also be subjected to rain drop erosion, the requirement of organic mat needs is not achieved.
Summary of the invention
Goal of the invention: in view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide a kind of organic mat special color
Slurry.
Another object of the present invention is to provide the preparation methods of above-mentioned organic mat special-used colour starch.
Technical solution: in order to achieve the above object of the invention, what the present invention was specifically performed by: a kind of organic mat
Special-used colour starch, the component including following parts by weight: 150 ~ 180 parts of deionized water, 20 ~ 40 parts of sodium polycarboxylate dipersant, 95%
1 ~ 5 part of the nonionic surfactant of active constituent, 1 ~ 5 part of hydramine ethers organic matter, 1 ~ 5 part of Lauryl Alcohol ester coalescing agent,
0.1 ~ 2 part of isothiazolinone biocide agent, 70 ~ 85 parts of propylene glycol and 0.5 ~ 2 part of fumed silica thickener.
Wherein, the nonionic surfactant is preferably polyoxyethylene-type, polyol type.
The method for preparing the organic mat special-used colour starch, comprising the following steps:
Dispersion stage:
(1) dispersing agent, wetting agent, multifunctional assistant and the coalescing agent of formula ratio are successively put into scuffing of cylinder bore, and are added and are matched
The deionized water of side's amount 90% starts high speed disperser for revolving speed and rises to 1000 ± 25RPM, and stirring 5 minutes is to uniform；
(2) it keeping revolving speed constant, sequentially adds the fungicide, organic solvent and thickener of formula ratio, revolving speed remains unchanged, point
It dissipates 10 minutes；
(3) revolving speed is turned down to 600 ± 25RPM, successively puts into iron oxide pigment powder, powder rate of feeding guarantees liquid level not heap
Product finishes and clean casing wall and agitator disk with washing cylinder water after material, adjusts revolving speed to 1500 ± 25RPM, dispersion 30 minutes；
(4) test temperature is lower than 55 DEG C and fineness is less than 15 microns, stops stirring；
The grinding stage:
(1) deionized water outside preceding formula is sanded to grinding gun barrel wash cycles 10min, is sanded after confirmation cleaning, sand
Mill sinciput output is to grind between the 1/3 ~ 1/2 of gun barrel volume, is packed into waste liquid barrel；
(2) it after getting out scattered mixed material, opens and electromechanical source is sanded, first open mateiral pump 2 ~ 4
After minute, sand mill is opened, is sanded 2 ~ 4 times；
(3) it has been sanded and has cleaned sand mill with the remaining deionized water of formula, and cleaning solution has been incorporated in sand milling slurry, stirring is equal
It is even, when viscosity stopping stirring after simultaneously fineness is less than 15 microns by 85 ~ 95KU；
It is let down:
Slurry investment will be sanded to be let down in cylinder, revolving speed is that 1000 ± 25RPM is stirred 10 minutes, and viscosity is controlled in 85 ~ 95KU, works as viscosity
Viscosity is not adjusted with deionized water in above range to the range, is every time 800 ± 25RPM dispersion 15 with revolving speed after charging
Minute sample detection again.
The utility model has the advantages that the present invention, compared with traditional technology, there are following advantages:
(1) present invention joined propylene glycol in formula, can play a part of waterborne film-forming, while as solvent, adding
Coalescing agent, completes the compatibility of system；
(2) because organic mat needs to be layered on soil from level to level on the ground, so many bacterium can be bred on beneath organic mat
The presence of class, mushroom can destroy the stability of mill base, so joined fungicide in formula；
(3) mill base produced of the present invention perfect can be applied to organic mat, after spraying is dried, with hand paper nearly all without
Mill base is smeared by method, and directly being rushed with water also can not rinse, stack fermentation process in will not because of bacterium colony growth and
Rotten fall off for generating mill base is faded.
Specific embodiment
Embodiment 1:
A kind of organic mat special-used colour starch, the component including following parts by weight: 150 parts of deionized water, sodium polycarboxylate salinity
20 parts of powder, 1 part of the nonionic surfactant of 95% active constituent, 1 part of hydramine ethers organic matter, Lauryl Alcohol ester film forming help
1 part of agent, 0.1 part of isothiazolinone biocide agent, 70 parts of propylene glycol and 0.5 part of fumed silica thickener.
Embodiment 2:
A kind of organic mat special-used colour starch, the component including following parts by weight: 180 parts of deionized water, sodium polycarboxylate salinity
40 parts of powder, 5 parts of the nonionic surfactant of 95% active constituent, 5 parts of hydramine ethers organic matter, Lauryl Alcohol ester film forming help
5 parts of agent, 2 parts of isothiazolinone biocide agent, 85 parts of propylene glycol and 2 parts of fumed silica thickener.
Embodiment 3:
A kind of organic mat special-used colour starch, the component including following parts by weight: 160 parts of deionized water, sodium polycarboxylate salinity
30 parts of powder, 3 parts of the nonionic surfactant of 95% active constituent, 2 parts of hydramine ethers organic matter, Lauryl Alcohol ester film forming help
3 parts of agent, 0.5 part of isothiazolinone biocide agent, 75 parts of propylene glycol and 1 part of fumed silica thickener.
Embodiment 4:
A kind of organic mat special-used colour starch, the component including following parts by weight: 170 parts of deionized water, sodium polycarboxylate salinity
25 parts of powder, 4 parts of the nonionic surfactant of 95% active constituent, 3 parts of hydramine ethers organic matter, Lauryl Alcohol ester film forming help
2 parts of agent, 0.5 part of isothiazolinone biocide agent, 75 parts of propylene glycol and 1.5 parts of fumed silica thickener.
Embodiment 5:
The method for preparing the organic mat special-used colour starch, including dispersion stage, grinding stage and be let down,
Dispersion stage: successively putting into dispersing agent, wetting agent, multifunctional assistant and the coalescing agent of formula ratio in scuffing of cylinder bore, and
The deionized water of formula ratio 90% is added, starts high speed disperser for revolving speed and rises to 1000 ± 25RPM, stirring 5 minutes is to uniform；
It keeps revolving speed constant, sequentially adds the fungicide, organic solvent and thickener of formula ratio, revolving speed remains unchanged, and disperses 10 points
Clock；Revolving speed to be turned down to 600 ± 25RPM, iron oxide pigment powder is successively put into, powder rate of feeding guarantees that liquid level is not accumulated,
It finishes and clean casing wall and agitator disk with washing cylinder water after material, adjust revolving speed to 1500 ± 25RPM, dispersion 30 minutes；Test temperature is low
In 55 DEG C, simultaneously fineness is less than 15 microns, stopping stirring.
The grinding stage: the deionized water outside preceding formula is sanded to grinding gun barrel wash cycles 10min, confirmation cleaning is laggard
Row is sanded, and it is to grind between the 1/3 ~ 1/2 of gun barrel volume that sinciput output, which is sanded, is packed into waste liquid barrel；By scattered mixture
After material is ready to, opens and electromechanical source is sanded, first open mateiral pump 2 ~ 4
After minute, sand mill is opened, is sanded 2 ~ 4 times；It has been sanded and has cleaned sand mill with the remaining deionized water of formula, and will cleaning
Liquid is incorporated in sand milling slurry, is stirred evenly, when viscosity stopping stirring after simultaneously fineness is less than 15 microns by 85 ~ 95KU.
Be let down: slurry investment will be sanded and be let down in cylinder, revolving speed is that 1000 ± 25RPM is stirred 10 minutes, viscosity control 85 ~
95KU, viscosity is adjusted with deionized water when viscosity is not in above range to the range, every time after charging with revolving speed be 800 ±
25RPM disperses 15 minutes sample detections again.
Claims (2)
1. a kind of organic mat special-used colour starch, which is characterized in that the component including following parts by weight: deionized water 150 ~
180 parts, 20 ~ 40 parts of sodium polycarboxylate dipersant, 1 ~ 5 part of nonionic surfactant, the hydramine ethers of 95% active constituent it is organic
1 ~ 5 part of object, 1 ~ 5 part of Lauryl Alcohol ester coalescing agent, 0.1 ~ 2 part of isothiazolinone biocide agent, 70 ~ 85 parts of propylene glycol and gas
0.5 ~ 2 part of aerosil thickener.
2. the method for preparing organic mat special-used colour starch described in claim 1, which comprises the following steps:
Dispersion stage:
(1) dispersing agent, wetting agent, multifunctional assistant and the coalescing agent of formula ratio are successively put into scuffing of cylinder bore, and are added and are matched
The deionized water of side's amount 90% starts high speed disperser for revolving speed and rises to 1000 ± 25RPM, and stirring 5 minutes is to uniform；
(2) it keeping revolving speed constant, sequentially adds the fungicide, organic solvent and thickener of formula ratio, revolving speed remains unchanged, point
It dissipates 10 minutes；
(3) revolving speed is turned down to 600 ± 25RPM, successively puts into iron oxide pigment powder, powder rate of feeding guarantees liquid level not heap
Product finishes and clean casing wall and agitator disk with washing cylinder water after material, adjusts revolving speed to 1500 ± 25RPM, dispersion 30 minutes；
(4) test temperature is lower than 55 DEG C and fineness is less than 15 microns, stops stirring；
The grinding stage:
(1) deionized water outside preceding formula is sanded to grinding gun barrel wash cycles 10min, is sanded after confirmation cleaning, sand
Mill sinciput output is to grind between the 1/3 ~ 1/2 of gun barrel volume, is packed into waste liquid barrel；
(2) it after getting out scattered mixed material, opens and electromechanical source is sanded, first open mateiral pump 2 ~ 4
After minute, sand mill is opened, is sanded 2 ~ 4 times；
(3) it has been sanded and has cleaned sand mill with the remaining deionized water of formula, and cleaning solution has been incorporated in sand milling slurry, stirring is equal
It is even, when viscosity stopping stirring after simultaneously fineness is less than 15 microns by 85 ~ 95KU；
It is let down:
Slurry investment will be sanded to be let down in cylinder, revolving speed is that 1000 ± 25RPM is stirred 10 minutes, and viscosity is controlled in 85 ~ 95KU, works as viscosity
Viscosity is not adjusted with deionized water in above range to the range, is every time 800 ± 25RPM dispersion 15 with revolving speed after charging
Minute sample detection again.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810818644.XA CN109354928A (en) | 2018-07-24 | 2018-07-24 | A kind of organic mat special-used colour starch and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810818644.XA CN109354928A (en) | 2018-07-24 | 2018-07-24 | A kind of organic mat special-used colour starch and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109354928A true CN109354928A (en) | 2019-02-19 |
Family
ID=65349757
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810818644.XA Pending CN109354928A (en) | 2018-07-24 | 2018-07-24 | A kind of organic mat special-used colour starch and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109354928A (en) |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060048675A1 (en) * | 2002-10-10 | 2006-03-09 | Basf Aktiengesellschaft | Use of preparations comprising pigments and dyestuffs for the decorative colouring of derived timber products |
| CN102352156A (en) * | 2011-06-22 | 2012-02-15 | 浙江虹越花卉有限公司 | Color paste for production of color green garden mulching material and preparation method thereof |
| CN102504649A (en) * | 2011-11-08 | 2012-06-20 | 陈绍球 | Polishing agent for wood surfaces and preparation method |
| CN104191481A (en) * | 2014-09-09 | 2014-12-10 | 天津工业大学 | New method for dyeing wood chips used as ground coverings of urban landscapes |
| CN104356761A (en) * | 2014-11-14 | 2015-02-18 | 赵旖春 | Pure solid wood organic mulch dyeing basic solution and production process thereof |
| CN105440925A (en) * | 2015-12-09 | 2016-03-30 | 三棵树涂料股份有限公司 | Waterborne woodware surface color modifier |
| US9579817B1 (en) * | 2012-12-18 | 2017-02-28 | Carlos Jose Mongalo Robleto | Process floor staining wood with fluorescent dyes and pigments |
| CN107903717A (en) * | 2017-11-29 | 2018-04-13 | 长春市林海景晟科技有限责任公司 | A kind of organic mat colouring compositions and preparation method thereof |
-
2018
- 2018-07-24 CN CN201810818644.XA patent/CN109354928A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060048675A1 (en) * | 2002-10-10 | 2006-03-09 | Basf Aktiengesellschaft | Use of preparations comprising pigments and dyestuffs for the decorative colouring of derived timber products |
| CN102352156A (en) * | 2011-06-22 | 2012-02-15 | 浙江虹越花卉有限公司 | Color paste for production of color green garden mulching material and preparation method thereof |
| CN102504649A (en) * | 2011-11-08 | 2012-06-20 | 陈绍球 | Polishing agent for wood surfaces and preparation method |
| US9579817B1 (en) * | 2012-12-18 | 2017-02-28 | Carlos Jose Mongalo Robleto | Process floor staining wood with fluorescent dyes and pigments |
| CN104191481A (en) * | 2014-09-09 | 2014-12-10 | 天津工业大学 | New method for dyeing wood chips used as ground coverings of urban landscapes |
| CN104356761A (en) * | 2014-11-14 | 2015-02-18 | 赵旖春 | Pure solid wood organic mulch dyeing basic solution and production process thereof |
| CN105440925A (en) * | 2015-12-09 | 2016-03-30 | 三棵树涂料股份有限公司 | Waterborne woodware surface color modifier |
| CN107903717A (en) * | 2017-11-29 | 2018-04-13 | 长春市林海景晟科技有限责任公司 | A kind of organic mat colouring compositions and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 韩丽莉等: "《种植屋面疑难问题解答》", 30 June 2018, 中国建材工业出版社 * |
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Application publication date: 20190219 |