CN109157489A - A kind of preparation method of skin care compositions and facial mask with antibacterial functions - Google Patents
A kind of preparation method of skin care compositions and facial mask with antibacterial functions Download PDFInfo
- Publication number
- CN109157489A CN109157489A CN201811089059.7A CN201811089059A CN109157489A CN 109157489 A CN109157489 A CN 109157489A CN 201811089059 A CN201811089059 A CN 201811089059A CN 109157489 A CN109157489 A CN 109157489A
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- care compositions
- skin care
- antibacterial functions
- facial mask
- film forming
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- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 57
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- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims abstract description 26
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- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims abstract description 19
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/04—Antibacterial agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Organic Chemistry (AREA)
- Communicable Diseases (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Chemical & Material Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Zoology (AREA)
- Oncology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Emergency Medicine (AREA)
- Biophysics (AREA)
- Molecular Biology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses the preparation methods of a kind of skin care compositions with antibacterial functions and facial mask.The raw material of the skin care compositions is made of Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, lecithin, Phenoxyethanol, triethanolamine etc..The above-mentioned skin care compositions with antibacterial functions can be facial mask, preparation method is specifically that film forming agent is added in deionized water, insulated and stirred to film forming agent is completely dissolved after heating, obtain base soln, again by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, alchlor, which is added in base soln, carries out insulated and stirred, Radix et Caulis Opuntiae Dillenii extract is added after solution cooling, nutgall extractive, lecithin, Phenoxyethanol, essence, preservative stirring, pH is adjusted again, finally move to stirring and emulsifying in mulser, it is filling after the screen to filtrate, obtain finished product facial mask.This has the effect of that the skin care compositions of antibacterial functions has and effectively inhibits the breeding of skin surface harmful bacteria, uses suitable for the crowd with bacterial dermatitis.
Description
Technical field
The present invention relates to cosmetic technical fields, more particularly to a kind of skin care compositions and facial mask with antibacterial functions
Preparation method.
Background technique
The principle of facial mask is temporarily isolating extraneous air and pollution, improves exactly using the of short duration time for being covered on face
Skin temperature, the pore expansion of skin, promotes sweat gland secretion and metabolism, increase the oxygen content of skin, be conducive to skin
The product of epidermal cell metabolism and the oil substances of accumulation are excluded, the moisture in facial mask penetrates into the cutin of skin epidermis
Layer, skin become soft, increase elasticity.Skin is naturally bright flexible, and aerobic color is presented.Facial mask is one kind of face beautifying health keeping product
Carrier, using fexible film as basic material, with contained thereon nourishing ingredient and direct facial contact, thus when reaching long
Between maintaining skin purpose.Since the face pack prescription of the prior art contains certain organic components, rear face hair is used
Kong Zhongyi residual organic matter increases microorganism in this case and colonizes risk.If staphylococcus aureus is exactly a kind of skin
The common bacterium in skin surface, this bacterium can cause a variety of diseases, for example, it be skin and Soft Tissue Abscess: An Experimental, furuncle and
The first cause of cellulitis.
Summary of the invention
The problem of not still being able to satisfy consumer demand the effect of inhibiting in terms of skin surface bacterium based on contemporary skin care product,
The present invention provides the preparation method of a kind of skin care compositions with antibacterial functions and facial mask.
A kind of skin care compositions with antibacterial functions, the raw material of the skin care compositions is by Radix et Caulis Opuntiae Dillenii extract, five times
Seed extract, lecithin, Phenoxyethanol, triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, hyaluronic acid
Sodium, glycerol, alchlor, essence, film forming agent, preservative, deionized water composition.
The above-mentioned skin care compositions with antibacterial functions contain be made of Radix et Caulis Opuntiae Dillenii extract, nutgall extractive it is natural
The functional components such as effective component and lecithin, Phenoxyethanol, triethanolamine, each component are giving full play to respective basic function
, can be synergistic except effect, effectively adjust human endocrine.The skin care compositions with antibacterial functions, which has, effectively to be inhibited
The effect of skin surface harmful bacteria breeding, uses suitable for the crowd with bacterial dermatitis.
In one of the embodiments, the raw material of the skin care compositions according to parts by weight, concrete composition are as follows:
Radix et Caulis Opuntiae Dillenii extract 1.5~2.5%
Nutgall extractive 0.8~2.2%
Lecithin 0.08~0.3%
Phenoxyethanol 0.6~3.0%
Triethanolamine 0.2~0.8%
Hydroxyethyl cellulose 0.4~2.5%
Talcum powder 0.08~1.2%
Polysorbate alcohol -801.5~3.0%
Sodium Hyaluronate 2.0~3.0%
Glycerol 2.5~8.5%
Alchlor 0.06~0.12%
Essence 0.05~0.09%
Film forming agent 5.0~7.5%
Preservative 0.3~1.0%
Deionized water surplus.
The raw material of the skin care compositions according to parts by weight, specifically comprises in one of the embodiments,
Radix et Caulis Opuntiae Dillenii extract 2.0%
Nutgall extractive 1.5%
Lecithin 0.19%
Phenoxyethanol 1.6%
Triethanolamine 0.5%
Hydroxyethyl cellulose 1.5%
Talcum powder 0.8%
Polysorbate alcohol -802.2%
Sodium Hyaluronate 2.5%
Glycerol 5.5%
Alchlor 0.09%
Essence 0.07%
Film forming agent 6.3%
Preservative 0.7%
Deionized water surplus.
The film forming agent is in polyvinyl alcohol, dextrin, hydroxymethyl cellulose, carragheen in one of the embodiments,
One or more.
The preservative is in ethylparaben, Nipasol, triclosan, sorbic acid in one of the embodiments,
One or more.
The skin care compositions is facial mask in one of the embodiments,.
The present invention also provides the preparation methods of the above-mentioned facial mask with antibacterial functions, comprise the steps of:
(1) film forming agent is added in deionized water, solution is then heated to 80~85 DEG C, keep the temperature 20~30 minutes, and
Being stirred according to 250~350 revs/min of rate to solution is completely dissolved film forming agent, obtains base soln；
(2) by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, trichlorine
Change aluminium to be added in step (1) resulting base soln, solution temperature is maintained 65~75 DEG C, according to 250~350 revs/min
The rate of clock stirs 25~35 minutes；
(3) step (2) resulting solution is cooled to 40~50 DEG C, Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, ovum is added
Phosphatide, Phenoxyethanol, essence, preservative stir 15~20 minutes according to 250~350 revs/min of rates, by mixture
PH is adjusted to 6~8, obtains intermediate solution；
(4) step (3) resulting intermediate solution is transferred in mulser, stirring and emulsifying 45 minutes, after the screen to filtrate
It is filling, obtain finished product facial mask.
The preparation method of the above-mentioned facial mask with antibacterial functions, raw material is easy to get, simple process, is suitable for heavy industrialization
Production.
The sodium hydroxide solution that concentration is 8% is selected to adjust mixture in the step (3) in one of the embodiments,
PH.
The rate of stirring and emulsifying is 1500~2500 revs/min in the step (4) in one of the embodiments,.
The present invention also provides application of the skin care compositions with antibacterial functions in mask product preparation.
Specific embodiment
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, below in conjunction with specific embodiment,
The present invention will be described in further detail.It should be appreciated that the specific embodiments described herein are only used to explain this hair
It is bright, it is not intended to limit the present invention.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention
The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term " and or " used herein includes one or more
Any and all combinations of relevant listed item.
Raw materials used and reagent is commercially available common raw material and reagent in following embodiment.
A kind of skin care compositions with antibacterial functions, the raw material of the skin care compositions is by Radix et Caulis Opuntiae Dillenii extract, five times
Seed extract, lecithin, Phenoxyethanol, triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, hyaluronic acid
Sodium, glycerol, alchlor, essence, film forming agent, preservative, deionized water composition.
Wherein, fleshy stem protein rich in, minerals, cellulose and the vitamin C etc. of cactus plumpness, simultaneously
The various actives functional components such as SOD, flavonoids and polysaccharide rich in.Radix et Caulis Opuntiae Dillenii extract may penetrate into skin inner layer,
It improves the anti-oxidant of skin and promotes moisturizing, dispel melanin, keep skin surface brilliant white.
Wherein, Chinese gall is parasitic times Aphidiadae insect horned gall aphid on the trees such as Anacardiaceae plant Chinese sumac, potanin sumac, redpunjab sumac root
Or the insect gall formed after berry-gall aphid.Chinese gall main component is tannic acid, to staphylococcus aureus, streptococcus, pneumococcus
And typhoid bacillus, paratyphosum Bacterium, shigella dysenteriae, bacillus anthracis, corynebacterium diphtheriae, Pseudomonas aeruginosa etc. have it is apparent antibacterial or
Bactericidal effect.Chinese gall has astringing lung-QI fall fire, relieving diarrhea with astringents, astringent sperm contracting urine, hidroschesis, hemostasis, removing toxic substances, sore as traditional Chinese medicine
Etc. various clinicals effect.
Wherein, lecithin, also known as lecithin are known as " third nutrient " arranged side by side with protein, vitamin.Lecithin
Rouge is the indispensable substance of each cell of human body, if lacked, will reduce the power of regeneration of Skin Cell, lead to skin
It is coarse, have wrinkle.As can suitably absorbing lecithin, skin regeneration vigor can be ensured, along with lecithin is good hydrophilic
Property and lipophilicity, skin are able to maintain gloss.
Wherein, Phenoxyethanol is a kind of fine chemical product and organic synthesis intermediate, and a kind of higher boiling, low volatility are molten
Agent, but be a kind of low sensitization, efficiently, the anticorrosion and bactericidal agent of wide spectrum.It is in the industrial applications frequency such as light industry, daily use chemicals, pesticide, medicine
It is higher and higher, there is very high realistic meaning and economic benefit.
The above-mentioned skin care compositions with antibacterial functions contain be made of Radix et Caulis Opuntiae Dillenii extract, nutgall extractive it is natural
The functional components such as effective component and lecithin, Phenoxyethanol, triethanolamine, each component are giving full play to respective basic function
, can be synergistic except effect, effectively adjust human endocrine.The skin care compositions with antibacterial functions, which has, effectively to be inhibited
The effect of skin surface harmful bacteria breeding, uses suitable for the crowd with bacterial dermatitis.
In a preferred embodiment, the raw material of the skin care compositions according to parts by weight, concrete composition are as follows:
Radix et Caulis Opuntiae Dillenii extract 1.5~2.5%
Nutgall extractive 0.8~2.2%
Lecithin 0.08~0.3%
Phenoxyethanol 0.6~3.0%
Triethanolamine 0.2~0.8%
Hydroxyethyl cellulose 0.4~2.5%
Talcum powder 0.08~1.2%
Polysorbate alcohol -801.5~3.0%
Sodium Hyaluronate 2.0~3.0%
Glycerol 2.5~8.5%
Alchlor 0.06~0.12%
Essence 0.05~0.09%
Film forming agent 5.0~7.5%
Preservative 0.3~1.0%
Deionized water surplus.
In one more preferably embodiment, the raw material of the skin care compositions according to parts by weight, is specifically comprised
Radix et Caulis Opuntiae Dillenii extract 2.0%
Nutgall extractive 1.5%
Lecithin 0.19%
Phenoxyethanol 1.6%
Triethanolamine 0.5%
Hydroxyethyl cellulose 1.5%
Talcum powder 0.8%
Polysorbate alcohol -802.2%
Sodium Hyaluronate 2.5%
Glycerol 5.5%
Alchlor 0.09%
Essence 0.07%
Film forming agent 6.3%
Preservative 0.7%
Deionized water surplus.
In a preferred embodiment, the film forming agent is selected from polyvinyl alcohol, dextrin, hydroxymethyl cellulose, carragheen
One or more of.
In a preferred embodiment, the preservative is selected from ethylparaben, Nipasol, triclosan, sorbic acid
One or more of.
In a preferred embodiment, the skin care compositions is facial mask.
The present invention also provides the preparation methods of the above-mentioned facial mask with antibacterial functions, comprise the steps of:
(1) film forming agent is added in deionized water, solution is then heated to 80~85 DEG C, keep the temperature 20~30 minutes, and
Being stirred according to 250~350 revs/min of rate to solution is completely dissolved film forming agent, obtains base soln；
(2) by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, trichlorine
Change aluminium to be added in step (1) resulting base soln, solution temperature is maintained 65~75 DEG C, according to 250~350 revs/min
The rate of clock stirs 25~35 minutes；
(3) step (2) resulting solution is cooled to 40~50 DEG C, Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, ovum is added
Phosphatide, Phenoxyethanol, essence, preservative stir 15~20 minutes according to 250~350 revs/min of rates, by mixture
PH is adjusted to 6~8, obtains intermediate solution；
(4) step (3) resulting intermediate solution is transferred in mulser, stirring and emulsifying 45 minutes, after the screen to filtrate
It is filling, obtain finished product facial mask.
In a preferred embodiment, the Radix et Caulis Opuntiae Dillenii extract, nutgall extractive the preparation method comprises the following steps: by corresponding
Vegetable raw material pulverize and sieve, obtained powder is added separately in ethanol solution, is filtered after ultrasonic treatment, by collection
Filtrate decompression distillation, obtains corresponding extract.
In a preferred embodiment, the sodium hydroxide solution that concentration is 8% is selected to adjust mixing in the step (3)
The pH of object.
In a preferred embodiment, the rate of stirring and emulsifying is 1500~2500 revs/min in the step (4).
The present invention also provides application of the above-mentioned skin care compositions with antibacterial functions in mask product preparation
Below by embodiment, the present invention is furture elucidated.It should be pointed out that the present invention is not intended to be limited to the reality
Apply example.
Embodiment 1
The face pack prescription with antibacterial functions of the present embodiment is as follows:
Radix et Caulis Opuntiae Dillenii extract 2.0%
Nutgall extractive 1.5%
Lecithin 0.19%
Phenoxyethanol 1.6%
Triethanolamine 0.5%
Hydroxyethyl cellulose 1.5%
Talcum powder 0.8%
Polysorbate alcohol -802.2%
Sodium Hyaluronate 2.5%
Glycerol 5.5%
Alchlor 0.09%
Essence 0.07%
Film forming agent 6.3%
Preservative 0.7%
Deionized water surplus.
The facial mask with antibacterial functions of the present embodiment is prepared in accordance with the following methods:
(1) film forming agent is added in deionized water, solution is then heated to 80 DEG C, keep the temperature 20 minutes, and according to 250
Rev/min rate solution be stirred be completely dissolved film forming agent, obtain base soln；
(2) by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, trichlorine
Change aluminium to be added in step (1) resulting base soln, solution temperature is maintained 65 DEG C, is stirred according to 250 revs/min of rate
It mixes 25 minutes；
(3) step (2) resulting solution is cooled to 40 DEG C, Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, lecithin is added
Rouge, Phenoxyethanol, essence, preservative stir 15 minutes according to 250 revs/min of rates, the sodium hydroxide for being 8% with concentration
Solution adjusts the pH of mixture to 6, obtains intermediate solution；
(4) step (3) resulting intermediate solution is transferred in mulser, stirs cream according to 1500 revs/min of rates
Change 45 minutes, it is filling after the screen to filtrate, finished product facial mask is obtained, S1 is denoted as.
Embodiment 2
The face pack prescription with antibacterial functions of the present embodiment is as follows:
Radix et Caulis Opuntiae Dillenii extract 2.0%
Nutgall extractive 1.5%
Lecithin 0.19%
Phenoxyethanol 1.6%
Triethanolamine 0.5%
Hydroxyethyl cellulose 1.5%
Talcum powder 0.8%
Polysorbate alcohol -802.2%
Sodium Hyaluronate 2.5%
Glycerol 5.5%
Alchlor 0.09%
Essence 0.07%
Film forming agent 6.3%
Preservative 0.7%
Deionized water surplus.
The facial mask with antibacterial functions of the present embodiment is prepared in accordance with the following methods:
(1) film forming agent is added in deionized water, solution is then heated to 83 DEG C, keep the temperature 25 minutes, and according to 300
Rev/min rate solution be stirred be completely dissolved film forming agent, obtain base soln；
(2) by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, trichlorine
Change aluminium to be added in step (1) resulting base soln, solution temperature is maintained 70 DEG C, is stirred according to 300 revs/min of rate
It mixes 25~35 minutes；
(3) step (2) resulting solution is cooled to 45 DEG C, Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, lecithin is added
Rouge, Phenoxyethanol, essence, preservative stir 18 minutes according to 300 revs/min of rates, the sodium hydroxide for being 8% with concentration
Solution adjusts the pH of mixture to 7, obtains intermediate solution；
(4) step (3) resulting intermediate solution is transferred in mulser, stirs cream according to 2000 revs/min of rates
Change 45 minutes, it is filling after the screen to filtrate, finished product facial mask is obtained, S2 is denoted as.
Embodiment 3
The face pack prescription with antibacterial functions of the present embodiment is as follows:
Radix et Caulis Opuntiae Dillenii extract 2.0%
Nutgall extractive 1.5%
Lecithin 0.19%
Phenoxyethanol 1.6%
Triethanolamine 0.5%
Hydroxyethyl cellulose 1.5%
Talcum powder 0.8%
Polysorbate alcohol -802.2%
Sodium Hyaluronate 2.5%
Glycerol 5.5%
Alchlor 0.09%
Essence 0.07%
Film forming agent 6.3%
Preservative 0.7%
Deionized water surplus.
The facial mask with antibacterial functions of the present embodiment is prepared in accordance with the following methods:
(1) film forming agent is added in deionized water, solution is then heated to 85 DEG C, keep the temperature 30 minutes, and according to 350
Rev/min rate solution be stirred be completely dissolved film forming agent, obtain base soln；
(2) by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, trichlorine
Change aluminium to be added in step (1) resulting base soln, solution temperature is maintained 75 DEG C, is stirred according to 350 revs/min of rate
It mixes 35 minutes；
(3) step (2) resulting solution is cooled to 50 DEG C, Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, lecithin is added
Rouge, Phenoxyethanol, essence, preservative stir 20 minutes according to 350 revs/min of rates, the sodium hydroxide for being 8% with concentration
Solution adjusts the pH of mixture to 8, obtains intermediate solution；
(4) step (3) resulting intermediate solution is transferred in mulser, stirs cream according to 2500 revs/min of rates
Change 45 minutes, it is filling after the screen to filtrate, finished product facial mask is obtained, S3 is denoted as.
Comparative example 1
Substantially with embodiment 2, difference is the formula and preparation method of the facial mask of this comparative example, does not add cactus and mentions
Object is taken, final facial mask obtained is denoted as C1.
Comparative example 2
Substantially with embodiment 2, difference is the formula and preparation method of the facial mask of this comparative example, does not add Chinese gall and mentions
Object is taken, final facial mask obtained is denoted as C2.
Comparative example 3
Substantially with embodiment 2, difference is the formula and preparation method of the facial mask of this comparative example, does not add lecithin,
Final facial mask obtained is denoted as C3.
Comparative example 4
Substantially with embodiment 1, difference is the formula and preparation method of the facial mask of this comparative example, does not add benzene oxygen second
Alcohol, final facial mask obtained are denoted as C4.
Performance test
The present embodiment carries out using effect test to facial mask prepared by Examples 1 to 3 and comparative example 1~4.
(1) experimental group: the selection age, the crowd with bacterial dermatitis was test object at 20~40 years old, random point
It is 7 groups, every group of 10 people, each group there are no significant in terms of skin health, organism endocrine difference, the 1st~7 group
Facial mask C1~C4 that the facial mask S1~S3 and comparative example 1~4 being prepared respectively using Examples 1 to 3 are prepared.
(2) application method of facial mask:
It is primary respectively at morning, evening each face mask film daily, 30 minutes every time.
(3) test result:
Comprehensive score is carried out using investigation point system.Every group of crowd is used continuously 3 months, fills in grade form on probation.Scoring
Every using effect total score is 10 points in table, and 9~10 points of expression effects are optimal；6~8 points of expression effects are preferable；4~5 points of expressions
Effect is general；3 points of following presentation effects are poor, and every using effect average situation is as shown in table 1:
Table 1
Test result is as shown above, and the facial mask of embodiment S1~S3 group is compared with the facial mask of comparative example C1~C4 group, tool
There is effect that is significantly more antibacterial and improving skin health.Illustrate the skin care compositions with antibacterial functions of the invention
Material composition between there is the facilitation that mutually cooperates with.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention
Range.
Claims (10)
1. a kind of skin care compositions with antibacterial functions, which is characterized in that the raw material of the skin care compositions is mentioned by cactus
Take object, nutgall extractive, lecithin, Phenoxyethanol, triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80,
Sodium Hyaluronate, glycerol, alchlor, essence, film forming agent, preservative, deionized water composition.
2. the skin care compositions according to claim 1 with antibacterial functions, which is characterized in that the skin care compositions
Raw material according to parts by weight, concrete composition are as follows:
Radix et Caulis Opuntiae Dillenii extract 1.5~2.5%
Nutgall extractive 0.8~2.2%
Lecithin 0.08~0.3%
Phenoxyethanol 0.6~3.0%
Triethanolamine 0.2~0.8%
Hydroxyethyl cellulose 0.4~2.5%
Talcum powder 0.08~1.2%
Polysorbate alcohol -80 1.5~3.0%
Sodium Hyaluronate 2.0~3.0%
Glycerol 2.5~8.5%
Alchlor 0.06~0.12%
Essence 0.05~0.09%
Film forming agent 5.0~7.5%
Preservative 0.3~1.0%
Deionized water surplus.
3. the skin care compositions according to claim 2 with antibacterial functions, which is characterized in that the skin care compositions
Raw material according to parts by weight, specifically comprises
Radix et Caulis Opuntiae Dillenii extract 2.0%
Nutgall extractive 1.5%
Lecithin 0.19%
Phenoxyethanol 1.6%
Triethanolamine 0.5%
Hydroxyethyl cellulose 1.5%
Talcum powder 0.8%
Polysorbate alcohol -80 2.2%
Sodium Hyaluronate 2.5%
Glycerol 5.5%
Alchlor 0.09%
Essence 0.07%
Film forming agent 6.3%
Preservative 0.7%
Deionized water surplus.
4. described in any item skin care compositions with antibacterial functions according to claim 1~3, which is characterized in that it is described at
Film is selected from one or more of polyvinyl alcohol, dextrin, hydroxymethyl cellulose, carragheen.
5. described in any item skin care compositions with antibacterial functions according to claim 1~3, which is characterized in that described anti-
Rotten agent is selected from one or more of ethylparaben, Nipasol, triclosan, sorbic acid.
6. described in any item skin care compositions with antibacterial functions according to claim 1~3, which is characterized in that the shield
Skin composition is facial mask.
7. a kind of preparation method of the facial mask with antibacterial functions as claimed in claim 6, which is characterized in that by following steps
Composition:
(1) film forming agent is added in deionized water, solution is then heated to 80~85 DEG C, keep the temperature 20~30 minutes, and according to
250~350 revs/min of rate, which is stirred solution, is completely dissolved film forming agent, obtains base soln；
(2) by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, alchlor
It is added in step (1) resulting base soln, solution temperature is maintained 65~75 DEG C, according to 250~350 revs/min
Rate stirs 25~35 minutes；
(3) step (2) resulting solution is cooled to 40~50 DEG C, Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, lecithin is added
Rouge, Phenoxyethanol, essence, preservative stir 15~20 minutes according to 250~350 revs/min of rates, by the pH of mixture
It adjusts to 6~8, obtains intermediate solution；
(4) step (3) resulting intermediate solution is transferred in mulser, it is stirring and emulsifying 45 minutes, filling after the screen to filtrate,
Obtain finished product facial mask.
8. the preparation method of the facial mask according to claim 7 with antibacterial functions, which is characterized in that the step (3)
The middle pH for selecting the sodium hydroxide solution that concentration is 8% to adjust mixture.
9. the preparation method of the facial mask according to claim 7 with antibacterial functions, which is characterized in that the step (4)
The rate of middle stirring and emulsifying is 1500~2500 revs/min.
10. described in any item skin care compositions with antibacterial functions are in mask product preparation according to claim 1~5
Using.
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Application publication date: 20190108 |
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