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CN108931846A - A kind of method and device of optical tweezer seeds implanted to high-accuracy ceramics - Google Patents

A kind of method and device of optical tweezer seeds implanted to high-accuracy ceramics Download PDF

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Publication number
CN108931846A
CN108931846A CN201810741210.4A CN201810741210A CN108931846A CN 108931846 A CN108931846 A CN 108931846A CN 201810741210 A CN201810741210 A CN 201810741210A CN 108931846 A CN108931846 A CN 108931846A
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accuracy
particle
optical
ceramics
ceramic material
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CN108931846B (en
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林建铃
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Fuzhou lijiada Intelligent Technology Co., Ltd
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Suzhou Meilicheng Electronic Technology Co Ltd
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Priority to CN202011153243.0A priority Critical patent/CN112230417A/en
Priority to CN202011112154.1A priority patent/CN112198650A/en
Priority to CN201810741210.4A priority patent/CN108931846B/en
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    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B21/00Microscopes
    • G02B21/32Micromanipulators structurally combined with microscopes
    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B21/00Microscopes
    • G02B21/06Means for illuminating specimens
    • G02B21/08Condensers

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  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Prostheses (AREA)
  • Materials For Medical Uses (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

The present invention provides a kind of optical tweezer seeds implanted to the method and device of high-accuracy ceramics, the transplantation device includes spherical laser wave machine, control box and electron microscopic eyepiece, the spherical laser wave machine is internally provided with optical pressure cavity, the optical pressure cavity is internally provided with optical pressure generator one, the side of the optical pressure generator one is provided with optical pressure generator two, operation bench is welded at the top of the spherical laser wave machine, the bottom of spherical laser wave machine is arranged in the control box, the transplantation method includes the dyeing of ceramic material, test the selection of particle, the preparation of ceramic material, test the record observation of implantation and the experiment of particle, the method and device of the optical tweezer seeds implanted to high-accuracy ceramics is novel in design, it is structurally reasonable, the completion particle for capableing of high accurancy and precision is transplanted to work in high-accuracy ceramic material.

Description

A kind of method and device of optical tweezer seeds implanted to high-accuracy ceramics
Technical field
The present invention is a kind of method and device of optical tweezer seeds implanted to high-accuracy ceramics, belongs to optical tweezer investigative technique neck Domain.
Background technique
Optical tweezer is when acting on particle or cell surface using spherical laser wave and single beam gradient force ligh trap, and generates power Effect a kind of optical technology, general people carry out tweezer and segmentation to cell, particle and large biological molecule using optical tweezer, but Some researches show that play the role of kind of particle to high-accuracy ceramic material with the change of certain physical property, due to high-accuracy pottery at present Ceramic material intensity with higher and wear-resisting property, therefore and experiment particle could only be carried out by optical tweezer effect not damaged Formula is implanted in high-accuracy ceramic material.
For this purpose, the present invention proposes a kind of optical tweezer seeds implanted to the method and device of high-accuracy ceramics.
Summary of the invention
In view of the deficienciess of the prior art, it is an object of the present invention to provide a kind of optical tweezer seeds implanteds to high-accuracy ceramics Method and device, to solve the problems mentioned in the above background technology, the present invention are novel in design, structurally reasonable, can be high accurate The completion particle of degree is transplanted to the work in high-accuracy ceramic material.
To achieve the goals above, the present invention is to realize by the following technical solutions: a kind of optical tweezer seeds implanted arrives The method of high-accuracy ceramics, include the following:
The dyeing of ceramic material: the high-accuracy ceramic particle of test is put into staining trough by experimenter first, by In the distinctive inoxidizability of high-accuracy ceramics and stronger corrosion resistance, it is therefore desirable to add the higher dye of concentration into staining trough Toner just obtains the high-accuracy ceramic particle being colored after enabling ceramic material impregnate 5min;
Test the selection of particle: population is placed under electron microscope by experimenter, and operator is chosen by observation Surface roughness is lower, and the single experiment particle that shape is more regular, convenient for the success of the implantation of experiment;
The preparation of ceramic material: due to high-accuracy ceramics intensity with higher and wear resistance, experimenter needs The ceramic particle being colored is carried out to roll crushing operation using high-strength crushing equipment, then puts the ceramic powders being colored It sets under electron microscope, after observation, operator should choose that stomata is less, and surface is relatively smooth, and physical property The high-accuracy ceramic material not being destroyed;
Test the implantation of particle: the experiment particle chosen is placed into the experimental implementation slot in control box by experimenter In, operator passes through the observation of electron microscopic eyepiece, the output power of optical pressure generator one and optical pressure generator two is controlled, so that The two issue have energy and momentum laser, while operator need it is poly- to control by control button corresponding on operation bench Each electric hydaulic bar inside anaclasis cylinder one and concentrating refractive cylinder two, so that control is refracted the angle of laser refraction Laser action afterwards generates gradient force ligh trap in experimental implementation slot on the surface of particle, and gradient force ligh trap can limit grain The spatial position of son, therefore particle can be allowed to be moved every empty, then experimenter can be by controlling spherical laser wave Machine, concentrating refractive cylinder one and concentrating refractive cylinder two are by particle every the empty good high-accuracy ceramic material of above-mentioned selection that is implanted to In inside;
The record of experiment and observation: experimenter will test seeds implanted to the overall process in high-accuracy ceramic material In, the change procedure and high-accuracy ceramic material that experiment particle can be observed by electron microscope eyepiece are in nature Change, then data are recorded, and can be generated in mobile chemical property in the ceramic material after implantation experiment particle Variation, detected by using different oxidant or reducing agent, and data are carried out to final record.
A kind of device of optical tweezer seeds implanted to high-accuracy ceramics, including spherical laser wave machine, control box and electron microscopic Eyepiece, the spherical laser wave machine are internally provided with optical pressure cavity, and the optical pressure cavity is internally provided with optical pressure generator One, the side of the optical pressure generator one is provided with optical pressure generator two, is welded with manipulation at the top of the spherical laser wave machine The bottom of spherical laser wave machine is arranged in platform, the control box, and connecting rod is welded on the control box, and the control box passes through Connecting rod is connect with spherical laser wave machine, and end cover is equipped at the top of the control box, is provided on the end cover Light-collecting lens, the control box are internally provided with operation cavity, and the rotating chassis that is internally provided with for operating cavity is described Experimental implementation slot is provided on rotating chassis, the side of the control box is provided with concentrating refractive cylinder one, the concentrating refractive cylinder One is internally provided with electric hydaulic bar, and the side of the concentrating refractive cylinder one is provided with purifying board one, the control box it is another Side is welded with concentrating refractive cylinder two, and the inside of the concentrating refractive cylinder two is also equipped with electric hydaulic bar, the electric hydaulic It is provided with output rod on bar, refractive power eyeglass is provided on the output rod.
As a kind of preferred embodiment of the invention, electron microscopic object lens case, the electricity are provided on the control box Sub- microcobjective case is internally provided with object phase mirror tube, and the electron microscopic eyepiece is welded on the side of electron microscopic object lens case.
As a kind of preferred embodiment of the invention, control button, the control button are provided on the operation bench It is connect respectively with electric hydaulic bar, optical pressure generator one and optical pressure generator two by electric wire.
As a kind of preferred embodiment of the invention, electric sealed door is provided on the control box.
As a kind of preferred embodiment of the invention, the quantity of the electric hydaulic bar is 6, the number of the connecting rod Amount is 2.
As a kind of preferred embodiment of the invention, the bottom of the concentrating refractive cylinder one and concentrating refractive cylinder two is all provided with It is equipped with support base, is provided with bolt aperture on the support base.
As a kind of preferred embodiment of the invention, the optical pressure cavity inside the spherical laser wave machine is sealing vacuum Chamber.
As a kind of preferred embodiment of the invention, the rotating chassis is internally provided with motor, described electronic Machine is threephase asynchronous.
As a kind of preferred embodiment of the invention, anti-glare anti-dazzling screen, institute are provided on the electron microscopic eyepiece The side for stating concentrating refractive cylinder two is provided with purifying board two, is provided with data spool on the purifying board two.
Beneficial effects of the present invention:
1. the method and device of the optical tweezer seeds implanted to high-accuracy ceramics is provided with concentrating refractive in the two sides of control box Cylinder one and concentrating refractive cylinder two, experimenter can control the output of spherical laser wave machine by the control button on operation bench Power to control the intensity for generating optical pressure, while can also control the refraction check and correction of laser, to realize to particle every sky Tweezer fixed function;
2. anti-glazing is arranged on the eyepiece of electron microscope in the method and device of the optical tweezer seeds implanted to high-accuracy ceramics Ocular lens, when can be avoided experimenter's opening electron microscope, strong light is mapped on electron microscopic eyepiece and injures through object lens The eye of operator;
3. the method and device of the optical tweezer seeds implanted to high-accuracy ceramics uses chemical dyeing technology, can will be difficult to The high-accuracy ceramic material observed carries out dyeing processing first, is then crushed, and the colored powder ceramic material of generation is just In the observation of experiment, and improve the success rate of seeds implanted.
It, can be high accurate 4. the method and device of the optical tweezer seeds implanted to high-accuracy ceramics is novel in design, structurally reasonable The completion particle of degree is transplanted to the work in high-accuracy ceramic material.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of device of the optical tweezer seeds implanted of the present invention to high-accuracy ceramics;
Fig. 2 is a kind of main view of device of the optical tweezer seeds implanted of the present invention to high-accuracy ceramics;
Fig. 3 is a kind of flow chart of method of the optical tweezer seeds implanted of the present invention to high-accuracy ceramics;
In figure: 1- spherical laser wave machine, 2- end cover, 3- concentrating refractive cylinder two, 4- purifying board two, 5- data spool, 6- operation bench, 7- light-collecting lens, 8- connecting rod, 9- control box, 10- concentrating refractive cylinder one, 11- purifying board one, 12- support base, 13- electron microscopic endoscope objective lens case, 14- electron microscopic eyepiece, 15- refractive power eyeglass, 16- optical pressure generator one, 17- rotating chassis, 18- experimental implementation slot, 19- optical pressure generator two, 20- electric hydaulic bar.
Specific embodiment
To be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, below with reference to Specific embodiment, the present invention is further explained.
It please refers to Fig.1 to Fig.3, the present invention provides a kind of technical solution: a kind of optical tweezer seeds implanted to high-accuracy ceramics Method, include the following:
The dyeing of ceramic material: the high-accuracy ceramic particle of test is put into staining trough by experimenter first, by In the distinctive inoxidizability of high-accuracy ceramics and stronger corrosion resistance, it is therefore desirable to add the higher dye of concentration into staining trough Toner just obtains the high-accuracy ceramic particle being colored after enabling ceramic material impregnate 5min;
Test the selection of particle: population is placed under electron microscope by experimenter, and operator is chosen by observation Surface roughness is lower, and the single experiment particle that shape is more regular, convenient for the success of the implantation of experiment;
The preparation of ceramic material: due to high-accuracy ceramics intensity with higher and wear resistance, experimenter needs The ceramic particle being colored is carried out to roll crushing operation using high-strength crushing equipment, then puts the ceramic powders being colored It sets under electron microscope, after observation, operator should choose that stomata is less, and surface is relatively smooth, and physical property The high-accuracy ceramic material not being destroyed;
Test the implantation of particle: the experiment particle chosen is placed into the experimental implementation slot in control box 9 by experimenter In 18, operator passes through the observation of electron microscopic eyepiece 14, controls the output of optical pressure generator 1 and optical pressure generator 2 19 Power so that the two issue have energy and momentum laser, while operator need by controlled accordingly on operation bench 6 by Button controls each electric hydaulic bar 20 of concentrating refractive cylinder 1 and the inside of concentrating refractive cylinder 23, so that laser is rolled in control The angle penetrated, the laser action after being refracted generate gradient force ligh trap in experimental implementation slot 18 on the surface of particle, gradient Power ligh trap can limit the spatial position of particle, therefore particle can be allowed to be moved every empty, and then experimenter can lead to It crosses control spherical laser wave machine 1, concentrating refractive cylinder 1 and concentrating refractive cylinder 23 and particle is implanted to above-mentioned selection every empty In the inside of good high-accuracy ceramic material;
The record of experiment and observation: experimenter will test seeds implanted to the overall process in high-accuracy ceramic material In, the change procedure of experiment particle and the property of high-accuracy ceramic material can be observed by electron microscope eyepiece 14 On change, then data are recorded, and the ceramic material after implantation experiment particle can generate mobile chemical property On variation, detected by using different oxidant or reducing agent, and data are carried out to final record
A kind of device of optical tweezer seeds implanted to high-accuracy ceramics, including spherical laser wave machine 1, control box 9 and electronic display Micro- eyepiece 14, the spherical laser wave machine 1 are internally provided with optical pressure cavity, and the optical pressure cavity is internally provided with optical pressure hair Raw device 1, the side of the optical pressure generator 1 is provided with optical pressure generator 2 19, the top of the spherical laser wave machine 1 It is welded with operation bench 6, the control box 9 is arranged in the bottom of spherical laser wave machine 1, is welded with connecting rod on the control box 9 8, the control box 9 is connect by connecting rod 8 with spherical laser wave machine 1, and the top of the control box 9 is equipped with end cover 2, Light-collecting lens 7 are provided on the end cover 2, the control box 9 is internally provided with operation cavity, the operation cavity It is internally provided with rotating chassis 17, experimental implementation slot 18, the side setting of the control box 9 are provided on the rotating chassis 17 There is concentrating refractive cylinder 1, the concentrating refractive cylinder 1 is internally provided with electric hydaulic bar 20, the concentrating refractive cylinder one 10 side is provided with purifying board 1, and the other side of the control box 9 is welded with concentrating refractive cylinder 23, the concentrating refractive The inside of cylinder 23 is also equipped with electric hydaulic bar 20, and output rod is provided on the electric hydaulic bar 20, is set on the output rod It is equipped with refractive power eyeglass 15.
As a kind of preferred embodiment of the invention, electron microscopic object lens case 13 is provided on the control box 9, it is described Electron microscopic object lens case 13 is internally provided with object phase mirror tube, and the electron microscopic eyepiece 14 is welded on electron microscopic object lens case 13 Side.
As a kind of preferred embodiment of the invention, control button, the control button are provided on the operation bench 6 It is connect respectively with electric hydaulic bar 20, optical pressure generator 1 and optical pressure generator 2 19 by electric wire.
As a kind of preferred embodiment of the invention, electric sealed door is provided on the control box 9.
As a kind of preferred embodiment of the invention, the quantity of the electric hydaulic bar 20 is 6, the connecting rod 8 Quantity be 2.
As a kind of preferred embodiment of the invention, the bottom of the concentrating refractive cylinder 1 and concentrating refractive cylinder 23 It is provided with support base 12, is provided with bolt aperture on the support base 12.
As a kind of preferred embodiment of the invention, the optical pressure cavity inside the spherical laser wave machine 1 is that sealing is true Cavity.
As a kind of preferred embodiment of the invention, the rotating chassis 17 is internally provided with motor, the electricity Motivation is threephase asynchronous.
As a kind of preferred embodiment of the invention, it is provided with anti-glare anti-dazzling screen on the electron microscopic eyepiece 14, The side of the concentrating refractive cylinder 23 is provided with purifying board 24, is provided with data spool 5 on the purifying board 24.
Working principle: the device of the optical tweezer seeds implanted to high-accuracy ceramics includes control box 9, spherical laser wave machine 1, gathers Anaclasis cylinder 1 and concentrating refractive cylinder 23, optical pressure generator 1 and optical pressure generator 2 19 inside spherical laser wave machine 1 For issuing the laser for having energy and momentum, and experimenter controls optical pressure by control button corresponding on operation bench 6 The output power of generator 1 and optical pressure generator 2 19, the light-collecting lens 7 that pass through of two beam laser vertically downward inject operation In case 9, two experimenters are controlled multiple electric hydaulic bars 20 by control button corresponding on operation bench 6 and worked, electronic liquid Refractive power eyeglass 15 is provided on output rod on compression bar 20, when electric hydaulic bar 20 is stretched, refractive power eyeglass 15 just can will swash Light carries out refraction action, and the refractive power eyeglass 15 that laser passes through different number can reflect different angles, and laser passes through refraction Effect can generate gradient force ligh trap to particle on particle surface afterwards, just can carry out mobile or tweezer every empty control particle It is fixed, it is then operated according to transplantation method, just can complete the experiment, the optical tweezer seeds implanted to the side of high-accuracy ceramics Method and device are novel in design, structurally reasonable, and the completion particle for capableing of high accurancy and precision is transplanted to work in high-accuracy ceramic material.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention, for this field skill For art personnel, it is clear that invention is not limited to the details of the above exemplary embodiments, and without departing substantially from spirit of the invention or In the case where essential characteristic, the present invention can be realized in other specific forms.Therefore, in all respects, should all incite somebody to action Embodiment regards exemplary as, and is non-limiting, the scope of the present invention by appended claims rather than on state Bright restriction, it is intended that including all changes that fall within the meaning and scope of the equivalent elements of the claims in the present invention It is interior.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art The other embodiments being understood that.

Claims (10)

1. a kind of optical tweezer seeds implanted is to the method for high-accuracy ceramics, which is characterized in that include the following:
The dyeing of ceramic material: the high-accuracy ceramic particle of test is put into staining trough by experimenter first, due to height The distinctive inoxidizability of high technology ceramics and stronger corrosion resistance, it is therefore desirable to the higher dyeing of concentration is added into staining trough Agent just obtains the high-accuracy ceramic particle being colored after enabling ceramic material impregnate 5min;
Test the selection of particle: population is placed under electron microscope by experimenter, and operator chooses surface by observation Roughness is lower, and the single experiment particle that shape is more regular, convenient for the success of the implantation of experiment;
The preparation of ceramic material: since high-accuracy ceramics intensity with higher and wear resistance, experimenter need to use High-strength crushing equipment carries out the ceramic particle being colored to roll crushing operation, is then placed into the ceramic powders being colored Under electron microscope, after observation, operator should choose that stomata is less, and surface is relatively smooth, and physical property does not have The high-accuracy ceramic material being destroyed;
Test the implantation of particle: the experiment particle chosen is placed into the experimental implementation slot in control box (9) by experimenter (18) in, operator passes through the observation of electron microscopic eyepiece (14), controls optical pressure generator one (16) and optical pressure generator two (19) output power, so that the two issues the laser for having energy and momentum, while operator needs by operation bench (6) Corresponding control button controls electric hydaulic bar each inside concentrating refractive cylinder one (10) and concentrating refractive cylinder two (3) (20), thus angle of the control to laser refraction, the surface of laser action particle in experimental implementation slot (18) after being refracted On, and gradient force ligh trap is generated, gradient force ligh trap can limit the spatial position of particle, therefore particle can be allowed to carry out every empty Mobile, then experimenter can pass through control spherical laser wave machine (1), concentrating refractive cylinder one (10) and concentrating refractive cylinder two (3) particle is implanted in the inside of the good high-accuracy ceramic material of above-mentioned selection every empty;
The record of experiment and observation: experimenter will test seeds implanted into the overall process in high-accuracy ceramic material, energy The qualitative of the change procedure and high-accuracy ceramic material for testing particle is enough observed by electron microscope eyepiece (14) Change, then record data, and can be generated in mobile chemical property in the ceramic material after implantation experiment particle Variation, is detected, and data are carried out to final record by using different oxidant or reducing agent.
2. a kind of optical tweezer seeds implanted is to the device of high-accuracy ceramics, which is characterized in that including spherical laser wave machine (1), operation Case (9) and electron microscopic eyepiece (14), the spherical laser wave machine (1) are internally provided with optical pressure cavity, the optical pressure cavity Be internally provided with optical pressure generator one (16), the side of the optical pressure generator one (16) is provided with optical pressure generator two (19), it is welded with operation bench (6) at the top of the spherical laser wave machine (1), the control box (9) is arranged in spherical laser wave machine (1) bottom is welded with connecting rod (8) on the control box (9), and the control box (9) passes through connecting rod (8) and light radiation pressure Power machine (1) connects, and is equipped with end cover (2) at the top of the control box (9), is provided with optically focused on the end cover (2) Eyeglass (7), the control box (9) are internally provided with operation cavity, and the operation cavity is internally provided with rotating chassis (17), it is provided with experimental implementation slot (18) on the rotating chassis (17), the side of the control box (9) is provided with concentrating refractive One (10) of cylinder, the concentrating refractive cylinder one (10) are internally provided with electric hydaulic bar (20), the concentrating refractive cylinder one (10) Side be provided with purifying board one (11), the other side of the control box (9) is welded with concentrating refractive cylinder two (3), the optically focused The inside of refraction cylinder two (3) is also equipped with electric hydaulic bar (20), is provided with output rod on the electric hydaulic bar (20), described Refractive power eyeglass (15) are provided on output rod.
3. a kind of optical tweezer seeds implanted according to claim 2 is to the device of high-accuracy ceramics, it is characterised in that: the behaviour To make to be provided with electron microscopic object lens case (13) on case (9), the electron microscopic object lens case (13) is internally provided with object phase mirror tube, The electron microscopic eyepiece (14) is welded on the side of electron microscopic object lens case (13).
4. a kind of optical tweezer seeds implanted according to claim 2 is to the device of high-accuracy ceramics, it is characterised in that: the behaviour Be provided with control button in control platform (6), the control button by electric wire respectively with electric hydaulic bar (20), optical pressure generator one (16) it is connected with optical pressure generator two (19).
5. a kind of optical tweezer seeds implanted according to claim 2 is to the device of high-accuracy ceramics, it is characterised in that: the behaviour Make to be provided with electric sealed door on case (9).
6. a kind of optical tweezer seeds implanted according to claim 2 is to the device of high-accuracy ceramics, it is characterised in that: the electricity The quantity of hydrodynamic compression bar (20) is 6, and the quantity of the connecting rod (8) is 2.
7. a kind of optical tweezer seeds implanted according to claim 2 is to the device of high-accuracy ceramics, it is characterised in that: described poly- The bottom of anaclasis cylinder one (10) and concentrating refractive cylinder two (3) is provided with support base (12), is arranged on the support base (12) There is bolt aperture.
8. a kind of optical tweezer seeds implanted according to claim 2 is to the device of high-accuracy ceramics, it is characterised in that: the light The internal optical pressure cavity of radiation pressure machine (1) is sealing vacuum chamber.
9. a kind of optical tweezer seeds implanted according to claim 2 is to the device of high-accuracy ceramics, it is characterised in that: described turn Dynamic chassis (17) are internally provided with motor, and the motor is threephase asynchronous.
10. a kind of optical tweezer seeds implanted according to claim 2 is to the device of high-accuracy ceramics, it is characterised in that: described Anti-glare anti-dazzling screen is provided on electron microscopic eyepiece (14), the side of the concentrating refractive cylinder two (3) is provided with purifying board two (4), data spool (5) are provided on the purifying board two (4).
CN201810741210.4A 2018-07-08 2018-07-08 Method and device for implanting optical tweezers particles into high-precision ceramic Active CN108931846B (en)

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CN202011153243.0A CN112230417A (en) 2018-07-08 2018-07-08 High-precision device for implanting ceramic particles
CN202011112154.1A CN112198650A (en) 2018-07-08 2018-07-08 Method for implanting particles into high-precision ceramic
CN201810741210.4A CN108931846B (en) 2018-07-08 2018-07-08 Method and device for implanting optical tweezers particles into high-precision ceramic

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王晓娜: "基于激光捕捉技术的微细加工", 《中国优秀硕士学位论文全文数据库 工程科技》 *

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