CN108835126A - A kind of agricultural insecticidal composite and its application containing nicotine compound and mineral oil - Google Patents
A kind of agricultural insecticidal composite and its application containing nicotine compound and mineral oil Download PDFInfo
- Publication number
- CN108835126A CN108835126A CN201810706015.8A CN201810706015A CN108835126A CN 108835126 A CN108835126 A CN 108835126A CN 201810706015 A CN201810706015 A CN 201810706015A CN 108835126 A CN108835126 A CN 108835126A
- Authority
- CN
- China
- Prior art keywords
- mineral oil
- agricultural insecticidal
- nicotine compound
- insecticidal composite
- containing nicotine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
- A01N61/02—Mineral oils; Tar oils; Tar; Distillates, extracts or conversion products thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N51/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds having the sequences of atoms O—N—S, X—O—S, N—N—S, O—N—N or O-halogen, regardless of the number of bonds each atom has and with no atom of these sequences forming part of a heterocyclic ring
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of agricultural insecticidal composite containing nicotine compound and mineral oil and its applications.The agricultural insecticidal composite includes the component of the following meter of score by weight：Nicotinic insecticide 1-10%, mineral oil 50-90%, surplus are auxiliary material；The weight ratio of the nicotinic insecticide and mineral oil is 0.1-50:10-99.Nicotine compound has two different insecticidal mechanisms with compounding for mineral oil in the agricultural insecticidal composite, has obvious synergistic function, improves control efficiency, expands insecticidal spectrum；Mineral oil is to distill out series of natural substances in petroleum, meets organic agriculture using standard, drug effect can be improved by being used in compounding with nicotine compound, can also improve Product Safety and the feature of environmental protection；The mixture of agricultural insecticidal composite reduces with nicotinoids pesticide volume, and the use of mineral oil is not in that agriculture is residual, therefore two kinds of ingredients are used in compounding and can reduce cost, mitigate the pollution and pesticide residue to environment.
Description
Technical field
The present invention relates to fields containing nicotinic insecticide, and in particular to a kind of agricultural containing nicotine compound and mineral oil
Pesticidal combination and its application.
Background technique
Chemical prevention is most important means of prevention in agricultural production, but with the increase of Pesticide use amount and not scientific is made
With the generation of the factors such as pesticide, pest resistance is caused to get worse, the pest species for generating resistance are increasing, especially to agriculture
Industry production endangers serious Lepidoptera class pest, since its breeding cycle is short, breeding amount is big, mobility is small, selfing degree is high, resists
Sexual development speed is relatively fast.Meanwhile it is high-intensitive use pesticide, result in exceeded Practice for Pesticide Residue in Agricultural Products, pollution environment and
A series of problems, such as peasant's drug cost increases is unfavorable for the sustainable development of agricultural.Therefore, it develops efficient, less toxic, low residual
It stays, different role mechanism, while having the compound preparation of synergistic function again, not only facilitate the production for delaying pest resistance to insecticide
It is raw, but also the service life of pesticide species can be extended, dosage is reduced, save the cost reduces the pollution to environment.
Imidacloprid is nicotinoids ultra high efficiency insecticide, has wide spectrum, efficient, low toxicity, low-residual, pest is not likely to produce anti-
Property the features such as to people, animal, plant and natural enemies security, and has and tags, the multiple actions such as stomach toxicity and interior suction.After contacting pests medicament,
Nervous centralis normal conduction is obstructed, and keeps its paralysis dead.Product quick-acting is good, has higher preventive effect within 1 day after medicine, residual life is long
Up to 25 days or so.Drug effect and temperature are positively correlated, and temperature is high, good disinsection effect.It is mainly used for preventing and treating sucking pest.
Mineral oil is that series of natural substances is distilled out out of petroleum；Kerosene, gas and oil and lubricating oil in intermediate range
It can be employed as pesticidal use；As the mineral oil of highly refined, light weight and low impurity occurs, phyto toxicity can be reduced, and
Start to use in the enterprising enforcement of the gardening prevention and control of plant diseases, pest control；Successfully be widely used on orchard in Australia with China (such as mandarin orange
Tangerine)；Applying also has very big development potentiality on ornamental plant and vegetables and fruits crop.The insecticidal mechanism of mineral oil works as insect and mineral
When oil directly contacts, meeting caused death or influence insect lipids, the mechanism of action being generally accepted includes that one is formed on crop
The thin oil film of layer, separates with pest and disease damage, achievees the effect that physical control；The absorption for hindering pest oxygen, influences eupnea, is led to
Suffocate or interferes its respiratory system；As ovicide, if ovum is persistently closed a rapid lapse of time by oil film and can be led to that embryo suffocates.
Summary of the invention
In view of the deficiencies of the prior art, the agriculture containing nicotine compound and mineral oil that the purpose of the present invention is to provide a kind of
With Pesticidal combination and its application, be mainly used for preventing and treating fruit tree, industrial crops, vegetables sucking pest Pesticidal combination.
A kind of agricultural insecticidal composite containing nicotine compound and mineral oil, the group including the following meter of score by weight
Point：Nicotinic insecticide 1-10%, mineral oil 50-90%, surplus are auxiliary material；The weight of the nicotinic insecticide and mineral oil
Than for 0.1-50:10-99.
It is that the nicotinic insecticide is one of imidacloprid, thiacloprid, Acetamiprid or Nitenpyram as improved
Or a variety of mixing.
It is the above-mentioned agricultural insecticidal composite containing nicotine compound and mineral oil as improved, including below by weight
Measure the component of score meter：Imidacloprid 5-10%, mineral oil 70-80%, surplus are auxiliary material.
It is that the dosage form of the agricultural insecticidal composite is missible oil, water and milk, microemulsion, dispersible oil suspension as improved
Agent, suspoemulsion or microcapsule suspending agent.
Application of the above-mentioned agricultural insecticidal composite containing nicotine compound and mineral oil in industrial crops insect pest.
It is that the industrial crops are citrus as improved, the insect pest is orange caterpillar or coccid.
Beneficial effect：
Compared with prior art, advantage of the invention is that：
1, nicotine compound has two different insecticidal mechanisms with compounding for mineral oil, has apparent synergistic work
With improving control efficiency, expand insecticidal spectrum；Aphid, plant hopper, the leafhopper not only mainly prevented and treated to nicotine compound is equivalent
Wing mesh and Thysanoptera have good effect, and to part mite class such as red spider, yellow spider and coccid, the food heart
Worm etc. also has good effect.
2, using two kinds of ingredient physics and chemical two kinds of insecticidal mechanisms, resistance development can be reduced；
3, mineral oil is to distill out series of natural substances in petroleum, meets organic agriculture using standard, with nicotine compound
Drug effect can be improved by being used in compounding, and can also improve Product Safety and the feature of environmental protection；
4, the mixture of agricultural insecticidal composite reduces with nicotinoids pesticide volume, and the use of mineral oil, which is not in that agriculture is residual, asks
Topic, therefore two kinds of ingredients are used in compounding the pollution and pesticide residue that can reduce cost, mitigation to environment.
Specific embodiment
The present invention is further described in detail below by specific embodiment.
The microemulsion that the weight fraction of 1 imidacloprid of embodiment and mineral oil is 10.1%
Take imidacloprid 0.1g, mineral oil 10g, solvent naphtha No. 150 10g, N-Methyl pyrrolidone 5g, agriculture breast 1600#10g, agriculture breast
500#5g, water complement to 100g.Above-mentioned formulation material is mixed, uniform stirring is in a stirring kettle to get imidacloprid and mineral oil
The microemulsion that weight fraction is 10.1%.
Imidacloprid alternatively forms new embodiment at Acetamiprid or Nitenpyram.
The aqueous emulsion that the weight fraction of 2 imidacloprid of embodiment and mineral oil is 30%.
Take imidacloprid 3g, mineral oil 27g, agriculture breast 500#5g, agriculture breast 600#9g, OP-10 5g, N-Methyl pyrrolidone 5g
Water complements to 100g.Above-mentioned formulation material is mixed, in a stirring kettle uniform stirring, it is uniform through high-speed shearing machine shear-mixed, i.e.,
The weight fraction of imidacloprid and mineral oil is obtained as 30% aqueous emulsion.
Imidacloprid is substituted for thiacloprid, Acetamiprid or Nitenpyram and forms new embodiment.
The suspoemulsion that the weight fraction of 3 imidacloprid of embodiment and mineral oil is 60%
Imidacloprid 15g, mineral oil 45g, ethylene oxide-propylene oxide block copolymer 2g, polycarboxylate 4g, ethylene glycol 4g are taken,
Agriculture breast 500#5g, agriculture breast 600#5g, water complements to 100g.
After stirring and dissolving is uniform, imidacloprid, then the ball milling 1- in sand mill is added in remaining ingredient after removing imidacloprid
The suspoemulsion that 2h is 60% to get the weight fraction of imidacloprid and mineral oil.
Imidacloprid is substituted for thiacloprid, Acetamiprid or Nitenpyram and forms new embodiment.
The dispersible oil-suspending agent that the weight fraction of 4 imidacloprid of embodiment and mineral oil is 75%
Take imidacloprid 5g, mineral oil 70g, ethylene oxide-propylene oxide block copolymer 2g, polycarboxylate 3g, castor oil polyoxy
Vinethene 5g, sorbierite match monostearate 10g, diatomite 5g.
By above-mentioned formula material stirring and dissolving it is uniform after, effective component is added, 1~2h of ball milling in sand mill can make
The dispersible oil-suspending agent for being 75% at the weight fraction of imidacloprid and mineral oil.
Imidacloprid is substituted for thiacloprid, Acetamiprid or Nitenpyram and forms new embodiment.
5 80% imidacloprid mineral oil missible oil of embodiment
Take imidacloprid 5g, mineral oil 75g, cyclohexanone 5g, N-Methyl pyrrolidone 10g, agriculture breast 1600#2g, agriculture breast 500#4g, second
Glycol 4g, polyethylene glycol 2g, silicone oil 0.4g, water complement to 100g.Effective component, solvent, emulsifier, co-emulsifier are added in one
It rises, so that being dissolved into homogeneous oil phase；Water, antifreeze, thickener, defoaming agent are mixed, at uniform water phase.In high-speed stirring
It mixes down, oily phase is added in water phase, that is, can be made into 20% imidacloprid high performance aqueous emulsion of cypermethrin.
Imidacloprid can also be substituted for thiacloprid, Acetamiprid, Nitenpyram and form new embodiment.
The missible oil that the weight fraction of 6 imidacloprid of embodiment and mineral oil is 91%
Take imidacloprid 1g, mineral oil 90g, N-Methyl pyrrolidone 5g, castor oil polyoxyethylene ether 4g.1g imidacloprid is added to
In 5g N-Methyl pyrrolidone, then stirring and dissolving adds mineral oil and emulsifier, is uniformly mixed to get imidacloprid
The missible oil that weight fraction with mineral oil is 91%.
Imidacloprid is substituted for thiacloprid, Acetamiprid or Nitenpyram and forms new embodiment.
Field trial measures imidacloprid and mineral oil compounding to the control efficiency of aphid.
Orange caterpillar is carried out using the agricultural insecticidal composite of 1-6 of the embodiment of the present invention and prevents and treats field trial, handles 1-6：
The agricultural insecticidal composite of example of formulations 1-6；Processing 7：5% imidacloprid missible oil of weight fraction processing 8：Weight fraction is 95%
Mineral oil missible oil.
Test site is located at two river village of Sichuan Province Pujiang County；
Experimental subjects is citrus, is carried out in citrus florescence using processing, 5 plants of each experimental plot fruit tree, cell random alignment,
Each cell water consumption is 3L, calculates extension rate according to active constituent content.
Aphid insect population is investigated before application, 3 days after application, each processing residual borer population living is investigated within 7 days respectively, with check plot
Natural insect population gradient calculates the control efficiency of each processing, while observing and recording each cell phytotoxicity a situation arises.Control efficiency is pressed
Following formula calculates：
PT in formula0：Before application, PT1：After application, PT：Chemicals treatment district, CK：Blank district.
It can be seen from the results above that agricultural insecticidal composite good disinsection effect of the invention, and nicotine compound and mineral
The mixing of oil, improves insecticidal effect.
The foregoing is only a preferred embodiment of the present invention, the scope of protection of the present invention is not limited to this, it is any ripe
Know those skilled in the art within the technical scope of the present disclosure, the letter for the technical solution that can be become apparent to
Altered or equivalence replacement are fallen within the protection scope of the present invention.
Claims (6)
1. a kind of agricultural insecticidal composite containing nicotine compound and mineral oil, which is characterized in that including following parts by weights
The component of number meter：Nicotinic insecticide 1-10%, mineral oil 50-90%, surplus are auxiliary material；The nicotinic insecticide and mineral oil
Weight ratio be 0.1-50:10-99.
2. a kind of agricultural insecticidal composite containing nicotine compound and mineral oil according to claim 1, feature exist
In the nicotinic insecticide is one of imidacloprid, thiacloprid, Acetamiprid or Nitenpyram or a variety of mixing.
3. a kind of agricultural insecticidal composite containing nicotine compound and mineral oil according to claim 2, feature exist
In, the above-mentioned agricultural insecticidal composite containing nicotine compound and mineral oil, the component including the following meter of score by weight：Pyrrole worm
Quinoline 5-10%, mineral oil 70-80%, surplus are auxiliary material.
4. a kind of agricultural insecticidal composite containing nicotine compound and mineral oil according to claim 1, feature exist
In the dosage form of the agricultural insecticidal composite is missible oil, water and milk, microemulsion, dispersible oil-suspending agent, suspoemulsion or microcapsule suspension
Agent.
5. based on a kind of agricultural insecticidal composite containing nicotine compound and mineral oil described in claim 1 in industrial crops
Application in insect pest.
6. application according to claim 5, which is characterized in that the industrial crops are citrus, and the insect pest is citrus aphid
Worm or coccid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810706015.8A CN108835126A (en) | 2018-06-27 | 2018-06-27 | A kind of agricultural insecticidal composite and its application containing nicotine compound and mineral oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810706015.8A CN108835126A (en) | 2018-06-27 | 2018-06-27 | A kind of agricultural insecticidal composite and its application containing nicotine compound and mineral oil |
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| Publication Number | Publication Date |
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| CN108835126A true CN108835126A (en) | 2018-11-20 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113662013A (en) * | 2021-08-02 | 2021-11-19 | 广州毅田生物技术有限公司 | Synergist for biological insecticide and use method thereof |
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