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CN108152169A - A kind of grain kinematic viscosity self-operated measuring unit and measuring method - Google Patents

A kind of grain kinematic viscosity self-operated measuring unit and measuring method Download PDF

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Publication number
CN108152169A
CN108152169A CN201810007129.3A CN201810007129A CN108152169A CN 108152169 A CN108152169 A CN 108152169A CN 201810007129 A CN201810007129 A CN 201810007129A CN 108152169 A CN108152169 A CN 108152169A
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solenoid valve
pipe
controller
video camera
kinematic viscosity
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丁峰元
张志刚
贾会
孙晓萍
雷军锋
任海涛
姜鲲
周彩霞
杨占旗
邹炳蔚
于美丽
班继民
许雪琼
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Henan Institute of Metrology
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Henan Institute of Metrology
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N11/00Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
    • G01N11/02Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material
    • G01N11/04Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material through a restricted passage, e.g. tube, aperture
    • G01N11/06Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material through a restricted passage, e.g. tube, aperture by timing the outflow of a known quantity

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Abstract

本发明涉及一种粮食运动粘度自动测量装置及测量方法,技术方案是,包括第一摄像机、第二摄像机、控制器、正压发生器和负压发生器,第一摄像机的镜头与上刻度线水平正对,第二摄像机的镜头与下刻度线水平正对,宽管的上端设置有用于密封和导通宽管上口部的第一电磁阀,正压发生器经第二电磁阀与压力进出管相连,负压发生器经第三电磁阀与压力进出管相连,构成毛细管粘度计的正、负压供应结构,第一摄像机、第二摄像机、第一电磁阀、第二电磁阀和第三电磁阀分别与控制器相连,本发明测量精度高,有效解决了粮食运动粘度测量时的人工肉眼判断糊化液流经上刻度线和下刻度线的时刻,以及用电子秒表手动计时所造成的误差。The invention relates to an automatic grain kinematic viscosity measuring device and a measuring method. The technical solution is to include a first camera, a second camera, a controller, a positive pressure generator and a negative pressure generator, the lens of the first camera and the upper scale line Horizontally facing, the lens of the second camera is facing the lower scale line horizontally, the upper end of the wide pipe is provided with a first solenoid valve for sealing and conducting the upper mouth of the wide pipe, and the positive pressure generator is connected with the pressure by the second solenoid valve. The inlet and outlet pipes are connected, and the negative pressure generator is connected with the pressure inlet and outlet pipes through the third solenoid valve to form the positive and negative pressure supply structure of the capillary viscometer. The first camera, the second camera, the first solenoid valve, the second solenoid valve and the second The three solenoid valves are respectively connected with the controller. The present invention has high measurement accuracy, which effectively solves the problems caused by artificial naked eyes judging the time when the gelatinized liquid flows through the upper scale line and the lower scale line when measuring grain kinematic viscosity, and manual timing with an electronic stopwatch. error.

Description

一种粮食运动粘度自动测量装置及测量方法A kind of grain kinematic viscosity automatic measuring device and measuring method

技术领域technical field

本发明涉及粮食运动粘度测量,特别是一种粮食运动粘度自动测量装置及测量方法。The invention relates to grain kinematic viscosity measurement, in particular to an automatic grain kinematic viscosity measurement device and a measurement method.

背景技术Background technique

GB/T 5516-2011《粮油检验粮食运动粘度测定毛细管粘度计法》规定,被测粮食为大米粉、小麦粉或玉米粉,先将粮食制备成糊化液,取15mL糊化液迅速从已置于恒温水浴的毛细管黏度计宽管上口注入毛细管粘度计,使其液面略高出下储器。恒温12min后用洗耳球及乳胶管将毛细管粘度计中糊化液缓慢吹起、吹下2次~3次,使均匀。第15min时将糊化液吸至并充满毛细管粘度计上储器,取下洗耳球,使糊化液自由流下,待糊化液流至毛细管粘度计计时球上刻度线时,按下计时按钮开始计时,当糊化液流至计时球下刻度线时,再按下计时按钮,停止计时,记录糊化液流经毛细管黏度计计时球的时间t1。重复测定2次,取平均值为该糊化液流经毛细管粘度计计时球上刻度线至下刻度线的时间为流出时间t。以流出时间t与毛细管粘度计的粘度常数C乘积为被测粮食的运动粘度v。GB/T 5516-2011 "Capillary Viscometer Method for Measuring Grain Kinematic Viscosity in Grain and Oil Inspection" stipulates that the grain to be tested is rice flour, wheat flour or corn flour. Inject the capillary viscometer into the upper opening of the wide tube of the capillary viscometer in a constant temperature water bath, so that the liquid level is slightly higher than the lower reservoir. After constant temperature for 12 minutes, use the ear wash ball and latex tube to slowly blow up and down the gelatinized liquid in the capillary viscometer for 2 to 3 times to make it even. At the 15th minute, suck the gelatinized liquid into and fill the upper reservoir of the capillary viscometer, remove the ear washing ball, let the gelatinized liquid flow down freely, and when the gelatinized liquid flows to the upper scale line of the capillary viscometer timing ball, press the timer Press the button to start timing. When the gelatinized liquid flows to the lower scale line of the timing ball, press the timing button again to stop timing, and record the time t 1 when the gelatinized liquid flows through the timing ball of the capillary viscometer. Repeat the measurement twice, and take the average value as the time from the upper scale line to the lower scale line of the capillary viscometer timing ball when the pasting liquid flows through the capillary viscometer, which is the outflow time t. The product of the outflow time t and the viscosity constant C of the capillary viscometer is the kinematic viscosity v of the measured grain.

实际测量中,时间测量仪器为电子秒表。操作者根据肉眼观察,待糊化液流至毛细管粘度计计时球上刻度线时,按下电子秒表开始计时,当糊化液流至计时球下刻度线时,再按下电子秒表停止计时,电子秒表的读数即为流出时间。粘度计常数C由计量检定证书获得,为固定值,因此影响运动粘度v准确性的主要因素为流出时间的测量。In actual measurement, the time measuring instrument is an electronic stopwatch. According to the naked eye observation, when the gelatinized liquid flows to the upper scale line of the capillary viscometer timing ball, press the electronic stopwatch to start timing, and when the gelatinized liquid flows to the lower scale line of the timing ball, press the electronic stopwatch to stop timing. The reading of the electronic stopwatch is the outflow time. The viscometer constant C is obtained from the measurement verification certificate and is a fixed value, so the main factor affecting the accuracy of the kinematic viscosity v is the measurement of the outflow time.

根据GB/T 5516-2011,流出时间的测量需人工用肉眼判断糊化液流经上刻度线和下刻度线的时刻,并用电子秒表进行计时,测量受人工按下秒表按钮、人员视差及糊化液流经刻度线时刻的判断等影响,测量准确性和重复性不高。因此,为确保粮食运动粘度的准确性,需要研制新的粮食运动粘度的毛细管粘度计自动测量方法。According to GB/T 5516-2011, the measurement of the outflow time needs to manually judge the moment when the gelatinized liquid flows through the upper and lower scale lines with the naked eye, and use an electronic stopwatch to time the time. The measurement accuracy and repeatability are not high due to the influence of the judgment of the time when the chemical liquid flows through the scale line. Therefore, in order to ensure the accuracy of grain kinematic viscosity, it is necessary to develop a new capillary viscometer automatic measurement method of grain kinematic viscosity.

发明内容Contents of the invention

针对上述情况,为克服现有技术之缺陷,本发明之目的就是提供一种粮食运动粘度自动测量装置及测量方法,可有效解决粮食运动粘度测量的准确性和重复性问题。In view of the above situation, in order to overcome the defects of the prior art, the object of the present invention is to provide an automatic grain kinematic viscosity measurement device and measurement method, which can effectively solve the problems of accuracy and repeatability of grain kinematic viscosity measurement.

本发明解决的技术方案是:The technical scheme that the present invention solves is:

一种粮食运动粘度自动测量装置,包括毛细管粘度计,毛细管粘度计是由竖直平行相间设置的宽管、窄管和将宽管、窄管的下端连接在一起的圆弧管构成的U形管路,宽管上端的侧壁上设置有与其内腔相连通的压力进出管,宽管下部设置向外凸起的下储器,窄管上设置有向外凸起的上储器,上储器中心的窄管外壁上设置有上刻度线,上储器下方的窄管外壁上设置有下刻度线,该粮食运动粘度自动测量装置还包括第一摄像机、第二摄像机、控制器、正压发生器和负压发生器,第一摄像机的镜头与上刻度线水平正对,第二摄像机的镜头与下刻度线水平正对,宽管的上端设置有用于密封和导通宽管上口部的第一电磁阀,正压发生器经第二电磁阀与压力进出管相连,负压发生器经第三电磁阀与压力进出管相连,构成毛细管粘度计的正、负压供应结构,第一摄像机、第二摄像机、第一电磁阀、第二电磁阀和第三电磁阀分别与控制器相连。An automatic measuring device for kinematic viscosity of grain, comprising a capillary viscometer, the capillary viscometer is a U-shaped tube composed of vertically parallel wide tubes, narrow tubes and arc tubes connecting the lower ends of the wide tubes and narrow tubes Pipeline, the side wall of the upper end of the wide pipe is provided with a pressure inlet and outlet pipe connected with the inner cavity, the lower part of the wide pipe is provided with an outwardly protruding lower reservoir, and the narrow pipe is provided with an outwardly protruding upper reservoir. The outer wall of the narrow tube in the center of the reservoir is provided with an upper scale line, and the outer wall of the narrow tube below the upper storage tank is provided with a lower scale line. The grain kinematic viscosity automatic measuring device also includes a first camera, a second camera, a controller, a positive pressure generator and negative pressure generator, the lens of the first camera is facing the upper scale line horizontally, the lens of the second camera is facing the lower scale line horizontally, and the upper end of the wide tube is provided with an upper port for sealing and conducting the wide tube The first solenoid valve in the first part, the positive pressure generator is connected with the pressure inlet and outlet pipe through the second solenoid valve, and the negative pressure generator is connected with the pressure inlet and outlet pipe through the third solenoid valve, forming the positive and negative pressure supply structure of the capillary viscometer. The first camera, the second camera, the first solenoid valve, the second solenoid valve and the third solenoid valve are respectively connected with the controller.

所述宽管上端装有与宽管上口部密封连接的延长管,第一电磁阀装在延长管上。The upper end of the wide pipe is equipped with an extension pipe sealedly connected with the upper mouth of the wide pipe, and the first electromagnetic valve is installed on the extension pipe.

一种粮食运动粘度自动测量方法,包括以下步骤:A method for automatically measuring grain kinematic viscosity, comprising the following steps:

1)、安装自动测量装置:1), install the automatic measuring device:

所述自动测量装置包括毛细管粘度计,毛细管粘度计是由竖直平行相间设置的宽管、窄管和将宽管、窄管的下端连接在一起的圆弧管构成的U形管路,宽管上端的侧壁上设置有与其内腔相连通的压力进出管,宽管下部设置向外凸起的下储器,窄管上设置有向外凸起的上储器,上储器中心的窄管外壁上设置有上刻度线,上储器下方的窄管外壁上设置有下刻度线,其特征在于,该粮食运动粘度自动测量装置还包括第一摄像机、第二摄像机、控制器、正压发生器和负压发生器,第一摄像机的镜头与上刻度线水平正对,第二摄像机的镜头与下刻度线水平正对,宽管的上端设置有用于密封和导通宽管上口部的第一电磁阀,正压发生器经第二电磁阀与压力进出管相连,负压发生器经第三电磁阀与压力进出管相连,构成毛细管粘度计的正、负压供应结构,第一摄像机、第二摄像机、第一电磁阀、第二电磁阀和第三电磁阀分别与控制器相连;Described automatic measuring device comprises capillary viscometer, and capillary viscometer is the U-shaped pipeline that is made of the wide tube that vertically parallels with each other, narrow tube and the arc tube that connects the lower end of wide tube, narrow tube together, wide tube, narrow tube The side wall of the upper end of the pipe is provided with a pressure inlet and outlet pipe connected with the inner cavity, the lower part of the wide pipe is provided with an outwardly protruding lower reservoir, the narrow pipe is provided with an outwardly protruding upper reservoir, and the center of the upper reservoir is The outer wall of the narrow tube is provided with an upper scale line, and the outer wall of the narrow tube below the upper reservoir is provided with a lower scale line. It is characterized in that the grain kinematic viscosity automatic measurement device also includes a first camera, a second camera, a controller, a positive pressure generator and negative pressure generator, the lens of the first camera is facing the upper scale line horizontally, the lens of the second camera is facing the lower scale line horizontally, and the upper end of the wide tube is provided with an upper port for sealing and conducting the wide tube The first solenoid valve in the first part, the positive pressure generator is connected with the pressure inlet and outlet pipe through the second solenoid valve, and the negative pressure generator is connected with the pressure inlet and outlet pipe through the third solenoid valve, forming the positive and negative pressure supply structure of the capillary viscometer. The first camera, the second camera, the first solenoid valve, the second solenoid valve and the third solenoid valve are respectively connected with the controller;

2)、糊化液混匀:2), gelatinized liquid mixing:

按照GB/T 5516-2011将制备好的糊化液注入已置于恒温水浴中的毛细管粘度计,使其液面略高出下储器;第一电磁阀通过延长管与宽管上口相连,第一电磁阀关闭;恒温12min后,控制器控制第二电磁阀开启,第三电磁阀关闭,正压发生器提供正压使糊化液上吹至窄管上的上刻度线时,第一摄像机自动感应并发出糊化液位置信号给控制器,控制器自动控制第二电磁阀关闭,第三电磁阀开启,负压发生器提供负压使糊化液下吸至窄管上的下刻度线时,第二摄像机自动感应并发出糊化液位置信号给控制器,控制器自动控制第二电磁阀开启,第三电磁阀关闭,重复以上操作3次,使糊化液混匀;According to GB/T 5516-2011, inject the prepared gelatinized liquid into the capillary viscometer which has been placed in the constant temperature water bath, so that the liquid level is slightly higher than the lower reservoir; the first solenoid valve is connected to the upper port of the wide pipe through the extension pipe , the first solenoid valve is closed; after 12 minutes of constant temperature, the controller controls the second solenoid valve to open, the third solenoid valve to close, and the positive pressure generator provides positive pressure to make the gelatinized liquid blow up to the upper scale line on the narrow tube, the first A camera automatically senses and sends a position signal of the gelatinized liquid to the controller. The controller automatically controls the second solenoid valve to close and the third solenoid valve to open. The negative pressure generator provides negative pressure to make the gelatinized liquid suck down to the bottom of the narrow tube When the scale line is reached, the second camera automatically senses and sends a position signal of the gelatinized liquid to the controller. The controller automatically controls the opening of the second solenoid valve and the closing of the third solenoid valve. Repeat the above operation 3 times to mix the gelatinized liquid;

3)、流出时间测定:3) Determination of outflow time:

糊化液混匀后,第三电磁阀关闭,第二电磁阀开启,第一电磁阀关闭,正压发生器提供正压使糊化液上吹至窄管上的上刻度线后,第一摄像机自动感应并发出糊化液位置信号给控制器,控制器自动控制第二电磁阀关闭,第一电磁阀开启,从而使毛细管粘度计内处于常压环境,糊化液自由流下,糊化液液面流经上刻度线时第一摄像机自动感应并激发控制器开始计时,糊化液液面流经下刻度线时第二摄像机自动感应并激发控制器结束计时,计时时间即为本次的流出时间t1,流出时间连续重复测定2次,其平均值为流出时间t;After the gelatinized liquid is mixed, the third solenoid valve is closed, the second solenoid valve is opened, the first solenoid valve is closed, and the positive pressure generator provides positive pressure to make the gelatinized liquid blow up to the upper scale line on the narrow tube. The camera automatically senses and sends a position signal of the gelatinized liquid to the controller, and the controller automatically controls the second solenoid valve to close and the first solenoid valve to open, so that the inside of the capillary viscometer is in a normal pressure environment, the gelatinized liquid flows down freely, and the gelatinized liquid When the liquid level flows through the upper scale line, the first camera automatically senses and activates the controller to start timing. When the gelatinized liquid level flows through the lower scale line, the second camera automatically senses and activates the controller to end the timing. The timing time is the current time. Outflow time t 1 , the outflow time is measured twice continuously, and the average value is the outflow time t;

4)、运动粘度计算:4) Calculation of kinematic viscosity:

流出时间t与毛细管粘度计的粘度常数C相乘,结果为被测粮食的运动粘度v。The outflow time t is multiplied by the viscosity constant C of the capillary viscometer, and the result is the kinematic viscosity v of the measured grain.

本发明自动测量装置结构新颖独特,简单合理,易生产,易操作,在现有毛细管粘度计的基础上进行改装即可,方法稳定可靠,测量精度高,有效解决了粮食运动粘度测量时的人工肉眼判断糊化液流经上刻度线和下刻度线的时刻,以及用电子秒表手动计时所造成的误差,有实际的应用价值,使用方便,效果好,是粮食运动粘度测量装置上的创新,经济与社会效益显著。The automatic measuring device of the present invention is novel and unique in structure, simple and reasonable, easy to produce and easy to operate, and can be refitted on the basis of the existing capillary viscometer. Judging the moment when the gelatinized liquid flows through the upper and lower scale lines with naked eyes, and the error caused by manual timing with an electronic stopwatch, has practical application value, is easy to use, and has good results. It is an innovation in the grain kinematic viscosity measurement device. Significant economic and social benefits.

附图说明Description of drawings

图1为本发明自动测量装置的结构示意图。Fig. 1 is a structural schematic diagram of the automatic measuring device of the present invention.

具体实施方式Detailed ways

以下结合附图对本发明的具体实施方式作进一步详细说明。The specific implementation manners of the present invention will be described in further detail below in conjunction with the accompanying drawings.

由图1给出:Given by Figure 1:

一种粮食运动粘度自动测量装置,包括毛细管粘度计,毛细管粘度计是由竖直平行相间设置的宽管1a、窄管1b和将宽管、窄管的下端连接在一起的圆弧管1c构成的U形管路,宽管1a上端的侧壁上设置有与其内腔相连通的压力进出管4,宽管1a下部设置向外凸起的下储器2,窄管1b上设置有向外凸起的上储器3,上储器3中心的窄管1b外壁上设置有上刻度线5,上储器3下方的窄管1b外壁上设置有下刻度线6,该粮食运动粘度自动测量装置还包括第一摄像机10、第二摄像机11、控制器13、正压发生器9a和负压发生器9b,第一摄像机10的镜头与上刻度线5水平正对,第二摄像机11的镜头与下刻度线6水平正对,宽管1a的上端设置有用于密封和导通宽管上口部的第一电磁阀8a,正压发生器9a经第二电磁阀8b与压力进出管4相连,负压发生器9b经第三电磁阀8c与压力进出管4相连,构成毛细管粘度计的正、负压供应结构,第一摄像机10、第二摄像机11、第一电磁阀8a、第二电磁阀8b和第三电磁阀8c分别与控制器12相连。An automatic measurement device for kinematic viscosity of grain, comprising a capillary viscometer, the capillary viscometer is composed of wide tubes 1a, narrow tubes 1b arranged vertically and parallel to each other, and an arc tube 1c connecting the lower ends of the wide tubes and narrow tubes together The U-shaped pipeline, the side wall of the upper end of the wide tube 1a is provided with a pressure inlet and outlet tube 4 communicating with its inner cavity, the lower part of the wide tube 1a is provided with an outwardly protruding lower reservoir 2, and the narrow tube 1b is provided with an outwardly protruding The raised upper reservoir 3, the outer wall of the narrow tube 1b at the center of the upper reservoir 3 is provided with an upper scale line 5, and the outer wall of the narrow tube 1b below the upper reservoir 3 is provided with a lower scale line 6, and the kinematic viscosity of the grain is automatically measured The device also includes a first camera 10, a second camera 11, a controller 13, a positive pressure generator 9a and a negative pressure generator 9b, the lens of the first camera 10 is horizontally facing the upper scale mark 5, and the lens of the second camera 11 Horizontally facing the lower scale line 6, the upper end of the wide pipe 1a is provided with a first solenoid valve 8a for sealing and conducting the upper mouth of the wide pipe, and the positive pressure generator 9a is connected to the pressure inlet and outlet pipe 4 through the second solenoid valve 8b , the negative pressure generator 9b is connected with the pressure inlet and outlet pipe 4 through the third electromagnetic valve 8c, forming the positive and negative pressure supply structure of the capillary viscometer, the first camera 10, the second camera 11, the first electromagnetic valve 8a, the second electromagnetic The valve 8b and the third solenoid valve 8c are connected to the controller 12, respectively.

为保证使用效果,所述宽管1a上端装有与宽管上口部密封连接的延长管7,第一电磁阀8a装在延长管上,延长管可采用乳胶管。In order to ensure the use effect, the upper end of the wide pipe 1a is equipped with an extension pipe 7 which is sealedly connected with the upper mouth of the wide pipe. The first solenoid valve 8a is installed on the extension pipe, and the extension pipe can be a latex pipe.

所述控制器12上装有与其相连的显示器14和操作面板13。The controller 12 is equipped with a display 14 and an operation panel 13 connected thereto.

所述上储器3是由串联的2个椭圆形构成的腔体,上刻度线5位于两椭圆形中间。The upper reservoir 3 is a cavity composed of two ellipses connected in series, and the upper scale line 5 is located in the middle of the two ellipses.

所述压力进出管4上装有三通,三通的第一个接口与压力进出管密封连接,第二个接口与第二电磁阀8b的一端相连,第二电磁阀8b的另一端与正压发生器9a的压力输出端相连,三通的第三个接口与第三电磁阀8c的一端相连,第三电磁阀8c的另一端与负压发生器9b的压力输出端相连,连接管路可采用乳胶管。The pressure inlet and outlet pipe 4 is equipped with a tee, the first interface of the tee is connected to the pressure inlet and outlet pipe, the second interface is connected to one end of the second electromagnetic valve 8b, and the other end of the second electromagnetic valve 8b is connected to the positive pressure generator. The pressure output end of the device 9a is connected, the third interface of the three-way is connected with one end of the third electromagnetic valve 8c, the other end of the third electromagnetic valve 8c is connected with the pressure output end of the negative pressure generator 9b, and the connecting pipeline can be latex tube.

所述的控制器为现有技术(市售产品),能够通过摄像机采集的图像信号对液面位置进行判断,并根据位置信号对各个电磁阀进行启、闭,如采用型号为STM32F429ZET6的开发板等;Described controller is prior art (commercially available product), can judge liquid level position by the image signal that camera collects, and each electromagnetic valve is opened and closed according to position signal, as adopting the development board that model is STM32F429ZET6 Wait;

所述的正压发生器9a和负压发生器9b为现有技术,如采用北京康斯特仪表科技股份有限公司生产的ConST711智能压力发生器,能够产生8kPa的正压和-8kPa负压。The positive pressure generator 9a and the negative pressure generator 9b are prior art, such as the ConST711 intelligent pressure generator produced by Beijing Const Instrument Technology Co., Ltd., which can generate a positive pressure of 8kPa and a negative pressure of -8kPa.

一种粮食运动粘度自动测量方法,包括以下步骤:A method for automatically measuring grain kinematic viscosity, comprising the following steps:

1)、安装自动测量装置:1), install the automatic measuring device:

所述自动测量装置包括毛细管粘度计,毛细管粘度计是由竖直平行相间设置的宽管1a、窄管1b和将宽管、窄管的下端连接在一起的圆弧管1c构成的U形管路,宽管1a上端的侧壁上设置有与其内腔相连通的压力进出管4,宽管1a下部设置向外凸起的下储器2,窄管1b上设置有向外凸起的上储器3,上储器3中心的窄管1b外壁上设置有上刻度线5,上储器3下方的窄管1b外壁上设置有下刻度线6,其特征在于,该粮食运动粘度自动测量装置还包括第一摄像机10、第二摄像机11、控制器13、正压发生器9a和负压发生器9b,第一摄像机10的镜头与上刻度线5水平正对,第二摄像机11的镜头与下刻度线6水平正对,宽管1a的上端设置有用于密封和导通宽管上口部的第一电磁阀8a,正压发生器9a经第二电磁阀8b与压力进出管4相连,负压发生器9b经第三电磁阀8c与压力进出管4相连,构成毛细管粘度计的正、负压供应结构,第一摄像机10、第二摄像机11、第一电磁阀8a、第二电磁阀8b和第三电磁阀8c分别与控制器12相连;Described automatic measuring device comprises capillary viscometer, and capillary viscometer is the U-shaped tube that is made of wide tube 1a, narrow tube 1b that vertical parallel is arranged and the arc tube 1c that connects the lower end of wide tube, narrow tube together The side wall of the upper end of the wide tube 1a is provided with a pressure inlet and outlet tube 4 communicating with its inner cavity, the lower part of the wide tube 1a is provided with an outwardly protruding lower reservoir 2, and the narrow tube 1b is provided with an outwardly protruding upper reservoir. Reservoir 3, the outer wall of the narrow tube 1b at the center of the upper reservoir 3 is provided with an upper scale line 5, and the outer wall of the narrow tube 1b below the upper reservoir 3 is provided with a lower scale line 6, which is characterized in that the kinematic viscosity of the grain is automatically measured The device also includes a first camera 10, a second camera 11, a controller 13, a positive pressure generator 9a and a negative pressure generator 9b, the lens of the first camera 10 is horizontally facing the upper scale mark 5, and the lens of the second camera 11 Horizontally facing the lower scale line 6, the upper end of the wide pipe 1a is provided with a first solenoid valve 8a for sealing and conducting the upper mouth of the wide pipe, and the positive pressure generator 9a is connected to the pressure inlet and outlet pipe 4 through the second solenoid valve 8b , the negative pressure generator 9b is connected with the pressure inlet and outlet pipe 4 through the third electromagnetic valve 8c, forming the positive and negative pressure supply structure of the capillary viscometer, the first camera 10, the second camera 11, the first electromagnetic valve 8a, the second electromagnetic The valve 8b and the third electromagnetic valve 8c are respectively connected with the controller 12;

2)、糊化液混匀:2), gelatinized liquid mixing:

按照GB/T 5516-2011将制备好的糊化液注入已置于恒温水浴中的毛细管粘度计,使其液面略高出下储器2,恒温水浴箱为透明箱,温度及控制精度为50℃±0.1℃;第一电磁阀8a通过延长管与宽管上口相连,第一电磁阀8a关闭;恒温12min后,控制器控制第二电磁阀8b开启,第三电磁阀8c关闭,正压发生器9a提供正压使糊化液上吹至窄管上的上刻度线5时,第一摄像机10自动感应并发出糊化液位置信号给控制器,控制器自动控制第二电磁阀8b关闭,第三电磁阀8c开启,负压发生器9b提供负压使糊化液下吸至窄管上的下刻度线6时,第二摄像机11自动感应并发出糊化液位置信号给控制器,控制器自动控制第二电磁阀8b开启,第三电磁阀8c关闭,重复以上操作3次,使糊化液混匀;According to GB/T 5516-2011, inject the prepared gelatinized liquid into the capillary viscometer placed in the constant temperature water bath, so that the liquid level is slightly higher than the lower reservoir 2, the constant temperature water bath is a transparent box, and the temperature and control accuracy are 50°C±0.1°C; the first solenoid valve 8a is connected to the upper port of the wide pipe through an extension tube, and the first solenoid valve 8a is closed; after 12 minutes of constant temperature, the controller controls the second solenoid valve 8b to open, the third solenoid valve 8c to close, and When the pressure generator 9a provides positive pressure to make the gelatinized liquid blow up to the upper scale line 5 on the narrow tube, the first camera 10 automatically senses and sends a position signal of the gelatinized liquid to the controller, and the controller automatically controls the second solenoid valve 8b Close, the third solenoid valve 8c is opened, and the negative pressure generator 9b provides negative pressure to make the gelatinized liquid suck down to the lower scale line 6 on the narrow tube, the second camera 11 automatically senses and sends the gelatinized liquid position signal to the controller , the controller automatically controls the opening of the second electromagnetic valve 8b, the closing of the third electromagnetic valve 8c, and repeats the above operation 3 times to mix the gelatinized liquid;

3)、流出时间测定:3) Determination of outflow time:

糊化液混匀后,第三电磁阀8c关闭,第二电磁阀8b开启,第一电磁阀8a关闭,正压发生器9a提供正压使糊化液上吹至窄管上的上刻度线5后,第一摄像机10自动感应并发出糊化液位置信号给控制器,控制器自动控制第二电磁阀8b关闭,第一电磁阀8a开启,从而使毛细管粘度计内处于常压环境,糊化液自由流下,糊化液液面流经上刻度线5时第一摄像机自动感应并激发控制器开始计时,糊化液液面流经下刻度线时下摄像机自动感应并激发控制器结束计时,计时时间即为本次的流出时间t1,流出时间连续重复测定2次,其平均值为流出时间t;After the gelatinized liquid is mixed, the third electromagnetic valve 8c is closed, the second electromagnetic valve 8b is opened, the first electromagnetic valve 8a is closed, and the positive pressure generator 9a provides positive pressure to make the gelatinized liquid blow up to the upper scale line on the narrow tube After 5, the first camera 10 automatically senses and sends a gelatinized liquid position signal to the controller, and the controller automatically controls the closing of the second solenoid valve 8b and the opening of the first solenoid valve 8a, so that the inside of the capillary viscometer is in a normal pressure environment, and the paste The chemical liquid flows down freely, the first camera automatically senses and activates the controller to start timing when the liquid level of the gelatinized liquid flows through the upper scale line 5, and the lower camera automatically senses and activates the controller to stop timing when the liquid level of the gelatinized liquid flows through the lower scale line, The timing time is the outflow time t 1 of this time, the outflow time is measured twice continuously, and the average value is the outflow time t;

4)、运动粘度计算:4) Calculation of kinematic viscosity:

流出时间t与毛细管粘度计的粘度常数C相乘,结果为被测粮食的运动粘度v。The outflow time t is multiplied by the viscosity constant C of the capillary viscometer, and the result is the kinematic viscosity v of the measured grain.

本发明经实际应用与计算,取得了非常满意的有益技术效果,以小麦、大米、玉米为被测样品,分别按照GB/T 5516-2011方法和本发明的方法进行运动粘度测量,对同一样品重复测量7次,7次测量结果用贝塞尔公式计算标准偏差,可有效表征测量结果的分散性。本方法测量结果的标准偏差为GB/T 5516-2011方法测量结果的标准偏差的1/3左右,表明本方法测量结果分散性小,测量结果的可靠性和一致性更高,有关实验数据如下:The present invention has achieved very satisfactory beneficial technical effects through practical application and calculation. Taking wheat, rice, and corn as tested samples, the kinematic viscosity is measured according to the GB/T 5516-2011 method and the method of the present invention respectively. For the same sample The measurement was repeated 7 times, and the standard deviation of the 7 measurement results was calculated using the Bessel formula, which can effectively characterize the dispersion of the measurement results. The standard deviation of the measurement results of this method is about 1/3 of the standard deviation of the measurement results of the GB/T 5516-2011 method, indicating that the dispersion of the measurement results of this method is small, and the reliability and consistency of the measurement results are higher. The relevant experimental data are as follows :

由上述情况可知,本发明通过安装测量设备、糊化液混匀、流出时间测定、运动粘度计算。通过压力发生器和电磁阀的开关,依次产生正压和负压,可替代洗耳球自动实现对糊化液的上吹和下吸,进行糊化液的自动混匀,通过上、下摄像机自动感应到糊化液流经毛细管粘度计上、下刻度线的时刻,并通过计时装置自动测定糊化液的流出时间,本方法测量结果的标准偏差为GB/T 5516-2011测量结果标准偏差的1/3左右,该发明不仅可以替代GB/T5516-2011方法,同时还能有效降低结果的分散性,使测量结果的可靠性和一致性更高,有实际的应用价值,用方便,效果好,是粮食运动粘度测量装置和方法上的创新,经济与社会效益显著。As can be seen from the foregoing, the present invention calculates by installing measuring equipment, mixing the gelatinized liquid, measuring outflow time, and kinematic viscosity. Through the switch of the pressure generator and the electromagnetic valve, positive pressure and negative pressure are generated in sequence, which can replace the ear washing ball to automatically realize the upward blowing and downward suction of the gelatinized liquid, and carry out automatic mixing of the gelatinized liquid. Through the upper and lower cameras Automatically sense the moment when the gelatinized liquid flows through the upper and lower scale lines of the capillary viscometer, and automatically measure the outflow time of the gelatinized liquid through the timing device. The standard deviation of the measurement results of this method is the standard deviation of the measurement results of GB/T 5516-2011 About 1/3 of that, the invention can not only replace the GB/T5516-2011 method, but also effectively reduce the dispersion of the results, so that the reliability and consistency of the measurement results are higher, it has practical application value, easy to use, and effective Well, it is an innovation in the grain kinematic viscosity measurement device and method, with remarkable economic and social benefits.

申请人要指出的是,本申请上述指出的仅仅是一种实施例,并不是用于限制本申请的保护范围,凡是用等同或等同替代手段所做出与本申请技术方案本质上相同的技术方案均属于本申请的保护范围。The applicant should point out that the above mentioned in the application is only an embodiment, and is not intended to limit the scope of protection of the application. Any technology that is essentially the same as the technical solution of the application is made by equivalent or equivalent replacement means The schemes all belong to the protection scope of the present application.

Claims (6)

1. a kind of grain kinematic viscosity self-operated measuring unit, including capillary viscometer, capillary viscometer is by vertical parallel Wide pipe (1a), narrow pipe (1b) and the U-shaped of arc tube (1c) composition that the lower end of wide pipe, narrow pipe links together of alternate setting Pipeline is provided with the pressure inlet/outlet pipe (4) being connected with its inner cavity, wide pipe (1a) lower part setting on the side wall of wide pipe (1a) upper end The lower reservoir (2) of outwardly convex is provided with the upper reservoir (3) of outwardly convex, the narrow pipe at upper reservoir (3) center in narrow pipe (1b) It is provided with high scale line (5) on (1b) outer wall, lower graduation mark (6) is provided on narrow pipe (1b) outer wall below upper reservoir (3), It is characterized in that, which further includes the first video camera (10), the second video camera (11), controller (13), positive pressure generator (9a) and negative pressure generator (9b), the camera lens and high scale line (5) of the first video camera (10) are horizontal just Right, the camera lens of the second video camera (11) and the horizontal face of lower graduation mark (6), the upper end of wide pipe (1a) is provided with to seal and lead Lead to the first solenoid valve (8a) of wide pipe upper oral part, positive pressure generator (9a) is through second solenoid valve (8b) and pressure inlet/outlet pipe (4) phase Even, negative pressure generator (9b) is connected through third solenoid valve (8c) with pressure inlet/outlet pipe (4), forms the positive and negative of capillary viscometer Press Supply Structure, the first video camera (10), the second video camera (11), the first solenoid valve (8a), second solenoid valve (8b) and third Solenoid valve (8c) is connected respectively with controller (12).
2. grain kinematic viscosity self-operated measuring unit according to claim 1, which is characterized in that described wide pipe (1a) upper end Equipped with the extension tube (7) being tightly connected with wide pipe upper oral part, the first solenoid valve (8a) is in extension tube.
3. grain kinematic viscosity self-operated measuring unit according to claim 1, which is characterized in that on the controller (12) Equipped with coupled display (14) and operation panel (13).
4. grain kinematic viscosity self-operated measuring unit according to claim 1, which is characterized in that the upper reservoir (3) is The cavity being made of 2 ellipses connected, high scale line (5) are intermediate positioned at two ellipses.
5. grain kinematic viscosity self-operated measuring unit according to claim 1, which is characterized in that the pressure inlet/outlet pipe (4) it is tightly connected on equipped with threeway, first interface and the pressure inlet/outlet pipe of threeway, second interface and second solenoid valve (8b) One end be connected, the other end of second solenoid valve (8b) is connected with the pressure output end of positive pressure generator (9a), the third of threeway A interface is connected with the one end of third solenoid valve (8c), the other end of third solenoid valve (8c) and the pressure of negative pressure generator (9b) Output terminal is connected.
6. a kind of grain kinematic viscosity method for automatic measurement, which is characterized in that include the following steps:
1), self-operated measuring unit is installed:
The self-operated measuring unit includes capillary viscometer, and capillary viscometer is the wide pipe set by vertical parallel spaced-apart The U-tube road that (1a), narrow pipe (1b) and the arc tube (1c) that the lower end of wide pipe, narrow pipe links together are formed, wide pipe (1a) The pressure inlet/outlet pipe (4) being connected with its inner cavity is provided on the side wall of upper end, wide pipe (1a) lower part is set under outwardly convex Reservoir (2) is provided with the upper reservoir (3) of outwardly convex in narrow pipe (1b), is set on narrow pipe (1b) outer wall at upper reservoir (3) center There is a high scale line (5), be provided with lower graduation mark (6) on narrow pipe (1b) outer wall below upper reservoir (3), which is characterized in that the grain Food kinematic viscosity self-operated measuring unit further includes the first video camera (10), the second video camera (11), controller (13), positive pressure and occurs Device (9a) and negative pressure generator (9b), camera lens and high scale line (5) horizontal face of the first video camera (10), the second video camera (11) camera lens and the horizontal face of lower graduation mark (6), the upper end of wide pipe (1a) is provided with to seal and be connected wide pipe upper oral part The first solenoid valve (8a), positive pressure generator (9a) is connected through second solenoid valve (8b) with pressure inlet/outlet pipe (4), negative pressure generator (9b) is connected through third solenoid valve (8c) with pressure inlet/outlet pipe (4), forms the positive and negative pressure Supply Structure of capillary viscometer, the One video camera (10), the second video camera (11), the first solenoid valve (8a), second solenoid valve (8b) and third solenoid valve (8c) are respectively It is connected with controller (12);
2), dextrin mixing:
The dextrin prepared according to GB/T 5516-2011 is injected to the capillary viscometer having been placed in water bath with thermostatic control, makes it Liquid level is slightly higher than lower reservoir (2);First solenoid valve (8a) by extension tube with width pipe it is suitable for reading be connected, the first solenoid valve (8a) pass It closes;After constant temperature 12min, controller control second solenoid valve (8b) is opened, and third solenoid valve (8c) is closed, positive pressure generator (9a) When providing positive pressure makes high scale line (5) being blown on dextrin in narrow pipe, the first video camera (10) automatic sensing simultaneously sends out gelatinization For liquid position signal to controller, controller automatically controls second solenoid valve (8b) closing, and third solenoid valve (8c) is opened, negative pressure hair When raw device (9b) offer negative pressure makes to be drawn to lower graduation mark (6) in narrow pipe under dextrin, the second video camera (11) automatic sensing is simultaneously Dextrin position signal is sent out to controller, controller automatically controls second solenoid valve (8b) unlatching, and third solenoid valve (8c) closes It closes, repeats above operation 3 times, make dextrin mixing;
3), the delivery time measures:
After dextrin mixing, third solenoid valve (8c) is closed, and second solenoid valve (8b) is opened, and the first solenoid valve (8a) is closed, just After pressure generator (9a) offer positive pressure makes the high scale line (5) being blown on dextrin in narrow pipe, the first video camera (10) is certainly dynamic Dextrin position signal should and be sent out to controller, controller automatically controls second solenoid valve (8b) closing, the first solenoid valve (8a) is opened, and so as to make in capillary viscometer under atmospheric pressure environment, dextrin free flow, dextrin liquid level flows through high scale The first video camera automatic sensing and controller is excited to start timing during line (5), dextrin liquid level flows through lower graduation mark and images at present Machine automatic sensing simultaneously excites controller to terminate timing, and timing time is this delivery time t1, the delivery time continuously repeats It measures 2 times, average value is delivery time t;
4), kinematic viscosity calculates:
Delivery time t is multiplied with the viscosity constant C of capillary viscometer, and result is the kinematic viscosity v of tested grain.
CN201810007129.3A 2018-01-04 2018-01-04 A kind of grain kinematic viscosity self-operated measuring unit and measuring method Pending CN108152169A (en)

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