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CN107935791A - Weed removal medicinal fertilizer for unmanned plane sprinkling and preparation method thereof - Google Patents

Weed removal medicinal fertilizer for unmanned plane sprinkling and preparation method thereof Download PDF

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Publication number
CN107935791A
CN107935791A CN201711243615.7A CN201711243615A CN107935791A CN 107935791 A CN107935791 A CN 107935791A CN 201711243615 A CN201711243615 A CN 201711243615A CN 107935791 A CN107935791 A CN 107935791A
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parts
fertilizer
unmanned plane
liquid
herbicide
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Inventor
潘小群
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Nanning Guangxi Kai Kai Technology Development Co Ltd
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Nanning Guangxi Kai Kai Technology Development Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/70Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting wettability, e.g. drying agents
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/24Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G1/00Mixtures of fertilisers belonging individually to different subclasses of C05
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/20Liquid fertilisers

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Environmental Sciences (AREA)
  • Dentistry (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Fertilizers (AREA)
  • Catching Or Destruction (AREA)

Abstract

The present invention relates to a kind of Herbicidal combination medicine fertilizer for unmanned plane sprinkling and preparation method thereof.The Herbicidal combination medicine fertilizer is using botanical herbicides, liquid fertilizer, auxiliary agent as raw material, the weight ratio of the herbicide and liquid fertilizer is 1: 1 30, and the production method of the Herbicidal combination medicine fertilizer for unmanned plane sprinkling includes preparing liquid, preparing herbicide, prepare Weed removal medicinal fertilizer.The present invention is easy to operate, with short production cycle, and the medicine fertilizer of production has notable synergistic prevention effect, friendly to environment, people and animals, has achieveed the purpose that saving of work and time human-saving using unmanned plane sprinkling.

Description

Weed removal medicinal fertilizer for unmanned plane sprinkling and preparation method thereof
Technical field
The present invention relates to medicine fertilizer field, more particularly to a kind of Weed removal medicinal fertilizer for unmanned plane sprinkling and its preparation side Method.
Background technology
Due to the long-time service of chemical herbicide, herbicide is in crops body, residual in soil and in environment etc. is asked Topic, also for Sustainable Development agricultural, strengthens environmental protection, research and development botanical herbicides just seem extremely important. China's plant resources and its abundant, has investigated thoroughly the species of more than 30,000 kind higher plants, wherein the plant of 30 Duo Ge sections and many Hundred kinds of native compounds with removing activity are found that in microorganism, a part has been developed that into natural herbicide.Due to planting Material resource herbicide has free from environmental pollution, to weeds be not likely to produce resistance the features such as safer to people and animals, so when people recognize Know ecological environment for the survival of mankind seriously polluted by chemical substance have urgent need purify when, study botanical herbicides It is imperative.
There are key technical problems such as quality uniformity, stability and application securities in Weed removal medicinal fertilizer production process, therefore And realize that the product of industrialization is few, but also there is many jejune aspects, it is necessary to which scientific worker removes research and probe. Research for Weed removal medicinal fertilizer, China are scarcely out of swaddling-clothes, and also have no the related report for being used for the medicine fertilizer that unmanned plane is applied.Through Retrieval, the patent " a kind of pesticide applied for unmanned plane and preparation method thereof " of patent publication No. CN105454224A, simply Sprayed insecticide using unmanned plane, do not illustrate the species and method sprayed insecticide using unmanned plane, also without fully profit With unmanned plane, achieve the purpose that real saving of work and time human-saving.
The disclosure of background above technology contents is only used for inventive concept and the technical solution that auxiliary understands the present invention, it is not The prior art of present patent application is necessarily belonged to, shows the applying date of the above in present patent application in no tangible proof In the case of disclosed, above-mentioned background technology should not be taken to the novelty and creativeness of evaluation the application.
The content of the invention
Present invention aims at a kind of Weed removal medicinal fertilizer for unmanned plane sprinkling and preparation method thereof is proposed, to solve to be used for The technological gap of the Weed removal medicinal fertilizer of unmanned plane sprinkling, realizes the technical problem that unmanned plane weeding fertilising is synchronously carried out.
For this reason, the present invention proposes a kind of Weed removal medicinal fertilizer for unmanned plane sprinkling.
A kind of Weed removal medicinal fertilizer for unmanned plane sprinkling, including herbicide, liquid fertilizer, auxiliary agent, herbicide and Liquid Fertilizer The weight ratio of material is 1: 1-30.
Further, the weight ratio of the Weed removal medicinal fertilizer for being used for unmanned plane sprinkling, herbicide and liquid fertilizer is 1: 10-20。
Further, the weight ratio of the Weed removal medicinal fertilizer for being used for unmanned plane sprinkling, herbicide and liquid fertilizer is 1: 15。
Further, the described Weed removal medicinal fertilizer for being used for unmanned plane sprinkling, herbicide are including following in units of parts by weight Raw material:70-112 parts of ribbon gum, pyrene are green pepper 55-80 parts clear, 50-65 parts of fish pelargonium, 30-75 parts of cineole, Carpesium cernuum Linn 45-80 Part, 35-55 parts of radix euphorbiae lantu, 25-38 parts of meteloidine, 35-85 parts of Ageratum conyzoides, 23-45 parts of yellow cinnamon leaf.
Further, the Weed removal medicinal fertilizer for being used for unmanned plane sprinkling, liquid fertilizer is clear liquid type, floating type, mud The one or more of type compound fertilizer.
Further, the Weed removal medicinal fertilizer for being used for unmanned plane sprinkling, auxiliary agent is by solvent, cosolvent, wetting agent, demulsification One or more kinds of compositions in agent, defoamer, dispersant, antifreezing agent.
Further, the described Weed removal medicinal fertilizer for being used for unmanned plane sprinkling, solvent are water, and cosolvent is organic acid, organic One kind of acid sodium-salt, amide-type, wetting agent are one kind of thio-alcohol, hydrazides and mercaptan acetals, and demulsifier is ethylene polyamine With one kind of polyoxyethylene polyoxypropylene polyether mixture, alkyl phenolic resin and polyoxyethylene mixture, defoamer is emulsification One kind of the fatty acid ester compounded thing of silicone oil, higher alcohols, polyoxyethylene polyoxypropylene pentaerythrite ether, dispersant for fatty acid, One kind of esters, antifreezing agent is acid phosphate amine salt, sodium chloride, one kind of urea.
Further, the present invention also provides a kind of preparation method of the Weed removal medicinal fertilizer for unmanned plane.
A kind of preparation method of the Weed removal medicinal fertilizer for being used for unmanned plane sprinkling, is made of following steps:
S1:By ribbon gum, the clear green pepper of pyrene, fish pelargonium, cineole, Carpesium cernuum Linn, radix euphorbiae lantu, meteloidine, Ageratum conyzoides, yellow cinnamon leaf Co-grinding, obtains mixture, adds mixture in ethanol, is 1 in solid-liquid ratio:13-17, ultrasonic power 160- 320W, concentration of alcohol 60%-78%, Extracting temperature are that liquid 18-30min is extracted at 64-75 DEG C, and liquid is made;
S2:Liquid made from step S1 is crossed into 10-20 mesh sieve, herbicide is made;
S3:Auxiliary agent and liquid fertilizer are added into herbicide made from step S2, stirring and dissolving at being 40-53 DEG C in temperature 25-32min, is made mixed liquor;
S4:Mixed liquor made from step S3 is diluted with 1000-8000 parts of water, is made and removes herbal medicine for unmanned plane sprinkling Fertilizer.
Further, the preparation method of the Weed removal medicinal fertilizer for being used for unmanned plane sprinkling, is stirred described in step S3 Rotating speed be 200-300r/min.
Further, the preparation method of the Weed removal medicinal fertilizer for being used for unmanned plane sprinkling, water is described in step S4 Deionized water.
Compared with prior art, the invention has the advantages that:
(1) present invention uses the herbicide of plant source, is natural herbicide, friendly to environment, people and animals, is not easy in soil Middle residual, pest are not likely to produce the resistance to the action of a drug;
(2) medicine fertilizer is used to unmanned plane for the first time spray, realizes that medicine fertilizer synchronously applies, mitigate the plantation burden of peasant, dropped Low labour;
(3) unmanned plane sprinkling medicine fertilizer, the pest on corps leaf surface can be killed, utterly destroy pest.
Embodiment
The present invention is described in further detail with reference to embodiment.It is emphasized that the description below is only Only it is exemplary, the scope being not intended to be limiting of the invention and its application.
First, Application Example
Embodiment 1
A kind of Weed removal medicinal fertilizer for unmanned plane sprinkling, including herbicide, liquid fertilizer, auxiliary agent, the herbicide and liquid The weight ratio of body fertilizer is 1: 1, i.e. 100 parts of herbicide, 100 parts of clear liquid type compound fertilizer.
The herbicide is made of the raw material of following parts by weight:55 parts of the clear green pepper of 70 parts of ribbon gum, pyrene, 50 parts of fish pelargonium, 30 parts of cineole, 45 parts of Carpesium cernuum Linn, 35 parts of radix euphorbiae lantu, 25 parts of meteloidine, 35 parts of Ageratum conyzoides, 23 parts of yellow cinnamon leaf.
The auxiliary agent is by 50 parts of wetting agent n- dodecyl mereaptan, three acyl glycosides of dispersant oily 30 parts, antifreezing agent acid phosphoric acid ester 60 parts of compositions of amine salt.
A kind of preparation method of Weed removal medicinal fertilizer for unmanned plane sprinkling is as follows:
S1:By ribbon gum, the clear green pepper of pyrene, fish pelargonium, cineole, Carpesium cernuum Linn, radix euphorbiae lantu, meteloidine, Ageratum conyzoides, yellow cinnamon leaf Co-grinding, obtains mixture, adds mixture in ethanol, is 1 in solid-liquid ratio:13, ultrasonic power 160W, ethanol Concentration is 60%, and Extracting temperature is that liquid 18min is extracted at 64 DEG C, and liquid is made;
S2:Liquid made from step S1 is crossed into 20 mesh sieve, herbicide is made;
S3:Auxiliary agent and liquid fertilizer are added into herbicide made from step S2, in the case where temperature is 40 DEG C, 200r/min is stirred Dissolving 25min is mixed, mixed liquor is made;
S4:Mixed liquor made from step S3 is diluted with 1000 parts of deionized waters, the weeding for unmanned plane sprinkling is made Medicine fertilizer.
Embodiment 2
A kind of Weed removal medicinal fertilizer for unmanned plane sprinkling, including herbicide, liquid fertilizer, auxiliary agent, the herbicide and liquid The weight ratio of body fertilizer is 1: 30, i.e. 100 parts of herbicide, 3000 parts of clear liquid type compound fertilizer.
The herbicide is made of the raw material of following parts by weight:80 parts of the clear green pepper of 112 parts of ribbon gum, pyrene, 65 parts of fish pelargonium, 75 parts of cineole, 80 parts of Carpesium cernuum Linn, 55 parts of radix euphorbiae lantu, 38 parts of meteloidine, 85 parts of Ageratum conyzoides, 45 parts of yellow cinnamon leaf.
The auxiliary agent is urea 60 by 50 parts of wetting agent O-amino benzoyl hydrazine, 30 parts of dispersant ethyl acetate, antifreezing agent Part composition.
A kind of preparation method of Weed removal medicinal fertilizer for unmanned plane sprinkling is as follows:
S1:By ribbon gum, the clear green pepper of pyrene, fish pelargonium, cineole, Carpesium cernuum Linn, radix euphorbiae lantu, meteloidine, Ageratum conyzoides, yellow cinnamon leaf Co-grinding, obtains mixture, adds mixture in ethanol, is 1 in solid-liquid ratio:17, ultrasonic power 320W, ethanol Concentration is 78%, and Extracting temperature is that liquid 30min is extracted at 75 DEG C, and liquid is made;
S2:Liquid made from step S1 is crossed into 10 mesh sieve, herbicide is made;
S3:Auxiliary agent and liquid fertilizer are added into herbicide made from step S2, in the case where temperature is 53 DEG C, 300r/min is stirred Dissolving 32min is mixed, mixed liquor is made;
S4:Mixed liquor made from step S3 is diluted with 8000 parts of deionized waters, the weeding for unmanned plane sprinkling is made Medicine fertilizer.
Embodiment 3
A kind of Weed removal medicinal fertilizer for unmanned plane sprinkling, including herbicide, liquid fertilizer, auxiliary agent, the herbicide and liquid The weight ratio of body fertilizer is 1: 15, i.e. 200 parts of herbicide, 3000 parts of floating type compound fertilizer.
The herbicide is made of the raw material of following parts by weight:60 parts of the clear green pepper of 75 parts of ribbon gum, pyrene, 52 parts of fish pelargonium, 40 parts of cineole, 50 parts of Carpesium cernuum Linn, 40 parts of radix euphorbiae lantu, 28 parts of meteloidine, 45 parts of Ageratum conyzoides, 25 parts of yellow cinnamon leaf.
The auxiliary agent is by 80 parts of wetting agent 3- dimercaptopropanes, demulsifier ethylene polyamine and polyoxyethylene polyoxypropylene polyethers 1: 60 parts of 3 50 parts of compatibilities, 50 parts of dispersant aliphatic alcohol polyethenoxy polyoxypropylene section graft copolymer, antifreezing agent sodium chloride compositions.
A kind of preparation method of Weed removal medicinal fertilizer for unmanned plane sprinkling is as follows:
S1:By ribbon gum, the clear green pepper of pyrene, fish pelargonium, cineole, Carpesium cernuum Linn, radix euphorbiae lantu, meteloidine, Ageratum conyzoides, yellow cinnamon leaf Co-grinding, obtains mixture, adds mixture in ethanol, is 1 in solid-liquid ratio:14, ultrasonic power 200W, ethanol Concentration is 65%, and Extracting temperature is that liquid 21min is extracted at 66 DEG C, and liquid is made;
S2:Liquid made from step S1 is crossed into 12 mesh sieve, herbicide is made;
S3:Auxiliary agent and liquid fertilizer are added into herbicide made from step S2, in the case where temperature is 42 DEG C, 220r/min is stirred Dissolving 28min is mixed, mixed liquor is made;
S4:Mixed liquor made from step S3 is diluted with 3000 parts of deionized waters, the weeding for unmanned plane sprinkling is made Medicine fertilizer.
Embodiment 4
A kind of Weed removal medicinal fertilizer for unmanned plane sprinkling, including herbicide, liquid fertilizer, auxiliary agent, the herbicide and liquid The weight ratio of body fertilizer is 1: 10, i.e. 200 parts of herbicide, 2000 parts of sludge-type compound fertilizer.
The herbicide is made of the raw material of following parts by weight:64 parts of the clear green pepper of 80 parts of ribbon gum, pyrene, 55 parts of fish pelargonium, 49 parts of cineole, 61 parts of Carpesium cernuum Linn, 43 parts of radix euphorbiae lantu, 31 parts of meteloidine, 56 parts of Ageratum conyzoides, 31 parts of yellow cinnamon leaf.
The auxiliary agent is by 100 parts of wetting agent n- dodecyl mereaptan, 40 parts of dispersant tristerin, demulsifier alkyl phenolic Resin and polyoxyethylene 1:60 parts of 1 60 parts of compatibility, 100 parts of the fatty acid ester compounded thing of defoamer higher alcohols, antifreezing agent methanol compositions.
A kind of preparation method of Weed removal medicinal fertilizer for unmanned plane sprinkling is as follows:
S1:By ribbon gum, the clear green pepper of pyrene, fish pelargonium, cineole, Carpesium cernuum Linn, radix euphorbiae lantu, meteloidine, Ageratum conyzoides, yellow cinnamon leaf Co-grinding, obtains mixture, adds mixture in ethanol, is 1 in solid-liquid ratio:15, ultrasonic power 240W, ethanol Concentration is 68%, and Extracting temperature is that liquid 24min is extracted at 70 DEG C, and liquid is made;
S2:Liquid made from step S1 is crossed into 14 mesh sieve, herbicide is made;
S3:Auxiliary agent and liquid fertilizer are added into herbicide made from step S2, in the case where temperature is 48 DEG C, 240r/min is stirred Dissolving 30min is mixed, mixed liquor is made;
S4:Mixed liquor made from step S3 is diluted with 5000 parts of deionized waters, the weeding for unmanned plane sprinkling is made Medicine fertilizer.
Embodiment 5
A kind of Weed removal medicinal fertilizer for unmanned plane sprinkling, including herbicide, liquid fertilizer, auxiliary agent, the herbicide and liquid The weight ratio of body fertilizer is 1: 20, i.e. 100 parts of herbicide, 1000 parts of clear liquid type compound fertilizer.
The herbicide is made of the raw material of following parts by weight:68 parts of the clear green pepper of 90 parts of ribbon gum, pyrene, 58 parts of fish pelargonium, 58 parts of cineole, 68 parts of Carpesium cernuum Linn, 46 parts of radix euphorbiae lantu, 33 parts of meteloidine, 65 parts of Ageratum conyzoides, 35 parts of yellow cinnamon leaf.
The auxiliary agent is by 1000 parts of sludge-type compound fertilizer, 50 parts of wetting agent O-amino benzoyl hydrazine, dispersant acetic acid fourth 80 parts of ester, 60 parts of antifreezing agent acid phosphate amine salt, demulsifier alkyl phenolic resin and polyoxyethylene 1:1 90 parts of compatibility, defoaming 110 parts of compositions of agent polyoxyethylene.
A kind of preparation method of Weed removal medicinal fertilizer for unmanned plane sprinkling is as follows:
S1:By ribbon gum, the clear green pepper of pyrene, fish pelargonium, cineole, Carpesium cernuum Linn, radix euphorbiae lantu, meteloidine, Ageratum conyzoides, yellow cinnamon leaf Co-grinding, obtains mixture, adds mixture in ethanol, is 1 in solid-liquid ratio:16, ultrasonic power 270W, ethanol Concentration is 70%, and Extracting temperature is that liquid 25min is extracted at 68 DEG C, and liquid is made;
S2:Liquid made from step S1 is crossed into 16 mesh sieve, herbicide is made;
S3:Auxiliary agent and liquid fertilizer are added into herbicide made from step S2, in the case where temperature is 48 DEG C, 260r/min is stirred Dissolving 28min is mixed, mixed liquor is made;
S4:Mixed liquor made from step S3 is diluted with 6000 parts of deionized waters, the weeding for unmanned plane sprinkling is made Medicine fertilizer.
Embodiment 6
A kind of Weed removal medicinal fertilizer for unmanned plane sprinkling, including herbicide, liquid fertilizer, auxiliary agent, the herbicide and liquid The weight ratio of body fertilizer is 1: 20, i.e. 200 parts of herbicide, 2000 parts of floating type compound fertilizer.
The herbicide is made of the raw material of following parts by weight:74 parts of the clear green pepper of 100 parts of ribbon gum, pyrene, 61 parts of fish pelargonium, 65 parts of cineole, 75 parts of Carpesium cernuum Linn, 49 parts of radix euphorbiae lantu, 35 parts of meteloidine, 73 parts of Ageratum conyzoides, 39 parts of yellow cinnamon leaf.
The auxiliary agent is by 2000 parts of sludge-type compound fertilizer, 100 parts of wetting agent nonylphenol polyoxyethylene ether, dispersant fat Sour 110 parts of methyl esters, demulsifier ethylene polyamine and polyoxyethylene polyoxypropylene polyethers 1:1 150 parts of compatibility, 100 parts of antifreezing agent urea Composition.
A kind of preparation method of Weed removal medicinal fertilizer for unmanned plane sprinkling is as follows:
S1:By ribbon gum, the clear green pepper of pyrene, fish pelargonium, cineole, Carpesium cernuum Linn, radix euphorbiae lantu, meteloidine, Ageratum conyzoides, yellow cinnamon leaf Co-grinding, obtains mixture, adds mixture in ethanol, is 1 in solid-liquid ratio:16, ultrasonic power 300W, ethanol Concentration is 74%, and Extracting temperature is that liquid 28min is extracted at 70 DEG C, and liquid is made;
S2:Liquid made from step S1 is crossed into 18 mesh sieve, herbicide is made;
S3:Auxiliary agent and liquid fertilizer are added into herbicide made from step S2, in the case where temperature is 49 DEG C, 280r/min is stirred Dissolving 30min is mixed, mixed liquor is made;
S4:Mixed liquor made from step S3 is diluted with 6000 parts of deionized waters, the weeding for unmanned plane sprinkling is made Medicine fertilizer.
Embodiment 7
A kind of Weed removal medicinal fertilizer for unmanned plane sprinkling, including herbicide, liquid fertilizer, auxiliary agent, the herbicide and liquid The weight ratio of body fertilizer is 1: 25, i.e. 200 parts of herbicide, 1500 parts of clear liquid type compound fertilizer.
The herbicide is made of the raw material of following parts by weight:78 parts of the clear green pepper of 108 parts of ribbon gum, pyrene, 64 parts of fish pelargonium, 72 parts of cineole, 79 parts of Carpesium cernuum Linn, 53 parts of radix euphorbiae lantu, 37 parts of meteloidine, 82 parts of Ageratum conyzoides, 43 parts of yellow cinnamon leaf.
The auxiliary agent is by 3500 parts of floating type compound fertilizer, 20 parts of wetting agent n- dodecyl mereaptan, dispersant ethyl acetate 50 Part, demulsifier alkyl phenolic resin and polyoxyethylene 1:60 parts of 2 120 parts of compatibilities, antifreezing agent sodium chloride compositions.
A kind of preparation method of Weed removal medicinal fertilizer for unmanned plane sprinkling is as follows:
S1:By ribbon gum, the clear green pepper of pyrene, fish pelargonium, cineole, Carpesium cernuum Linn, radix euphorbiae lantu, meteloidine, Ageratum conyzoides, yellow cinnamon leaf Co-grinding, obtains mixture, adds mixture in ethanol, is 1 in solid-liquid ratio:14, ultrasonic power 310W, ethanol Concentration is 76%, and Extracting temperature is that liquid 29min is extracted at 74 DEG C, and liquid is made;
S2:Liquid made from step S1 is crossed into 20 mesh sieve, herbicide is made;
S3:Auxiliary agent and liquid fertilizer are added into herbicide made from step S2, in the case where temperature is 52 DEG C, 290r/min is stirred Dissolving 31min is mixed, mixed liquor is made;
S4:Mixed liquor made from step S3 is diluted with 7000 parts of deionized waters, the weeding for unmanned plane sprinkling is made Medicine fertilizer.
2nd, field trial
The test of pesticide effectiveness 1 prevents the field trial of rice weed
Test method:(1) three groups, test group are set:The made obtained sample of above-mentioned formulation application embodiment 7 is dilute Release, unmanned plane sprinkling is respectively adopted and traditional hand-rail type sprays;Positive controls:3.5% prometryn, is respectively adopted unmanned plane spray Spill and traditional hand-rail type sprays;Blank control group:Clear water, is sprayed using unmanned plane.(2) using the anti-therapy of unmanned plane spraying, press Dosage adds water 50kg even sprayings per acre, per cell 100m2For a processing, separated between processing with the small ridge and set protection row. (3) carry out preventive effect investigation within 7 days, 20 days and 45 days after medicine, calculate prevention effect.Result of the test refers to table 1.
1 rice weed field efficacy checking test data of table
Table of field test results is bright, and the Weed removal medicinal fertilizer that the present invention is used for unmanned plane sprinkling can effectively prevent rice weed, And effect is better than the prevention effect of traditional approach sprinkling, the herbicidal effect that better than 3.5% prometryn individually sprays.
The test of pesticide effectiveness 2 prevents the field trial of rice weed
Test method:(1) three groups, test group are set:The made obtained sample of above-mentioned formulation application embodiment 4 is dilute Release, unmanned plane sprinkling is respectively adopted and traditional hand-rail type sprays;Positive controls:3.5% propanil, is respectively adopted unmanned plane sprinkling Sprayed with traditional hand-rail type;Blank control group:Clear water, is sprayed using unmanned plane.(2) using the anti-therapy of unmanned plane spraying, by every Mu dosage adds water 50kg even sprayings, is a processing per cell 100m2, is separated between processing with the small ridge and sets protection row.(3) Carry out preventive effect investigation within 7 days, 20 days and 45 days after medicine, calculate prevention effect.Result of the test refers to table 2.
2 rice weed field efficacy checking test data of table
Table of field test results is bright, and the Weed removal medicinal fertilizer that the present invention is used for unmanned plane sprinkling can effectively prevent rice weed, And effect is better than the prevention effect of traditional approach sprinkling, the herbicidal effect that better than 3.5% propanil individually sprays.
The field trial of 3 rice yield of the test of pesticide effectiveness
Above-mentioned formulation application embodiment 7 made obtained sample unmanned plane sprinkling Weed removal medicinal fertilizer is applied to rice, is tried Test and be divided into 7 groups, every group of 100m2, using ridge as boundary.
3 rice yield checking test data of table
Above-mentioned result of the test shows that the Weed removal medicinal fertilizer for being used for unmanned plane sprinkling of the invention can improve the yield of rice 14.61%, number of productive ear and bear fruit grains are improved, and the mode of unmanned plane sprinkling is better than spraying insecticide using traditional hand-rail type.
Above content is to combine specific/preferred embodiment further description made for the present invention, it is impossible to Assert that the specific implementation of the present invention is confined to these explanations.Come for general technical staff of the technical field of the invention Say, without departing from the inventive concept of the premise, it can also make some replacements or modification to the embodiment that these have been described, And these are substituted or variant should all be considered as belonging to protection scope of the present invention.

Claims (10)

  1. A kind of 1. Weed removal medicinal fertilizer for unmanned plane sprinkling, it is characterised in that:It is described to remove including herbicide, liquid fertilizer, auxiliary agent The weight ratio of careless agent and liquid fertilizer is 1: 1-30.
  2. 2. the Weed removal medicinal fertilizer for unmanned plane sprinkling as claimed in claim 1, it is characterised in that:The herbicide and Liquid Fertilizer The weight ratio of material is 1: 10-20.
  3. 3. the Weed removal medicinal fertilizer for unmanned plane sprinkling as claimed in claim 2, it is characterised in that:The herbicide and Liquid Fertilizer The weight ratio of material is 1: 15.
  4. 4. as claim 1-3 any one of them is used for the Weed removal medicinal fertilizer of unmanned plane sprinkling, it is characterised in that:The herbicide In units of parts by weight, including following raw material:70-112 parts of ribbon gum, pyrene are green pepper 55-80 parts clear, 50-65 parts of fish pelargonium, cineole 30-75 parts, 45-80 parts of Carpesium cernuum Linn, 35-55 parts of radix euphorbiae lantu, 25-38 parts of meteloidine, 35-85 parts of Ageratum conyzoides, yellow cinnamon leaf 23-45 Part.
  5. 5. as claim 1-3 any one of them is used for the Weed removal medicinal fertilizer of unmanned plane sprinkling, it is characterised in that:The Liquid Fertilizer Expect for clear liquid type, floating type, sludge-type compound fertilizer one or more.
  6. 6. as claim 1-3 any one of them is used for the Weed removal medicinal fertilizer of unmanned plane sprinkling, it is characterised in that:The auxiliary agent by One or more compositions in solvent, cosolvent, wetting agent, demulsifier, defoamer, dispersant, antifreezing agent.
  7. 7. the Weed removal medicinal fertilizer for unmanned plane sprinkling as claimed in claim 6, it is characterised in that:The solvent is water, hydrotropy Agent is organic acid, organic acid sodium salt, one kind of amide-type, and wetting agent is one kind of thio-alcohol, hydrazides and mercaptan acetals, is broken Emulsion is ethylene polyamine and polyoxyethylene polyoxypropylene polyether mixture, the one of alkyl phenolic resin and polyoxyethylene mixture Kind, defoamer is silicone emulsion, the fatty acid ester compounded thing of higher alcohols, one kind of polyoxyethylene polyoxypropylene pentaerythrite ether, point Powder is fatty acid, one kind of esters, and antifreezing agent is acid phosphate amine salt, sodium chloride, one kind of urea.
  8. 8. a kind of preparation method for the Weed removal medicinal fertilizer for being used for unmanned plane sprinkling such as claim 1-3 any one of them, its feature It is, is made of following steps:
    S1:Ribbon gum, the clear green pepper of pyrene, fish pelargonium, cineole, Carpesium cernuum Linn, radix euphorbiae lantu, meteloidine, Ageratum conyzoides, yellow cinnamon leaf are mixed Crush, obtain mixture, add mixture in ethanol, be 1 in solid-liquid ratio:13-17, ultrasonic power 160-320W, Concentration of alcohol is 60%-78%, and Extracting temperature is that liquid 18-30min is extracted at 64-75 DEG C, and liquid is made;
    S2:Liquid made from step S1 is crossed into 10-20 mesh sieve, herbicide is made;
    S3:Auxiliary agent and liquid fertilizer are added into herbicide made from step S2, stirring and dissolving 25- at being 40-53 DEG C in temperature 32min, is made mixed liquor;
    S4:Mixed liquor made from step S3 is diluted with 1000-8000 parts of water, the Weed removal medicinal fertilizer for unmanned plane sprinkling is made.
  9. 9. the preparation method of the Weed removal medicinal fertilizer sprayed as claimed in claim 8 for unmanned plane, it is characterised in that:In step S3 The rotating speed of the stirring is 200-300r/min.
  10. 10. the preparation method of the Weed removal medicinal fertilizer sprayed as claimed in claim 8 for unmanned plane, it is characterised in that:Step S4 Described in water be deionized water.
CN201711243615.7A 2017-11-30 2017-11-30 Weed removal medicinal fertilizer for unmanned plane sprinkling and preparation method thereof Pending CN107935791A (en)

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Application publication date: 20180420