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CN107764586A - Vertical freezing sampling apparatus and its application method - Google Patents

Vertical freezing sampling apparatus and its application method Download PDF

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Publication number
CN107764586A
CN107764586A CN201711308764.7A CN201711308764A CN107764586A CN 107764586 A CN107764586 A CN 107764586A CN 201711308764 A CN201711308764 A CN 201711308764A CN 107764586 A CN107764586 A CN 107764586A
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sampler
copper tube
liquid
tube probe
sample
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金光球
苗雪
张向阳
郝永飞
唐洪武
陈奕林
金凯
李凌
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Hohai University HHU
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Hohai University HHU
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/04Devices for withdrawing samples in the solid state, e.g. by cutting
    • G01N1/08Devices for withdrawing samples in the solid state, e.g. by cutting involving an extracting tool, e.g. core bit

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
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  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
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  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

本发明公开了一种垂直冷冻采样装置及其使用方法,采样装置包括作业船、自动控制平台、提升系统、液态CO2供应装置、采样器和安装在采样器上的调整支架,自动控制平台、提升系统和液态CO2供应装置依次固定在作业船上,提升系统与采样器通过缆绳连接,调整支架位于采样器下部。采样器中的中空铜管探针通过液态CO2输入管线与液态CO2供应装置连接。自动控制平台中的自动水准调平系统控制调整支架,使铜管探针垂直插入沉积层,冷冻并采集试样。与现有技术相比,本发明可用于深水和浅水区域沉积物的原位采集,采样器中的铜管探针垂直插入沉积物,保证了深水和较高流速情况下的采样成功率。

The invention discloses a vertical freezing sampling device and its use method. The sampling device includes an operation ship, an automatic control platform, a lifting system, a liquid CO2 supply device, a sampler and an adjustment bracket installed on the sampler, the automatic control platform, The lifting system and the liquid CO2 supply device are fixed on the workboat in turn, the lifting system is connected with the sampler through cables, and the adjustment bracket is located at the lower part of the sampler. The hollow copper tube probe in the sampler was connected to the liquid CO supply through the liquid CO input line. The automatic leveling system in the automatic control platform controls and adjusts the bracket, so that the copper tube probe is vertically inserted into the deposition layer, and the sample is frozen and collected. Compared with the prior art, the present invention can be used for in-situ collection of sediments in deep water and shallow water areas, and the copper tube probe in the sampler is vertically inserted into the sediments, ensuring the success rate of sampling in deep water and higher flow rates.

Description

垂直冷冻采样装置及其使用方法Vertical freeze sampling device and method of use thereof

技术领域technical field

本发明涉及采样装置,尤其涉及垂直冷冻采样装置及其使用方法。The invention relates to a sampling device, in particular to a vertical freezing sampling device and a method for using the same.

背景技术Background technique

自然河流中,地表水与浅层地下水双向迁移和混合的区域称为潜流带。潜流带是活跃的生态群落交错区,是河流中颗粒和溶质交换、新陈代谢和储存的主要场所,对河流生命体的生命循环和河流健康具有重要意义。In natural rivers, the area where surface water and shallow groundwater migrate and mix in both directions is called the hyporheic zone. The hyporheic zone is an active ecotone zone and the main place for the exchange, metabolism and storage of particles and solutes in rivers, which is of great significance to the life cycle of river organisms and river health.

目前,广泛用于水底沉积物取样的设备主要有抓斗式采泥器和重力式沉积物采样器。其中,抓斗式采泥器只能采集表层沉积物,使用时对样品产生极大的扰动,破坏了沉积物的原始状态,无法满足日益精细的沉积物检测分析;传统的重力式沉积物采样器依靠仪器本身的重力砸入沉积物中,采样的深度取决于仪器重力,较为笨重,使用不方便,对样品产生的扰动较大,而且采样时重力式采样器容易产生倾斜,导致采集不到沉积物样品,采样成功率低。At present, the equipment widely used for bottom sediment sampling mainly includes grab mud sampler and gravity sediment sampler. Among them, the grab mud extractor can only collect surface sediments, which greatly disturbs the samples when used, destroys the original state of the sediments, and cannot meet the increasingly fine sediment detection and analysis; the traditional gravity sediment sampling The gravity sampler relies on the gravity of the instrument itself to drop into the sediment, and the sampling depth depends on the gravity of the instrument, which is cumbersome, inconvenient to use, and has a large disturbance to the sample, and the gravity sampler is prone to tilt during sampling, resulting in failure to collect. For sediment samples, the sampling success rate is low.

发明内容Contents of the invention

发明目的:本发明的目的是提供用于深水和浅水区域沉积物的原位采集的垂直冷冻采样装置及其使用方法。Purpose of the invention: The purpose of the present invention is to provide a vertical frozen sampling device for in-situ collection of sediments in deep and shallow water areas and a method of use thereof.

技术方案:垂直冷冻采样装置包括作业船、自动控制平台、提升系统、液态CO2供应装置、采样器和安装在采样器上的调整支架;自动控制平台、提升系统和液态CO2供应装置固定在作业船上,采样器与提升系统通过缆绳连接,采样器中的铜管探针通过液态CO2输入管线与液态CO2供应装置连接,自动控制平台的自动水准调平系统控制调整支架,使铜管探针垂直插入沉积层,冷冻并采集试样。Technical solution: The vertical freezing sampling device includes a working boat, an automatic control platform, a lifting system, a liquid CO2 supply device, a sampler and an adjustment bracket installed on the sampler; the automatic control platform, the lifting system and the liquid CO2 supply device are fixed on On the workboat, the sampler is connected to the hoisting system through a cable, the copper pipe probe in the sampler is connected to the liquid CO2 supply device through the liquid CO2 input pipeline, and the automatic leveling system of the automatic control platform controls and adjusts the bracket so that the copper pipe The probe is inserted vertically into the sediment, and the sample is frozen and collected.

自动控制平台内设的定位系统接收无线信号发射装置和水下摄像头实时传回的图像、数据。The positioning system built in the automatic control platform receives the images and data sent back in real time by the wireless signal transmitter and the underwater camera.

采样器中的重力锤的激发装置由自动控制平台控制。The excitation device of the gravity hammer in the sampler is controlled by an automatic control platform.

调整支架由三支调节长度的支架,以及支架间的平衡调整装置组成。The adjustment bracket is composed of three length-adjusting brackets and a balance adjustment device between the brackets.

还包括位于平衡调整装置上方的无线信号发射装置和水下摄像头,定位系统接收无线信号发射装置和水下摄像头实时传回的图像、数据。It also includes a wireless signal transmitter and an underwater camera located above the balance adjustment device, and the positioning system receives images and data sent back in real time by the wireless signal transmitter and the underwater camera.

垂直冷冻采样装置的使用方法,包括以下步骤:The using method of vertical freezing sampling device comprises the following steps:

(1)将作业船开至需要采样处,控制采样器使其缓慢降至河底;(1) Drive the operation boat to the place where sampling is required, and control the sampler to slowly lower it to the bottom of the river;

(2)通过无线信号发射装置和水下摄像头实时传回的数据调整采样器位置;(2) adjust the position of the sampler by the data sent back in real time by the wireless signal transmitter and the underwater camera;

(3)确定采样器位置后,通过自动水准调平系统控制调整支架,使铜管探针垂直于沉积层;(3) After determining the position of the sampler, control and adjust the bracket through the automatic leveling system so that the copper tube probe is perpendicular to the deposition layer;

(4)激发重力锤,将铜管探针垂直插入沉积层;(4) Excite the gravity hammer, and insert the copper tube probe vertically into the deposition layer;

(5)打开阀门,使液态CO2通过CO2输入管线进入铜管探针中,液态CO2汽化吸热,铜管探针周围的沉积物被迅速的冷冻,产生的CO2气体由CO2输出管线排出;(5) Open the valve so that liquid CO 2 enters the copper tube probe through the CO 2 input pipeline, the liquid CO 2 vaporizes and absorbs heat, the deposits around the copper tube probe are rapidly frozen, and the generated CO 2 gas is composed of CO 2 output line discharge;

(6)待温度传感器传回的数据达到稳定状态时,控制提升系统,将采样器提出,取下铜管探针及试样;(6) When the data returned by the temperature sensor reaches a stable state, control the lifting system, lift the sampler, and remove the copper tube probe and sample;

(7)向铜管探针中倒入热水,使试样与铜管探针分离,将试样装入样本盒,并放入冰箱中。(7) Pour hot water into the copper tube probe to separate the sample from the copper tube probe, put the sample into a sample box, and put it in a refrigerator.

有益效果:与现有技术相比,本发明具有以下优点:(1)既可用于深水区域柱状沉积物的原位采集,也可以直接将配备液态CO2供应装置的采样器用于浅水区域沉积物的原位采集,且保证了较高流速下设备的采样成功率;(2)使试样中的生物化学活动降至最低,保证了试样的原始状态;(3)减少了采样器对样本结构的破坏,以及河水对试样成分的影响。Beneficial effects: Compared with the prior art, the present invention has the following advantages: (1) It can be used for in-situ collection of columnar sediments in deep water areas, and can also directly use a sampler equipped with a liquid CO2 supply device for sediments in shallow water areas in-situ collection, and ensure the sampling success rate of the equipment at a higher flow rate; (2) minimize the biochemical activity in the sample and ensure the original state of the sample; (3) reduce the impact of the sampler on the sample damage to the structure, and the effect of river water on the composition of the sample.

附图说明Description of drawings

图1为本发明结构示意图;Fig. 1 is a structural representation of the present invention;

图2为采样器的结构示意图;Fig. 2 is the structural representation of sampler;

图3为可调整支架的结构示意图。Fig. 3 is a schematic structural diagram of the adjustable bracket.

具体实施方式Detailed ways

如图1所示,垂直冷冻采样装置包括作业船1、自动控制平台2、提升系统3、液态CO2供应装置5、采样器6和安装在采样器上的调整支架7;自动控制平台2、提升系统3和液态CO2供应装置5固定在作业船1上,安装在调整支架7上的采样器6与提升系统3通过缆绳4连接,采样器6中的铜管探针8通过液态CO2输入管线13与液态CO2供应装置5连接,自动控制平台2的自动水准调平系统控制调整支架7,使铜管探针8垂直插入沉积层,冷冻并采集试样。As shown in Figure 1, the vertical freezing sampling device includes an operation ship 1, an automatic control platform 2, a lifting system 3, a liquid CO2 supply device 5, a sampler 6 and an adjustment bracket 7 installed on the sampler; the automatic control platform 2, The lifting system 3 and the liquid CO 2 supply device 5 are fixed on the workboat 1, the sampler 6 installed on the adjustment bracket 7 is connected to the lifting system 3 through the cable 4, and the copper tube probe 8 in the sampler 6 passes through the liquid CO 2 The input pipeline 13 is connected to the liquid CO2 supply device 5, and the automatic leveling system of the automatic control platform 2 controls and adjusts the bracket 7, so that the copper tube probe 8 is vertically inserted into the sediment layer, and samples are frozen and collected.

自动控制平台2内设的定位系统接收无线信号发射装置19和水下摄像头10实时传回的图像、数据。The positioning system installed in the automatic control platform 2 receives images and data sent back by the wireless signal transmitter 19 and the underwater camera 10 in real time.

如图2所示,采样器6包括中空铜管探针8、温度传感器16、无线信号发射装置9、摄像头10、温度探针11、重力锤12、液态CO2输入管线13和CO2输出管线14,其中铜管探针8可拆卸,通过螺栓15与上部结构相连接;中空铜管探针8通过液态CO2输入管线13与液态CO2供应装置5连接;重力锤12的激发装置由自动控制平台2进行控制。As shown in Figure 2, the sampler 6 includes a hollow copper tube probe 8, a temperature sensor 16, a wireless signal transmitter 9, a camera 10, a temperature probe 11, a gravity hammer 12, a liquid CO input pipeline 13 and a CO output pipeline 14, wherein the copper tube probe 8 is detachable and connected to the upper structure through bolts 15; the hollow copper tube probe 8 is connected to the liquid CO 2 supply device 5 through the liquid CO 2 input pipeline 13; the excitation device of the gravity hammer 12 is controlled by the automatic The control platform 2 performs control.

如图3所示,调整支架7由三支可以调节长度的支架19,以及支架间的平衡调整装置18组成,由自动水准调平系统进行控制。As shown in FIG. 3 , the adjustment bracket 7 is composed of three length-adjustable brackets 19 and a balance adjustment device 18 between the brackets, and is controlled by an automatic leveling system.

垂直冷冻采样装置的使用方法,包括以下步骤:The using method of vertical freezing sampling device comprises the following steps:

(1)将作业船1开至需要采样处,控制采样器6使其缓慢降至河底;(1) Drive the operation boat 1 to the place where sampling is required, and control the sampler 6 to slowly lower it to the bottom of the river;

(2)通过无线信号发射装置9和水下摄像头10实时传回的图像、数据选择适宜的采样环境,并调整采样器6的位置;(2) select a suitable sampling environment by the images and data sent back in real time by the wireless signal transmitter 9 and the underwater camera 10, and adjust the position of the sampler 6;

(3)确定采样器6位置后,通过自动水准调平系统调整三角支架19,使铜管探针8垂直于沉积层;(3) After determining the position of the sampler 6, adjust the tripod 19 through the automatic leveling system so that the copper tube probe 8 is perpendicular to the deposition layer;

(4)激发重力锤12,将铜管探针8垂直插入沉积层;(4) Excite the gravity hammer 12, and insert the copper pipe probe 8 vertically into the deposition layer;

(5)打开阀门,使液态CO2通过液态CO2输入管线13进入铜管探针8中,由于液态CO2汽化吸热,铜管探针8周围的沉积物被迅速的冷冻,为了保证铜管探针中始终保持大气压强,产生的CO2气体可以由CO2输出管线14排出;(5) Open the valve so that liquid CO2 enters the copper tube probe 8 through the liquid CO2 input pipeline 13. Because the liquid CO2 vaporizes and absorbs heat, the deposits around the copper tube probe 8 are quickly frozen. Atmospheric pressure is always maintained in the tube probe, and the CO produced can be discharged from the CO output line 14;

(6)待温度传感器16传回的数据基本达到稳定状态时,控制提升系统3,将采样器6提出,旋转螺栓15取下铜管探针8及试样;(6) When the data returned by the temperature sensor 16 reaches a stable state substantially, the lifting system 3 is controlled, the sampler 6 is proposed, and the screw 15 is rotated to take off the copper pipe probe 8 and the sample;

(7)向铜管探针8中倒入热水,使试样与铜管探针8分离,将试样装入样本盒,并放入冰箱中,或根据需要,用小刀切取试样,放入采样瓶中。(7) Pour hot water into the copper tube probe 8 to separate the sample from the copper tube probe 8, put the sample into the sample box, and put it in the refrigerator, or cut the sample with a knife as required, Put into sampling bottle.

Claims (6)

1.一种垂直冷冻采样装置,其特征在于:包括作业船(1)、自动控制平台(2)、提升系统(3)、液态CO2供应装置(5)、采样器(6)和安装在采样器上的调整支架(7);所述自动控制平台(2)、提升系统(3)和液态CO2供应装置(5)固定在作业船(1)上,所述自动控制平台(2)内设定位系统和自动水准调平系统,所述定位系统与所述提升系统(3)连接,所述自动水准调平系统与所述采样器(6)连接;所述采样器(6)包括中空铜管探针(8)、液态CO2输入管线(13)和CO2输出管线(14),所述中空铜管探针(8)通过液态CO2输入管线(13)与液态CO2供应装置(5)连接,所述自动水准调平系统控制调整支架(7),使铜管探针(8)垂直插入沉积层,冷冻并采集试样。1. a vertical freezing sampling device is characterized in that: comprise operation vessel (1), automatic control platform (2), lifting system (3), liquid CO supply device (5), sampler (6) and be installed in The adjustment bracket (7) on the sampler; the automatic control platform (2), the lifting system (3) and the liquid CO supply device (5) are fixed on the workboat (1), and the automatic control platform (2) Built-in positioning system and automatic leveling system, the positioning system is connected with the lifting system (3), the automatic leveling system is connected with the sampler (6); the sampler (6) includes Hollow copper tube probe (8), liquid CO input line (13) and CO output line (14), the hollow copper tube probe (8) is supplied with liquid CO through the liquid CO input line (13) The device (5) is connected, and the automatic leveling system controls and adjusts the bracket (7), so that the copper tube probe (8) is vertically inserted into the deposition layer, and the sample is frozen and collected. 2.根据权利要求1所述的垂直冷冻采样装置,其特征在于:所述中空铜管探针(8)为可拆卸式,探针内设温度传感器。2. The vertical cryo-sampling device according to claim 1, characterized in that: the hollow copper tube probe (8) is detachable, and the probe is equipped with a temperature sensor. 3.根据权利要求1所述的垂直冷冻采样装置,其特征在于:根据水深选择采样器(6)的配重,配重的激发装置由自动控制平台(2)进行控制。3. The vertical freezing sampling device according to claim 1, characterized in that: the counterweight of the sampler (6) is selected according to the water depth, and the excitation device of the counterweight is controlled by the automatic control platform (2). 4.根据权利要求1所述的垂直冷冻采样装置,其特征在于:所述调整支架(7),由可调节长度的支架(19),以及支架间的平衡调整装置(18)组成。4. The vertical cryo-sampling device according to claim 1, characterized in that: the adjustment bracket (7) is composed of a length-adjustable bracket (19) and a balance adjustment device (18) between the brackets. 5.根据权利要求1所述的垂直冷冻采样装置,其特征在于:还包括位于平衡调整装置(18)上方的无线信号发射装置(9)和水下摄像头(10),所述定位系统接收无线信号发射装置(9)和水下摄像头(10)实时传回的图像、数据。5. The vertical freezing sampling device according to claim 1, characterized in that: it also includes a wireless signal transmitting device (9) and an underwater camera (10) positioned above the balance adjustment device (18), and the positioning system receives wireless signals. The images and data sent back by the signal transmitting device (9) and the underwater camera (10) in real time. 6.一种垂直冷冻采样装置的使用方法,其特征在于:包括以下步骤:6. A method for using a vertical freezing sampling device, characterized in that: comprising the following steps: (1)将作业船(1)开至需要采样处,控制采样器(6)使其缓慢降至河底;(1) Drive the operation boat (1) to the place where sampling is required, and control the sampler (6) to slowly lower it to the bottom of the river; (2)通过无线信号发射装置(9)和水下摄像头(10)实时传回的图像、数据调整采样器(6)位置;(2) adjust the position of the sampler (6) by the image and data sent back in real time by the wireless signal transmitter (9) and the underwater camera (10); (3)确定采样器(6)位置后,通过自动水准调平系统控制调整支架(7),使铜管探针(8)垂直于沉积层;(3) After determining the position of the sampler (6), control and adjust the bracket (7) through the automatic leveling system so that the copper tube probe (8) is perpendicular to the deposition layer; (4)激发重力锤(12),将铜管探针(8)垂直插入沉积层;(4) Excite the gravity hammer (12), and insert the copper tube probe (8) vertically into the deposition layer; (5)打开阀门,使液态CO2通过CO2输入管线(13)进入铜管探针(8)中,液态CO2吸热,铜管探针周围的沉积物被迅速的冷冻,产生的CO2气体由CO2输出管线(14)排出;(5) Open the valve to make liquid CO2 enter the copper tube probe (8) through the CO2 input pipeline (13), the liquid CO2 absorbs heat, and the deposits around the copper tube probe are rapidly frozen, and the produced CO 2. The gas is discharged from the CO output pipeline (14); (6)待温度传感器(16)传回的数据达到稳定状态时,控制提升系统(3),将采样器(6)提出,取下铜管探针(8)及试样;(6) When the data returned by the temperature sensor (16) reaches a stable state, the lifting system (3) is controlled, the sampler (6) is proposed, and the copper tube probe (8) and the sample are removed; (7)向铜管探针(8)中倒入热水,使试样与铜管探针(8)分离,将试样装入样本盒,并放入冰箱中。(7) Pour hot water into the copper tube probe (8) to separate the sample from the copper tube probe (8), put the sample into a sample box, and put it in a refrigerator.
CN201711308764.7A 2017-12-11 2017-12-11 Vertical freezing sampling apparatus and its application method Pending CN107764586A (en)

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CN109959525A (en) * 2019-03-21 2019-07-02 浙江大学 A deep-sea thermal insulation biological sampler
CN113309478A (en) * 2021-06-25 2021-08-27 中国科学院地球环境研究所 Freezing system of boring that is fit for operation on water and ice
CN113324797A (en) * 2021-06-10 2021-08-31 中国科学院烟台海岸带研究所 Hidden DGT passive sampler throwing device
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CN108760400A (en) * 2018-07-24 2018-11-06 中国地质科学院 A kind of underwater sediment sampler
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CN113324797A (en) * 2021-06-10 2021-08-31 中国科学院烟台海岸带研究所 Hidden DGT passive sampler throwing device
CN113309478A (en) * 2021-06-25 2021-08-27 中国科学院地球环境研究所 Freezing system of boring that is fit for operation on water and ice
CN117268843B (en) * 2022-06-30 2024-05-14 广州海洋地质调查局 Method for rapidly predicting methane diffusion flux of sediment in target area of cold spring area
RU2805750C1 (en) * 2023-03-15 2023-10-23 Федеральное государственное бюджетное учреждение науки Институт проблем безопасного развития атомной энергетики Российской академии наук (ИБРАЭ РАН) Fluid sampling device

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