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CN107746750A - The preparation method of rosebud water - Google Patents

The preparation method of rosebud water Download PDF

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Publication number
CN107746750A
CN107746750A CN201711118503.9A CN201711118503A CN107746750A CN 107746750 A CN107746750 A CN 107746750A CN 201711118503 A CN201711118503 A CN 201711118503A CN 107746750 A CN107746750 A CN 107746750A
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China
Prior art keywords
rosebud
distillation
water
condensing unit
temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711118503.9A
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Chinese (zh)
Inventor
邓宗伦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Laizhou Bai Shi Tong Rose Industry Development Ltd By Share Ltd
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Laizhou Bai Shi Tong Rose Industry Development Ltd By Share Ltd
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Application filed by Laizhou Bai Shi Tong Rose Industry Development Ltd By Share Ltd filed Critical Laizhou Bai Shi Tong Rose Industry Development Ltd By Share Ltd
Priority to CN201711118503.9A priority Critical patent/CN107746750A/en
Publication of CN107746750A publication Critical patent/CN107746750A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/027Recovery of volatiles by distillation or stripping
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/022Refining

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Epidemiology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Birds (AREA)
  • Mycology (AREA)
  • Dermatology (AREA)
  • Fats And Perfumes (AREA)
  • Cosmetics (AREA)

Abstract

The present invention is applied to skin care item preparing technical field, there is provided a kind of preparation method of rosebud water, comprises the following steps:Early morning 5~8 point are manually won by rose;It is preferred that rosebud, fresh roseleaf, reject leaf, limb and other debris;Rosebud, fresh roseleaf and incense drug grass are mixed, then pickled;The material for pickling completion is placed in distillation space and distilled, 3~5h of distillation is carried out to it using the high temperature distilled in space, distillation space temperature is 80~120 °, and distillation space pressure is 0.07~0.1MPa;It vapor and essential oil steam will be introduced caused by distillation by mozzle in condensing unit, and carry out 1~3h of condensation to it using condensing unit, the temperature in condensing unit is 15~40 °;Liquid after condensation generation enters in purifying plant through mozzle carries out purification & isolation.Whereby, the present invention can be with the extraction rose of effective and safe.

Description

The preparation method of rosebud water
Technical field
The present invention relates to skin care item preparing technical field, more particularly to a kind of preparation method of rosebud water.
Background technology
Hydrosol (also known as crystal's oil, Hydrolat), refers to the water that essential oil stays during distillation extraction, is essential oil A kind of byproduct, it is a kind of hydrosol for 100% saturation separated during essential oil is refined, composition is naturally pure, fragrance It is light pleasant.During distillation, profit can be separated, asked plants essential oil, in essential oil liquid after distillation, can also leave one A little moisture, because density is different, essential oil can be swum in above, and moisture can be deposited in following, and these moisture are just hydrosol.Pure dew In contain micro acid and lipid material, chemical constitution is different from general pure water, to body nurse one's health it is helpful.
The fresh rose flower plucked in rose plant base, it is necessary to immediately treat, avoid effective aromatic substance from volatilizing, reduce Extraction of essential oil amount.The method of use is to seal that fresh flower is fragrant with salt stirring, and the fresh flower after sealing can carry out distillation processing. Fresh flower is put into alembic, and steam heating distillation under pressure, the steam cooling condensation after distillation forms distilled water, into water-oil separating Device.For essential oil in upper distillate under, the extraction of essential oil after separation enters essential oil storage container to oil water separator at low temperature, below Distillate be recycled into alembic and continue heating evaporation.Because this part distillate includes the essential oil either with or without defecation.Such as This moves in circles, until extraction of essential oil finishes.Remaining liquid is exactly hydrosol.Hydrosol is last in the form of close to colourless distilled water Produce.But in process of production, the essential oil extracted can be short of with hydrosol quality.
In summary, prior art there will naturally be inconvenience and defect in actual use, and it is therefore necessary to improved.
The content of the invention
For it is above-mentioned the defects of, it is an object of the invention to provide a kind of preparation method of rosebud water, it can pacify Complete efficient extraction rose.
To achieve these goals, the present invention provides a kind of preparation method of rosebud water, comprises the following steps:
A, early morning 5~8 point are manually won to rose;
B, preferably rosebud, fresh roseleaf, leaf, limb and other debris are rejected;
C, rosebud, fresh roseleaf and incense drug grass are mixed, then pickled;
D, the material for pickling completion is placed in distillation space and distilled, it is entered using the high temperature distilled in space Row 3~5h of distillation, distillation space temperature is 80~120 °, and distillation space pressure is 0.07~0.1MPa;
E, vapor and essential oil steam are introduced in condensing unit by mozzle caused by distilling, and utilize condensing unit pair It carries out 1~3h of condensation, and the temperature in condensing unit is 15~40 °;
F, the liquid after condensation produces enters in purifying plant through mozzle carries out purification & isolation;
G, by isolated hydrosol and pure water according to 2:15 ratio is sufficiently mixed.
According to the preparation method of the rosebud water of the present invention, the distillation space temperature is 110 °, the distillation time For 4.5h, the distillation space pressure is 0.09MPa.
According to the preparation method of the rosebud water of the present invention, the temperature in the condensing unit is 30 °, and condensation time is 2.5h。
According to the preparation method of the rosebud water of the present invention, the salting period is 3h, and the incense drug straw bag includes fragrant honeybee Grass or lavender or chamomile.
According to the preparation method of the rosebud water of the present invention, water and oil separator is installed in the purifying plant, and carry The pure time is 1h.
According to the preparation method of the rosebud water of the present invention, the incense drug grass also includes rose oxide, leaf-alcohol and geranyl ether.
Beneficial effects of the present invention:Efficiently quickly rose can be extracted, while during taking, can To ensure the Quality Safety of rose, strengthen the practicality of rose, improve the quality of rose.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention It is further elaborated, it will be appreciated that the specific embodiments described herein are merely illustrative of the present invention, is not used to Limit the present invention.
The invention provides a kind of preparation method of rosebud water, this method comprises the following steps:
A, early morning 5~8 point are manually won to rose;
B, preferably rosebud, fresh roseleaf, leaf, limb and other debris are rejected;
C, rosebud, fresh roseleaf and incense drug grass are mixed, then pickled;
D, the material for pickling completion is placed in distillation space and distilled, it is entered using the high temperature distilled in space Row 3~5h of distillation, distillation space temperature is 80~120 °, and distillation space pressure is 0.07~0.1MPa;
E, vapor and essential oil steam are introduced in condensing unit by mozzle caused by distilling, and utilize condensing unit pair It carries out 1~3h of condensation, and the temperature in condensing unit is 15~40 °;
F, the liquid after condensation produces enters in purifying plant through mozzle carries out purification & isolation;
G, by isolated hydrosol and pure water according to 2:15 ratio is sufficiently mixed.
Preferably, distillation space temperature of the invention is 110 °, and the distillation time is 4.5h, distillation space pressure Power is 0.09MPa, rose is sufficiently mixed with vanilla medicine by distillation, ensures product while strengthening its aroma effect Quality.
In addition, the temperature in the condensing unit of the present invention is 30 °, condensation time 2.5h, vapor and essential oil can be made Steam fully solidifies to form water and essential oil.
Further, salting period of the invention is 3h, and the incense drug straw bag includes balm or lavender or chamomile, is led to Cross incense drug grass and enough fragrance is provided rose, make it more pleasant in use.
Preferably, water and oil separator is installed, and the purification time is 1h, passes through water oil and separates in purifying plant of the invention Device carries out separating-purifying to hydrosol and essential oil, can be used separately, suitable for different crowds.
Embodiment 1:To ensure the quality of rose, need start manually to pluck rose for 5 points or so, entirely adopted in the morning The process of plucking must be completed before 8 points, preferential to pluck rosebud and fresh rose petal, will pluck the rose of completion Bud and roseleaf are cleared up, and are rejected the debris such as leaf and limb, are then mixed rose and incense drug grass, fragrant Medicinal herbs use balm or lavender or chamomile, need to be added it according to different clients, incense drug grass also includes rose Rare ether, leaf-alcohol and geranyl ether, rose oxide, leaf-alcohol and the geranyl ether for then corresponding to the not year-on-year part of addition carry out Titian to it, corresponding It is than part:4:2:1, mixed material is pickled, pickles 3h, the material pickled is placed in distillation space and carried out Distillation.Distillation space includes loading plate and container, and loading plate is 1.5 meters apart from container distance, and water is housed inside container, passes through appearance Heater below device heats to the water in container, makes its boiling, distills in space and is additionally provided with temperature-detecting device, leads to Excess temperature detection means determines the temperature in distillation container, its temperature is maintained at 80 °, by the hot water of boiling to loading plate On mixing material distilled, distillation time 3h, the pressure distilled in space is 0.07MPa, vapor caused by distillation And essential oil steam is entered in condensing unit by mozzle.Condensing unit is connected with water inlet pipe, is filled by water inlet pipe to condensation Middle injection cold water is put, the temperature in condensing unit is confirmed by the temperature-detecting device in condensing unit, keeps it in 15 °, The vapor and essential oil steam flowed through using the temperature in condensing unit to condenser Inner guide pipe is condensed, and condensation time is 1h, caused liquid enters through mozzle after condensation carries out purification & isolation in purifying plant, and water oil is provided with purifying plant Separator, condensed liquid are separated by water and oil separator, form hydrosol and essential oil, during separating-purifying, are needed To the liquid-purifying 1h of condensation, to ensure the quality of hydrosol and essential oil, by isolated hydrosol and pure water according to 2:15 Ratio is sufficiently mixed, and rosebud water is obtained after mixing.
Embodiment 2:To ensure the quality of rose, need start manually to pluck rose for 5 points or so, entirely adopted in the morning The process of plucking must be completed before 8 points, preferential to pluck rosebud and fresh rose petal, will pluck the rose of completion Bud and roseleaf are cleared up, and are rejected the debris such as leaf and limb, are then mixed rose and incense drug grass, fragrant Medicinal herbs use balm or lavender or chamomile, need to be added it according to different clients, incense drug grass also includes rose Rare ether, leaf-alcohol and geranyl ether, rose oxide, leaf-alcohol and the geranyl ether for then corresponding to the not year-on-year part of addition carry out Titian to it, corresponding It is than part:6:3:1, mixed material is pickled, pickles 3h, the material pickled is placed in distillation space and carried out Distillation.Distillation space includes loading plate and container, and loading plate is 1.5 meters apart from container distance, and water is housed inside container, passes through appearance Heater below device heats to the water in container, makes its boiling, distills in space and is additionally provided with temperature-detecting device, leads to Excess temperature detection means determines the temperature in distillation container, its temperature is maintained at 110 °, by the hot water of boiling to loading plate On mixing material distilled, distillation time 4.5h, distill space in pressure be 0.09MPa, caused by distillation water steaming Gas and essential oil steam are entered in condensing unit by mozzle.Condensing unit is connected with water inlet pipe, by water inlet pipe to condensation Cold water is injected in device, the temperature in condensing unit is confirmed by the temperature-detecting device in condensing unit, kept it in 30 °, the vapor and essential oil steam flowed through using the temperature in condensing unit to condenser Inner guide pipe is condensed, during condensation Between be 2.5h, caused liquid enters through mozzle after condensation carries out purification & isolation in purifying plant, install in purifying plant There is water and oil separator, condensed liquid is separated by water and oil separator, hydrosol and essential oil is formed, in separating-purifying process In, need to be to the liquid-purifying 1h of condensation, to ensure the quality of hydrosol and essential oil, by isolated hydrosol and pure water according to 2: 15 ratio is sufficiently mixed, and rosebud water is obtained after mixing.
Embodiment 3:To ensure the quality of rose, need start manually to pluck rose for 5 points or so, entirely adopted in the morning The process of plucking must be completed before 8 points, preferential to pluck rosebud and fresh rose petal, will pluck the rose of completion Bud and roseleaf are cleared up, and are rejected the debris such as leaf and limb, are then mixed rose and incense drug grass, fragrant Medicinal herbs use balm or lavender or chamomile, need to be added it according to different clients, incense drug grass also includes rose Rare ether, leaf-alcohol and geranyl ether, rose oxide, leaf-alcohol and the geranyl ether for then corresponding to the not year-on-year part of addition carry out Titian to it, corresponding It is than part:2:2:1, mixed material is pickled, pickles 3h, the material pickled is placed in distillation space and carried out Distillation.Distillation space includes loading plate and container, and loading plate is 1.5 meters apart from container distance, and water is housed inside container, passes through appearance Heater below device heats to the water in container, makes its boiling, distills in space and is additionally provided with temperature-detecting device, leads to Excess temperature detection means determines the temperature in distillation container, its temperature is maintained at 120 °, by the hot water of boiling to loading plate On mixing material distilled, distillation time 5h, distill space in pressure be 0.1MPa, vapor caused by distillation and Essential oil steam is entered in condensing unit by mozzle.Condensing unit is connected with water inlet pipe, by water inlet pipe to condensing unit Middle injection cold water, the temperature in condensing unit is confirmed by the temperature-detecting device in condensing unit, keep it in 40 °, profit The vapor and essential oil steam flowed through with the temperature in condensing unit to condenser Inner guide pipe condenses, and condensation time is 3h, caused liquid enters through mozzle after condensation carries out purification & isolation in purifying plant, and water oil is provided with purifying plant Separator, condensed liquid are separated by water and oil separator, form hydrosol and essential oil, during separating-purifying, are needed To the liquid-purifying 1h of condensation, to ensure the quality of hydrosol and essential oil, by isolated hydrosol and pure water according to 2:15 Ratio is sufficiently mixed, and rosebud water is obtained after mixing.
45kg rosebud water is made using 3kg roses in embodiment 1, and hydrosol content is 45%, and embodiment 2 utilizes 3kg 45kg rosebud water is made in rose, and hydrosol content is 70%, and 45kg rosebuds are made using 3kg roses in embodiment 3 Water, hydrosol content are 55 percentages, and rosebud water quality made from last is analyzed according to embodiment and drawn, with reality Apply rosebud water performance optimal made from example 2.
Certainly, the present invention can also have other various embodiments, ripe in the case of without departing substantially from spirit of the invention and its essence Know those skilled in the art when can be made according to the present invention it is various it is corresponding change and deformation, but these corresponding change and become Shape should all belong to the protection domain of appended claims of the invention.

Claims (6)

1. a kind of preparation method of rosebud water, it is characterised in that comprise the following steps:
A, early morning 5~8 point are manually won to rose;
B, preferably rosebud, fresh roseleaf, leaf, limb and other debris are rejected;
C, rosebud, fresh roseleaf and incense drug grass are mixed, then pickled;
D, the material for pickling completion is placed in distillation space and distilled, it is steamed using the high temperature distilled in space 3~5h is evaporated, distillation space temperature is 80~120 °, and distillation space pressure is 0.07~0.1MPa;
E, vapor and essential oil steam are introduced in condensing unit by mozzle caused by distilling, and it is entered using condensing unit Go and condense 1~3h, the temperature in condensing unit is 15~40 °;
F, the liquid after condensation produces enters in purifying plant through mozzle carries out purification & isolation;
G, by isolated hydrosol and pure water according to 2:15 ratio is sufficiently mixed.
2. the preparation method of rosebud water according to claim 1, it is characterised in that it is described distillation space temperature be 110 °, the distillation time is 4.5h, and the distillation space pressure is 0.09MPa.
3. the preparation method of rosebud water according to claim 1, it is characterised in that the temperature in the condensing unit For 30 °, condensation time 2.5h.
4. the preparation method of rosebud water according to claim 1, it is characterised in that the salting period is 3h, institute State incense drug straw bag and include balm or lavender or chamomile.
5. the preparation method of rosebud water according to claim 1, it is characterised in that be provided with the purifying plant Water and oil separator, and the purification time is 1h.
6. the preparation method of rosebud water according to claim 4, it is characterised in that the incense drug grass also includes rose Ether, leaf-alcohol and geranyl ether.
CN201711118503.9A 2017-11-13 2017-11-13 The preparation method of rosebud water Pending CN107746750A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109758536A (en) * 2019-01-30 2019-05-17 厦门水叮当数据科技有限公司 A kind of formula plant mixes with tea oil purifies the liquid sole skin-care agent that adds white wine to be synthetically generated
CN111840170A (en) * 2020-08-26 2020-10-30 浙江千芊凝生物科技有限公司 Rose essence and preparation method thereof
CN114432734A (en) * 2022-01-21 2022-05-06 云南八街王大爹农业科技有限公司 Yunnan red double-petal rose bud water and preparation method thereof

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CN106244324A (en) * 2016-08-16 2016-12-21 文县恒水玫瑰开发有限公司 A kind of Flos Rosae Rugosae quintessence oil extracts and purification process

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109758536A (en) * 2019-01-30 2019-05-17 厦门水叮当数据科技有限公司 A kind of formula plant mixes with tea oil purifies the liquid sole skin-care agent that adds white wine to be synthetically generated
CN111840170A (en) * 2020-08-26 2020-10-30 浙江千芊凝生物科技有限公司 Rose essence and preparation method thereof
CN114432734A (en) * 2022-01-21 2022-05-06 云南八街王大爹农业科技有限公司 Yunnan red double-petal rose bud water and preparation method thereof

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