CN107557195A - A kind of gleditsia sinensis ganoderma lucidum laundry soap and preparation method thereof - Google Patents
A kind of gleditsia sinensis ganoderma lucidum laundry soap and preparation method thereof Download PDFInfo
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- CN107557195A CN107557195A CN201710687327.4A CN201710687327A CN107557195A CN 107557195 A CN107557195 A CN 107557195A CN 201710687327 A CN201710687327 A CN 201710687327A CN 107557195 A CN107557195 A CN 107557195A
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- 239000000344 soap Substances 0.000 title claims abstract description 105
- 240000008397 Ganoderma lucidum Species 0.000 title claims abstract description 46
- 235000001637 Ganoderma lucidum Nutrition 0.000 title claims abstract description 46
- 241000931143 Gleditsia sinensis Species 0.000 title claims abstract description 42
- 238000002360 preparation method Methods 0.000 title claims description 26
- 239000000284 extract Substances 0.000 claims abstract description 86
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 50
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 32
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 28
- AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Chemical compound OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 claims abstract description 20
- 241000628997 Flos Species 0.000 claims abstract description 18
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 16
- 229930006000 Sucrose Natural products 0.000 claims abstract description 14
- 235000019864 coconut oil Nutrition 0.000 claims abstract description 14
- 239000003240 coconut oil Substances 0.000 claims abstract description 14
- 230000000694 effects Effects 0.000 claims abstract description 14
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- 239000005720 sucrose Substances 0.000 claims abstract description 14
- -1 sucrose ester Chemical class 0.000 claims abstract description 12
- 238000000605 extraction Methods 0.000 claims description 19
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- 235000018274 Cunila origanoides Nutrition 0.000 claims description 18
- 235000014866 Dictamnus albus Nutrition 0.000 claims description 18
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 18
- 239000011347 resin Substances 0.000 claims description 18
- 229920005989 resin Polymers 0.000 claims description 18
- 239000002904 solvent Substances 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 15
- 239000002994 raw material Substances 0.000 claims description 13
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims description 12
- 238000005406 washing Methods 0.000 claims description 12
- 240000005250 Chrysanthemum indicum Species 0.000 claims description 10
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- 239000000843 powder Substances 0.000 claims description 8
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- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 2
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- 238000004140 cleaning Methods 0.000 abstract description 9
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- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
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- RYYVLZVUVIJVGH-UHFFFAOYSA-N caffeine Chemical compound CN1C(=O)N(C)C(=O)C2=C1N=CN2C RYYVLZVUVIJVGH-UHFFFAOYSA-N 0.000 description 2
- 230000008859 change Effects 0.000 description 2
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- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 1
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 241001478240 Coccus Species 0.000 description 1
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- LPHGQDQBBGAPDZ-UHFFFAOYSA-N Isocaffeine Natural products CN1C(=O)N(C)C(=O)C2=C1N(C)C=N2 LPHGQDQBBGAPDZ-UHFFFAOYSA-N 0.000 description 1
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 description 1
- 241000589517 Pseudomonas aeruginosa Species 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 239000004115 Sodium Silicate Substances 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
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- 239000003513 alkali Substances 0.000 description 1
- 229930013930 alkaloid Natural products 0.000 description 1
- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
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- 229910021538 borax Inorganic materials 0.000 description 1
- 229960001948 caffeine Drugs 0.000 description 1
- VJEONQKOZGKCAK-UHFFFAOYSA-N caffeine Natural products CN1C(=O)N(C)C(=O)C2=C1C=CN2C VJEONQKOZGKCAK-UHFFFAOYSA-N 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
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- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 239000002516 radical scavenger Substances 0.000 description 1
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- 229940095696 soap product Drugs 0.000 description 1
- 235000019795 sodium metasilicate Nutrition 0.000 description 1
- 229960001922 sodium perborate Drugs 0.000 description 1
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- 239000004328 sodium tetraborate Substances 0.000 description 1
- 235000010339 sodium tetraborate Nutrition 0.000 description 1
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Landscapes
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of gleditsia sinensis ganoderma lucidum laundry soap, the gleditsia sinensis ganoderma lucidum laundry soap is by 7 ~ 9 parts of Fructus Gleditsiae Abnormalis extract, 3 ~ 5 parts of Ganodenna Lucidum P.E, 7 ~ 9 parts of Flos Chrysanthemi Indici extract, 5 ~ 7 parts of Cortex Dictamni extract, 10 ~ 20 parts of glycerine, 10 ~ 20 parts of sucrose ester, 4 ~ 6 parts of ethanol, 4 ~ 6 parts of orange peel Normal juice, 4 ~ 6 parts of coconut oil, 25 parts of water, Glycolic acid is made in right amount.Laundry soap prepared by the present invention is natural and organic ingredients, and gentle decontamination, the hydrolysate after cleaning is degradable, environmentally friendly；Have simultaneously sterilization except tinea, moisturizing is non-stimulated the effect of, moreover it can be used to facial basic cleaning, be not in the situation of dry and cracked layering after water soaks for a long time, shelf life is obviously prolonged.
Description
Technical field
The present invention relates to cleaning product and its production technology field, and in particular to one kind is green, pro-skin skin care is stingless
Swash, sterilization remove tinea, deposit or after water soaks be not in the gleditsia sinensis ganoderma lucidum laundry soap of dry and cracked layering for a long time.
Background technology
Existing market is sold and people's detergent used in everyday is mainly soap and synthetic detergent.Soap mainly with
Natural oil or oil foot form after carrying out saponification with alkali for primary raw material through saltouing and adding waterglass, saltcake etc., then pass through
Arrange, the process such as shaping is made, solubility is small under cryogenic for soap, inconvenient for use, disperse during washing it is irregular, after influence is washed
The feel of clothing, makes washings turn to be yellow sometimes, today of hand washing is especially largely substituted with washing machine, its is inconvenient for use
The defects of seem more prominent.It is larger that people by extensive work develop solubility under cryogenic, is uniformly dispersed, uses
Convenient extraction object detergent and synthetic detergent powder.Synthetic detergent powder mainly has surfactant containing benzene, washing assisant and water
Deng being prepared after mixture by drying process with atomizing, alkalescence is big, difficult rinsing, easily residual, is more suitable for cleaning jean, thickness
Overcoat and curtain, sofa cover of weight etc..Because surfactant, washing assisant contain hazardous substance, have to human body skin stronger
Stimulation, some harmful substances may be sucked by skin and the organ such as liver stolen goods is damaged in human body, made in production and in
Into environmental pollution.Doing washing, extract is relatively gentle, and a variety of laundry extracts also occurs in succession in market, extract of relatively commonly doing washing
Have the advantages that alkalescence is small, do not stimulate gently, be antibacterial, hypo-allergenic, exactly because but also these functional characteristics, laundry extract
In add some chemical substances unavoidably and do antiseptic, bacteriostatic agent, essence etc., it is difficult to accomplish pure natural to add without chemistry.
Advocate environmental protection, in the modern life for paying attention to health, except good clean effect, improve various spot problems,
Green natural, safe and non-toxic, the natural plants laundry extract of gentle nutrition is increasingly subject to the favor of people.Gleditsia sinensis is China people
Between conventional washing articles for use, due to the development of modern synthesis of detergent product, be gradually backed out the life of people in recent decades.But due to
The advantages of synthesis of detergent articles for use have the shortcomings that pollution environmental damage skin, and people gradually re-recognize natural gleditsia sinensis, natural soap
The abundant plant nutrient such as fat, protein, polysaccharide, saponin, caffeine and alkaloid are contained in angle, do not decompose grease spot only
Characteristic, it extracts extract and can be also effectively combined with oil, and with health-care sterilization and other effects, laundry extraction made of gleditsia sinensis
For thing to scavenger surface without any corrosion, it is better than other any chemicals, is optimal efficiency natural surface
Active cleaning agent.
CN1052750C discloses a kind of concentrated spaonin powder and its production method, and the concentrated spaonin powder of this method production is with day
Right material is made up of primary raw material, and pollution will not be produced to environment during use, and illeffects will not be also produced to human body, but
Still the materials such as sodium perborate, borax, lauryl sodium sulfate, sodium metasilicate are with the addition of, and preparation technology is relative complex.
CN100390262C discloses a kind of gleditsia sinensis laundry soap and preparation method thereof, is made of pure natural raw material, without alkaline matter,
It is nontoxic, safe and environment-friendly for neutral degradable carbohydrate, it is non-stimulated to skin, both can oil removing de-sludging, have again the tender face of moisturizing,
Take care of hair anti-dandruff effect, better than synthesis of detergent soap product, but the defects of layering, bittiness occur after improving long-term place.
Based on above-mentioned analysis, the hydrolysate after a kind of composition natural organic, strong detergency, cleaning is easily degraded, to environment
Taste is pure and fresh after friendly, cleaning clothing, sterilization except tinea moisturizing is non-stimulated, long-term storage or after water soaks be not in it is dry and cracked,
Layering, bittiness laundry soap are badly in need of in industry.
The content of the invention
In view of above-mentioned deficiency, it is an object of the invention to provide a kind of pure plant formula, without chemical addition agent, go
Dirty ability is strong, it is gentle it is safe and non-stimulating, to skin not damaged, environmentally friendly, long-term storage or after water soaks be not in
Dry and cracked, layering, bittiness gleditsia sinensis ganoderma lucidum laundry soap and preparation method thereof.
In order to achieve the above object, present invention employs following technical scheme, the dosage of each component of the present invention is also process
Inventor carries out largely groping to summarize what is drawn, the gleditsia sinensis ganoderma lucidum laundry soap that each component dosage is prepared in the range of following weight
It is respectively provided with good effect：
A kind of gleditsia sinensis ganoderma lucidum laundry soap, is made up of the raw material of following weight：
7 ~ 9 parts of Fructus Gleditsiae Abnormalis extract, 3 ~ 5 parts of Ganodenna Lucidum P.E, 7 ~ 9 parts of Flos Chrysanthemi Indici extract, 5 ~ 7 parts of Cortex Dictamni extract, glycerine
10 ~ 20 parts, 10 ~ 20 parts of sucrose ester, 4 ~ 6 parts of ethanol, 4 ~ 6 parts of orange peel Normal juice, 4 ~ 6 parts of coconut oil, 25 parts of water, appropriate Glycolic acid.
Further, described gleditsia sinensis ganoderma lucidum laundry soap is made up of the raw material of following weight：
8 parts of Fructus Gleditsiae Abnormalis extract, 4 parts of Ganodenna Lucidum P.E, 8 parts of Flos Chrysanthemi Indici extract, 6 parts of Cortex Dictamni extract, 15 parts of glycerine, sucrose
15 parts of ester, 5 parts of ethanol, 5 parts of orange peel Normal juice, 5 parts of coconut oil, 25 parts of water, appropriate Glycolic acid.
Further, the preparation method of the Fructus Gleditsiae Abnormalis extract comprises the following steps：
Gleditsia sinensis is dissolved in the water of 10 ~ 30 times of gleditsia sinensis dry weights, extracted at 60 ~ 80 DEG C 2 ~ 4 times, 2 ~ 3h, merges extract solution every time
Afterwards, filter, carry out decompression extraction under the conditions of filtrate is placed in into 60 ~ 70 DEG C, pressure is -0.05 ~ 0.095MPa, recycling design, very
Sky is condensed into Fructus Gleditsiae Abnormalis extract.
Further, the preparation method of the Ganodenna Lucidum P.E comprises the following steps：
Ganoderma lucidum is dissolved in 40% ~ 60% ethanol solution of 10 ~ 20 times of ganoderma lucidum dry weights, extracts 1 ~ 3 time at 60 ~ 70 DEG C, every time
1.5 ~ 2.5h, merge extract solution, filtering, carry out that solvent is recovered under reduced pressure under the conditions of filtrate is placed in into 50 ~ 60 DEG C, pressure is -0.09
~ -0.05MPa, ganoderma lucidum runic thing is concentrated in vacuo into, adds water, ganoderma lucidum runic thing is stirred into suspension, and adjust the ratio of suspension
Weigh to 1.05 ~ 1.30, saturation is adsorbed to using macroporous adsorbing resin for purification, goes to pole with the washing more than 2 times of amount of resin for the first time
Property impurity, target substance is eluted with 1 ~ 3 times of amount of resin/h flow velocity with 30 ~ 60% ethanol solution of 4 ~ 8 times of amount of resin again,
Filtrate is under the conditions of -0.09 ~ -0.05MPa, 50 ~ 65 DEG C, through solvent is recovered under reduced pressure, is concentrated in vacuo after resin isolates and purifies
Ganodenna Lucidum P.E.
Further, the preparation method of the Flos Chrysanthemi Indici extract comprises the following steps：
Chrysanthemum indicum is added into ethanol water solvent, seepage pressure effects 8h, extraction solution is concentrated into no alcohol taste after terminating, then will concentration
Liquid pH value is adjusted to 10, is stood, is taken supernatant acid for adjusting pH filtering precipitation, to take macroreticular resin on supernatant to 7 ~ 8, first use
Water elution, the then ethanol water and 50% ~ 80% ethanol water elution with 10% ~ 30%, collect 50% ~ 80% cut, with
Concentrate, dry afterwards, obtain Flos Chrysanthemi Indici extract.
Further, the preparation method of the Cortex Dictamni extract comprises the following steps：
Using multi-function extractor, the volume ratio of plant root bark of shaggy-fruited dittany complete stool powder and organic solvent ethanol is 1: 4 ~ 6, repeatedly diacolation
Extraction 4 ~ 8 times, or 12 ~ 16h of continuous circumfluence extraction, is filtered, and is dried, is obtained root bark of shaggy-fruited dittany whole strain extract, using methanol by the root bark of shaggy-fruited dittany
After whole strain extract dissolving, it is placed in closed extractor, is used with chloroform solvent with the ratio of volume ratio 10: 12 and methanol
Liquid-liquid distribution method extracts, final to collect chloroform extraction phase and depressurize dense with solvent polarity from small to large for the extraction order of solvent
It is reduced to the root bark of shaggy-fruited dittany complete stool extract that relative density is 0.78 ~ 1g/cm3 ointment shapes.
Further, the preparation method of the orange peel Normal juice comprises the following steps：Take orange peel to clean, add 3 ~ 5 times of amounts
Water, with pulverizer crush be thin pulp extract, stir 2 ~ 3h after be filtered by vacuum, obtain orange peel Normal juice, then pass through vacuum decompression
Concentration tank is concentrated into paste, evaporating pressure 20Mpa.
A kind of preparation method of gleditsia sinensis ganoderma lucidum laundry soap comprises the following steps：
(1) by Fructus Gleditsiae Abnormalis extract, Ganodenna Lucidum P.E, Flos Chrysanthemi Indici extract, Cortex Dictamni extract, glycerine, sucrose ester, ethanol, orange
Skin Normal juice, coconut oil, water are added in blending bin and are well mixed, and are adjusted pH value to 6.0 ~ 6.5 using Glycolic acid, are obtained mixture
Material；
(2) mixed material is introduced after three Kun machines are ground twice and enters the extruding of spiral shaping pump, then obtained with screen cloth sieving
Obtain soap bar；
(3) soap bar is sent into vacuum transport belt, vacuum pressure 0.52Mpa, positional dissection is carried out with rotary chain cutter；
(4) preferable shape is struck out, produces gleditsia sinensis ganoderma lucidum laundry soap.
The beneficial effects of the present invention are：
(1) laundry soap prepared by the present invention is natural and organic ingredients, and ability of cleaning greasy dirt is strong, and the hydrolysate after cleaning easily drops
Solution, it is environmentally friendly；
(2) properties of product of the present invention are gently minimum to skin irritation, clean when being suitable for having a bath, wash one's face and removing ornaments and formal dress
Skin；
(3) it is smooth rich in light delicate fragrance, feel, people can be allowed to releive after use, loosen mood, chrysanthemum indicum is added and the root bark of shaggy-fruited dittany carries
Thing is taken, the sterilization for strengthening laundry soap removes tinea effect, persistently antibacterial；
(4) product of the present invention is rich in the lipid that skin needs, and lubrication moistening effect is good, skin is moistened gloss；It is very suitable for
Dry and winter use, and have certain skin makeup effect；
(5) traditional soap base is substituted using glycerine, sucrose ester, ethanol, coconut oil, the alkalescence for avoiding soap base causes to do to skin
Dry, sensitive and stimulation, while add the long-term use of effect that there is the tender skin of skin care, improve cutaneous immunisation of Ganodenna Lucidum P.E；
(6) raw material proportioning in the present invention is inseparable with technique, mutually collaboration, is an indispensable integrated artistic, only
Have under inventive formulation and process conditions, grease and moisture between each raw material could be balanced well, draw long-term storage or
Not dry and cracked, the not stratified gleditsia sinensis ganoderma lucidum laundry soap after water soaks.
Obviously, according to the above of the present invention, according to the ordinary technical knowledge and means of this area, this hair is not being departed from
Under the premise of bright above-mentioned basic fundamental thought, the modification, replacement or change of other diversified forms can also be made.
Embodiment
We will the invention will be further elaborated with reference to embodiment below.
Embodiment 1
(1) Fructus Gleditsiae Abnormalis extract comprises the following steps：Gleditsia sinensis is dissolved in the water of 10 ~ 30 times of gleditsia sinensis dry weights, carried at 60 ~ 80 DEG C
Take 2 ~ 4 times, 2 ~ 3h, after merging extract solution, filtering, decompression extraction, pressure is carried out under the conditions of filtrate is placed in into 60 ~ 70 DEG C every time
For -0.05 ~ 0.095MPa, recycling design, 65 parts of Fructus Gleditsiae Abnormalis extract is concentrated in vacuo into.
(2) Ganodenna Lucidum P.E comprises the following steps：Ganoderma lucidum is dissolved in 40% ~ 60% ethanol of 10 ~ 20 times of ganoderma lucidum dry weights
In solution, extracted at 60 ~ 70 DEG C 1 ~ 3 time, 1.5 ~ 2.5h, merges extract solution, filtering, filtrate is placed in into 50 ~ 60 DEG C of bars every time
Carry out that solvent is recovered under reduced pressure under part, pressure is -0.09 ~ -0.05MPa, is concentrated in vacuo into ganoderma lucidum runic thing, adds water, and ganoderma lucidum is thick
Body thing stirs into suspension, and the proportion for adjusting suspension reaches 1.05 ~ 1.30, is adsorbed to using macroporous adsorbing resin for purification full
With, for the first time with the washing depolarization impurity more than 2 times of amount of resin, again with 30 ~ 60% ethanol solution of 4 ~ 8 times of amount of resin with
1 ~ 3 times of amount of resin/h flow velocity elution target substance, filtrate is under the conditions of -0.09 ~ -0.05MPa, 50 ~ 65 DEG C, through being recovered under reduced pressure
Solvent, vacuum concentration resin obtain 8 parts of Ganodenna Lucidum P.E after isolating and purifying.
(3) chrysanthemum indicum takes thing to comprise the following steps：Chrysanthemum indicum is added into ethanol water solvent, seepage pressure effects 8h, after terminating
Extraction solution is concentrated into no alcohol taste, then concentrate pH value is adjusted to 10, stood, takes supernatant acid for adjusting pH to 7 ~ 8,
Filtering precipitation, take macroreticular resin on supernatant, be first eluted with water, then with 10% ~ 30% ethanol water and 50% ~ 80% second
Alcohol water elution, 50% ~ 80% cut is collected, then concentrate, dry, obtain 25 parts of Flos Chrysanthemi Indici extract.
(4) Cortex Dictamni extract comprises the following steps：Using multi-function extractor, plant root bark of shaggy-fruited dittany complete stool powder is with having
The volume ratio of solvent ethanol is 1: 4 ~ 6, seepage pressure effects 4 ~ 8 times repeatedly, or 12 ~ 16h of continuous circumfluence extraction, is filtered, and dries, obtains
Root bark of shaggy-fruited dittany whole strain extract, after using methanol, root bark of shaggy-fruited dittany whole strain extract is dissolved, it is placed in closed extractor, it is molten with chloroform
Matchmaker is extracted with the ratio of volume ratio 10: 12 and methanol using liquid-liquid distribution method, with solvent polarity from small to large for the extraction of solvent
Sequentially, finally collect chloroform extraction phase and be concentrated under reduced pressure into the root bark of shaggy-fruited dittany complete stool that relative density is 0.78 ~ 1g/cm3 ointment shapes and extract
Take 15 parts of thing.
(5) orange peel Normal juice is made by following preparation method：Take orange peel to clean, add the water of 3 ~ 5 times of amounts, with pulverizer powder
Broken is thin pulp extract, is filtered by vacuum after stirring 2 ~ 3h, obtains 5 parts of orange peel Normal juice, be then concentrated into by vacuum decompressioning and concentrating tank
Paste, evaporating pressure 20Mpa.
(6) 8 parts of Fructus Gleditsiae Abnormalis extract, 4 parts of Ganodenna Lucidum P.E, 8 parts of Flos Chrysanthemi Indici extract, 6 parts of Cortex Dictamni extract, glycerine are taken
15 parts, 15 parts of sucrose ester, 5 parts of ethanol, 5 parts of orange peel Normal juice, 5 parts of coconut oil, 25 parts of water, which is added in blending bin, to be well mixed, and is used
Glycolic acid adjusts pH value to 6.3, obtains mixed material；
(7) mixed material is introduced after three Kun machines are ground twice and enters the extruding of spiral shaping pump, then obtained with screen cloth sieving
Obtain soap bar；
(8) soap bar is sent into vacuum transport belt, positional dissection, the vacuum pressure of vacuum transport belt is carried out with rotary chain cutter
Strong is 0.52Mpa；
(9) preferable shape is struck out, produces gleditsia sinensis ganoderma lucidum laundry soap.
Embodiment 2
Gleditsia sinensis ganoderma lucidum laundry soap：
Preparation method is made up with embodiment 1, the simply laundry soap of the raw material of following parts by weight：7 parts of Fructus Gleditsiae Abnormalis extract, ganoderma lucidum carries
Take 3 parts of thing, 7 parts of Flos Chrysanthemi Indici extract, 5 parts of Cortex Dictamni extract, 10 parts of glycerine, 10 parts of sucrose ester, 4 parts of ethanol, orange peel Normal juice 4
Part, 4 parts of coconut oil, 25 parts of water, Glycolic acid adjusts pH value to 6.0.
Embodiment 3
Gleditsia sinensis ganoderma lucidum laundry soap：
Preparation method is made up with embodiment 1, the simply laundry soap of the raw material of following parts by weight：9 parts of Fructus Gleditsiae Abnormalis extract, ganoderma lucidum carries
Take 5 parts of thing, 9 parts of Flos Chrysanthemi Indici extract, 7 parts of Cortex Dictamni extract, 20 parts of glycerine, 20 parts of sucrose ester, 6 parts of ethanol, orange peel Normal juice 6
Part, 6 parts of coconut oil, 25 parts of water, Glycolic acid adjusts pH value to 6.5.
Test example 1
1. test material：
Gleditsia sinensis ganoderma lucidum laundry soap：Gleditsia sinensis ganoderma lucidum laundry soap prepared by embodiment 1（Contain Fructus Gleditsiae Abnormalis extract in every piece of laundry soap
8.3%th, Ganodenna Lucidum P.E 4.2%, Flos Chrysanthemi Indici extract 8.3%, Cortex Dictamni extract 6.3%）, abbreviation compound soap 1.
Gleditsia sinensis ganoderma lucidum laundry soap：（Compared to embodiment 1, glycerine, sucrose ester, ethanol, coconut oil are replaced with into soap base, every piece
Contain Fructus Gleditsiae Abnormalis extract 8.3%, Ganodenna Lucidum P.E 4.2%, Flos Chrysanthemi Indici extract 8.3%, Cortex Dictamni extract 6.3% in laundry soap）,
Abbreviation compound soap 2.
Single Fructus Gleditsiae Abnormalis extract laundry soap：With reference to the preparation method of embodiment 1, contain Fructus Gleditsiae Abnormalis extract in every piece of laundry soap
27.1%, abbreviation gleditsia sinensis soap.
Single Ganodenna Lucidum P.E laundry soap：With reference to the preparation method of embodiment 1, contain Ganodenna Lucidum P.E in every piece of laundry soap
27.1%, abbreviation ganoderma lucidum soap.
Single Flos Chrysanthemi Indici extract laundry soap：With reference to the preparation method of embodiment 1, extracted in every piece of laundry soap containing chrysanthemum indicum
Thing 27.1%, abbreviation chrysanthemum indicum soap.
Single Cortex Dictamni extract laundry soap：With reference to the preparation method of embodiment 1, extracted in every piece of laundry soap containing the root bark of shaggy-fruited dittany
Thing 27.1%, abbreviation root bark of shaggy-fruited dittany soap.
2. fungistatic effect is tested
Various laundry soaps carry out fungistatic effect test in Example 1 and test example 1, and product fungistatic effect of the present invention, which is examined, to be performed
The evaluation method QB/T 2738-2012 of People's Republic of China's light industry professional standard --- daily chemical products antibacterial bacteriostatic effect
（It is antibacterial around-France）, selected strain is：Staphylococcus aureus, Escherichia coli, Candida albicans, Pseudomonas aeruginosa, wherein table
1st, "-" represents inhibition zone diameter ＜ 7mm in table 2, and test specimen comprises the following steps that without bacteriostasis：
(1) preparation of bacteria inhibition tablet：0.5g laundry soap sample Sterile standard hard water is dissolved and is diluted to normal concentration（1:
100）, sterile dry filter paper piece is taken, the every dropwise addition μ l of test sample solution 20, then filter paper is lain against to sterile plane ware
It is interior, uncap to put in 37 DEG C of insulating box and dry, it is standby；
(2) preparation of control sample：Sterile dry filter paper piece is taken, every is added dropwise the μ l of sterile distilled water 20, standby after drying；
(3) inoculation of test organisms：Concentration is dipped as 5 × 10 with sterile cotton swab4Cfu/ml tests bacteria suspension, is trained in nutrient agar
Support base planar surface uniformly to smear three times, often smear a flat board and rotate 60 °, finally covered flat around flat board one week with cotton swab
Ware, put drying at room temperature 5 minutes；
(4) bacteriostatic test print is placed with：Experiment is placed with a microbiological contamination flat board every time, and each flat board is placed with six experiment prints, and one
Piece compares print, is placed with aseptic nipper coupongs in planar surface, at a distance of more than 25mm between each print center, with flat board week
Edge is placed with afterwards with the light pressure-like piece of aseptic nipper at a distance of more than 15mm, it is close to planar surface, cover plate, be placed in 37 DEG C
Result is observed after insulating box culture 16h, with the diameter of vernier caliper measurement antibacterial ring size（Including paster）And record, experiment repeats three
Secondary, final result is averaged.Embodiment physical and chemical index inspection result with it is antibacterial the results detailed in Table 1 and table 2.
The physical and chemical index testing result of 1 embodiment of table 1
。
The bacteriostatic test result of the embodiment 1 of table 2 and test example
。
As shown in Table 2, the antibacterial ring size of compound soap 1 is maximum, illustrates that the fungistatic effect of compound soap 1 is optimal, and right in control group
No biocidal property is indicated when staphylococcus aureus, Candida albicans and E.coli LT .LT.LT 7mm, compound soap 1 is to golden yellow grape
Coccus, Candida albicans and Escherichia coli have an obvious fungistatic effect, and gleditsia sinensis soap, ganoderma lucidum soap, chrysanthemum indicum soap, root bark of shaggy-fruited dittany soap
Control group standard is not up to, and the substantially less than fungistatic effect of compound soap 1, the bacteriostasis of compound soap 2 are significantly higher than gleditsia sinensis
Soap, ganoderma lucidum soap, chrysanthemum soap, root bark of shaggy-fruited dittany soap, slightly worse than compound soap 1, thus illustrate there was only ability under four kinds of extract collective effects
The bacteriostasis of collaboration is played, and fungistatic effect is better than each single extract group, illustrates the present invention by four kinds of different extracts
Mutual compatibility, played synergistic function, obtained more preferably bacteriostasis efficacy.
3. skin effect is tested
The laundry soap of Example 1 carries out skin effect test, subject totally 4 people, the people of women 2, the people of male 2, age 15-25
In year, adhere to using product of the present invention daily, continue two months observation faces and hand skin change, refer to table 3.
The skin care result of table 3 compares
。
As shown in Table 3,4 have the subject of skin problem after using this laundry soap 15 days, and skin of face has inclination
Turn, and improvement rate more than 50% and more than, hand skin compare use before it is substantially moist, soft and smooth, glossy, illustrate embodiment institute
The laundry soap obtained can not only wash to clothing, and the cleaning for skin of face also has safe and reliable effect.
4. laundry soap state stability is evaluated
Various laundry soaps carry out state stability test in Example 1 and test example 1, by gained in embodiment 1 and test example 1
Product, which is placed in clear water, is placed in heat drying in baking box after 20 ~ 30min of immersion, 20 ~ 30 DEG C of drying temperature, and drying time 6 ~
8h, the soap face sense organ of four groups of laundry soaps is evaluated after terminating, the results detailed in Table 4.
The state stability of the embodiment of table 4 and test example is evaluated
。
By table 4, compound soap 1, gleditsia sinensis soap, ganoderma lucidum soap, chrysanthemum indicum soap, laundry soap made from root bark of shaggy-fruited dittany soap are in baking box
After 6 ~ 8h of middle progress drying, laundry soap still can keep soap shape to rectify, uniform color, and no layering is with dry and cracked, and that touches is smooth, firmly
Spend moderate, no smell.And dry and cracked, layering occurs in the soap body of compound soap 2, gross distortion, color and luster inequality color and luster is uneven, and sense of touch is owed
It is smooth, have granular sensation, dry partially, it is tactile drying, rough, difficult to handle, and slightly smell；Compared to compound soap 1, soap is being used
After base substituted glycerol, sucrose ester, ethanol, coconut oil, state stability of the laundry soap under moist, dry alternate environment gradually becomes
Difference, and shelf life also substantially shortens, and is layered after immersion, thus illustrates, only in glycerine, sucrose ester, ethanol, coconut oil connection
Under cooperation is used, the character of laundry soap could be improved, the laundry soap ability soap shape produced is rectified, and uniform color, no layering is with doing
Split, that touches is smooth, and hardness is moderate, no smell.
In summary, the raw material proportioning in the present invention is inseparable with technique, mutually collaboration, is indispensable one whole
Body technology, only under inventive formulation and process conditions, grease and moisture between each raw material could be balanced well, draws length
Phase deposits or not dry and cracked, not stratified gleditsia sinensis ganoderma lucidum laundry soap after water soaks.
Claims (8)
- A kind of 1. gleditsia sinensis ganoderma lucidum laundry soap, it is characterised in that：The laundry soap is made up of the raw material of following weight：7 ~ 9 parts of Fructus Gleditsiae Abnormalis extract, 3 ~ 5 parts of Ganodenna Lucidum P.E, 7 ~ 9 parts of Flos Chrysanthemi Indici extract, 5 ~ 7 parts of Cortex Dictamni extract, glycerine 10 ~ 20 parts, 10 ~ 20 parts of sucrose ester, 4 ~ 6 parts of ethanol, 4 ~ 6 parts of orange peel Normal juice, 4 ~ 6 parts of coconut oil, 25 parts of water, appropriate Glycolic acid.
- 2. gleditsia sinensis ganoderma lucidum laundry soap according to claim 1, it is characterised in that：The laundry soap is by following weight Raw material is made：8 parts of Fructus Gleditsiae Abnormalis extract, 4 parts of Ganodenna Lucidum P.E, 8 parts of Flos Chrysanthemi Indici extract, 6 parts of Cortex Dictamni extract, 15 parts of glycerine, sucrose 15 parts of ester, 5 parts of ethanol, 5 parts of orange peel Normal juice, 5 parts of coconut oil, 25 parts of water, appropriate Glycolic acid.
- 3. gleditsia sinensis ganoderma lucidum laundry soap according to claim 1 or 2, it is characterised in that：The preparation side of the Fructus Gleditsiae Abnormalis extract Method comprises the following steps：Gleditsia sinensis is dissolved in the water of 10 ~ 30 times of gleditsia sinensis dry weights, extracted at 60 ~ 80 DEG C 2 ~ 4 times, 2 ~ 3h, merges extract solution every time Afterwards, filter, carry out decompression extraction under the conditions of filtrate is placed in into 60 ~ 70 DEG C, pressure is -0.05 ~ 0.095MPa, recycling design, very Sky is condensed into Fructus Gleditsiae Abnormalis extract.
- 4. gleditsia sinensis ganoderma lucidum laundry soap according to claim 1 or 2, it is characterised in that：The preparation side of the Ganodenna Lucidum P.E Method comprises the following steps：Ganoderma lucidum is dissolved in 40% ~ 60% ethanol solution of 10 ~ 20 times of ganoderma lucidum dry weights, extracts 1 ~ 3 time at 60 ~ 70 DEG C, every time 1.5 ~ 2.5h, merge extract solution, filtering, carry out that solvent is recovered under reduced pressure under the conditions of filtrate is placed in into 50 ~ 60 DEG C, pressure is -0.09 ~ -0.05MPa, ganoderma lucidum runic thing is concentrated in vacuo into, adds water, ganoderma lucidum runic thing is stirred into suspension, and adjust the ratio of suspension Weigh to 1.05 ~ 1.30, saturation is adsorbed to using macroporous adsorbing resin for purification, goes to pole with the washing more than 2 times of amount of resin for the first time Property impurity, target substance is eluted with 1 ~ 3 times of amount of resin/h flow velocity with 30 ~ 60% ethanol solution of 4 ~ 8 times of amount of resin again, Filtrate is under the conditions of -0.09 ~ -0.05MPa, 50 ~ 65 DEG C, through solvent is recovered under reduced pressure, is concentrated in vacuo after resin isolates and purifies Ganodenna Lucidum P.E.
- 5. gleditsia sinensis ganoderma lucidum laundry soap according to claim 1 or 2, it is characterised in that：The preparation of the Flos Chrysanthemi Indici extract Method comprises the following steps：Chrysanthemum indicum is added into ethanol water solvent, seepage pressure effects 8h, extraction solution is concentrated into no alcohol taste after terminating, then will concentration Liquid pH value is adjusted to 10, is stood, is taken supernatant acid for adjusting pH filtering precipitation, to take macroreticular resin on supernatant to 7 ~ 8, first use Water elution, the then ethanol water and 50% ~ 80% ethanol water elution with 10% ~ 30%, collect 50% ~ 80% cut, with Concentrate, dry afterwards, obtain Flos Chrysanthemi Indici extract.
- 6. gleditsia sinensis ganoderma lucidum laundry soap according to claim 1 or 2, it is characterised in that：The preparation of the Cortex Dictamni extract Method comprises the following steps：Using multi-function extractor, the volume ratio of plant root bark of shaggy-fruited dittany complete stool powder and organic solvent ethanol is 1: 4 ~ 6, repeatedly diacolation Extraction 4 ~ 8 times, or 12 ~ 16h of continuous circumfluence extraction, is filtered, and is dried, is obtained root bark of shaggy-fruited dittany whole strain extract, using methanol by the root bark of shaggy-fruited dittany After whole strain extract dissolving, it is placed in closed extractor, is used with chloroform solvent with the ratio of volume ratio 10: 12 and methanol Liquid-liquid distribution method extracts, final to collect chloroform extraction phase and depressurize dense with solvent polarity from small to large for the extraction order of solvent It is reduced to the root bark of shaggy-fruited dittany complete stool extract that relative density is 0.78 ~ 1g/cm3 ointment shapes.
- 7. gleditsia sinensis ganoderma lucidum laundry soap according to claim 1 or 2, it is characterised in that：The preparation method of the orange peel Normal juice Comprise the following steps：Take orange peel to clean, add the water of 3 ~ 5 times of amounts, it is thin pulp extract to be crushed with pulverizer, after stirring 2 ~ 3h Vacuum filtration, obtains orange peel Normal juice, is then concentrated into paste, evaporating pressure 20Mpa by vacuum decompressioning and concentrating tank.
- A kind of 8. preparation method according to any described gleditsia sinensis ganoderma lucidum laundry soap of claim 1 ~ 7, it is characterised in that：This method Comprise the following steps：(1) by Fructus Gleditsiae Abnormalis extract, Ganodenna Lucidum P.E, Flos Chrysanthemi Indici extract, Cortex Dictamni extract, glycerine, sucrose ester, ethanol, orange Skin Normal juice, coconut oil, water are added in blending bin and are well mixed, and are adjusted pH value to 6.0 ~ 6.5 using Glycolic acid, are obtained mixture Material；(2) mixed material is introduced after three Kun machines are ground twice and enters the extruding of spiral shaping pump, then obtained with screen cloth sieving Obtain soap bar；(3) soap bar is sent into vacuum transport belt, vacuum pressure 0.52Mpa, positional dissection is carried out with rotary chain cutter；(4) preferable shape is struck out, produces gleditsia sinensis ganoderma lucidum laundry soap.
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| CN111944621A (en) * | 2019-05-17 | 2020-11-17 | 叶顺建 | Mite-removing handmade soap, preparation method and application thereof |
| CN114540820A (en) * | 2022-02-15 | 2022-05-27 | 珠海谦信新材料有限公司 | Natural plant extract modified compound corrosion inhibitor, and preparation method and application thereof |
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| CN1958060A (en) * | 2006-11-10 | 2007-05-09 | 尹思源 | Washing soap with effects of antiinflammation and bacteriostasis |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111944621A (en) * | 2019-05-17 | 2020-11-17 | 叶顺建 | Mite-removing handmade soap, preparation method and application thereof |
| CN114540820A (en) * | 2022-02-15 | 2022-05-27 | 珠海谦信新材料有限公司 | Natural plant extract modified compound corrosion inhibitor, and preparation method and application thereof |
| CN114540820B (en) * | 2022-02-15 | 2023-09-29 | 珠海谦信新材料有限公司 | Natural plant extract modified compound corrosion inhibitor, and preparation method and application thereof |
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