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CN107511317A - Piezoelectric ultrasonic transducer and preparation method thereof - Google Patents

Piezoelectric ultrasonic transducer and preparation method thereof Download PDF

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Publication number
CN107511317A
CN107511317A CN201710643625.3A CN201710643625A CN107511317A CN 107511317 A CN107511317 A CN 107511317A CN 201710643625 A CN201710643625 A CN 201710643625A CN 107511317 A CN107511317 A CN 107511317A
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CN
China
Prior art keywords
vibrating diaphragm
piezoelectric
ultrasonic transducer
substrate
electrode
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Granted
Application number
CN201710643625.3A
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Chinese (zh)
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CN107511317B (en
Inventor
朱雁青
兰晓东
童贝
李杨
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AAC Technologies Pte Ltd
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AAC Technologies Pte Ltd
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Priority to CN201710643625.3A priority Critical patent/CN107511317B/en
Publication of CN107511317A publication Critical patent/CN107511317A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B06GENERATING OR TRANSMITTING MECHANICAL VIBRATIONS IN GENERAL
    • B06BMETHODS OR APPARATUS FOR GENERATING OR TRANSMITTING MECHANICAL VIBRATIONS OF INFRASONIC, SONIC, OR ULTRASONIC FREQUENCY, e.g. FOR PERFORMING MECHANICAL WORK IN GENERAL
    • B06B1/00Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency
    • B06B1/02Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency making use of electrical energy
    • B06B1/06Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency making use of electrical energy operating with piezoelectric effect or with electrostriction
    • B06B1/0607Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency making use of electrical energy operating with piezoelectric effect or with electrostriction using multiple elements

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Transducers For Ultrasonic Waves (AREA)

Abstract

The present invention provides a kind of piezoelectric ultrasonic transducer and preparation method thereof, piezoelectric ultrasonic transducer includes vibrating diaphragm and the piezoelectric film on vibrating diaphragm that is sticked, and fringe region of the vibrating diaphragm close to substrate direction, which is provided with, can produce the electric resistance structure that Joule heat rises vibrating diaphragm local temperature under "on" position.Due to the material that vibrating diaphragm is risen using Young's modulus such as silica with temperature and is reduced, heating can cause the integral, flexible coefficient of vibrating diaphragm to reduce, and the electromechanical coupling factor increase of transducer, acoustic pressure output changes;On the other hand, resonant frequency during diaphragm oscillations reduces with the reduction of coefficient of elasticity, realizes the dynamic adjustment of ultrasonic output frequency.

Description

Piezoelectric ultrasonic transducer and preparation method thereof
Technical field
The present invention relates to sonac field, more particularly to a kind of piezoelectric ultrasonic transducer and preparation method thereof.
Background technology
Sonac is had a wide range of applications in social production life, including Ultrasonic machining, localization by ultrasonic, ultrasound are visited The each side such as survey, ultrasonic imaging.The device mutually changed as electric energy and mechanical energy, ultrasonic transducer are the weights of sonac Want building block.Traditional ultrasonic transducer is typically based on machining and is made, thus with volume it is larger, machining accuracy compared with Low, processing cost is higher, it is difficult to the shortcomings of forming array structure.Based on MEMS (Microelectromechanical Systems, MEMS) technology ultrasonic transducer because being process using microelectronic technique, diameter dimension can be reduced to Micron level, resonant frequency can reach hundreds of megahertzs, the precision that higher resonant frequency is added significantly to be imaged and detected.Separately Outside, the ultrasonic transducer unit being processed into by MEMS technology can form large scale array, and unit uniformity is preferable, be easy to use phase Position control technology realizes the functions such as the focusing of ultrasonic beam, discrete, direct scan, greatly strengthen the flexible of ultrasonic technique application Property.
Current MEMS ultrasonic transducers mainly have two kinds of condenser type and piezoelectric type, wherein MEMS capacitive ultrasonic transducer It is made up of upper and lower two battery lead plates, by the static-electronic driving between battery lead plate, has that electromechanical coupling factor is larger, resonant frequency The advantages of higher, but there is also driving voltage it is higher, be difficult to by effect of parasitic capacitance is larger, electricity output impedance is larger Match somebody with somebody, the shortcomings of receiving efficiency and emission effciency are difficult to take into account;Compared with capacitive ultrasound transducer, piezoelectric type ultrasonic transducer by Piezoelectric layer, vibration level and upper and lower metal electrode are formed, and have driving voltage is low, output impedance is low, launches receiving efficiency to take into account Advantage, therefore applied in many occasions.But after the physical dimension of MEMS piezoelectric type ultrasonic transducers is fixed, transducer Output performance such as resonant frequency, output acoustic pressure etc. also fixed, and on the other hand, because the output of different resonant frequencies surpasses Penetration depth of the sound wave in air or liquid is inconsistent, and in different applications, transducer, which needs to provide, different penetrates depth Degree and output acoustic pressure, therefore the adjustable MEMS piezoelectric ultrasonic transducers of realisation dynamic are technologies in the urgent need to address at present Problem, have great importance to realizing the optimization of sensor performance and reducing testing cost.
Therefore, it is necessary that providing a kind of new piezoelectric ultrasonic transducer solves the above problems in fact.
The content of the invention
The present invention provides a kind of piezoelectric ultrasonic transducer to realize the optimization in different application occasion lower sensor performance.
In order to solve the above technical problems, the invention provides a kind of piezoelectric ultrasonic transducer, including center to be provided with cavity Substrate, fixed vibrating diaphragm on the substrate, the piezoelectric film being connected with the vibrating diaphragm, the piezoelectric film include the close vibrating diaphragm First surface and away from the vibrating diaphragm second surface, the piezoelectric ultrasonic transducer also include be arranged at the first surface First electrode and be arranged at the second electrode of the second surface, the vibrating diaphragm is provided with energization close to the fringe region of substrate The electric resistance structure that Joule heat rises the local temperature of the vibrating diaphragm can be produced under state.
Preferably, the electric resistance structure is arranged at vibrating diaphragm close to the surface of piezoelectric film.
Preferably, the size of the piezoelectric film is less than the size of vibrating diaphragm, and the piezoelectric film is arranged in the vibrating diaphragm Heart position.
Preferably, the electric resistance structure is set around the piezoelectric film.
Preferably, the electric resistance structure is foldable structure, linear structure or block structure.
Preferably, the substrate is prepared using any one in silicon, sapphire, ceramics, glass or polymer.
Preferably, the vibrating diaphragm use silica, polysilicon, silicon nitride or polymer in any one prepare and Into.
Preferably, the piezoelectric film is prepared using any one in aluminium nitride, zinc oxide or lead zirconate titanate.
The first electrode, second electrode use any one conductive material in molybdenum, platinum or aluminium to be prepared.
To solve the above problems, the present invention also provides a kind of preparation method of piezoelectric supersonic converter as described above, its Comprise the following steps:
Substrate is prepared, and vibrating diaphragm is deposited in substrate;
First electrode is prepared in the center of a side surface of the vibrating diaphragm away from substrate, and resistance junction is prepared at the edge of vibrating diaphragm Structure;
Piezoelectric film is prepared on surface of the first electrode away from vibrating diaphragm;
Second electrode is prepared on piezoelectric film surface;
Etched in substrate to form cavity.
Compared to prior art, piezoelectric ultrasonic transducer of the invention includes vibrating diaphragm and the piezoelectric film being arranged on vibrating diaphragm, Vibrating diaphragm is provided with close to the fringe region of substrate can produce the resistance that Joule heat rises vibrating diaphragm local temperature under "on" position Structure.Due to the material that vibrating diaphragm is risen using Young's modulus such as silica with temperature and is reduced, heating can cause the whole of vibrating diaphragm Body elasticity coefficient is reduced, and the electromechanical coupling factor increase of transducer, acoustic pressure output is changed;On the other hand, diaphragm oscillations When resonant frequency reduce with the reduction of coefficient of elasticity, realize ultrasonic output frequency dynamic adjustment.
Brief description of the drawings
Fig. 1 is the structural representation of piezoelectric ultrasonic transducer of the present invention;
Fig. 2 is the overlooking the structure diagram of piezoelectric ultrasonic transducer of the present invention;
Fig. 3 is the flow chart of piezoelectric ultrasonic transducer preparation method of the present invention.
Embodiment
Below in conjunction with drawings and embodiments, the invention will be further described.
As shown in figure 1, the piezoelectric ultrasonic transducer of present embodiment, including substrate 1, fixed vibrating diaphragm 2 on the base 1 with And the piezoelectric film 4 on vibrating diaphragm 2 that is sticked.Substrate 1 is provided centrally with cavity 10, and vibrating diaphragm 2 is fixed on the base 1 and covers cavity 10。
Vibrating diaphragm is provided with the electric resistance structure 3 that Joule heat can be produced under "on" position close to the fringe region of substrate 1.Resistance Structure 3 can cause the local temperature of vibrating diaphragm 2 to rise, so as to change the coefficient of elasticity of vibrating diaphragm.
Piezoelectric film 4 includes the first surface 41 close to vibrating diaphragm 2 and the second surface 42 away from vibrating diaphragm 2.Electrode is to be sticked Battery lead plate on piezoelectric film 4, specifically, including the first electrode 5 that is sticked on the first surface 41 of piezoelectric film 4 and being arranged on the Second electrode 6 on two surfaces 42.
Projected area of the piezoelectric film 4 on vibrating diaphragm 2 is less than vibrating diaphragm 2.Piezoelectric film 4 is arranged on the middle position of vibrating diaphragm 2.The One electrode 5, second electrode 6 are consistent with the profile of piezoelectric film 4.
As shown in Fig. 2 electric resistance structure 3 is arranged on vibrating diaphragm 2 on the first surface 41 of the side of piezoelectric film 4, and piezoelectricity The size less than vibrating diaphragm of film 4, it is preferred that piezoelectric film 4 is arranged at the center of vibrating diaphragm 2.Electric resistance structure 3 is arranged on vibrating diaphragm and leaned on The fringe region of nearly substrate 1, specifically, to be arranged on the fringe region that vibrating diaphragm 2 deviates from the side surface of substrate 1 one.The ring of electric resistance structure 3 Set around piezoelectric film 4, be spaced specially around first electrode 5 and with first electrode 5 and insulation set.Electric resistance structure 3 is metal Resistance, can produce Joule heat in the energized state rises the local temperature of vibrating diaphragm 2.Electric resistance structure 3 can be foldable structure or The resistance wire or resistor disc of linear structure or block structure, as long as play under "on" position so that local temperature is raised to change The integral, flexible coefficient of vibrating diaphragm, it is to implement to adapt to the demand under different occasions.
The material for preparing of substrate 1 can be using silicon, sapphire, ceramics, glass or polymer etc., it is preferred that in this implementation It is silicon base in mode;Vibrating diaphragm 2 prepares material and can use silica, polysilicon, silicon nitride or polymer etc., specifically In the present embodiment, it is silica;Piezoelectric film 4 prepare material can use AlN (aluminium nitride), ZnO (zinc oxide) or PZT (piezoelectric ceramic transducer, lead titanate piezoelectric ceramics);The material for preparing of electrode uses Mo (molybdenum), Pt (platinum) or Al (aluminium), wherein first electrode 5 and second electrode 6 can use identical material to prepare, and can also use It is prepared by different materials.
Due to vibrating diaphragm 2 using a kind of Young's modulus of silica, polysilicon, silicon nitride or polymer with temperature The material for rising and reducing, therefore the heating of electric resistance structure 3 can cause the integral, flexible coefficient of vibrating diaphragm to reduce, the mechanical-electric coupling of transducer Coefficient increases, and acoustic pressure output is changed;On the other hand, resonant frequency during diaphragm oscillations subtracts with the reduction of coefficient of elasticity It is small, realize the dynamic adjustment of ultrasonic output frequency.So, under specific occasion, piezoelectric ultrasonic transducer can be by right Electric resistance structure carries out heating power and changes the performance of product, to adapt to the demand of corresponding occasion.
As shown in figure 3, for the preparation method of piezoelectric ultrasonic transducer of the present invention, specifically comprise the following steps:
A., substrate 1 prepared by silicon materials is provided, and deposition prepares vibrating diaphragm 2 on the base 1, the vibrating diaphragm uses titanium dioxide Any one in silicon, polysilicon, silicon nitride or polymer is prepared, and specific method is:First respectively with acidic cleaning solution and Alkaline cleaning fluid cleans substrate 1, is afterwards again rinsed well substrate 1 with deionized water;Followed by low-pressure chemical vapor deposition Equipment is in the surface deposit thickness of substrate 1Vibrating diaphragm 2;
B. prepare first electrode 5 on vibrating diaphragm 2 and electric resistance structure 3, specific method are:Utilize vacuum evaporation equipment or sputtering Equipment is prepared on vibrating diaphragm 2The first electrode 5 of thickness, the first electrode 5 can be by molybdenum, platinum or aluminium One of formed, or can be composite bed, the composite bed of titanium and platinum to form chromium and gold;Then resist coating, photolithographic exposure, Form litho pattern;With corrosion corrosion metal film, the first electrode 5 and the structure of resistance 3 of figure needed for formation, residual light is removed Photoresist, complete the preparation of first electrode 5 and electric resistance structure 3;
C. piezoelectric film 4 is prepared on the surface of first electrode 5, specific method is:Using true first on the surface of first electrode 5 It is prepared by empty evaporated device or sputtering equipmentThe piezoelectric material layer of thickness, then resist coating, photolithographic exposure, shape Into litho pattern;With corrosion corrosion piezoelectric material layer, figure needed for formation, residual photoresist is removed, complete the system of piezoelectric film 4 It is standby;
D. second electrode 6 is prepared on the surface of piezoelectric film 4, specific method is:The resist coating on piezoelectric film 4, photoetching expose Light, the anti-graphics of second electrode 6 are formed, i.e., need not form the opening position resist coating of second electrode 6;Vacuum is steamed successively again Plating or magnetron sputtering The second electrode lay of thickness, the selection of its material and the material phase selection of first electrode 5 are same; Photoresist is removed with acetone, completes the preparation of second electrode 6;
E, etch on the base 1 to form cavity 10, specific method is:The front of substrate 1 is tied first by photoresist Structure protects (i.e. close to the structure on the surface of vibrating diaphragm), is formed sediment using low pressure chemical vapor deposition equipment on the back side of substrate 1 Accumulating thickness isSilicon dioxide layer, the resist coating on the back side of substrate 1, photolithographic exposure, need etch release The place in hole forms litho pattern;Silicon dioxide etching liquid is put into after development is dried, corroding needs mask window, removes residual Remaining light photoresist, is then placed in the etching that back side release aperture is carried out in dry method deep silicon etching equipment, and etching depth isComplete the release of diaphragm for transducer 2.Certainly, in this step, silica is formed at the back side of substrate 1 Layer is not necessary, directly substrate 1 can be performed etching to form cavity 10 yet, and it is to pass through titanium dioxide to set silica Silicon preferably controls the depth of etching.
Compared to prior art, piezoelectric ultrasonic transducer of the invention includes vibrating diaphragm and the piezoelectric film being arranged on vibrating diaphragm, Fringe region of the vibrating diaphragm close to substrate direction be provided with can be produced under "on" position Joule heat make vibrating diaphragm local temperature rise Electric resistance structure.Due to the material that vibrating diaphragm is risen using Young's modulus such as silica with temperature and is reduced, heating can cause vibrating diaphragm Integral, flexible coefficient reduce, the electromechanical coupling factor of transducer increase, acoustic pressure output is changed;On the other hand, vibrating diaphragm Resonant frequency during vibration reduces with the reduction of coefficient of elasticity, realizes the dynamic adjustment of ultrasonic output frequency.
Embodiments of the invention are the foregoing is only, are not intended to limit the scope of the invention, it is every to utilize this hair The equivalent structure or equivalent flow conversion that bright specification and accompanying drawing content are made, or directly or indirectly it is used in other related skills Art field, is included within the scope of the present invention.

Claims (10)

1. a kind of piezoelectric ultrasonic transducer, including center be provided with the substrate of cavity, fixed vibrating diaphragm on the substrate, with it is described The connected piezoelectric film of vibrating diaphragm, the piezoelectric film include the first surface close to the vibrating diaphragm and the second table away from the vibrating diaphragm Face, the piezoelectric ultrasonic transducer also include being arranged at the first electrode of the first surface and are arranged at the second surface Second electrode, it is characterised in that the vibrating diaphragm is provided with "on" position close to the fringe region of substrate can produce Joule heat The electric resistance structure for making the local temperature of the vibrating diaphragm increase.
2. piezoelectric ultrasonic transducer according to claim 1, it is characterised in that it is close that the electric resistance structure is arranged at vibrating diaphragm The surface of piezoelectric film.
3. piezoelectric ultrasonic transducer according to claim 2, it is characterised in that the size of the piezoelectric film is less than vibrating diaphragm Size, and the piezoelectric film is arranged at the center of the vibrating diaphragm.
4. piezoelectric ultrasonic transducer according to claim 3, it is characterised in that the electric resistance structure is around the piezoelectric film Set.
5. piezoelectric ultrasonic transducer according to claim 1, it is characterised in that the electric resistance structure is foldable structure, directly Cable architecture or block structure.
6. piezoelectric ultrasonic transducer according to claim 1, it is characterised in that the substrate is using silicon, sapphire, pottery Any one in porcelain, glass or polymer is prepared.
7. piezoelectric ultrasonic transducer according to claim 1, it is characterised in that the vibrating diaphragm is using silica, polycrystalline Any one in silicon, silicon nitride or polymer is prepared.
8. piezoelectric ultrasonic transducer according to claim 1, it is characterised in that the piezoelectric film is using aluminium nitride, oxidation Any one in zinc or lead zirconate titanate is prepared.
9. piezoelectric ultrasonic transducer according to claim 1, it is characterised in that the first electrode, second electrode use Any one conductive material in molybdenum, platinum or aluminium is prepared.
10. a kind of preparation method of piezoelectric supersonic converter as claimed in claim 1, it comprises the following steps:
Substrate is prepared, and vibrating diaphragm is deposited in substrate;
First electrode is prepared in the center of a side surface of the vibrating diaphragm away from substrate, and electric resistance structure is prepared at the edge of vibrating diaphragm;
Piezoelectric film is prepared on surface of the first electrode away from vibrating diaphragm;
Second electrode is prepared on piezoelectric film surface;
Etched in substrate to form cavity.
CN201710643625.3A 2017-07-31 2017-07-31 Piezoelectric ultrasonic transducer and preparation method thereof Expired - Fee Related CN107511317B (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108433744A (en) * 2018-04-23 2018-08-24 中国科学院苏州生物医学工程技术研究所 Ultrasonic transducer, ultrasonic probe, ultrasonic probe and ultrasonic hydrophone
CN109231150A (en) * 2018-09-06 2019-01-18 西安交通大学 A kind of combined film pMUTs and preparation method thereof
CN109798944A (en) * 2018-12-25 2019-05-24 浙江大学 Flowmeter and transition time measuring device based on micromechanics piezoelectric supersonic wave transducer
CN117225676A (en) * 2023-11-14 2023-12-15 南京声息芯影科技有限公司 Integrated structure of ultrasonic transducer array and CMOS circuit and manufacturing method

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1628977A (en) * 2003-12-10 2005-06-22 佳能株式会社 Dielectric thin film element, piezoelectric actuator and liquid discharge head, and method for manufacturing the same
US7683522B2 (en) * 2006-03-03 2010-03-23 Industrial Technology Research Institute Composite mode transducer and cooling device having the composite mode transducer
JP2016138810A (en) * 2015-01-28 2016-08-04 パナソニックIpマネジメント株式会社 Ultrasonic transducer and ultrasonic flowmeter using the same

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1628977A (en) * 2003-12-10 2005-06-22 佳能株式会社 Dielectric thin film element, piezoelectric actuator and liquid discharge head, and method for manufacturing the same
US7683522B2 (en) * 2006-03-03 2010-03-23 Industrial Technology Research Institute Composite mode transducer and cooling device having the composite mode transducer
JP2016138810A (en) * 2015-01-28 2016-08-04 パナソニックIpマネジメント株式会社 Ultrasonic transducer and ultrasonic flowmeter using the same

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108433744A (en) * 2018-04-23 2018-08-24 中国科学院苏州生物医学工程技术研究所 Ultrasonic transducer, ultrasonic probe, ultrasonic probe and ultrasonic hydrophone
CN108433744B (en) * 2018-04-23 2023-11-28 中国科学院苏州生物医学工程技术研究所 Ultrasonic transducer, ultrasonic probe and ultrasonic hydrophone
CN109231150A (en) * 2018-09-06 2019-01-18 西安交通大学 A kind of combined film pMUTs and preparation method thereof
CN109231150B (en) * 2018-09-06 2022-09-30 西安交通大学 Combined film pMUTs and preparation method thereof
CN109798944A (en) * 2018-12-25 2019-05-24 浙江大学 Flowmeter and transition time measuring device based on micromechanics piezoelectric supersonic wave transducer
CN117225676A (en) * 2023-11-14 2023-12-15 南京声息芯影科技有限公司 Integrated structure of ultrasonic transducer array and CMOS circuit and manufacturing method

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Granted publication date: 20200218