CN1073700A - Novel thermal barrier coating composition - Google Patents
Novel thermal barrier coating composition Download PDFInfo
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- CN1073700A CN1073700A CN 92105363 CN92105363A CN1073700A CN 1073700 A CN1073700 A CN 1073700A CN 92105363 CN92105363 CN 92105363 CN 92105363 A CN92105363 A CN 92105363A CN 1073700 A CN1073700 A CN 1073700A
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Abstract
A novel heat-insulating paint composition comprises 2-20 wt% of polyvinyl acetal resin, 0-30 wt% of ketone resin, 0-30 wt% of pigment, 5-60 wt% of filler such as heat-insulating material, and 5-45 wt% of diluent. The paint of the present invention may be used in various buildings, industrial equipment, outer side of vehicle, ship, etc. needing direct heat radiation isolation and heat conduction. The heat insulation effect of the heat insulation material at high temperature of more than 30 ℃ and the like reaches about 10 ℃.
Description
The present invention relates to a kind of heat insulation coating composition of using of novelty.
Up to now, for improving concrete structures such as dwelling house, factory building, the heat-insulating cooling effect of equipment such as industrial oil tank, pipeline and parts thereof, existing many people have done extensive, deep research and development to this.The heat insulation coating of using of application, because of its preparation, easy and simple to handle, suitability extensively and especially is subjected to user's attention.A kind of composition is disclosed as in No. the 4362826th,, the United States Patent (USP), said composition by one in component, have active hydrogen polyimide heat stable resin and with it blended dimaleimide compound or derivatives thereof form.Said composition is used for the surface coatings of metal foil sheet material, can keep this sheet metal tool preferably effect of heat insulation the time, also can strengthen its tear strength and elongation etc.
Though above-mentioned United States Patent (USP) has related to said composition tool thermotolerance, do not provide the experimental data and the performance index of this respect.
Again, the Japanese Patent spy opens that to have disclosed for clear 60-190470 number a kind of be heat insulation, preventing water coating composition main component, that be used for roofs such as slabstone, cement with naphthene series oil pitch prill, kaolin and fibrous magnesium silicate.The thermofin that said composition forms, its effect is still very limited.And it is bigger that it is coated with thicknesses of layers, so the said composition material is not suitable for being used for other some occasions.
Recently, the alkyd adiabatic gum model of domestic according to reports existing a kind of black is (C98-2) (having another name called the heat insulation deadener of black), it is said to completely cut off extraneous photothermal conduction, but through coating property being measured, there is no what heat-proof quality on the spot.
For overcoming the deficiency of above-mentioned prior art, an object of the present invention is: a kind of composition of insulating mold coating of novelty is provided, but this coating composition application, cover with paint, lacquer, colour wash, etc. in the house, buildings, all types of industries be with outer surfaces such as equipment and car, ships; Can reach the thermal radiation and the thermal conduction of isolated effectively daylight, industrial heat resources etc. significantly.
Another purpose of the present invention is: when a kind of radiation of isolated effectively thermal source and conduction heat are provided, also have a composition of insulating mold coating of the clinging power of excellence, wear-resisting wiping, high-peeling strength and weathering resistance.
The following realization of purpose of the present invention.
The prescription of the composition of insulating mold coating that the present invention adopts is:
Polyvinyl acetal-based resin 2-20%(weight)
Ketone resin
(" AAROCAL-K80 ") West Germany Beyer Co., Ltd produces 0-30%(weight)
Pigment 0-30%(weight)
Filler 5-60%(weight such as lagging material)
Thinner 5-45%(weight)
As forming the polyvinyl acetal-based resin that the present invention adopts, its principal monomer general structure is as follows:
In the formula, n=200-2000, R
1Be H, C
1-C
6Alkyl.
Preferably, we can use R
1Be C
3-C
6Alkyl, the polyvinyl acetal-based resin of formula (A) general formula that n is 800-1000.
As ketone resin used among the present invention, we can adopt following general formula (B) is monomer structure,
(in the formula, R
2Expression C
3-C
10Alkyl, n is 200-1200) ketone resin of (trade(brand)name " AARO-CAL-K80 " West Germany Chemical Bayer Ltd. product).
Preferably, we enumerate above-mentioned R
2Be C
6Alkyl, n are the ketone resin of 600-1000.(article number " AAROCAL-K80 ", West Germany Bayer chemistry department produces).
As pigment, we can enumerate as, titanium dioxide, zinc oxide, lithopone, magnesium oxide etc., and select wherein one or more for use.
As fillers such as lagging materials, we can list as antimonous oxide, magnesium oxide, titanium dioxide, talcum powder, barium sulfate (or ground barium sulfate), lime carbonate (heavy, lightweight) wollastonite powder, mica powder etc., and can select wherein one or more arbitrarily for use.
As thinner, we can enumerate alcohols, ketone, ester class and the agent of arene group.
As available alcohols thinner of the present invention, can enumerate: methyl alcohol, ethanol, propyl alcohol, Virahol, butanols, isopropylcarbinol, primary isoamyl alcohol, sugar alcohol, ethylene glycol etc.
As available ketone thinner of the present invention, can enumerate: ketone in acetone, butanone, mibk, Methyl isobutyl ketone, the positive acetone of methyl, diethyl ketone, methyl n-butyl ketone, methylpentanone, the ethyl butyl ketone and two.
Have as available benzene class thinner of the present invention: toluene, p-Xylol, benzene, penta benzene and ethylbenzene etc.
Have as available ester class thinner of the present invention: methyl-formiate, ethyl formate, propyl formate, methyl acetate, ethyl acetate, propyl acetate, tetryl formate, methyl propionate, butyrolactone etc.
Preferably select alcohols or ketone auxiliary agent for use, more preferably, select acetone and ethanol for use.
Composition of insulating mold coating of the present invention can be realized by following common technology behind the synthetic insulating resin.
(1) prescription
Mixtures such as 5-60% such as pigment 0-30%, filler is even;
(2) be equipped with resin, thinner
Above-mentioned gained mixture is added polyvinyl acetal group 2-20% after synthetic, be preferably 10-15% and ketone resin 0-30%, be preferably 6-10%, add thinner 5-45%, be preferably 10-20%, make it into paste, pulpous state.
(3) grind
With grinding plant, for example ball mill etc. is ground the 3-5 road to paste, the paste mixture of above-mentioned operation gained, and when strict about 3 hours, to being used for the coating composition of cement surfaces such as application buildings, be ground to 20 orders-250 order, to being used for the coating composition of occasions such as coating metal surface.Be ground to order-325 order 60 times.To obtain dispersion, uniform coating composition.
Through as above prepared coating composition of the present invention, its some performance index such as table one.Its oxygen index report sees Table two.
Table-
| Performance | Parameter |
| Viscosity, (being coated with-4 glasss) proportion flash-point surface drying time of drying, (normal temperature) is done solid work, the validity period of filming (normal temperature) storage period | >30S >1.3g/cm 231 ℃ of 15 minutes 1.5 hours 2 years 5-6 |
Table two oxygen index test report
The specimen size specification
100 * 6.5 * 1mm
Sample quantities
Test result
Below, further specify the present invention with enforcement, experimental example.
Embodiment
Behind filler formulations such as lagging material, pigment in described each composition of table three, add polymer acetals and ketone resin, dilute this mixture to paste, pulpous state with thinner.Be ground to certain fineness with ball mill, sand mill etc., after high speed dispersor dispersion, three roll machine roll extrusion evenly, become composition of insulating mold coating of the present invention again.
Table three
Experimental example 1
At temperature is that will be painted on volume by the 1 prepared coating composition of the present invention of embodiment in the table three was 500m in 30 ℃, daylight were contained
3The empty oil tank outer surface of metal, brush two roads, the about 100 μ m of thickness, consumption 260g/m
2, after about more than 1 hour, all dry.
Experimental example 2
Temperature be 31 ℃, daylight Shengs day, will be painted on volume by embodiment 2 made coating compositions of the present invention is 500m
3The empty oil tank outer surface of metal, brush three roads, the about 100 μ m of thickness, consumption is 300g/m
2, all dry after about 1.5 hours.
Reference examples 1
Under condition similarly to Example 1, replace paint spraying of the present invention four empty oil tank outside surfaces of onesize metals in addition with silver paint.
Reference examples 2
Under meteorological conditions similarly to Example 2, silver paint is replaced paint spraying of the present invention in other four the empty test of onesize metals oil tanks.
After 1 hour, record temperature in two groups of empty oil tanks of the metal in the example respectively, the result is shown in table four, table five.
Table four
Table five
By above-mentioned two groups of examples as seen, be coated with temperature in the metallic oil tank of coating of the present invention being coated with low 8-12 ℃ with silver paint, and, can find out that when outside temperature degree of liter, the temperature difference of its test also increases.
Experimental example 3
Temperature be 32 ℃, daylight Shengs day, will be painted on the outer surface of the metal oil pipeline of diameter 40cm by embodiment 2 made coating of the present invention, brush three roads, the about 100 μ m of (doing) thickness, consumption 280g/m
2, about more than 1 hour of time of drying.
Reference examples 3
With the black protective paint replace paint spraying of the present invention in experimental example 3 similarity conditions under another unidimensional metallic conduit.
Contrast above-mentioned two examples, be coated with temperature in the pipeline of coating of the present invention and be about 37 ℃, be coated with pitch-dark and be about 48 ℃, exceed the former 11 ℃.
Experimental example 4
To the about 15m of certain unit one area
2About, the four sides do not have by room, five faces and is subjected to the roof in brick structured bungalow reception room of the sun and wall application with the embodiment of the invention 3 prepared composition of insulating mold coating.When summer, the highest temperature reached 35-36 ℃, only 23-27 ℃ of room temp round the clock indoor on duty, felt that temperature obviously descends.
And before this, in one to summer, indoor wall, tables and chairs all generate heat, daytime room temp (at 1 o'clock in afternoon) can't be on duty in doors up to 36 ℃.
Experimental example 5
At temperature is 30 ℃, and the Liege will be about 120m in an area by embodiment 4 made paint finishings of the present invention when the day of sky
2The exterior wall of two layers of Xiao Lou buildings identical.The Xiao Lou window is airtight, and only the gate, gangway is often opened.The meridian hour, the scorching sun right overhead, temperature has reached 35-37 ℃ under the outdoor sunlight, and is indoor only about 22,23 ℃.Comfort this building exterior wall wall with hand, even be in irradiation place, Liege, this is coated with the about 21-22 of exterior wall wall ℃ of the coating of the present invention also significant shady and cool sense of tool, is not coated with cement face with any coating and comfort this Xiao Lou building entrance step etc. with hand, and then feel is hot significantly.
Experimental example 6
Embodiment 5 made coating of the present invention are applied to the airport hardstand of burning sun under being exposed to the sun, 32 ℃ of temperature, the cement flooring temperature that is not coated with coating of the present invention under the burning sun has reached about 40-50 ℃, and is coated with (two roads, 280g/m with coating of the present invention
3) only 26 ℃ on ground, cement hardstand.
Experimental example 7
Embodiment 6 prepared coating of the present invention are applied to the automobile cab roof, brush three road 300g/m
2, 30 ℃ of temperature, automobile is not turned on the aircondition the descending approaching of burning sun one hour, no common feeling of oppression and heat in the wheel house.And feel nice and cool.
The heat insulation test of experimental example 8(simulation thermal source)
Add the square tinplate bucket of human relations to 1, its bottom surface application is with the coating of the embodiment of the invention 6 and 7 gained, and its numbering is respectively 1 and No. 2, and its coating is respectively two layers and three layers.Thick 400 and 600 μ m.All the other five with sponge wrapping insulation, and place, bucket top inserts temperature in the thermometer measure bucket.Locate irradiation (heating) with 250W infrared source 10 inch (25.4cm) at the bottom of this barrel.After 1 hour 15 minutes, temperature rise is tending towards saturated in the bucket, surveys its temperature variation such as table six.
Reference examples 8
One of them of similarly to Example 8 two 1 gallon of square tinplate buckets is not coated with any coating (No. 3), and wherein another is coated with cement (thick about 500-600 μ m) with binding agent, records under same heating condition that variation sees Table six in its bucket.
Table six
Actual observation record
By as seen 1. heating (irradiation bottom surface) after 1 hour 15 minutes of table six, a temperature rise is tending towards saturated in the bucket, and 2. the compare example No. 3, No. 4 buckets come, and is coated with 1,2 barrel of its effect of heat insulation of coating of the present invention preferablely, will hang down 11 and 22 ℃ respectively.
The heat insulation test of experimental example 9(simulation thermal source)
To application is with two, two, three layers of the coating of embodiments of the invention 8,9,10 gained respectively with the same tinplate bucket of experimental example 8, its bucket is numbered 3,2,1.Recording temperature variation such as table seven in its bucket under the test condition similarly to Example 8.
Reference examples 9
To being coated with cement (No. 4 buckets), record temperature variation such as table seven in its bucket with the same tinplate bucket of experimental example 9.
Table seven
Actual observation record
Experimental example 10
To certain chemical plant office building wall and roof application with the coating of pressing embodiment 10 gained of the present invention after, stop using electric fan in this building after, indoor have pleasantly cool sense by comparison with the office that does not use coating of the present invention significantly.Room temp obviously reduces.Roofing is through field inspection, and the temperature difference is very big under the sunlight.
Coating compound of the present invention can cover with paint, lacquer, colour wash, etc. in as dwelling house, office building, auditoriums, hotels, factory building, freezer, plant etc. be with the concrete main material buildings top and around outer wall surface, reaching good heat-insulating cooling effect, few with or without air-conditioning; Also can be coated on the outer surface of equipment such as industrial metal jar, groove, pipeline, as oil depot, oil tank, oil groove, liquefied gas class spherical tank, chemical pipeline and refrigerator car, ship etc., and need not with cryogens such as cold water spray, to prolong the work-ing life of equipment, the Ordinary Wear and Tear of minimizing oil plant etc., save energy.What coating composition of the present invention can be used for all kinds of vehicles such as car, ship, facility, place etc. again falls the heat drop temperature; Even also can be painted on each based article member outer surface such as the plastics that need directly heat insulation and heat control in thermal source radiation, conduction scope, wood.
Through the buildings of outside surface brushing coating composition of the present invention, industrial equipments such as oil tank and car, ship etc. can be effectively, infrared radiation, the conduction heat of thermals source such as isolated daylight significantly, reduce temperature to reach about 10 ℃, and be an ideal heat insulation and heat control coating.
In addition, coating composition strong adhesion of the present invention, wear resistance is good, and the good weathering resistance of tool again can stand stern climate conditions such as ultraviolet ray, hot and cold and Exposure to Sunlight rain and dew, and its effective service life, reached more than 5 years.
Moreover coating composition of the present invention preparation is simple, easy to use, with methods such as common brushing, roller coating or spraying get final product, generally wet, build is respectively 300 and 100 μ m.But as film thick slightly also harmless, phenomenons such as wrinkling, sagging can not take place.Coating composition of the present invention behind coated about 15～30 minutes be surface drying, 1-1.5 hour is all dry, also is applicable to the coating decoration that the construction period requirement is short.Again, coating composition recoatability of the present invention is good, as brushing again on the old film of this coating, then because of the sequestering action of solvent etc., can increase the adhewsive action between new old coating film, makes new old coating film fuse one, plays the effect of repairing sth. old and making it as good as new.
At last, film coated surface of the present invention is inferior photosensitiveness, certain ornamental of tool, and it also has certain Corrosion Protection to the metal outer surface.
Through adding an amount of thickening material, coating composition of the present invention can be stored 2 years at normal temperatures to 3 years.The validity period of filming of coating of the present invention is more than 5 years.
Claims (10)
1, a kind of composition of insulating mold coating is characterized in that, described composition comprises:
Represent the monomeric polyvinyl acetal-based resin of structure with following formula,
(in the formula, R
1Be H or C
1-C
10Alkyl, n is 200-2000)
2-20% (weight)
Represent the monomeric ketone resin of structure with following formula,
(R in the formula
2Table C
3-C
10Alkyl, n is 200-1200)
0-30% (weight)
Pigment 0-30% (weight)
Stopping composition 5-60% (weight) such as lagging material
Thinner 5-45% (weight)
2, composition of insulating mold coating as claimed in claim 1 is characterized in that, R in the polyvinyl acetal-based resin of wherein said formula (A)
1Be H or C
3Alkyl.
3, composition of insulating mold coating as claimed in claim 1 or 2 is characterized in that, the polymer acetal-based resin content of described formula A is 10-15%(weight).
4, composition of insulating mold coating as claimed in claim 1 is characterized in that, wherein, and the ketone resin of described formula (B).
In, R
2Expression C
6Alkyl n be 600-1000.
As claim 1 or 4 described composition of insulating mold coating, it is characterized in that 5, wherein, the ketone resin content of described formula (B) is 6-10(weight).
6, composition of insulating mold coating as claimed in claim 1 is characterized in that, wherein, and described thinner such as alcohols, ester class, ketone and arene thinner.
As claim 1 or 6 described composition of insulating mold coating, it is characterized in that 7, wherein, described thinner consumption is 10-20%.
8, composition of insulating mold coating as claimed in claim 1 is characterized in that, wherein, described pigment comprises: titanium dioxide, lithopone, zinc oxide and magnesian one or more.
9, composition of insulating mold coating as claimed in claim 1, it is characterized in that, wherein, stopping composition such as described lagging material comprises: one or more of antimonous oxide, titanium dioxide, zinc oxide, talcum powder, barium sulfate, lime carbonate (heavy, lightweight), magnesium oxide, wollastonite powder and mica powder.
10, composition of insulating mold coating as claimed in claim 1 is characterized in that, in the used monomeric polyvinyl acetal-based resin of the structure of representing with following formula;
R
1Be H, C
1-C
10Alkyl, n is 800-1000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92105363 CN1030142C (en) | 1992-06-30 | 1992-06-30 | Novel thermal barrier coating composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92105363 CN1030142C (en) | 1992-06-30 | 1992-06-30 | Novel thermal barrier coating composition |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1073700A true CN1073700A (en) | 1993-06-30 |
| CN1030142C CN1030142C (en) | 1995-10-25 |
Family
ID=4941338
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 92105363 Expired - Lifetime CN1030142C (en) | 1992-06-30 | 1992-06-30 | Novel thermal barrier coating composition |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1030142C (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1074025C (en) * | 1998-06-05 | 2001-10-31 | 深圳市金岁丰实业有限公司 | Coating capable of reflecting sun-heat |
| CN1099448C (en) * | 1999-10-25 | 2003-01-22 | 张炳强 | Heat-insulating waterproof coating |
| CN1318526C (en) * | 2004-06-07 | 2007-05-30 | 华东船舶工业学院 | Infrared radiative energy-saving coating and preparing method thereof |
| CN100357378C (en) * | 2005-01-05 | 2007-12-26 | 中国科学院过程工程研究所 | Insulating mold coating and its uses |
| CN101928483B (en) * | 2009-11-17 | 2013-02-06 | 郭宪强 | Composition capable of reflecting sun heat radiation |
| CN102936440A (en) * | 2012-11-30 | 2013-02-20 | 康力电梯股份有限公司 | Wear-resistant paint for staircase |
| CN102942828A (en) * | 2012-11-30 | 2013-02-27 | 康力电梯股份有限公司 | Heat insulating coating for escalator |
| CN103289486A (en) * | 2013-06-04 | 2013-09-11 | 苏州艾特斯环保材料有限公司 | Polyvinyl butyral-containing waterproof heat-resistant coating |
-
1992
- 1992-06-30 CN CN 92105363 patent/CN1030142C/en not_active Expired - Lifetime
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1074025C (en) * | 1998-06-05 | 2001-10-31 | 深圳市金岁丰实业有限公司 | Coating capable of reflecting sun-heat |
| CN1099448C (en) * | 1999-10-25 | 2003-01-22 | 张炳强 | Heat-insulating waterproof coating |
| CN1318526C (en) * | 2004-06-07 | 2007-05-30 | 华东船舶工业学院 | Infrared radiative energy-saving coating and preparing method thereof |
| CN100357378C (en) * | 2005-01-05 | 2007-12-26 | 中国科学院过程工程研究所 | Insulating mold coating and its uses |
| CN101928483B (en) * | 2009-11-17 | 2013-02-06 | 郭宪强 | Composition capable of reflecting sun heat radiation |
| CN102936440A (en) * | 2012-11-30 | 2013-02-20 | 康力电梯股份有限公司 | Wear-resistant paint for staircase |
| CN102942828A (en) * | 2012-11-30 | 2013-02-27 | 康力电梯股份有限公司 | Heat insulating coating for escalator |
| CN103289486A (en) * | 2013-06-04 | 2013-09-11 | 苏州艾特斯环保材料有限公司 | Polyvinyl butyral-containing waterproof heat-resistant coating |
| CN103289486B (en) * | 2013-06-04 | 2015-11-25 | 苏州艾特斯环保材料有限公司 | A kind of waterproof heat resistant coating containing polyvinyl butyral acetal |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1030142C (en) | 1995-10-25 |
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Address after: 201108, No. 4289, Jin Du Road, Xin Min hi tech park, Shanghai Patentee after: Shanghai Datong High-tech Material Co., Ltd. Address before: 201111 No. 1188, Shanghai, Caobao Road Patentee before: Shanghai Datong Applied Chemistry Research Institute |
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Effective date of registration: 20080912 Address after: No. 4289 Jindu Road, Minhang District, Shanghai: 201108 Patentee after: Shanghai Datong High-tech Material Co., Ltd. Address before: Postal code 1188 Caobao Road, Shanghai: 201111 Patentee before: Shanghai Datong Applied Chemistry Research Institute |
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