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CN107162436A - A kind of crystal glass printing opacity encaustic and its manufacture craft - Google Patents

A kind of crystal glass printing opacity encaustic and its manufacture craft Download PDF

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Publication number
CN107162436A
CN107162436A CN201710223882.1A CN201710223882A CN107162436A CN 107162436 A CN107162436 A CN 107162436A CN 201710223882 A CN201710223882 A CN 201710223882A CN 107162436 A CN107162436 A CN 107162436A
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China
Prior art keywords
temperature
ground
glass
encaustic
coat enamel
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CN201710223882.1A
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Chinese (zh)
Inventor
张柳松
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Individual
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Individual
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Priority to CN201710223882.1A priority Critical patent/CN107162436A/en
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/3411Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B44DECORATIVE ARTS
    • B44DPAINTING OR ARTISTIC DRAWING, NOT OTHERWISE PROVIDED FOR; PRESERVING PAINTINGS; SURFACE TREATMENT TO OBTAIN SPECIAL ARTISTIC SURFACE EFFECTS OR FINISHES
    • B44D2/00Special techniques in artistic painting or drawing, e.g. oil painting, water painting, pastel painting, relief painting
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C1/00Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
    • C03C1/04Opacifiers, e.g. fluorides or phosphates; Pigments
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/02Frit compositions, i.e. in a powdered or comminuted form
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/14Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Glass Compositions (AREA)

Abstract

A kind of crystal glass printing opacity encaustic, the clear glass that the encaustic is not less than 700 DEG C using softening point temperature is used as substrate, low temperature ground-coat enamel of the firing temperature below 800 DEG C is sprayed as binder course in transparent glass surface, drawn a picture again in the air brushing of ground-coat enamel surface, enter the firing of low-temperature primary below 800 DEG C of kiln to form, wherein containing the sodium acid carbonate or sodium carbonate for accounting for its gross mass 1/4 1/3 in the ground-coat enamel.Encaustic of the present invention, first from low temperature glaze, the glass of high softening-point solves glaze shaping and the contradiction of Glass Transition;Secondly it is added under substantial amounts of sodium salt, high temperature in the ground-coat enamel for be sprayed on transparent glass surface to form binder course with glass reaction, glaze is firmly combined in glass surface.

Description

A kind of crystal glass printing opacity encaustic and its manufacture craft
Technical field
The present invention relates to encaustic technical field, specially a kind of crystal glass printing opacity encaustic and its manufacture craft.
Background technology
Traditional encaustic is all that special chemical color handwritten drawings, glazing are used on porcelain plate usually, then is burnt through high temperature A kind of plane ceramic handicraft of system.Encaustic can be used as to view and admire in mounting or embedded screen.Encaustic can be traced back to earliest Qin Han dynasty, and encaustic truly then occurs from Ming Dynasty's mid-term.The orientation direction of encaustic since Qing Dynasty's mid-term It is prosperous.In existing encaustic, in addition to the artistic value of paintings, its structure type is stereotyped, is in thick and heavy white porcelain On plate, draw a picture, glazing again through high temperature once, it is secondary fire, the encaustic of this quasi-tradition is used as basic, cost from thick and heavy porcelain plate It is just higher first;Next to that more heavy, weight is larger, is not easy to carry, install or dismantle.In addition, being particularly wall-mounted on Outdoor large-scale encaustic, only just plays on daytime and views and admires decorative value, and once to night, the light is dusky, just loses Ornamental value, is even illuminated using single irradiation light polishing, in view of the property of ceramics, its actual effect is not yet It is good.
In consideration of it, applicant's intention abandon by traditional porcelain plate as substrate carry out encaustic creation in the way of, and It is relatively low compared with light, cost from quality itself, and it is crucial that it is capable of the glass of printing opacity as the substrate of encaustic, in clear glass Surface carries out glazing, draws a picture and form by a firing, the problem of this intention can be good at solving above-mentioned, and even at night In evening, due to glass transmission, irradiation light is radiated at the Opal glass picture back side, the bright such as lamp of the positive paintings of encaustic is not only solved Night views and admires problem, and can also play a part of illumination, while having had art and the value used concurrently.But this intention There are problems:1)Because glass is noncrystal, it, which is reached, just starts softening after critical-temperature, it is impossible to carry out high-temperature firing, And the glaze of glass surface needs high-temperature firing to be molded;2)Glass surface is smooth, is sprayed on the glaze of glass surface in high temperature After shaping, it is impossible to be completely combined and be integrated with glass, generally fire in the finished product completed, otherwise glass softening transform already, The glaze layer of glass surface early has disengaged from glass surface, has a style of one's own.
The content of the invention
In order to solve the above problems, the purpose of the present invention is to propose to a kind of crystal glass printing opacity encaustic and its manufacture craft, Low temperature glaze is selected first, and the glass of high softening-point solves glaze shaping and the contradiction of Glass Transition;Secondly be sprayed on it is transparent It is added under substantial amounts of sodium salt, high temperature in the ground-coat enamel of glass surface to form binder course with glass reaction, enable glaze It is firm to combine in glass surface.
The present invention is for the taken technical scheme that solves the above problems:A kind of crystal glass printing opacity encaustic, the porcelain The clear glass for being not less than 700 DEG C using softening point temperature is drawn as substrate, firing temperature is sprayed at 800 DEG C in transparent glass surface Following low temperature ground-coat enamel is drawn a picture as binder course, then in the air brushing of ground-coat enamel surface, is entered the firing of low-temperature primary below 800 DEG C of kiln and is formed, Contain the sodium acid carbonate or sodium carbonate for accounting for its gross mass 1/4-1/3 in wherein described ground-coat enamel.
As preferred, the thickness of the clear glass is at least 5-10mm.
As preferred, the thickness of the ground-coat enamel is 0.2-0.8mm.
A kind of manufacture craft of crystal glass printing opacity encaustic, comprises the following steps:
Step 1: processing substrate
Choose the clear glass of size needed for composition of drawing a picture, polishing cleaning carried out to transparent glass surface, to clear glass it is penetrating, Surface is without dirty no marking;
Step 2: processing ground-coat enamel binder course
Low temperature glaze of the firing temperature below 800 DEG C is chosen, and addition accounts for its total amount 1/4-1/3's in the glaze completed to allotment Sodium acid carbonate or sodium carbonate, uniform mixing, are made ground-coat enamel;
Ground-coat enamel even application is handled to the transparent glass surface of completion in step one;
Step 3: air brushing is drawn a picture
1)The inorganic former stone of colour system, is made a variety of coloured glazes, using coloured glaze as raw material, on ground-coat enamel surface needed for grinding allotment is drawn a picture Computer painting is drawn a picture;
2)According to air brushing picture effect, to carrying out Freehandhand-drawing processing at details, semi-finished product are obtained after the completion of processing;
Step 4: kiln-firing
Obtained semi-finished product are inserted in kiln, heating and cooling under whole oxidation environment, its heating and cooling process is as follows:
1)Temperature-rise period
Kiln top air port is opened, and bottom tuyeres are closed;
Room temperature rises to 500 DEG C:Not higher than 50 DEG C/h;
500 DEG C rise to 700-720 DEG C:30℃/h;
Wherein, more than 650 DEG C at the air port of kiln top into kiln towards semi-finished product with 3-6m/s wind speed balanced ventilations, extremely Temperature reaches out-of-blast after 700-720 DEG C;
2)Temperature-fall period
700-720 DEG C is down to 600 DEG C:Kiln top air port, bottom tuyeres are opened, from kiln bottom tuyeres into kiln direction Semi-finished product are uniformly dried with 5-8m/s wind speed, close all air ports rapidly when temperature is down to 600 DEG C, form closed environment;
600 DEG C are down to 500 DEG C:30℃/h;
500 DEG C are down to 100 DEG C:Time-consuming 36h, opens during to 100 DEG C and is taken out after wicket, natural cooling, got product.
Compared with prior art, the invention has the advantages that:
First, a kind of crystal glass printing opacity encaustic of the present invention has overturned the Creation form of traditional encaustic, and intention is put Abandon in the way of traditional porcelain plate carries out encaustic creation as substrate, and selected quality itself relatively low compared with light, cost, and most closed Key is to be capable of the glass of printing opacity as the substrate of encaustic, carries out glazing in transparent glass surface, draws a picture and form by a firing, this Individual intention, which can be good at solving the big thick and heavy quality of traditional encaustic, inconvenient carrying and installation and outdoor environment lower night, to be viewed and admired The problem of, and even, due to glass transmission, irradiation light is radiated at the Opal glass picture back side, the positive paintings of encaustic at night Bright such as lamp, not only solves the problem of viewing and admiring at night, and can also play a part of illumination, while having had art concurrently with using Value.
Second, a kind of crystal glass printing opacity encaustic of the present invention needs high temperature and glass is not through to solve glaze The contradiction of high temperature is played, after it have passed through experiment several times, low temperature glaze of the firing temperature at 700-800 DEG C is selected on glaze, And glass of the softening point at 700 DEG C or so is selected simultaneously, in sintering procedure, even if temperature has exceeded the softening point of glass, glass Glass starts softening, but this process duration is shorter the problem of be higher than softening point enters cooling, and during this, ground-coat enamel Thinner thickness, temperature once reaches, it is not necessary to the high-temperature residence of long period can glaze become shaping, therefore solve well Glaze is molded the contradiction with Glass Transition, establishes the basis that glass is combined creation encaustic with glaze.
3rd, a kind of crystal glass printing opacity encaustic of the present invention, for asking of solving that glaze is difficult to be combined with glass Topic, by experiment several times, selection is changed on the composition of ground-coat enamel, i.e., substantial amounts of sodium salt, sodium salt are added in ground-coat enamel Additional proportion occupy the 1/4-1/3 of overall ground-coat enamel total amount, wherein, the sodium salt of best results is sodium acid carbonate, sodium acid carbonate Decompose in high temperature environments and obtain a large amount of sodium carbonate;And the composition of glass is mainly under silica, hot environment, sodium carbonate is held Continuous to generate sodium metasilicate and carbon dioxide with silicon dioxde reaction, the formation of sodium metasilicate makes glaze greatly combine in glass table Face, solves the problem of glaze is difficult to be combined with glass;The final surface formation being combined with glaze in glass using sodium metasilicate as The binder course of main body, realizes the strong bonded of glaze and glass, is that the creation of Opal glass picture establishes firm foundation.
4th, a kind of manufacture craft of crystal glass printing opacity encaustic of the present invention, in temperature-rise period, when temperature reaches During to more than 650 DEG C, selection at the air port of kiln top into kiln towards semi-finished product with 3-6m/s wind speed balanced ventilations, extremely Temperature reach it is out-of-blast after 700-720 DEG C because glass slowly show softening after temperature reaches more than 600 DEG C Tendency, glass of the softening point even specially selected at 700 DEG C or so, when temperature reaches more than 650 DEG C after, also can be slowly Show the sign of softening, and during this, the glaze of glass surface be still required for it is persistently overheating, therefore, in order to solve this The aggravation that individual temperature-rise period Glass Transition occurs, specially selects uniform towards semi-finished product into kiln at the air port of kiln top Air-supply, this air-supply process, on the one hand, accelerate circulating between kiln furnace air and outdoor air so that in kiln The pigment that gasifies present in air is moved out, it is to avoid the partial gasification color drops down onto the dirt that paintings are caused in encaustic after cooling It is turbid;On the other hand, circulating for air can reduce the local temperature of glass, slow down the appearance of preliminarily softened, it is ensured that after Continue being smoothed out for firing.
5th, a kind of manufacture craft of crystal glass printing opacity encaustic of the present invention, in temperature-fall period, in 700-720 DEG C be down to during 600 DEG C, kiln top air port, bottom tuyeres are opened, from kiln bottom tuyeres into kiln towards half into Product are uniformly dried with 5-8m/s wind speed;This process realizes the cyclical acceleration flowing of kiln interior air-flow from the bottom to top, and kiln Interior temperature drop is violent, on the one hand, local very fast cooling makes glass complete tempering, drastically increases the pressure of glass surface Stress, improves the bulk strength of glass, the problem of Opal glass picture intensity after shaping is ensure that well, can realize glass Carrying, loading and the outdoor installation exercise of encaustic;On the other hand, it is rapid to close in wicket formation kiln after very fast cooling Sealed environment, is changed to uniform speed slow cooling by very fast cooling, has further consolidated the performance of safety glass.
Embodiment
The present invention is elaborated with reference to specific embodiment, the present embodiment premised on technical solution of the present invention, Give detailed embodiment and specific operating process.
Embodiment 1
The present invention is a kind of crystal glass printing opacity encaustic, and the encaustic is used as base by 700 DEG C of clear glass of softening point temperature Plate, low temperature ground-coat enamel of the firing temperature below 700 DEG C is sprayed as binder course in transparent glass surface, then in the air brushing of ground-coat enamel surface Draw a picture, enter the firing of low-temperature primary below 800 DEG C of kiln and form, wherein containing the sodium acid carbonate for accounting for its gross mass 1/4 in the ground-coat enamel.
A kind of manufacture craft of crystal glass printing opacity encaustic, comprises the following steps:
Step 1: processing substrate
Choose the clear glass of size needed for composition of drawing a picture, polishing cleaning carried out to transparent glass surface, to clear glass it is penetrating, Surface is without dirty no marking;
Step 2: processing ground-coat enamel binder course
Low temperature glaze of the firing temperature at 700 DEG C is chosen, and the bicarbonate for accounting for its total amount 1/4 is added in the glaze completed to allotment Sodium, uniform mixing, is made ground-coat enamel;
Ground-coat enamel even application is handled to the transparent glass surface of completion in step one;
Step 3: air brushing is drawn a picture
1)The inorganic former stone of colour system, is made a variety of coloured glazes, using coloured glaze as raw material, on ground-coat enamel surface needed for grinding allotment is drawn a picture Inkjet printing is drawn a picture;
2)According to air brushing picture effect, to carrying out Freehandhand-drawing processing at details, semi-finished product are obtained after the completion of processing;
Step 4: kiln-firing
Obtained semi-finished product are inserted in kiln, heating and cooling under whole oxidation environment, its heating and cooling process is as follows:
1)Temperature-rise period
Kiln top air port is opened, and bottom tuyeres are closed;
Room temperature rises to 500 DEG C:Not higher than 50 DEG C/h;
500 DEG C rise to 700 DEG C:30℃/h;
Wherein, more than 650 DEG C at the air port of kiln top into kiln towards semi-finished product with 3m/s wind speed balanced ventilations, to temperature Degree reaches out-of-blast after 700 DEG C;
2)Temperature-fall period
700 DEG C are down to 600 DEG C:Kiln top air port, bottom tuyeres are opened, from kiln bottom tuyeres into kiln towards half into Product are uniformly dried with 5m/s wind speed, close all air ports rapidly when temperature is down to 600 DEG C, form closed environment;
600 DEG C are down to 500 DEG C:30℃/h;
500 DEG C are down to 100 DEG C:Time-consuming 36h, opens during to 100 DEG C and is taken out after wicket, natural cooling, and it is matt to produce ground-coat enamel Finished product.
Above for the present invention basic embodiment, can more than on the basis of be improved further, optimize or limit.
Further, the thickness of the clear glass is at least 5mm.
Further, the thickness of the ground-coat enamel is 0.2mm.
Embodiment 2
A kind of crystal glass printing opacity encaustic, the encaustic using softening point temperature be 700 DEG C of clear glass as substrate, transparent Glass surface sprays firing temperature and drawn a picture in 750 DEG C of low temperature ground-coat enamel as binder course, then in the air brushing of ground-coat enamel surface, enters kiln 800 Low-temperature primary below DEG C is fired and formed, wherein containing the sodium acid carbonate for accounting for its gross mass 1/3 in the ground-coat enamel.
A kind of manufacture craft of crystal glass printing opacity encaustic, comprises the following steps:
Step 1: processing substrate
Choose the clear glass of size needed for composition of drawing a picture, polishing cleaning carried out to transparent glass surface, to clear glass it is penetrating, Surface is without dirty no marking;
Step 2: processing ground-coat enamel binder course
Low temperature glaze of the firing temperature at 750 DEG C is chosen, and the bicarbonate for accounting for its total amount 1/3 is added in the glaze completed to allotment Sodium, uniform mixing, is made ground-coat enamel;
Ground-coat enamel even application is handled to the transparent glass surface of completion in step one;
Step 3: air brushing is drawn a picture
1)The inorganic former stone of colour system, is made a variety of coloured glazes, using coloured glaze as raw material, on ground-coat enamel surface needed for grinding allotment is drawn a picture Inkjet printing is drawn a picture;
2)According to air brushing picture effect, to carrying out Freehandhand-drawing processing at details, semi-finished product are obtained after the completion of processing;
Step 4: kiln-firing
Obtained semi-finished product are inserted in kiln, heating and cooling under whole oxidation environment, its heating and cooling process is as follows:
1)Temperature-rise period
Kiln top air port is opened, and bottom tuyeres are closed;
Room temperature rises to 500 DEG C:Not higher than 50 DEG C/h;
500 DEG C rise to 750 DEG C:30℃/h;
Wherein, more than 650 DEG C at the air port of kiln top into kiln towards semi-finished product with 6m/s wind speed balanced ventilations, to temperature Degree reaches out-of-blast after 750 DEG C;
2)Temperature-fall period
750 DEG C are down to 600 DEG C:Kiln top air port, bottom tuyeres are opened, from kiln bottom tuyeres into kiln towards half into Product are uniformly dried with 8m/s wind speed, close all air ports rapidly when temperature is down to 600 DEG C, form closed environment;
600 DEG C are down to 500 DEG C:30℃/h;
500 DEG C are down to 100 DEG C:Time-consuming 36h, opens during to 100 DEG C and is taken out after wicket, natural cooling, and it is light to produce ground-coat enamel Finished product.
Further, the thickness of the clear glass is at least 10mm.
Further, the thickness of the ground-coat enamel is 0.8mm.
Embodiment 3
A kind of crystal glass printing opacity encaustic, the encaustic using softening point temperature be 700 DEG C of clear glass as substrate, transparent Glass surface sprays firing temperature and drawn a picture in 720 DEG C of low temperature ground-coat enamel as binder course, then in the air brushing of ground-coat enamel surface, enters kiln 800 Low-temperature primary below DEG C is fired and formed, wherein containing the sodium carbonate for accounting for its gross mass 1/4 in the ground-coat enamel.
A kind of manufacture craft of crystal glass printing opacity encaustic, comprises the following steps:
Step 1: processing substrate
Choose the clear glass of size needed for composition of drawing a picture, polishing cleaning carried out to transparent glass surface, to clear glass it is penetrating, Surface is without dirty no marking;
Step 2: processing ground-coat enamel binder course
Low temperature glaze of the firing temperature at 720 DEG C is chosen, and addition accounts for the sodium carbonate of its total amount 1/4 in the glaze completed to allotment, Uniform mixing, is made ground-coat enamel;
Ground-coat enamel even application is handled to the transparent glass surface of completion in step one;
Step 3: air brushing is drawn a picture
1)The inorganic former stone of colour system, is made a variety of coloured glazes, using coloured glaze as raw material, on ground-coat enamel surface needed for grinding allotment is drawn a picture Inkjet printing is drawn a picture;
2)According to air brushing picture effect, to carrying out Freehandhand-drawing processing at details, semi-finished product are obtained after the completion of processing;
Step 4: kiln-firing
Obtained semi-finished product are inserted in kiln, heating and cooling under whole oxidation environment, its heating and cooling process is as follows:
1)Temperature-rise period
Kiln top air port is opened, and bottom tuyeres are closed;
Room temperature rises to 500 DEG C:Not higher than 50 DEG C/h;
500 DEG C rise to 725 DEG C:30℃/h;
Wherein, more than 650 DEG C at the air port of kiln top into kiln towards semi-finished product with 3-6m/s wind speed balanced ventilations, extremely Temperature reaches out-of-blast after 725 DEG C;
2)Temperature-fall period
725 DEG C are down to 600 DEG C:Kiln top air port, bottom tuyeres are opened, from kiln bottom tuyeres into kiln towards half into Product are uniformly dried with 7m/s wind speed, close all air ports rapidly when temperature is down to 600 DEG C, form closed environment;
600 DEG C are down to 500 DEG C:30℃/h;
500 DEG C are down to 100 DEG C:Time-consuming 36h, opens during to 100 DEG C and is taken out after wicket, natural cooling, got product.
Further, the thickness of the clear glass is at least 8mm.
Further, the thickness of the ground-coat enamel is 0.5mm.
The above described is only a preferred embodiment of the present invention, any formal limitation not is made to the present invention, though So the present invention is described as above with preferred embodiment, but is not limited to the present invention, any to be familiar with this professional technology people Member, without departing from the scope of the present invention, when a little change or modification made using technology contents described above It is the equivalent embodiment of equivalent variations, as long as being the technical spirit according to the present invention without departing from technical solution of the present invention content Any simple modification, equivalent variations and the modification made to above example, in the range of still falling within technical solution of the present invention.

Claims (4)

1. a kind of crystal glass printing opacity encaustic, it is characterised in that:The encaustic is not less than 700 DEG C of transparent glass with softening point temperature Glass sprays low temperature ground-coat enamel of the firing temperature below 800 DEG C as binder course as substrate in transparent glass surface, then in ground-coat enamel Surface air brushing is drawn a picture, and is entered the firing of low-temperature primary below 800 DEG C of kiln and is formed, its gross mass 1/4-1/ is accounted for wherein containing in the ground-coat enamel 3 sodium acid carbonate or sodium carbonate.
2. a kind of crystal glass printing opacity encaustic as claimed in claim 1, it is characterised in that:The thickness of the clear glass is at least For 5-10mm.
3. a kind of crystal glass printing opacity encaustic as claimed in claim 1, it is characterised in that:The thickness of the ground-coat enamel is 0.2- 0.8mm。
4. the manufacture craft of a kind of crystal glass printing opacity encaustic as described in claim 1-3 is any, it is characterised in that including such as Lower step:
Step 1: processing substrate
Choose the clear glass of size needed for composition of drawing a picture, polishing cleaning carried out to transparent glass surface, to clear glass it is penetrating, Surface is without dirty no marking;
Step 2: processing ground-coat enamel binder course
Low temperature glaze of the firing temperature below 800 DEG C is chosen, and addition accounts for its total amount 1/4-1/3's in the glaze completed to allotment Sodium acid carbonate or sodium carbonate, uniform mixing, are made ground-coat enamel;
Ground-coat enamel even application is handled to the transparent glass surface of completion in step one;
Step 3: air brushing is drawn a picture
1)The inorganic former stone of colour system, is made a variety of coloured glazes, using coloured glaze as raw material, on ground-coat enamel surface needed for grinding allotment is drawn a picture Inkjet printing is drawn a picture;
2)According to air brushing picture effect, to carrying out Freehandhand-drawing processing at details, semi-finished product are obtained after the completion of processing;
Step 4: kiln-firing
Obtained semi-finished product are inserted in kiln, heating and cooling under whole oxidation environment, its heating and cooling process is as follows:
1)Temperature-rise period
Kiln top air port is opened, and bottom tuyeres are closed;
Room temperature rises to 500 DEG C:Not higher than 50 DEG C/h;
500 DEG C rise to 700-750 DEG C:30℃/h;
Wherein, more than 650 DEG C at the air port of kiln top into kiln towards semi-finished product with 3-6m/s wind speed balanced ventilations, extremely Temperature reaches out-of-blast after 700-750 DEG C;
2)Temperature-fall period
700-750 DEG C is down to 600 DEG C:Kiln top air port, bottom tuyeres are opened, from kiln bottom tuyeres into kiln direction Semi-finished product are uniformly dried with 5-8m/s wind speed, close all air ports rapidly when temperature is down to 600 DEG C, form closed environment;
600 DEG C are down to 500 DEG C:30℃/h;
500 DEG C are down to 100 DEG C:Time-consuming 36h, opens during to 100 DEG C and is taken out after wicket, natural cooling, got product.
CN201710223882.1A 2017-04-07 2017-04-07 A kind of crystal glass printing opacity encaustic and its manufacture craft Pending CN107162436A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110627371A (en) * 2019-09-27 2019-12-31 张柳松 Method for making Ru art jade porcelain picture with picture under glaze layer

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1137495A (en) * 1995-06-02 1996-12-11 张锦朋 Producing technology for coloured facing glass and its heat treatment equipment
CN2451584Y (en) * 2000-09-20 2001-10-03 明达玻璃(厦门)有限公司 Enamelled decorative glass

Patent Citations (2)

* Cited by examiner, † Cited by third party
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Application publication date: 20170915