CN107157828A - A kind of anti-oxidant moisture-keeping cosmetics of Moringa - Google Patents

Abstract

The invention discloses a moringa anti-oxidation and moisturizing cosmetic, which is composed of the following components in parts by mass: 0-10 parts of moringa seed oil, 0-20 parts of moringa seed protein, 0-2 parts of moringa fruit acid, moringa oleifera 0-20 parts of flower hydrosol and 57.1-96 parts of auxiliary materials, wherein the moringa seed oil, moringa seed protein, moringa fruit acid and moringa flower hydrosol are not zero at the same time. The present invention uses the phytochemical extraction and separation method to separate and purify the cosmetic components therein to obtain Moringa seed oil, Moringa protein, Moringa flower hydrosol and Moringa fruit acid, which have high concentration of active components and obvious cosmetic effect, Using Moringa as raw material, it is non-toxic and has no side effects. It is a natural, non-toxic, efficient and non-irritating beauty and skin care product.

Description

A kind of moringa antioxidant moisturizing cosmetic

technical field

The invention relates to a Moringa anti-oxidation and moisturizing cosmetic, which belongs to the technical field of extraction and application of natural products.

Background technique

Moringa ( Moringaoleifera ) is a tropical deciduous woody vegetable and oil plant belonging to Moringaceae (Moringaceae) Moringa Adans. The leaves and fruit pods of Moringa are rich in various minerals, vitamins, proteins and amino acids, etc. ingredients, and the fat content is low, and its active ingredients have anti-oxidation and liver protection, lowering blood sugar, lowering blood fat and blood pressure, antibacterial and anti-inflammatory and other health effects.

The main nutrients of Moringa are vitamins A, B, B1, B2, B3, C, E, high protein and high fiber. It also contains six mineral elements (calcium, magnesium, phosphorus, potassium, sodium, sulfur), five trace elements (zinc, copper, iron, manganese, selenium), and eleven amino acids (eight of which are essential amino acids that cannot be synthesized by themselves). Amino acid is an important element for activating cells, enhancing immunity and strengthening sexual ability.

The nutrient content of Moringa seeds is: water: 6.3%, crude fat: 39.25%, protein: 36%, crude fiber: 1.2%, calcium: 0.145%, magnesium: 0.315%, phosphorus: 1.63%, potassium: 1.13%, Copper (mg/kg): 22, Zinc (mg/kg): 77.3, Iron (mg/kg): 28.8, Sodium (mg/kg): 103, Manganese (mg/kg): 22.2, Brass: 0.03% , vitamins (mg/mg): 10.

Vitamins and amino acids are very important for everyone's daily healthy diet. A person needs enough nutrients such as vitamins, minerals and protein for the development and maintenance of the body. A lack of any of these nutrients will cause health problems. Since Moringa was proved to be a plant with high nutritional value, countries such as Europe, America and Japan have actively developed Moringa food. Because of its high-protein, low-fat, high-fiber, high-vitamin content characteristics, and special health effects of lowering blood sugar, antibacterial and anti-inflammatory, and enhancing immunity, it has become a new favorite in the health food industry.

Moringa oil, extracted at low temperature from moringa seeds, is a mild, yellowish oil with a typical nutty flavor. Moringa seed kernels contain about 40% oil by mass fraction. Among them, the content of oleic acid can be between 62% and 78%, and the content of total unsaturated fatty acids is much higher than 80%. Among them, the content of behenic acid, behenic acid, which affects the naming of Moringa oil, is also relatively high, about 4 to 8%. Because the fatty acid composition of moringa oil is very similar to that of olives, especially the content of oleic acid, it is often used as a raw material for cosmetics.

Moringa seed oil produces natural fruit acids during the extraction process. The most essential principle of fruit acid beauty is because it is an acid. When the acid acts on the skin, it will be corrosive to a certain extent, so that the epidermis will peel off in varying degrees. When the epidermis peels off, new epidermis must grow again. Fruit acid products can reduce the cohesion of skin cutin and promote skin metabolism. As a result, some aging cuticles peel off, new epidermal cells grow out, and the skin becomes more delicate. Moreover, when the aging cuticle peels off, it will naturally remove some superficial dark spots, acne, acne, precipitated pigment, and fine wrinkles. That's why it's called cosmetic surgery.

Moringa seeds and leaves are also rich in plant protein. From the perspective of beauty, the use of Moringa plant protein can repair damaged cells, lock calcium and water, and shrink pores. Remove dark circles, wrinkles, breast enhancement. Plant protein contains a unique amino acid - hydroxyproline, which cannot be synthesized by the human body. It has been proved that pure plant protein is the best way to ensure the synthesis of new collagen in the skin, keep the skin moist and supple, and effectively help Reconstruction of proteins in the body and regeneration and renewal of elastin.

Therefore, it is necessary to research and develop how to apply the nutrients in Moringa seeds, leaves and fruits in an all-round way to prepare natural skin care products.

Contents of the invention

In order to achieve the above object, the invention provides a kind of Moringa as raw material to prepare the method for natural cosmetics, take Moringa as main raw material, prepare Moringa natural skin care products such as lotion, lotion, face cream, eye cream, and apply it In the field of daily chemicals.

The present invention is realized through the following technical solutions: a Moringa anti-oxidation moisturizing cosmetic, which consists of the following components in parts by mass: 0-10 parts of Moringa seed oil, 0-20 parts of Moringa seed protein, 0-20 parts of Moringa fruit acid 2 parts, 0-20 parts of moringa flower hydrosol, 57.1-96 parts of auxiliary materials, wherein moringa seed oil, moringa seed protein, moringa fruit acid and moringa flower hydrosol are not zero at the same time.

The Moringa oleifera seed oil is obtained through the following operations: fresh or dried Moringa oleifera fruits are removed from the pods, crushed and passed through a 20-mesh medicine sieve, and the solid-to-liquid ratio kg/L is calculated as 1: (5-10) , adding absolute ethanol, leaching at room temperature for 48-72 hours, stirring intermittently, suction filtration once every 12 hours, continuing leaching after replacing absolute ethanol, collecting Moringa oleifera seed residue, combining the leaching filtrate, and reducing pressure at 40-50°C After concentrating and evaporating the solvent, the Moringa oleifera seed oil is obtained, that is, the Moringa oleifera seed oil is obtained.

The Moringa oleifera seed protein is obtained through the following operations: drying the moringa oleifera seed dregs at 60-80°C for 2-3 hours, pulverizing until all the powder passes through a 20-mesh sieve, and the solid-to-liquid ratio kg/L is calculated as 1:(10 ~20) Add distilled water, adjust the pH of the solution to 8~11 with NaOH with a concentration of 1mol/L, then heat and stir in a water bath for extraction for 1~2h, the temperature of the water bath is 40~60°C, let it stand for stratification, and use HCl for the supernatant Adjust the pH to 4-5, take the precipitate, suction filter, pulverize, and pass through a 200-mesh sieve to obtain Moringa seed protein.

The moringa fruit acid is obtained through the following operations: extruding fresh moringa fruit pods to obtain a stock solution of moringa fruit pods, and the volume ratio of the stock solution of moringa oleifera fruit pods to concentrated sulfuric acid ethanol solution is 1:(3～2 ), add 1-5% concentrated sulfuric acid ethanol solution to the stock solution of Moringa oleifera pods, and precipitate out, put the mixed solution in a 4-6°C refrigerator and let it stand for 6-12 hours, until the precipitate is completely precipitated, then add sodium hydroxide , adjust the pH to 10-11, remove the precipitate, take the supernatant, add 3-5 times the volume of hydrochloric acid with a concentration of 1-5wt%, let it stand for recrystallization, and refine it in a refrigerator at 4-6°C for 6-12 hours. Filter to obtain moringa acid.

The Moringa flower pure dew is prepared by the following operations: use fresh Moringa flower petals, add distilled water to soak, and then extract by steam distillation, distill for 2-3 hours, and the Moringa flower essential oil is condensed by the condenser along with the water vapor. Stop heating until the moringa flower essential oil is no longer precipitated; the essential oil and the moringa flower hydrosol are extracted at the same time, and placed in a refrigerator at 4-5°C to refrigerate and stratify. .

The moringa anti-oxidation moisturizing cosmetics include moringa anti-oxidation spray, moringa anti-oxidation moisturizing emulsion, moringa anti-oxidation essence, moringa essential oil soap and the like.

The auxiliary materials include one or more of water, emulsifier, plant hydrosol, plant antibacterial agent, plant essential oil, Chinese medicinal material extract, chelating agent, foaming agent, preservative, and soap base.

The advantages and effects of the present invention: the raw materials of the present invention are all from Moringa itself, and the beauty ingredients in it are separated and purified through the phytochemical extraction and separation method to obtain Moringa seed oil, Moringa protein and Moringa flower pure Luhe moringa fruit acid has high active ingredient concentration and obvious cosmetic effect. Moringa is used as raw material, which is non-toxic and has no side effects. Compared with the prior art, most of the cosmetics and skin care products currently on the market are based on chemical raw materials. Some plant extracts are added to promote the concept, but chemicals are still used as the main functional ingredients. Long-term use will not only cause skin diseases to consumers, but also cause certain damage and damage to the skin. The present invention uses Moringa extract as the main raw material, Moringa oil as the oil phase, and Moringa flower hydrosol as the water phase, which is naturally rich in the fragrance of Moringa without essence and pigment, and then uses Moringa fruit acid, The joint effect of Moringa vegetable protein and Moringa seed oil, natural beauty and skin care, can not only maximize the beauty effect of Moringa, but also enhance the content and efficacy of active ingredients through plant extraction methods. It is a natural, non-toxic, efficient and non-toxic Stimulating beauty and skin care products.

Description of drawings

Fig. 1 is the DPPH free radical scavenging activity assay result of the Moringa oleifera seed oil obtained in Example 1.

detailed description

The present invention will be further described below in conjunction with embodiment.

Example 1

Moringa anti-oxidant moisturizing spray is composed of the following components by mass: 20 parts of Moringa flower hydrosol, 10 parts of propylene glycol, 20 parts of glycerin, 4.9 parts of ethanol, 0.01 part of antibacterial agent, 0.1 part of Moringa flower essential oil, deionized 24.99 parts of water.

The Moringa flower pure dew is prepared by the following operations: use fresh Moringa flower petals, add distilled water to soak, and then extract by steam distillation, distill for 2-3 hours, and the Moringa flower essential oil is condensed by the condenser along with the water vapor. Stop heating until the moringa flower essential oil is no longer precipitated; the essential oil and the moringa flower hydrosol are extracted at the same time, and placed in a refrigerator at 4-5°C to refrigerate and stratify. .

Example 2

Moringa anti-oxidant moisturizing lotion, composed of the following components by mass: 10 parts of Moringa seed oil, 5 parts of Moringa seed protein, 13 parts of Moringa flower hydrosol, 2 parts of emulsifier, 0.05 part of antibacterial agent, plant essential oil 0.05 parts, 55 parts of deionized water.

Mix the moringa seed oil and the plant essential oil, and then mix the other remaining components, and then stir and mix them to form a uniform emulsion.

The Moringa oleifera seed oil is obtained through the following operations: the fresh or dried Moringa oleifera fruit is removed from the pods, crushed and passed through a 20-mesh medicine sieve, and the solid-to-liquid ratio kg/L is 1:8, and anhydrous Ethanol, leaching at room temperature for 60 hours, stirring intermittently, suction filtration once every 12h, continuing leaching after replacing absolute ethanol, collecting Moringa oleifera seed residue, combining the leaching filtrate, concentrating under reduced pressure at 45°C, and evaporating the solvent to obtain spicy Moringa seed oil is obtained.

The Moringa oleifera seed protein is prepared by the following operations: dry the Moringa oleifera seed dregs at 70°C for 2 hours, pulverize until all the powder passes through a 20-mesh sieve, add distilled water according to the solid-liquid ratio kg/L as 1:15, and use a concentration of Use 1mol/L NaOH to adjust the pH of the solution to 9, then heat and stir in a water bath for 1 hour, the temperature of the water bath is 50°C, let it stand for stratification, adjust the pH of the supernatant to 4-5 with HCl, take the precipitate, filter it with suction, and crush it , all pass through a 200 mesh sieve to obtain Moringa seed protein.

The Moringa flower pure dew is obtained through the following operations: use fresh Moringa flower petals, add distilled water to soak, then extract with steam distillation, distill for 2 hours, and the Moringa flower essential oil is condensed by a condenser with water vapor until the pepper The oleifera essential oil is no longer precipitated, and the heating is stopped; the essential oil and moringa flower hydrosol are extracted at the same time, and placed in a refrigerator at 4°C to refrigerate and stratify.

Example 3

Moringa anti-oxidant essence consists of the following components by mass: 8 parts of Moringa seed oil, 20 parts of Moringa seed protein, 2 parts of Moringa fruit acid, 20 parts of Moringa flower hydrosol, 2 parts of emulsifier, 1 part of hyaluronic acid, 5 parts of mannan, 0.05 part of antibacterial agent, 0.05 part of plant essential oil, 61.9 parts of deionized water.

The Moringa oleifera seed oil is obtained through the following operations: the fresh or dried Moringa oleifera fruit is removed from the pods, crushed and passed through a 20-mesh drug sieve, and the solid-to-liquid ratio kg/L is 1:5, adding anhydrous Ethanol, leaching at room temperature for 48 hours, stirring intermittently, suction filtration once every 12h, continuing leaching after replacing absolute ethanol, collecting Moringa oleifera seed residue, combining the leaching filtrate, concentrating at 40°C under reduced pressure, and evaporating the solvent to obtain spicy Moringa seed oil is obtained.

The Moringa oleifera seed protein is obtained through the following operations: drying the moringa oleifera seed dregs at 60-80°C for 2-3 hours, pulverizing until all the powder passes through a 20-mesh sieve, and the solid-to-liquid ratio kg/L is calculated as 1:(10 ~20) Add distilled water, adjust the pH of the solution to 8~11 with NaOH with a concentration of 1mol/L, then heat and stir in a water bath for extraction for 1~2h, the temperature of the water bath is 40~60°C, let it stand for stratification, and use HCl for the supernatant Adjust the pH to 4-5, take the precipitate, suction filter, pulverize, and pass through a 200-mesh sieve to obtain Moringa seed protein.

The Moringa flower pure dew is prepared by the following operations: use fresh Moringa flower petals, add distilled water to soak, and then extract by steam distillation, distill for 2-3 hours, and the Moringa flower essential oil is condensed by the condenser along with the water vapor. Stop heating until the moringa flower essential oil is no longer precipitated; the essential oil and the moringa flower hydrosol are extracted at the same time, and placed in a refrigerator at 4-5°C to refrigerate and stratify. .

The moringa fruit acid is obtained through the following operations: extruding fresh moringa fruit pods to obtain a stock solution of moringa fruit pods, and the volume ratio of the stock solution of moringa oleifera fruit pods to concentrated sulfuric acid ethanol solution is 1:(3～2 ), add 1-5% concentrated sulfuric acid ethanol solution to the stock solution of Moringa oleifera pods, and precipitate out, put the mixed solution in a 4-6°C refrigerator and let it stand for 6-12 hours, until the precipitate is completely precipitated, then add sodium hydroxide , adjust the pH to 10-11, remove the precipitate, take the supernatant, add 3-5 times the volume of hydrochloric acid with a concentration of 1-5wt%, let it stand for recrystallization, and refine it in a refrigerator at 4-6°C for 6-12 hours. Filter to obtain moringa acid.

Example 4

Moringa anti-oxidant moisturizing soap is composed of the following components in parts by mass: 4 parts of Moringa seed oil, 0.01 part of orthophosphoric acid, 0.03 part of disodium edetate, 1 part of sodium lauryl sulfate, and 10 parts of glycerin , 44.95 parts of deionized water, 0.01 part of Moringa flower essential oil, and 40 parts of soap base.

Heat and melt the soap base, add Moringa oleifera seed oil, chelating agent disodium edetate, foaming agent sodium lauryl sulfate, dissolve glycerin in deionized water to obtain a mixed water phase, and heat the mixed water phase Stir slowly under the condition (60-80°C) and add to the melted soap base. After stirring evenly, add Moringa flower essential oil and preservative orthophosphoric acid, pour into the handmade soap model, and put it in a refrigerator at 4-6°C for 4-6 hours. Take the handmade soap out of the model, pack it, and store it in a cool place.

The Moringa oleifera seed oil is obtained through the following operations: the fresh or dried Moringa oleifera fruit is removed from the pods, crushed and passed through a 20-mesh medicine sieve, and the solid-to-liquid ratio kg/L is 1:10, adding anhydrous Ethanol, leaching at room temperature for 72 hours, stirring intermittently, suction filtration once every 12h, continuing leaching after replacing absolute ethanol, collecting Moringa oleifera seed residue, combining the leaching filtrate, concentrating at 50°C under reduced pressure, and evaporating the solvent to obtain spicy Moringa seed oil is obtained.

The DPPH free radical scavenging activity assay result of embodiment 1 gained Moringa oleifera seed oil is as follows:

Table 1 Determination of DPPH free radical scavenging activity of Moringa oil Concentrationug/ml 100 200 300 400 500 600 700 800 900 1000 IP% 25.16 45.5 58.4 73.2 86.07 91.1 93.6 94.4 94.99 95.94

The Moringa Antioxidant Spray (A), Moringa Antioxidant Moisturizing Emulsion (B), and Moringa Antioxidant Essence (C) obtained in the above examples have passed the antioxidant test and moisturizing test and commercially available similar products, such as a domestic rose The difference between antioxidant spray (D) and a DIY homemade antioxidant moisturizing milk (E) is shown in the table below:

Table 2 Determination of DPPH free radical scavenging activity of Moringa cosmetics No. A B C D. E. IP% 87.1 76.5 58.4 73.2 86.07

Claims (7)

1. a kind of anti-oxidant moisture-keeping cosmetics of Moringa, it is characterised in that be made up of the component of following mass parts：Seed oil of Moringa oleigera 0~10 Part, 0~20 part of moringa seeds albumen, 0~2 part of Moringa tartaric acid, 0~20 part of hydrosol of Moringa flower, wherein 57.1~96 parts of auxiliary material, Moringa Seed oil, moringa seeds albumen, Moringa tartaric acid are zero when different with Moringa flower hydrosol.

2. the anti-oxidant moisture-keeping cosmetics of Moringa according to claim 1, it is characterised in that：The seed oil of Moringa oleigera passes through following Operation is made：Moringa fruit that is fresh or drying is removed into outer Fruit pod, is sieved, is calculated as by solid-to-liquid ratio kg/L by 20 mesh medicines after pulverizing 1:（5~10）, absolute ethyl alcohol is added, room temperature is extracted 48~72 hours, intermittent stirring, per 12h suction filtrations once, changes absolute ethyl alcohol Continue to extract afterwards, collect moringa seeds slag, merge extraction filtrate, be concentrated under reduced pressure with 40~50 DEG C, volatilize and moringa seeds are obtained after solvent Oil, that is, obtain seed oil of Moringa oleigera.

3. the anti-oxidant moisture-keeping cosmetics of Moringa according to claim 1, it is characterised in that：The moringa seeds albumen is under Row operation is made：Moringa seeds slag is dried into 2~3h at 60~80 DEG C, whole powder are crushed to by 20 mesh sieves, by solid-to-liquid ratio Kg/L is calculated as 1:（10~20）Distilled water is added, the NaOH for being 1mol/L with concentration adjusts pH value of solution to 8~11, then in water-bath Middle heating stirring extracts 1~2h, and 40~60 DEG C of bath temperature, stratification, supernatant adjusts pH to 4~5 with HCl, takes precipitation Through suction filtration, crush, all by 200 mesh sieves, that is, obtain moringa seeds albumen.

4. the anti-oxidant moisture-keeping cosmetics of Moringa according to claim 1, it is characterised in that：The Moringa tartaric acid passes through following Operation is made：Fresh Moringa Fruit pod is extruded, Moringa Fruit pod stoste is obtained, it is molten by Moringa Fruit pod stoste and concentrated sulfuric acid ethanol The volume ratio of liquid is 1:（3~2）, 1~5% concentrated sulfuric acid ethanol solution is added into Moringa Fruit pod stoste, precipitation is separated out, this is mixed Close liquid and be put into 4~6 DEG C of refrigerators 6~12h of standing, thing to be precipitated is separated out completely, is added sodium hydroxide, is adjusted pH to 10~11, go Precipitation, takes supernatant, and the concentration for adding 3~5 volumes times is 1~5wt% hydrochloric acid, recrystallization is stood, in 4~6 DEG C of refrigerators Refined 6~12h, filtering obtains Moringa tartaric acid.

5. the anti-oxidant moisture-keeping cosmetics of Moringa according to claim 1, it is characterised in that：The Moringa spends hydrosol under Row operation is made：Petal is spent using fresh Moringa, distilled water immersion is added, then is extracted with steam distillation, distillation 2 ~3h, Moringa flower essential oil is condensed pipework condensation with vapor, until Moringa flower essential oil is no longer separated out, stops heating；Essential oil and peppery Wood flower hydrosol is extracted simultaneously, places and layering is refrigerated in 4~5 DEG C of refrigerators, and upper strata is Moringa flower essential oil, and lower aqueous solution is Moringa spends hydrosol.

6. the anti-oxidant moisture-keeping cosmetics of Moringa according to claim 1, it is characterised in that：The auxiliary material includes water, emulsification One in agent, plant hydrosol, plant antimicrobial, plants essential oil, Chinese medicinal material extract, chelating agent, foaming agent, preservative, soap base Plant or several.

7. the anti-oxidant moisture-keeping cosmetics of Moringa according to claim 1, it is characterised in that：The anti-oxidant moisturizing of Moringa Cosmetic includes the anti-oxidant spraying of Moringa, the anti-oxidant moisturizing emulsion of Moringa, the anti-oxidant Essence of Moringa, Moringa essential oil soap.