CN107152478A - A kind of basalt fibre brake block and preparation method thereof - Google Patents
A kind of basalt fibre brake block and preparation method thereof Download PDFInfo
- Publication number
- CN107152478A CN107152478A CN201710390383.1A CN201710390383A CN107152478A CN 107152478 A CN107152478 A CN 107152478A CN 201710390383 A CN201710390383 A CN 201710390383A CN 107152478 A CN107152478 A CN 107152478A
- Authority
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- Prior art keywords
- basalt fibre
- brake block
- weight
- parts
- powder
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920002748 Basalt fiber Polymers 0.000 title claims abstract description 87
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 23
- 239000011159 matrix material Substances 0.000 claims abstract description 20
- 239000000945 filler Substances 0.000 claims abstract description 18
- 239000000835 fiber Substances 0.000 claims abstract description 15
- 239000000843 powder Substances 0.000 claims description 65
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical group [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 claims description 37
- 238000010792 warming Methods 0.000 claims description 30
- 229920001568 phenolic resin Polymers 0.000 claims description 29
- 239000002994 raw material Substances 0.000 claims description 20
- SZVJSHCCFOBDDC-UHFFFAOYSA-N iron(II,III) oxide Inorganic materials O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 claims description 14
- 239000005011 phenolic resin Substances 0.000 claims description 13
- 239000004593 Epoxy Substances 0.000 claims description 11
- 244000226021 Anacardium occidentale Species 0.000 claims description 10
- MBMLMWLHJBBADN-UHFFFAOYSA-N Ferrous sulfide Chemical compound [Fe]=S MBMLMWLHJBBADN-UHFFFAOYSA-N 0.000 claims description 10
- 239000004902 Softening Agent Substances 0.000 claims description 10
- 235000020226 cashew nut Nutrition 0.000 claims description 10
- 239000010459 dolomite Substances 0.000 claims description 10
- 229910000514 dolomite Inorganic materials 0.000 claims description 10
- 239000000428 dust Substances 0.000 claims description 10
- 239000010433 feldspar Substances 0.000 claims description 10
- 239000005995 Aluminium silicate Substances 0.000 claims description 9
- 229910001369 Brass Inorganic materials 0.000 claims description 9
- 229920000459 Nitrile rubber Polymers 0.000 claims description 9
- 239000004734 Polyphenylene sulfide Substances 0.000 claims description 9
- 235000012211 aluminium silicate Nutrition 0.000 claims description 9
- 239000010951 brass Substances 0.000 claims description 9
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical group O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 9
- 229920000069 polyphenylene sulfide Polymers 0.000 claims description 9
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 8
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims description 8
- 239000000314 lubricant Substances 0.000 claims description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 7
- -1 boron modified phenolic resin Chemical class 0.000 claims description 7
- 239000010439 graphite Substances 0.000 claims description 7
- 229910002804 graphite Inorganic materials 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- 239000003921 oil Substances 0.000 claims description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- 229910021536 Zeolite Inorganic materials 0.000 claims description 6
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 6
- 239000010457 zeolite Substances 0.000 claims description 6
- 239000006229 carbon black Substances 0.000 claims description 5
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 claims description 5
- 235000014571 nuts Nutrition 0.000 claims description 5
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 5
- 239000004952 Polyamide Substances 0.000 claims description 4
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 4
- 239000005083 Zinc sulfide Substances 0.000 claims description 4
- OMZSGWSJDCOLKM-UHFFFAOYSA-N copper(II) sulfide Chemical compound [S-2].[Cu+2] OMZSGWSJDCOLKM-UHFFFAOYSA-N 0.000 claims description 4
- 239000000395 magnesium oxide Substances 0.000 claims description 4
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 4
- 229920002647 polyamide Polymers 0.000 claims description 4
- DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical compound [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 claims description 4
- 238000005299 abrasion Methods 0.000 claims description 3
- 229940007424 antimony trisulfide Drugs 0.000 claims description 3
- NVWBARWTDVQPJD-UHFFFAOYSA-N antimony(3+);trisulfide Chemical compound [S-2].[S-2].[S-2].[Sb+3].[Sb+3] NVWBARWTDVQPJD-UHFFFAOYSA-N 0.000 claims description 3
- 229910052796 boron Inorganic materials 0.000 claims description 3
- 229910052976 metal sulfide Inorganic materials 0.000 claims description 3
- 229910052982 molybdenum disulfide Inorganic materials 0.000 claims description 3
- 239000004814 polyurethane Substances 0.000 claims description 3
- 229920002635 polyurethane Polymers 0.000 claims description 3
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 claims description 2
- 125000002777 acetyl group Chemical class [H]C([H])([H])C(*)=O 0.000 claims description 2
- 229910001610 cryolite Inorganic materials 0.000 claims description 2
- 239000010445 mica Substances 0.000 claims description 2
- 229910052618 mica group Inorganic materials 0.000 claims description 2
- 238000012986 modification Methods 0.000 claims description 2
- 229920005989 resin Polymers 0.000 claims description 2
- 239000010455 vermiculite Substances 0.000 claims description 2
- 229910052902 vermiculite Inorganic materials 0.000 claims description 2
- 235000019354 vermiculite Nutrition 0.000 claims description 2
- 229920002554 vinyl polymer Polymers 0.000 claims description 2
- 239000011787 zinc oxide Substances 0.000 claims description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 1
- 229920003986 novolac Polymers 0.000 claims 1
- 239000011347 resin Substances 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- 239000010703 silicon Substances 0.000 claims 1
- 239000004575 stone Substances 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 14
- 238000000034 method Methods 0.000 abstract description 8
- 230000007613 environmental effect Effects 0.000 abstract description 4
- 231100000252 nontoxic Toxicity 0.000 abstract description 4
- 230000003000 nontoxic effect Effects 0.000 abstract description 4
- 230000001681 protective effect Effects 0.000 abstract description 4
- 239000000203 mixture Substances 0.000 description 45
- 229920000180 alkyd Polymers 0.000 description 8
- 239000010466 nut oil Substances 0.000 description 8
- 238000001816 cooling Methods 0.000 description 7
- 235000013824 polyphenols Nutrition 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- 239000002783 friction material Substances 0.000 description 5
- 235000019198 oils Nutrition 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- 239000003365 glass fiber Substances 0.000 description 4
- 239000011435 rock Substances 0.000 description 4
- 229910052725 zinc Inorganic materials 0.000 description 4
- 239000011701 zinc Substances 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 238000005470 impregnation Methods 0.000 description 3
- 238000009413 insulation Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 241001163600 Bathylaco nigricans Species 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 229920006305 unsaturated polyester Polymers 0.000 description 2
- 238000004073 vulcanization Methods 0.000 description 2
- 239000010456 wollastonite Substances 0.000 description 2
- 229910052882 wollastonite Inorganic materials 0.000 description 2
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical group C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 1
- 229920000049 Carbon (fiber) Polymers 0.000 description 1
- 239000004372 Polyvinyl alcohol Substances 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229920006231 aramid fiber Polymers 0.000 description 1
- 239000010425 asbestos Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004917 carbon fiber Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000002657 fibrous material Substances 0.000 description 1
- LCDFWRDNEPDQBV-UHFFFAOYSA-N formaldehyde;phenol;urea Chemical class O=C.NC(N)=O.OC1=CC=CC=C1 LCDFWRDNEPDQBV-UHFFFAOYSA-N 0.000 description 1
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 description 1
- 229910052738 indium Inorganic materials 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000012783 reinforcing fiber Substances 0.000 description 1
- 239000012779 reinforcing material Substances 0.000 description 1
- 229910052895 riebeckite Inorganic materials 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
- 238000005491 wire drawing Methods 0.000 description 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16D—COUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
- F16D69/00—Friction linings; Attachment thereof; Selection of coacting friction substances or surfaces
- F16D69/02—Composition of linings ; Methods of manufacturing
- F16D69/025—Compositions based on an organic binder
- F16D69/026—Compositions based on an organic binder containing fibres
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16D—COUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
- F16D69/00—Friction linings; Attachment thereof; Selection of coacting friction substances or surfaces
- F16D69/02—Composition of linings ; Methods of manufacturing
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16D—COUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
- F16D2200/00—Materials; Production methods therefor
- F16D2200/0004—Materials; Production methods therefor metallic
- F16D2200/0026—Non-ferro
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16D—COUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
- F16D2200/00—Materials; Production methods therefor
- F16D2200/0034—Materials; Production methods therefor non-metallic
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16D—COUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
- F16D2200/00—Materials; Production methods therefor
- F16D2200/0034—Materials; Production methods therefor non-metallic
- F16D2200/0052—Carbon
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16D—COUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
- F16D2200/00—Materials; Production methods therefor
- F16D2200/006—Materials; Production methods therefor containing fibres or particles
- F16D2200/0065—Inorganic, e.g. non-asbestos mineral fibres
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16D—COUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
- F16D2200/00—Materials; Production methods therefor
- F16D2200/0082—Production methods therefor
- F16D2200/0086—Moulding materials together by application of heat and pressure
Landscapes
- Engineering & Computer Science (AREA)
- General Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Braking Arrangements (AREA)
Abstract
The present invention provides a kind of basalt fibre brake block and preparation method thereof, is related to auto parts machinery field.The preparation method of basalt fibre brake block, including：The filler of the basalt fibre of 30~60 parts by weight, the bonding matrix, the rubbing agent of 10~25 parts by weight and 10~35 parts by weight of 10~20 parts by weight is well mixed, at 150~180 DEG C of temperature and 10~30MPa pressure after hot-forming 1~10min, 8~10h of curing process at a temperature of 100~200 DEG C.This basalt fibre brake block is using natural fiber basalt fibre as framework material, and coordinating bonding matrix, rubbing agent and filler to be made, lightweight is inexpensive, higher and antifriction damage tolerant the brake block of intensity.Meanwhile, the advantages of possessing nontoxic and ecological, environmental protective.
Description
Technical field
The present invention relates to auto parts machinery field, and more particularly to a kind of basalt fibre brake block and preparation method thereof.
Background technology
At present, the research and application that the friction material of automobile brake sheet is directed to both at home and abroad are still to concentrate on：Material composition, system
In terms of taking method, process route, structure design and analysis of experiments.But the above is mainly for existing asbestos less friction
The fields such as material, semimetal friction material.
In addition, mainly have a glass fibre and organic synthetic fibers as brake friction material reinforcing fiber, such as carbon fiber,
Aramid fiber etc., these fibrous material performances are homogeneous, are ideal reinforcing materials.But their raw material petroleum resources
But increasingly depleted, while the manufacturing process of fiber can also consume mass energy, wear debris pollution environment.Exploitation meets brake block
Friction material application new-type friction material it is too impatient to wait.
The content of the invention
It is an object of the invention to provide a kind of basalt fibre brake block, using natural fiber basalt fibre as skeleton material
Material, coordinating bonding matrix, rubbing agent and filler to be made, lightweight is inexpensive, higher and antifriction damage tolerant the brake block of intensity.Meanwhile, possess
The advantages of nontoxic and ecological, environmental protective.
Another object of the present invention is to provide a kind of preparation method of basalt fibre brake block, with quick and a large amount of systems
Take above-mentioned basalt fibre brake block.
The present invention is solved its technical problem and realized using following technical scheme.
The present invention proposes a kind of basalt fibre brake block, is mainly made up of following raw material：The Black Warrior of 30~60 parts by weight
The filler for being bonded matrix, the rubbing agent of 10~25 parts by weight and 10~35 parts of parts by weight of rock fiber, 10~20 parts by weight.
A kind of preparation method of basalt fibre brake block, including：
By the basalt fibre of 30~60 parts by weight, 10~20 parts by weight bonding matrix, 10~25 parts by weight friction
The filler of agent and 10~35 parts by weight is well mixed, hot-forming 1 at 150~180 DEG C of temperature and 10~30MPa pressure~
After 10min, 8~10h of curing process at a temperature of 100~200 DEG C.
The beneficial effect of the embodiment of the present invention is：
The basalt fibre brake block of the embodiment of the present invention coordinates bonding using natural fiber basalt fibre as framework material
The obtained lightweight of matrix, rubbing agent and filler is inexpensive, higher and antifriction damage tolerant the brake block of intensity.Meanwhile, possess it is nontoxic and
The advantages of ecological, environmental protective.
The preparation method of the basalt fibre brake block of the embodiment of the present invention, can quickly and largely produce the above-mentioned Black Warrior
Rock fiber brake block.With it is simple to operate and safe and efficient the features such as.
Embodiment
, below will be in the embodiment of the present invention to make the purpose, technical scheme and advantage of the embodiment of the present invention clearer
Technical scheme be clearly and completely described.Unreceipted actual conditions person, builds according to normal condition or manufacturer in embodiment
The condition of view is carried out.Agents useful for same or the unreceipted production firm person of instrument, are the conventional production that can be obtained by commercially available purchase
Product.
Basalt fibre brake block of the embodiment of the present invention and preparation method thereof is specifically described below.
A kind of basalt fibre brake block, is mainly made up of following raw material：The basalt fibre of 30~60 parts by weight, 10~
The filler for being bonded matrix, the rubbing agent of 10~25 parts by weight and 10~35 parts of parts by weight of 20 parts by weight.
Basalt fibre is the framework material of this basalt fibre brake block, can be made by the following manner：
Using basalt ore as raw material, broken rear basalt ore is melted at a temperature of 1450 DEG C~1550 DEG C
Melt, obtain fused mass.Fused mass is first pulled into after crude fibre by bushing, then crude fibre is drawn into continuously by wire drawing machine
Basalt fibre.That is, this basalt fibre is the non-twist coarse sand of basalt fibre.
Obtained basalt fibre is delivered into Nanjing Glass Fibre Research and Design Institute Product Quality Verification Centers (i.e.：National glass fibre
Product quality supervision and inspection center), performance detection, its survey report are carried out to basalt fibre according to GB/T 25-45-2010
For：Glass quality inspection (TSW) word, (16060418) number.Its testing result such as table 1.It is appreciated that basalt fibre possesses such as table
1 technical indicator.
The basalt fibre technical indicator of table 1
Note 1：Alkali resistance treatment conditions are：Sample soaks in 60 DEG C of temperature and 1.0mol/L NaOH solution
120min。
Heatproof treatment conditions are：Sample places 120min at a temperature of 300 DEG C.
Note 2：Impregnation yarn sample uses SW2511-1A/BS epoxy resin.Condition of cure：24h is handled at a temperature of 25 DEG C,
8h is handled at a temperature of 80 DEG C.Impregnation yarn tensile strength and tensile modulus of elasticity are using glass density as 2.60g/cm3Calculated.
Note 3：Bar-shaped composite uses the P65-901 unsaturated polyester (UP) trees that Nanjing DSM resin Co., Ltd produces
Fat makes.Condition of cure：24h is handled at a temperature of 24h, 80 DEG C are handled at a temperature of 20~20 DEG C.It is bar-shaped to meet material glass
Fiber quality content is 63.6%.
As it can be seen from table 1 the requirement that the basic technical indicator of basalt fibre is up to state standards.Also, basalt
Temperature tolerance, alkali resistance and the impregnation tensile property of fiber further illustrate that it can be applied to field of brake pad, and are used as the Black Warrior
The framework material of rock fiber brake block.It is appreciated that the diameter of this basalt fibre is advisable with 10~20 μm.
It is bonded matrix and is selected from least one of phenolic resin and phenol-formaldehyde resin modified.It is appreciated that bonding matrix can be with
Phenolic resin is independently chosen from, phenol-formaldehyde resin modified can also be independently chosen from, phenolic resin and phenol-formaldehyde resin modified is also selected from
Mixture.Preferably, bonding matrix is selected from phenol-formaldehyde resin modified.By from being modified changing of obtaining to phenolic resin
Property phenolic resin, it is ensured that preparation basalt fibre brake raw material between bonding while can reduce bonding matrix it is hard
Fragility.
Wherein, phenol-formaldehyde resin modified is selected from cashew nut oil modified alkyd resin, boron modified phenolic resin, polyamide modified phenol
Urea formaldehyde, dicyandiamide modified phenolic resin, epoxy modified phenolic resin, Pioloform, polyvinyl acetal phenol-formaldehyde resin modified, melamine-
At least one of cashew nut shell oil double-modification phenolic resin, epoxy phenolics and polyurethane phenolic resin.That is, modified phenolic resin
Fat can select any one of above-mentioned a variety of phenol-formaldehyde resin modifieds, can also select in above-mentioned a variety of phenol-formaldehyde resin modifieds extremely
The mixture of few two kinds arbitrary proportion.
Rubbing agent is that increasing rubs agent.Rubbing agent is selected from carborundum, high wear-resistant carbon black, white carbon, zinc oxide, magnesia, oxygen
Change at least one of aluminium, magnetite powder, brass miberal powder, troilite powder, chromite powder, feldspar powder, dolomite dust and zeolite powder.
As a kind of preferred scheme, rubbing agent is selected from least one of carborundum, high wear-resistant carbon black and white carbon and oxygen
Change the mixture of at least one of zinc, magnesia, aluminum oxide, magnetite powder, brass miberal powder, troilite powder and chromite powder.
Further preferably, the mixture selected from least one of carborundum, high wear-resistant carbon black and white carbon with magnetite powder.
As another preferred scheme, rubbing agent is selected from least one of feldspar powder, dolomite dust and zeolite powder and oxygen
Change the mixture of at least one of zinc, magnesia, aluminum oxide, magnetite powder, brass miberal powder, troilite powder and chromite powder.
Further preferably, the mixture selected from least one of feldspar powder, dolomite dust and zeolite powder with magnetite powder.
By above-mentioned preferred scheme, the filler of this basalt fibre brake block includes metal packing.Therefore, prepare
Basalt fibre brake block be a kind of semi-metallic brake pad.
Hold above-mentioned, by adding rubbing agent in the raw material to basalt fibre brake block, basalt fibre can be adjusted and stopped
The piece frictional behaviour of car, improves its friction system in cold stage (- 250 DEG C of room temperature) and hot stage (250 DEG C~400 DEG C)
Number, to ensure the extensive purposes and stable performance of basalt fibre brake block.
Filler is selected from least one of kaolin, wollastonite, blanc fixe, vermiculite power, mica powder and cryolite powder.Fill out
Material can as space between framework material basalt fibre supplement, moreover, the frictional behaviour of basalt fibre can be strengthened
And impact resistance.
For the performance indications of further basalt fibre brake block, its raw material proportioning is further optimized, including：35~
The basalt fibre of 50 parts by weight, the bonding matrix of 12~15 parts by weight, the rubbing agent of 10~20 parts by weight and 20~30 weight
The filler of part.By the raw material proportioning for optimizing basalt fibre brake block, it is possible to increase its hardness, wear-resisting, anti-corrosion and life-span.
In another implementation of this basalt fibre brake block, raw material also includes lubricant.By fine to basalt
Lubricant is added in the raw material for tieing up brake block, friction, lubrication film can be formed in the frictional interface of basalt fibre brake block, both
The coefficient of friction of basalt fibre brake block can be reduced can reduce the abrasion of basalt fibre brake block again, so as to improve the Black Warrior
The service life of rock fiber brake block.In order to ensure coordination and the balance of basalt fibre brake block raw material proportioning, lubricant is with 5
The addition of~15 parts by weight is advisable.
Lubricant is selected from least one of Delanium, metal sulfide, crystalline flake graphite and molybdenum disulfide.Wherein, it is golden
Belong to sulfide and be selected from least one of zinc sulphide, antimony trisulfide, copper sulfide, molybdenum sulfide.
In the another implementation of this basalt fibre brake block, softening agent is also included in raw material.By adding softening
Agent can reduce hardness and the abrasion of basalt fibre brake block, meanwhile, basalt fibre brake block can be improved at high temperature
Stability.Softening agent is advisable with the addition of 0.1~1 parts by weight.
Softening agent selects at least one of nitrile rubber and polyphenylene sulfide.Preferably, softening agent is selected from nitrile rubber
With the mixture of polyphenylene sulfide.Wherein, the content of acrylonitrile unit can be 15~50wt% in nitrile rubber；Polyphenylene sulfide
Crystallinity can be 55~65%.
Further, it is also possible to add above-mentioned lubricant and softening agent simultaneously in the raw material of basalt fibre brake block.
A kind of preparation method of basalt fibre brake block, including：
Raw material is on the waiting list, includes basalt fibre, the bonding matrix of 10~20 parts by weight, 10~25 weights of 30~60 parts by weight
Measure the rubbing agent of part and the filler of 10~35 parts by weight.
Above-mentioned basalt fibre, bonding matrix, rubbing agent and filler are well mixed, mixture is obtained.
Said mixture is carried out hot-forming.Specifically, hot-forming condition is：Temperature is 150~180 DEG C, pressure
Power is 10~30MPa, and the time is 1~10min.Preferably, hot-forming condition is：Temperature is 150~170 DEG C, and pressure is
12~25MPa, the time is 1.5~8min.It is highly preferred that hot-forming condition is：Temperature is 150~160 DEG C, and pressure is
13~20MPa, the time is 2~7min.
Mixture after will be hot-forming carries out 5~10h of heat treatment at a temperature of 100~200 DEG C and is made.Heat treatment
By the process of heating, insulation and cooling, to obtain a kind of metal heat processing technique of intended tissue and pre-determined characteristics.Specifically
Ground, heat treatment heating, insulation and cooling procedure include：
First stage：In 0.5~1.5h, will be hot-forming after mixture be warming up to 100~120 DEG C, it is and warm herein
Spend 1~3h of scope inside holding；
Second stage：In 0.5~1h, the mixture after the first stage is handled is warming up to 150~180 DEG C, and
In 2~4h of this temperature range inside holding；
Phase III, in 0.5~1.5h, the mixture after second stage is handled is warming up to 200 DEG C, and herein
Temperature keeps 0.5~1.5h；Come out of the stove after cooling.
Hold above-mentioned, be the preparation for completing basalt fibre brake block by said process.It is directed to above-mentioned preferred side
Case, can by the basalt fibre of 30~60 parts by weight, 10~20 parts by weight bonding matrix, 10~25 parts by weight friction
After agent, the filler of 10~35 parts by weight, the lubricant of 5~15 parts by weight and 0.1~1 parts by weight softening agent are well mixed, carry out
Above-mentioned hot-forming and heat treatment.
It should be further stated that, prepare the feelings that the various raw materials of basalt fibre are engaged with mean particle diameter
Condition is advisable.By from the close various materials of specification, ensure that raw material mixing and scattered uniform, so as to ensure that the Black Warrior
The preparation effect of rock fiber brake block.
The feature and performance to the present invention are described in further detail with reference to embodiments.
Embodiment 1
By 30kg basalt fibre, 5kg cashew nut oil modified alkyd resin, 5kg boron modified phenolic resin, 2kg
High wear-resistant carbon black, 4kg magnetite powder, 4kg troilite powders, 10kg kaolin, 1kg Delanium, 5kg vulcanization
The polyphenylene sulfide of zinc, 0.1kg nitrile rubber and 0.1kg is well mixed, and obtains mixture.
By mixture at a temperature of 150 DEG C and under 15MPa pressure after hot-forming 5min, obtain it is hot-forming after
Mixture.
Mixture after will be hot-forming is heat-treated as follows successively：100 DEG C are warming up in 1h enough and are protected in the temperature
Warm 1.5h；160 DEG C are warming up in 1h and in this temperature 2.5h；200 DEG C are warming up in 0.5h and in this temperature 0.5h；
Afterwards, come out of the stove, produce after cooling.
Embodiment 2
By 40kg basalt fibre, 5kg cashew nut oil modified alkyd resin, 5kg epoxy modified phenolic resin,
4kg epoxy phenolics, 1kg feldspar powder, 1kg dolomite dust, 10kg magnetite powder, 15kg blanc fixe, 2kg
Delanium, 4kg copper sulfide, 2kg crystalline flake graphite and 0.5kg softening agent be well mixed, obtain mixture.
By mixture at a temperature of 155 DEG C and under 18MPa pressure after hot-forming 4min, obtain it is hot-forming after
Mixture.
Mixture after will be hot-forming is heat-treated as follows successively：105 DEG C are warming up in 1h enough and are protected in the temperature
Warm 1h；170 DEG C are warming up in 0.75h and in this temperature 3h；200 DEG C are warming up in 0.5h and in this temperature
0.75h；Afterwards, come out of the stove, produce after cooling.
Embodiment 3
By 50kg basalt fibre, 10kg polyamide modified phenolic resin, 6kg polyurethane phenolic resin, 3kg
White carbon, 8kg magnetite powder, 3kg zeolite powder, 20kg kaolin, 5kg Delanium, 5kg crystalline flake graphite,
0.2kg nitrile rubber and 0.5kg polyphenylene sulfide are well mixed, obtain mixture.
By mixture at a temperature of 170 DEG C and under 20MPa pressure after hot-forming 3min, obtain it is hot-forming after
Mixture.
Mixture after will be hot-forming is heat-treated as follows successively：100 DEG C are warming up to enough and in the temperature in 1.25h
Degree insulation 1.25h；170 DEG C are warming up in 1h and in this temperature 3h；200 DEG C are warming up in 1h and in this temperature
0.75h；Afterwards, come out of the stove, produce after cooling.
Embodiment 4
By 40kg basalt fibre, 1kg phenolic resin, 2kg cashew nut oil modified alkyd resin, 3kg polyamides
Amine-modified phenol-formaldehyde resin, 4kg dicyandiamide modified phenolic resin, 5kg epoxy modified phenolic resin, 5kg polyvinyl alcohol contracting
Aldehyde phenol-formaldehyde resin modified, 1kg carborundum, 2kg aluminum oxide, 2kg magnetite powder, 2kg brass miberal powder, 3kg sulphur
Iron Ore Powder, 3kg chromite powder, 1kg feldspar powder, 1kg dolomite dust, 1kg zeolite powder, 5kg kaolin, 10kg
Wollastonite, 10kg blanc fixe, 2kg Delanium, 2kg crystalline flake graphite, 2kg molybdenum disulfide, 2kg vulcanization
Zinc, 2kg antimony trisulfide, 2kg copper sulfide, 0.4kg nitrile rubber and 0.6kg polyphenylene sulfide are well mixed, and are mixed
Thing.
By mixture at a temperature of 160 DEG C and under 22MPa pressure after hot-forming 2min, obtain it is hot-forming after
Mixture.
Mixture after will be hot-forming is heat-treated as follows successively：100 DEG C are warming up to enough and in the temperature in 1.5h
It is incubated 1h；170 DEG C are warming up in 0.75h and in this temperature 4h；200 DEG C are warming up in 1.5h and in this temperature
0.5h；Afterwards, come out of the stove, produce after cooling.
Embodiment 5
35kg basalt fibre, 6kg cashew nut oil modified alkyd resin, 3kg melamine-cashew nut shell oil is double
Phenol-formaldehyde resin modified, 3kg epoxy phenolics, 2kg magnetite powder, 2kg brass miberal powder, 2kg troilite powder, 2kg
Chromite powder, 2kg feldspar powder, 1kg dolomite dust, 5.5kg kaolin, 3kg blanc fixe, 4kg ice crystal
Powder, 2kg Delanium, 3kg crystalline flake graphite, 2kg zinc sulphide, 0.15kg nitrile rubber and 2kg polyphenylene sulfide are mixed
Close uniform, obtain mixture.
By mixture at a temperature of 150 DEG C and under 15MPa pressure after hot-forming 5min, obtain it is hot-forming after
Mixture.
Mixture after will be hot-forming is heat-treated as follows successively：100 DEG C are warming up in 1h enough and are protected in the temperature
Warm 1h；160 DEG C are warming up in 1h and in this temperature 4h；200 DEG C are warming up in 1h and in this temperature 1h；Afterwards, drop
Come out of the stove, produce after temperature.
Embodiment 6
35kg basalt fibre, 6kg cashew nut oil modified alkyd resin, 3kg melamine-cashew nut shell oil is double
Phenol-formaldehyde resin modified, 3kg epoxy phenolics, 2kg magnetite powder, 2kg brass miberal powder, 2kg troilite powder, 2kg
Chromite powder, 2kg feldspar powder, 1kg dolomite dust, 5.5kg kaolin, 3kg blanc fixe and 4kg ice crystal
Powder is well mixed, and obtains mixture.
By mixture at a temperature of 150 DEG C and under 15MPa pressure after hot-forming 5min, obtain it is hot-forming after
Mixture.
Mixture after will be hot-forming is heat-treated as follows successively：100 DEG C are warming up in 1h enough and are protected in the temperature
Warm 1h；160 DEG C are warming up in 1h and in this temperature 4h；200 DEG C are warming up in 1h and in this temperature 1h；Afterwards, drop
Come out of the stove, produce after temperature.
Comparative example 1
35kg basalt fibre, 6kg cashew nut oil modified alkyd resin, 3kg melamine-cashew nut shell oil is double
Phenol-formaldehyde resin modified, 3kg epoxy phenolics, 2kg magnetite powder, 2kg brass miberal powder, 2kg troilite powder, 2kg
Chromite powder, 2kg feldspar powder, 1kg dolomite dust, 5.5kg kaolin, 3kg blanc fixe, 4kg ice crystal
Powder, 2kg Delanium, 3kg crystalline flake graphite and 2kg zinc sulphide are well mixed, and obtain mixture.
By mixture at a temperature of 150 DEG C and under 15MPa pressure after hot-forming 5min, obtain it is hot-forming after
Mixture.
Mixture after will be hot-forming is heat-treated as follows successively：100 DEG C are warming up in 1h enough and are protected in the temperature
Warm 1h；160 DEG C are warming up in 1h and in this temperature 4h；200 DEG C are warming up in 1h and in this temperature 1h；Afterwards, drop
Come out of the stove, produce after temperature.
Comparative example 2
35kg basalt fibre, 6kg cashew nut oil modified alkyd resin, 3kg melamine-cashew nut shell oil is double
Phenol-formaldehyde resin modified, 3kg epoxy phenolics, 2kg magnetite powder, 2kg brass miberal powder, 2kg troilite powder, 2kg
Chromite powder, 2kg feldspar powder, 1kg dolomite dust, 5.5kg kaolin, 3kg blanc fixe, 4kg ice crystal
The polyphenylene sulfide of powder, 0.15kg nitrile rubber and 2kg is well mixed, and obtains mixture.
By mixture at a temperature of 150 DEG C and under 15MPa pressure after hot-forming 5min, obtain it is hot-forming after
Mixture.
Mixture after will be hot-forming is heat-treated as follows successively：100 DEG C are warming up in 1h enough and are protected in the temperature
Warm 1h；160 DEG C are warming up in 1h and in this temperature 4h；200 DEG C are warming up in 1h and in this temperature 1h；Afterwards, drop
Come out of the stove, produce after temperature.
Basalt fibre brake block entering according to GB/T 5763-2008 prepared by embodiment 1~6 and comparative example 1~2
Row performance detection, its testing result is shown in Table 2, table 3 and table 4.
The basalt fibre brake block coefficient of friction of table 2a(μ) testing result
The basalt fibre brake block of table 3 specifies tolerance (△ μ) testing result of coefficient of friction
The basalt fibre brake block wear rate (V)/[10 of table 4-7cm3/ (Nm)] testing result
From table 2 into table 4 as can be seen that basalt fibre brake block meets the standard of 1~4 class liner, disclosure satisfy that in
Application in fields such as car, sport utility vehicle (SUV) or commercial cars (MPV).Simultaneously, it can be seen that embodiment
The 5 basalt brake blocks prepared are further illustrated better than basalt brake block prepared by embodiment 6, comparative example 1 and comparative example 2
Its raw material screening and proportioning can further lift the performance of basalt fibre brake block.
In summary, the basalt fibre brake block of the embodiment of the present invention is using natural fiber basalt fibre as skeleton material
Material, coordinating bonding matrix, rubbing agent and filler to be made, lightweight is inexpensive, higher and antifriction damage tolerant the brake block of intensity.Meanwhile, possess
The advantages of nontoxic and ecological, environmental protective.
The preparation method of the basalt fibre brake block of the embodiment of the present invention, can quickly and largely produce the above-mentioned Black Warrior
Rock fiber brake block.With it is simple to operate and safe and efficient the features such as.
Embodiments described above is a part of embodiment of the invention, rather than whole embodiments.The reality of the present invention
The detailed description for applying example is not intended to limit the scope of claimed invention, but is merely representative of the selected implementation of the present invention
Example.Based on the embodiment in the present invention, what those of ordinary skill in the art were obtained under the premise of creative work is not made
Every other embodiment, belongs to the scope of protection of the invention.
Claims (10)
1. a kind of basalt fibre brake block, it is characterised in that be mainly made up of following raw material：The basalt of 30~60 parts by weight
The filler for being bonded matrix, the rubbing agent of 10~25 parts by weight and 10~35 parts of parts by weight of fiber, 10~20 parts by weight.
2. basalt fibre brake block according to claim 1, it is characterised in that the weight of basalt fibre 35~50
Part, 12~15 parts of the matrix of bonding, the parts by weight of rubbing agent 10~20, the parts by weight of filler 20~30.
3. basalt fibre brake block according to claim 1, it is characterised in that the raw material also includes 5~15 weight
The lubricant of part, the lubricant is selected from least one of Delanium, metal sulfide, crystalline flake graphite and molybdenum disulfide；
Wherein, the metal sulfide is selected from least one of zinc sulphide, antimony trisulfide, copper sulfide, molybdenum sulfide.
4. basalt fibre brake block according to claim 1, it is characterised in that the raw material also includes 0.1~1 weight
The softening agent of part, the softening agent selects at least one of nitrile rubber and polyphenylene sulfide.
5. basalt fibre brake block according to claim 1, it is characterised in that the bonding matrix is selected from phenolic resin
At least one of with phenol-formaldehyde resin modified.
6. basalt fibre brake block according to claim 5, it is characterised in that the phenol-formaldehyde resin modified is selected from cashew nut
Shell oil modified phenolic resin, boron modified phenolic resin, polyamide modified phenolic resin, dicyandiamide modified phenolic resin, epoxy change
Property phenolic resin, Pioloform, polyvinyl acetal phenol-formaldehyde resin modified, melamine-cashew nut shell oil double-modification phenolic resin, epoxy novolac
At least one of resin and polyurethane phenolic resin.
7. basalt fibre brake block according to claim 1, it is characterised in that the rubbing agent is selected from carborundum, height
Abrasion resistant carbon black, white carbon, zinc oxide, magnesia, aluminum oxide, magnetite powder, brass miberal powder, troilite powder, chromite powder, feldspar
At least one of powder, dolomite dust and zeolite powder.
8. basalt fibre brake block according to claim 1, it is characterised in that the filler is selected from kaolin, silicon ash
At least one of stone, blanc fixe, vermiculite power, mica powder and cryolite powder.
9. a kind of preparation method of basalt fibre brake block, it is characterised in that including：
By the basalt fibre of 30~60 parts by weight, 10~20 parts by weight bonding matrix, the rubbing agent of 10~25 parts by weight and
The filler of 10~35 parts by weight is well mixed, hot-forming 1 at 150~180 DEG C of temperature and 15~30MPa pressure~
After 10min, 5~10h is heat-treated at a temperature of 100~200 DEG C.
10. the preparation method of basalt fibre brake block according to claim 9, it is characterised in that heat treatment includes：
100~120 DEG C are warming up in 0.5~1.5h and after this temperature keeps 1~3h, 150~180 DEG C are warming up in 0.5~1h
And after this temperature keeps 2~4h, 200 DEG C are warming up in 0.5~1.5h and is cooled after this temperature keeps 0.5~1.5h.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108456395A (en) * | 2018-02-02 | 2018-08-28 | 西安交通大学 | A kind of basalt reinforced resin base braking composite material and preparation method thereof |
| CN109058335A (en) * | 2018-08-02 | 2018-12-21 | 黄石市鑫溢矿产有限公司 | A kind of preparation method of composite sulfuration composition formula friction block |
| CN109488710A (en) * | 2018-10-19 | 2019-03-19 | 南京航空航天大学溧水仿生产业研究院有限公司 | A kind of high-performance non-asbestos brake block |
| CN109666454A (en) * | 2018-12-25 | 2019-04-23 | 山东安途制动材料有限公司 | A kind of automobile-used disc brake pad friction material of heavy type and brake block preparation process |
| CN109812524A (en) * | 2019-01-31 | 2019-05-28 | 齐鲁工业大学 | An environmentally friendly blend matrix friction material composition for automobile brake pads |
| CN110903731A (en) * | 2019-10-17 | 2020-03-24 | 山东金麒麟股份有限公司 | Baking-free etching agent for brake pad, preparation and application methods and brake pad |
| CN111043202A (en) * | 2019-12-31 | 2020-04-21 | 北京天宜上佳高新材料股份有限公司 | Friction material, composite brake shoe and preparation method |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108456395A (en) * | 2018-02-02 | 2018-08-28 | 西安交通大学 | A kind of basalt reinforced resin base braking composite material and preparation method thereof |
| CN109058335A (en) * | 2018-08-02 | 2018-12-21 | 黄石市鑫溢矿产有限公司 | A kind of preparation method of composite sulfuration composition formula friction block |
| CN109488710A (en) * | 2018-10-19 | 2019-03-19 | 南京航空航天大学溧水仿生产业研究院有限公司 | A kind of high-performance non-asbestos brake block |
| CN109666454A (en) * | 2018-12-25 | 2019-04-23 | 山东安途制动材料有限公司 | A kind of automobile-used disc brake pad friction material of heavy type and brake block preparation process |
| CN109812524A (en) * | 2019-01-31 | 2019-05-28 | 齐鲁工业大学 | An environmentally friendly blend matrix friction material composition for automobile brake pads |
| CN110903731A (en) * | 2019-10-17 | 2020-03-24 | 山东金麒麟股份有限公司 | Baking-free etching agent for brake pad, preparation and application methods and brake pad |
| CN110903731B (en) * | 2019-10-17 | 2021-09-28 | 山东金麒麟股份有限公司 | Baking-free etching agent for brake pad, preparation and application methods and brake pad |
| CN111043202A (en) * | 2019-12-31 | 2020-04-21 | 北京天宜上佳高新材料股份有限公司 | Friction material, composite brake shoe and preparation method |
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Effective date of registration: 20170927 Address after: 553000 No. 9 building, standard factory building, Shuicheng Economic Development Zone, Shuicheng County, Guizhou, Liupanshui Applicant after: Guizhou stone basalt Technology Co., Ltd. Address before: 553000 Guizhou Shuicheng Economic Development Zone Engineering Technology Center, Shuicheng County, Liupanshui, Guizhou Applicant before: Guizhou basalt New Material Engineering Technology Development Co Ltd |
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