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CN107032854A - The method that stalk fermentation biogas residue prepares organic fertilizer - Google Patents

The method that stalk fermentation biogas residue prepares organic fertilizer Download PDF

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Publication number
CN107032854A
CN107032854A CN201710397483.7A CN201710397483A CN107032854A CN 107032854 A CN107032854 A CN 107032854A CN 201710397483 A CN201710397483 A CN 201710397483A CN 107032854 A CN107032854 A CN 107032854A
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CN
China
Prior art keywords
biogas residue
fermentation
organic fertilizer
stalk
stalk fermentation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710397483.7A
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Chinese (zh)
Inventor
代永志
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Anhui Forever Ring Technology Co Ltd
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Anhui Forever Ring Technology Co Ltd
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Publication date
Application filed by Anhui Forever Ring Technology Co Ltd filed Critical Anhui Forever Ring Technology Co Ltd
Priority to CN201710397483.7A priority Critical patent/CN107032854A/en
Publication of CN107032854A publication Critical patent/CN107032854A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F9/00Fertilisers from household or town refuse
    • C05F9/04Biological compost
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/30Fuel from waste, e.g. synthetic alcohol or diesel

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Fertilizers (AREA)

Abstract

A kind of method that stalk fermentation biogas residue prepares organic fertilizer, comprises the following steps:Biogas slurry in fermentation vat is removed, makes biogas residue natural air drying;Organic solvent is added into fermentation vat to soak biogas residue 23 days;Biogas residue is taken out into ventilation from fermentation vat to dry and carry out pulverization process;Biogas residue after pulverization process and leavening are mixed and stirred for uniform compound;Mixing stockpile is subjected to aerobic fermentation in fermenting cellar;Additive is added into compound and stir after aerobic fermentation;Regulation water content is granulated, and obtains the organic fertilizer.Organic fertilizer produced by the present invention can effectively retain the element such as the organic matter contained in biogas residue and nitrogen, phosphorus, potassium, at the same balanced composition, comprehensively, comprehensive nutrient can be provided for plant growth.

Description

The method that stalk fermentation biogas residue prepares organic fertilizer
Technical field
The present invention relates to crop fertilizer preparation field, and in particular to a kind of method that stalk fermentation biogas residue prepares organic fertilizer.
Background technology
With the sustainable development of the ecological agriculture, the enthusiasm more and more higher of people's development biogas ecology agricultural, the use of biogas residue Way is also gradually exploited.Biogas residue is the semi-solid material that methane-generating pit bottom is remained in after biogas fermentation, is had containing abundant Machine matter, humic acid, crude protein, nitrogen, phosphorus, potassium and various trace elements and auximone.
Biogas residue is due to rich in organic matter etc., therefore biogas residue aerobic compost production organic fertilizer turns into one kind that biogas residue is handled gradually Main trend.When utilization biogas residue produces organic fertilizer, due to the difference for the original material that ferments, if any utilization livestock manure fermented shape Into biogas residue, have using fermentation of plant straws formation biogas residue, have using sludge formation biogas residue, different fermentations material formation Biogas residue has very big difference in terms of quality, composition, needs to be respectively processed when organic fertilizer is made, while prior art When preparing organic fertilizer using biogas residue on the one hand it cannot be guaranteed that the equilibrium of the nutrient of obtained fertilizer, was on the other hand prepared Nutrient in journey in biogas residue is easily lost in, and two aspect reasons cause that obtained organic fertilizer fertilizer efficiency is poor, and application effect is not obvious.
The content of the invention
In order to alleviate shortcomings and deficiencies of the prior art, it is an object of the invention to provide a kind of preparation of stalk fermentation biogas residue The method of organic fertilizer, preparation method of the present invention is simple, and obtained organic fertilizer nutrition is balanced, fertilizer efficiency is high.
The technical problems to be solved by the invention are realized using following technical scheme:
A kind of method that stalk fermentation biogas residue prepares organic fertilizer, comprises the following steps:
(1) biogas slurry in fermentation vat is removed, makes biogas residue natural air drying;
(2) organic solvent is added into fermentation vat to soak biogas residue 2-3 days;
(3) biogas residue is taken out to ventilation from fermentation vat to dry and carry out pulverization process;
(4) biogas residue after pulverization process and leavening are mixed and stirred for uniform compound;
(5) mixing stockpile is subjected to aerobic fermentation in fermenting cellar;
(6) additive is added after aerobic fermentation into compound and is stirred;
(7) regulation water content is granulated, and obtains the organic fertilizer.
Step (2) organic solvent is ether, chloroform, hexane mixture;
The organic solvent is 0.05 with biogas residue mass ratio:1.
Leavening is made up of soft rotten fungi, brown rot fungus, white-rot fungi in the step (4).
Windrow is no less than 5 cubes, 1.0 meters of feed height -1.2 meters, environment during aerobic fermentation in the step (5) When below 18 DEG C of temperature, covered, when internal temperature is raised to 30 DEG C, covering is opened, heap temperature rise to 50 with film or straw screen or mat DEG C when begin to tip over, then turned over once every 2-3 days.
One is set to enclose cage ring on windrow surrounding ground during aerobic fermentation in the step (5), the cage ring is by chlorine Change calcium, sodium hypochlorite powder constituent.The close of fly worm during the fermentation is prevented by the cage ring.
Aerobic fermentation takes disinfectant measure in the step (5) after terminating, and the disinfectant measure can be used to fermenting cellar Spray disinfectant, or disinfection by ultraviolet light light irradiation is used, by taking disinfectant measure to prevent bacterium in fermentation process, viral production It is raw, it is ensured that the organic matter in biogas residue is not decomposed consumption.
Additive is made up of calcium sulfate, ammonium nitrate and potassium phosphate in the step (6).
Beneficial effects of the present invention are:Organic solvent pretreatment straw biogas residue can destroy the wax and lignin on its top layer with Covalent bond between hemicellulose, realizes the separation of cellulose and lignin and hemicellulose, improves straw biogas residue and is mixed with leavening Conversion ratio during conjunction, accelerates course of fermentation, shortens fermentation period, the fertile cost of reduction system;Cage ring is set in fermenting cellar, fermented After take disinfectant measure, can farthest retain the compositions such as organic matter, humic acid, crude protein, nitrogen, phosphorus, potassium in biogas residue, keep away Exempt to be polluted during the fermentation, while extending the storage life of organic fertilizer;By analyzing stalk fermentation biogas residue composition, Add additive and cause obtained organic fertilizer effect more fully, be applicable to multiple kinds of crops, such as vegetable melon and fruit or grain Crop.
Embodiment
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below Embodiment is closed, the present invention is expanded on further.
Embodiment 1
A kind of method that stalk fermentation biogas residue prepares organic fertilizer, comprises the following steps:
(1) biogas slurry in fermentation vat is removed, makes biogas residue natural air drying;
(2) organic solvent being made up of ether, chloroform, n-hexane is added into fermentation vat to soak biogas residue 2 days;
(3) biogas residue is taken out to ventilation from fermentation vat to dry and carry out pulverization process;
(4) biogas residue after pulverization process is mixed and stirred with the leavening being made up of soft rotten fungi, brown rot fungus, white-rot fungi Mix uniform compound;
(5) mixing stockpile is subjected to aerobic fermentation in fermenting cellar:5 cubes of a windrow, 1.0 meters of feed height, environment When below 18 DEG C of temperature, covered, when internal temperature is raised to 30 DEG C, covering is opened, heap temperature rise to 50 with film or straw screen or mat DEG C when begin to tip over, then turned over once every 2 days;One is set to enclose cage ring on windrow surrounding ground, the cage ring is by chlorine Change calcium, sodium hypochlorite powder constituent, the close of fly worm during the fermentation is prevented by the cage ring;Taken after fermentation ends Disinfectant measure, the disinfectant measure can be used to fermenting cellar spray disinfectant, or uses disinfection by ultraviolet light light irradiation, by adopting Disinfectant measure is taken to prevent bacterium in fermentation process, the generation of virus, it is ensured that the organic matter in biogas residue is not decomposed consumption;
(6) additive being made up of calcium sulfate, ammonium nitrate and potassium phosphate and stirring are added after aerobic fermentation into compound Uniformly;
(7) regulation water content is granulated, and obtains the organic fertilizer.
Embodiment 2
A kind of method that stalk fermentation biogas residue prepares organic fertilizer, comprises the following steps:
(1) biogas slurry in fermentation vat is removed, makes biogas residue natural air drying;
(2) organic solvent being made up of ether, chloroform, n-hexane is added into fermentation vat to soak biogas residue 2.5 days;
(3) biogas residue is taken out to ventilation from fermentation vat to dry and carry out pulverization process;
(4) biogas residue after pulverization process is mixed and stirred with the leavening being made up of soft rotten fungi, brown rot fungus, white-rot fungi Mix uniform compound;
(5) mixing stockpile is subjected to aerobic fermentation in fermenting cellar:8 cubes of a windrow, 1.1 meters of feed height, environment When below 18 DEG C of temperature, covered, when internal temperature is raised to 30 DEG C, covering is opened, heap temperature rise to 50 with film or straw screen or mat DEG C when begin to tip over, then turned over once every 2.5 days;On windrow surrounding ground set one enclose cage ring, the cage ring by Calcium chloride, sodium hypochlorite powder constituent, the close of fly worm during the fermentation is prevented by the cage ring;Adopted after fermentation ends Disinfectant measure is taken, the disinfectant measure can be used to fermenting cellar spray disinfectant, or uses disinfection by ultraviolet light light irradiation, passed through Disinfectant measure is taken to prevent bacterium in fermentation process, the generation of virus, it is ensured that the organic matter in biogas residue is not decomposed consumption;
(6) additive being made up of calcium sulfate, ammonium nitrate and potassium phosphate and stirring are added after aerobic fermentation into compound Uniformly;
(7) regulation water content is granulated, and obtains the organic fertilizer.
Embodiment 3
A kind of method that stalk fermentation biogas residue prepares organic fertilizer, comprises the following steps:
(1) biogas slurry in fermentation vat is removed, makes biogas residue natural air drying;
(2) organic solvent being made up of ether, chloroform, n-hexane is added into fermentation vat to soak biogas residue 3 days;
(3) biogas residue is taken out to ventilation from fermentation vat to dry and carry out pulverization process;
(4) biogas residue after pulverization process is mixed and stirred with the leavening being made up of soft rotten fungi, brown rot fungus, white-rot fungi Mix uniform compound;
(5) mixing stockpile is subjected to aerobic fermentation in fermenting cellar:15 cubes of a windrow, 1.2 meters of feed height, environment When below 18 DEG C of temperature, covered, when internal temperature is raised to 30 DEG C, covering is opened, heap temperature rise to 50 with film or straw screen or mat DEG C when begin to tip over, then turned over once every 3 days;One is set to enclose cage ring on windrow surrounding ground, the cage ring is by chlorine Change calcium, sodium hypochlorite powder constituent, the close of fly worm during the fermentation is prevented by the cage ring;Taken after fermentation ends Disinfectant measure, the disinfectant measure can be used to fermenting cellar spray disinfectant, or uses disinfection by ultraviolet light light irradiation, by adopting Disinfectant measure is taken to prevent bacterium in fermentation process, the generation of virus, it is ensured that the organic matter in biogas residue is not decomposed consumption;
(6) additive being made up of calcium sulfate, ammonium nitrate and potassium phosphate and stirring are added after aerobic fermentation into compound Uniformly;
(7) regulation water content is granulated, and obtains the organic fertilizer.
Organic fertilizer made from embodiment 1-3 is detected and contrasted with common organic fertilizer and composite fertilizer, it is as follows Table:
General principle, principal character and the advantages of the present invention of the present invention has been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and that described in above-described embodiment and specification is only the present invention Preference, be not intended to limit the present invention, without departing from the spirit and scope of the present invention, the present invention also have it is various Changes and improvements, these changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention is by institute Attached claims and its equivalent thereof.

Claims (9)

1. a kind of method that stalk fermentation biogas residue prepares organic fertilizer, it is characterised in that comprise the following steps:
(1) biogas slurry in fermentation vat is removed, makes biogas residue natural air drying;
(2) organic solvent is added into fermentation vat to soak biogas residue 2-3 days;
(3) biogas residue is taken out to ventilation from fermentation vat to dry and carry out pulverization process;
(4) biogas residue after pulverization process and leavening are mixed and stirred for uniform compound;
(5) mixing stockpile is subjected to aerobic fermentation in fermenting cellar;
(6) additive is added after aerobic fermentation into compound and is stirred;
(7) regulation water content is granulated, and obtains the organic fertilizer.
2. the method that stalk fermentation biogas residue as claimed in claim 1 prepares organic fertilizer, it is characterised in that the step (2) has Machine solvent is ether, chloroform, hexane mixture.
3. the method for preparing organic fertilizer using stalk fermentation biogas residue as claimed in claim 2, it is characterised in that described organic molten Agent is 0.05 with biogas residue mass ratio:1.
4. the method that stalk fermentation biogas residue as claimed in claim 1 prepares organic fertilizer, it is characterised in that in the step (4) Leavening is made up of soft rotten fungi, brown rot fungus, white-rot fungi.
5. the method that stalk fermentation biogas residue as claimed in claim 1 prepares organic fertilizer, it is characterised in that in the step (5) Windrow is no less than 5 cubes during aerobic fermentation, 1.0 meters -1.2 meters of feed height, when below 18 DEG C of environment temperature, uses film Or straw screen or mat covering, when internal temperature is raised to 30 DEG C, covering is opened, begun to tip over when heap temperature rise is to 50 DEG C, then every Turn over once within 2-3 days.
6. the method that stalk fermentation biogas residue as claimed in claim 1 prepares organic fertilizer, it is characterised in that in the step (5) One is set to enclose cage ring on windrow surrounding ground during aerobic fermentation, the cage ring is by calcium chloride, sodium hypochlorite powder constituent.
7. the method that stalk fermentation biogas residue as claimed in claim 1 prepares organic fertilizer, it is characterised in that in the step (5) Aerobic fermentation takes disinfectant measure after terminating.
8. the method that stalk fermentation biogas residue as claimed in claim 1 prepares organic fertilizer, it is characterised in that the disinfectant measure can To use to fermenting cellar spray disinfectant, or use disinfection by ultraviolet light light irradiation.
9. the method for preparing organic fertilizer using stalk fermentation biogas residue as claimed in claim 1, it is characterised in that the step (6) additive is made up of calcium sulfate, ammonium nitrate and potassium phosphate in.
CN201710397483.7A 2017-05-31 2017-05-31 The method that stalk fermentation biogas residue prepares organic fertilizer Pending CN107032854A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108358672A (en) * 2018-04-18 2018-08-03 黑龙江新天地能源开发有限公司 A method of producing organic fertilizer with straw biogas residue
CN109456133A (en) * 2019-01-07 2019-03-12 中广核生物燃气河北有限公司 Biogas residue containing rice husk prepares organic fertilizer technique
CN113024325A (en) * 2021-04-22 2021-06-25 中国水稻研究所 Liquid bacterial fertilizer prepared from biogas slurry in pig farm, and preparation method and application method thereof
CN116589308A (en) * 2023-05-22 2023-08-15 中国农业科学院农业资源与农业区划研究所 A self-heating straw decomposing agent and its preparation method and application

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102257150A (en) * 2008-12-19 2011-11-23 纳幕尔杜邦公司 Organic solvent pretreatment of biomass to enhance enzymatic saccharification
CN104805151A (en) * 2014-01-24 2015-07-29 华东理工大学 Lignocellulosic feedstock pretreatment method without prepreg
CN106242725A (en) * 2016-07-22 2016-12-21 北京西拓联合生态科技有限公司 One makees organic fertilizer and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102257150A (en) * 2008-12-19 2011-11-23 纳幕尔杜邦公司 Organic solvent pretreatment of biomass to enhance enzymatic saccharification
CN104805151A (en) * 2014-01-24 2015-07-29 华东理工大学 Lignocellulosic feedstock pretreatment method without prepreg
CN106242725A (en) * 2016-07-22 2016-12-21 北京西拓联合生态科技有限公司 One makees organic fertilizer and preparation method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108358672A (en) * 2018-04-18 2018-08-03 黑龙江新天地能源开发有限公司 A method of producing organic fertilizer with straw biogas residue
CN109456133A (en) * 2019-01-07 2019-03-12 中广核生物燃气河北有限公司 Biogas residue containing rice husk prepares organic fertilizer technique
CN113024325A (en) * 2021-04-22 2021-06-25 中国水稻研究所 Liquid bacterial fertilizer prepared from biogas slurry in pig farm, and preparation method and application method thereof
CN116589308A (en) * 2023-05-22 2023-08-15 中国农业科学院农业资源与农业区划研究所 A self-heating straw decomposing agent and its preparation method and application

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Application publication date: 20170811

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