CN106542804A - A kind of aging resistance porcelain and its processing technology - Google Patents
A kind of aging resistance porcelain and its processing technology Download PDFInfo
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Abstract
The present invention relates to ceramic field, and in particular to a kind of aging resistance porcelain, by weight, containing following raw material components：35 45 parts of clay, modified 10 14 parts of calcinated argil, modified 10 14 parts of aethiops vegetabilis, 8 12 parts of porcelain sand, 8 12 parts of tourmaline, 8 12 parts of bentonite, 12 parts of guar gum ether, 0.5 1 parts of iron-amino acid chelate, 24 parts of zinc powder, 24 parts of titanium valve of nitridation, 24 parts of titanium dioxide zirconium powder.Porcelain material matching of the present invention is reasonable, stock dispersion is uniform, during sintering, zinc powder forms Zinc Oxide with dioxygen oxidation, Zinc Oxide hinders Oxidation, so that porcelain antioxygenic property is very good, made by porcelain can for a long time used in oils and fatss, antibacterial environment, using its surface after 5 years still without aging speckle, and porcelain can also be releasing far infrared, there is certain benefit to human body.
Description
Technical field
The present invention relates to ceramic field, and in particular to a kind of aging resistance porcelain and its processing technology.
Background technology
With the vessel of potter's clay firing on pottery, with the vessel of china clay firing porcelain.It is ceramic then be pottery, stoneware and porcelain
General name.Every potter's clay and china clay both clays of different nature are raw material, through works such as dispensing, molding, drying, roastings
Made by skill flow process, implements can be ceramics.
Ceramics development history be Chinese civilization history an important ingredient, China as four major acids ancient country it
One, it is that the progress and development of human society is made that remarkable contribution, wherein the invention of ceramics and development are with more unique meaning
Justice, on Chinese history, each Chao Gedai has different artistic style and different technical characteristics." china " existing China in English
The meaning, the meaning for having ceramics again clearly demonstrate that China is exactly " native places of ceramics ".Porcelain manufacture skill is grasped early in European
Before art more than 1,000 years, Han nationality has just produced very exquisite ware.China be in the world earliest using pottery country it
One, and Chinese porcelain enjoys the high praise of common people because of its high practicality and artistry.
With the development of modern science technology, many new ceramic kinds are occurred in that in the last hundred years again.They do not use
Or the traditional ceramicses raw material such as clay, Anhydrite, quartz is rarely employed, but other special materials are used, or even expand non-silicic acid to
Salt, the scope of non-oxidized substance, and occur in that many new techniques.US and European some national documents will
" Ceramic " word is interpreted as the common name of various inorganic non-metal solid materials.Therefore the implication of ceramics actually much surpasses
More pass by narrow traditional view.
The ceramic industry of China is of long standing and well established, with a long history.Pottery, the raw material used by porcelain are mostly natural inorganic
Nonmetallic mineral, these raw materials by processing and refining, cooperation, shaping, high-temperature physics chemical reaction, just formed it is a kind of with original group
Into the completely different new material of material, it is ceramics.China's pottery have passed through three phases to porcelain development：Pottery-original pottery
Device-porcelain.Porcelain raw material is different at present, and technique is different, but porcelain always be present on raw material and technique, cause
Porcelain service life is short.
The content of the invention
The technical problem to be solved is to provide a kind of aging resistance porcelain and its processing technology, and porcelain raw material is taken
With reasonable, stock dispersion is uniform, and during sintering, zinc powder forms Zinc Oxide with dioxygen oxidation, and Zinc Oxide hinders Oxidation so that porcelain
Device antioxygenic property is very good, made by porcelain can for a long time used in oils and fatss, antibacterial environment, using its surface after 5 years still
Without aging speckle, and porcelain can also be releasing far infrared, has certain benefit to human body.
The technical problem to be solved employs the following technical solutions to realize：
A kind of aging resistance porcelain, by weight, containing following raw material components：Clay 35-45 parts, modified calcinated argil
10-14 parts, modified aethiops vegetabilis 10-14 parts, porcelain sand 8-12 parts, tourmaline 8-12 parts, bentonite 8-12 parts, guar gum ether 1-2
Part, iron-amino acid chelate 0.5-1 parts, zinc powder 2-4 parts, nitridation titanium valve 2-4 parts, titanium dioxide zirconium powder 2-4 parts.
The modified calcinated argil is prepared by following methods：Calcinated argil is fired to into 700-800 DEG C, then calcinated argil
It is soaked in the acetum of 4.2% concentration, calcinated argil is taken out after 10 minutes and 750-800 DEG C is fired to, then is put it into
Soak 1 hour in soak, continue to be fired to 800-850 DEG C after taking-up, then room temperature was cooled in 1 minute.
The soak is made up of following raw material：Tartaric acid 20-30 parts, malic acid 20-30 parts, cinnamic acid 20-
30 parts, hydroxyethyl cellulose 5-10 parts, xylitol 5-10 parts, chitosan 5-10 parts, medical borax 5-10 part, by each raw material mix
20 times of clear water of their weight portions are added to stir.
The modified aethiops vegetabilis is prepared by following methods：Aethiops vegetabilis is heated to into 80-100 DEG C, 50-60 DEG C is soaked in
Hydrogen peroxide, aethiops vegetabilis is heated to into 260-300 DEG C then, then room temperature was cooled in 1 minute.
A kind of processing technology of aging resistance porcelain, comprises the following steps：
(1) each raw material is weighed by weight, and the mixing of each raw material is milled to into the fine powder of 500-600 mesh；
(2) fine powder molding is made according to design requirement, repaired biscuit is plain in 1000 DEG C of -1100 DEG C of stoves by the base substrate for trimming
Burn, after biscuiting 30 minutes, biscuit is polished smooth；
(3) biscuit glazing is added and is turned green, and kiln temperature is risen to 1280-1380 DEG C, continues sintering 1 hour, is then gone out
Stove.
Pure oxygen was passed through every 10 minutes in stove in sintering process, makes oxygen concentration in stove maintain 25.5-
28.4%.
It is 1300-1350 DEG C that biscuit continues sintering temperature.
The invention has the beneficial effects as follows：Rationally, stock dispersion is uniform, zinc powder and oxygen during sintering for porcelain material matching of the present invention
Gas aoxidizes to form Zinc Oxide, and Zinc Oxide hinders Oxidation so that porcelain antioxygenic property is very good, made by porcelain can be long-term
Used in oils and fatss, antibacterial environment, using its surface after 5 years still without aging speckle, and porcelain can also be releasing far infrared,
There is certain benefit to human body.
Specific embodiment
In order that technological means, creation characteristic, reached purpose and effect that the present invention is realized are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1
A kind of aging resistance porcelain, by weight, containing following raw material components：40 parts of clay, modified 12 parts of calcinated argil,
12 parts of modified aethiops vegetabilis, 10 parts of porcelain sand, 10 parts of tourmaline, 10 parts of bentonite, 1.5 parts of guar gum ether, iron-amino acid chelate 0.8
Part, 3 parts of zinc powder, 3 parts of titanium valve of nitridation, 3 parts of titanium dioxide zirconium powder.
The modified calcinated argil is prepared by following methods：Calcinated argil is fired to into 700-800 DEG C, then calcinated argil
It is soaked in the acetum of 4.2% concentration, calcinated argil is taken out after 10 minutes and 750-800 DEG C is fired to, then is put it into
Soak 1 hour in soak, continue to be fired to 800-850 DEG C after taking-up, then room temperature was cooled in 1 minute.
The soak is made up of following raw material：25 parts of tartaric acid, 25 parts of malic acid, 25 parts of cinnamic acid, hydroxyl second
The mixing of each raw material is added 20 times of their weight portions clear by 8 parts of base cellulose, 8 parts of xylitol, 8 parts of chitosan, 8 parts of medical borax
Water stirs.
The modified aethiops vegetabilis is prepared by following methods：Aethiops vegetabilis is heated to into 80-100 DEG C, 50-60 DEG C is soaked in
Hydrogen peroxide, aethiops vegetabilis is heated to into 260-300 DEG C then, then room temperature was cooled in 1 minute.
A kind of processing technology of aging resistance porcelain, comprises the following steps：
(1) each raw material is weighed by weight, and the mixing of each raw material is milled to into the fine powder of 550 mesh；
(2) fine powder molding, repaired biscuit, by the base substrate for trimming biscuiting in 1050 DEG C of stoves, biscuiting are made according to design requirement
After 30 minutes, biscuit is polished smooth；
(3) biscuit glazing is added and is turned green, and kiln temperature is risen to 1330 DEG C, continues sintering 1 hour, then goes out stove.
Pure oxygen was passed through every 10 minutes in stove in sintering process, makes oxygen concentration in stove maintain 26.8%.
Embodiment 2
A kind of aging resistance porcelain, by weight, containing following raw material components：35 parts of clay, modified 10 parts of calcinated argil,
10 parts of modified aethiops vegetabilis, 8 parts of porcelain sand, 8 parts of tourmaline, 8 parts of bentonite, 1 part of guar gum ether, 0.5 part of iron-amino acid chelate, zinc
2 parts of powder, 2 parts of titanium valve of nitridation, 2 parts of titanium dioxide zirconium powder.
The modified calcinated argil is prepared by following methods：Calcinated argil is fired to into 700-800 DEG C, then calcinated argil
It is soaked in the acetum of 4.2% concentration, calcinated argil is taken out after 10 minutes and 750-800 DEG C is fired to, then is put it into
Soak 1 hour in soak, continue to be fired to 800-850 DEG C after taking-up, then room temperature was cooled in 1 minute.
The soak is made up of following raw material：20 parts of tartaric acid, 20 parts of malic acid, 20 parts of cinnamic acid, hydroxyl second
The mixing of each raw material is added 20 times of their weight portions clear by 5 parts of base cellulose, 5 parts of xylitol, 5 parts of chitosan, 5 parts of medical borax
Water stirs.
The modified aethiops vegetabilis is prepared by following methods：Aethiops vegetabilis is heated to into 80-100 DEG C, 50-60 DEG C is soaked in
Hydrogen peroxide, aethiops vegetabilis is heated to into 260-300 DEG C then, then room temperature was cooled in 1 minute.
A kind of processing technology of aging resistance porcelain, comprises the following steps：
(1) each raw material is weighed by weight, and the mixing of each raw material is milled to into the fine powder of 500 mesh；
(2) fine powder molding, repaired biscuit, by the base substrate for trimming biscuiting in 1000 DEG C of stoves, biscuiting are made according to design requirement
After 30 minutes, biscuit is polished smooth；
(3) biscuit glazing is added and is turned green, and kiln temperature is risen to 1280 DEG C, continues sintering 1 hour, then goes out stove.
Pure oxygen was passed through every 10 minutes in stove in sintering process, makes oxygen concentration in stove maintain 25.5%.
Embodiment 3
A kind of aging resistance porcelain, by weight, containing following raw material components：45 parts of clay, modified 14 parts of calcinated argil,
14 parts of modified aethiops vegetabilis, 12 parts of porcelain sand, 12 parts of tourmaline, 12 parts of bentonite, 2 parts of guar gum ether, 1 part of iron-amino acid chelate,
4 parts of zinc powder, 4 parts of titanium valve of nitridation, 4 parts of titanium dioxide zirconium powder.
The modified calcinated argil is prepared by following methods：Calcinated argil is fired to into 700-800 DEG C, then calcinated argil
It is soaked in the acetum of 4.2% concentration, calcinated argil is taken out after 10 minutes and 750-800 DEG C is fired to, then is put it into
Soak 1 hour in soak, continue to be fired to 800-850 DEG C after taking-up, then room temperature was cooled in 1 minute.
The soak is made up of following raw material：30 parts of tartaric acid, 30 parts of malic acid, 30 parts of cinnamic acid, hydroxyl second
The mixing of each raw material is added their weight portions 20 by 10 parts of base cellulose, 10 parts of xylitol, 10 parts of chitosan, 10 parts of medical borax
Times clear water stirs.
The modified aethiops vegetabilis is prepared by following methods：Aethiops vegetabilis is heated to into 80-100 DEG C, 50-60 DEG C is soaked in
Hydrogen peroxide, aethiops vegetabilis is heated to into 260-300 DEG C then, then room temperature was cooled in 1 minute.
A kind of processing technology of aging resistance porcelain, comprises the following steps：
(1) each raw material is weighed by weight, and the mixing of each raw material is milled to into the fine powder of 600 mesh；
(2) fine powder molding, repaired biscuit, by the base substrate for trimming biscuiting in 1100 DEG C of stoves, biscuiting are made according to design requirement
After 30 minutes, biscuit is polished smooth；
(3) biscuit glazing is added and is turned green, and kiln temperature is risen to 1380 DEG C, continues sintering 1 hour, then goes out stove.
Pure oxygen was passed through every 10 minutes in stove in sintering process, makes oxygen concentration in stove maintain 28.4%.
Experiment
Porcelain performance such as following table compared with common porcelain made by the present embodiment 1,2,3：
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Common porcelain |
| Ratio of briquetting (%) | 99 | 98 | 97 | 83 |
| Apparent porosity (%) | 0.234 | 0.278 | 0.322 | 0.495 |
| Mohs' hardness | 7 | 7 | 6 | 5 |
As seen from the above table, porcelain performance of the invention is substantially better than common porcelain.
The ultimate principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel it should be appreciated that the present invention is not restricted to the described embodiments, the simply explanation described in above-described embodiment and description this
The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these changes
Change and improvement is both fallen within scope of the claimed invention.The claimed scope of the invention by appending claims and its
Equivalent thereof.
Claims (7)
1. a kind of aging resistance porcelain, it is characterised in that by weight, containing following raw material components：It is clay 35-45 parts, modified
Calcinated argil 10-14 parts, modified aethiops vegetabilis 10-14 parts, porcelain sand 8-12 parts, tourmaline 8-12 parts, bentonite 8-12 parts, melon ear
Glue ether 1-2 parts, iron-amino acid chelate 0.5-1 parts, zinc powder 2-4 parts, nitridation titanium valve 2-4 parts, titanium dioxide zirconium powder 2-4 parts.
2. a kind of aging resistance porcelain according to claim 1, it is characterised in that the modified calcinated argil is by following methods
Prepare：Calcinated argil is fired to into 700-800 DEG C, then calcinated argil is soaked in the acetum of 4.2% concentration, 10 minutes
Calcinated argil is taken out afterwards and 750-800 DEG C is fired to, then is soaked 1 hour in putting it into soak, continue to be fired to after taking-up
800-850 DEG C, then room temperature was cooled in 1 minute.
3. a kind of aging resistance porcelain according to claim 2, it is characterised in that the soak is by following raw material
Make：Tartaric acid 20-30 parts, malic acid 20-30 parts, cinnamic acid 20-30 parts, hydroxyethyl cellulose 5-10 parts, xylitol 5-10
The mixing of each raw material is added 20 times of clear water of their weight portions to stir i.e. by part, chitosan 5-10 parts, medical borax 5-10 part
Can.
4. a kind of aging resistance porcelain according to claim 1, it is characterised in that the modified aethiops vegetabilis is by following methods system
It is standby：Aethiops vegetabilis is heated to into 80-100 DEG C, 50-60 DEG C of hydrogen peroxide is soaked in, aethiops vegetabilis is heated to into 260-300 then
DEG C, then room temperature was cooled in 1 minute.
5. a kind of processing technology of the aging resistance porcelain described in any one of claim 1-4 is made, it is characterised in that including following
Step：
(1) each raw material is weighed by weight, and the mixing of each raw material is milled to into the fine powder of 500-600 mesh；
(2) fine powder molding, repaired biscuit, by the base substrate for trimming biscuiting in 1000 DEG C of -1100 DEG C of stoves, element are made according to design requirement
After burning 30 minutes, biscuit is polished smooth；
(3) biscuit glazing is added and is turned green, and kiln temperature is risen to 1280-1380 DEG C, continues sintering 1 hour, then goes out stove.
6. the processing technology of a kind of aging resistance porcelain according to claim 5, it is characterised in that every 10 in sintering process
Minute is passed through pure oxygen in stove, makes oxygen concentration in stove maintain 25.5-28.4%.
7. the processing technology of a kind of aging resistance porcelain according to claim 5, it is characterised in that biscuit continues sintering temperature
Spend for 1300-1350 DEG C.
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| CN103358797A (en) * | 2013-06-20 | 2013-10-23 | 俞永民 | Manufacturing technology for ceramic plate paintings |
| CN104072084A (en) * | 2014-06-30 | 2014-10-01 | 南通蛇类治疗研究所 | Nano mineral powder multiple-effect elastic ceramic ware |
| CN104944910A (en) * | 2015-06-02 | 2015-09-30 | 安徽省含山瓷业股份有限公司 | Ageing cracking resistant ceramic bowl and preparation method thereof |
| CN105060856A (en) * | 2015-08-11 | 2015-11-18 | 长沙秋点兵信息科技有限公司 | Formula and manufacturing process of porcelain |
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Application publication date: 20170329 |