CN106431198A - Manufacturing method of glazed ceramic exterior wall tile - Google Patents
Manufacturing method of glazed ceramic exterior wall tile Download PDFInfo
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- CN106431198A CN106431198A CN201610813088.8A CN201610813088A CN106431198A CN 106431198 A CN106431198 A CN 106431198A CN 201610813088 A CN201610813088 A CN 201610813088A CN 106431198 A CN106431198 A CN 106431198A
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- exterior wall
- glazed ceramic
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
The invention discloses a manufacturing method of a glazed ceramic exterior wall tile, and relates to the technical field of building material production. The glazed ceramic exterior wall tile is prepared from the following raw materials by weight percent: 25-30% of clay, 25-35% of Tongfu soil, 20-22% of gravel stone and 20-25% of potassium sand; the total aluminum content of the glazed ceramic exterior wall tile is 14.5-18%, and the total iron content of the glazed ceramic exterior wall tile is less than or equal to 2%. The manufacturing method comprises the steps of adding water into the raw materials, wherein the amount of the water is 10% of the total amount of the raw materials, carrying out ball-milling, then deironing and sieving, carrying out spray drying to obtain granules, and staling for 48h or more; pressing a green body under the pressure of 180-230MPa, and drying to obtain a green tile with the water content of 0.5-1%; spraying glaze water onto the surface of the green tile, then putting the green tile into a roller kiln, drying at a temperature region of 200-400 DEG C, and then sending to a temperature region of 1210-1220 DEG C for sintering until the water absorption of a tile body is 1-3%, so as to obtain the glazed ceramic exterior wall tile. The manufacturing method provided by the invention solves the problems that a glazed ceramic exterior wall tile manufactured by the existing production technology is high in water absorption, and is not wear-resistant, pressure-resistant and cold-resistant.
Description
Technical field
The present invention relates to construction material production technical field, especially a kind of method for manufacturing outdoor tile.
Background technology
Glazed ceramic exterior wall tile is the outdoor tile being made up of adobe and two parts of glaze, and glaze is applied on adobe surface
Glaze burns till, and can obtain abundant decorative effect, and its have antifouling, easy to clean, the advantages of without the need for special nursing, thus extensively
Liked by consumer.A kind of existing glazed ceramic exterior wall tile be by clay, quartz sand and other inorganic non-metallic raw materials,
Through dispensing, ball milling, spray drying, compressing, burn till the technique productions such as biscuit, glaze spraying, glaze firing and make, this technique includes
Burn till twice, the temperature for burning till biscuit for the first time is 800～900 DEG C, it is glaze firing after glaze spraying to burn till for the second time, temperature of glaze firing
At 1000 DEG C or so, the glazed ceramic exterior wall tile that this technique manufacture is obtained has the following disadvantages：1st, water absorption rate is higher, easily takes off
Color, is unfavorable for decoration of exterior wall；2nd, easily crack because of warm and humid change, not wear-resisting, not pressure and can not resist cold.
Content of the invention
It is an object of the invention to provide a kind of manufacture method of glazed ceramic exterior wall tile, this method can solve existing life
The presence water absorption rate of glazed ceramic exterior wall tile obtained in production. art is high, not wear-resisting, not pressure and frigolabile problem.
In order to solve the above problems, the technical solution used in the present invention is：The manufacture method of this glazed ceramic exterior wall tile
It is obtained using the raw material of following percentage by weight：Clay 25～30%, with good fortune soil 25～35%, Herba Epigeneii fargesii 20～22%, potassium sand 20～
25%, wherein, total aluminum content of raw material is 14.5～18%, total iron-holder≤2%；
Its manufacture method is comprised the following steps：
A, by the 10% of the raw material of aforementioned proportion amount of calculation and raw material total amount water, add ball mill be milled to granularity for 45 μm～
50 μm, after then the slip for grinding being sieved except ferrum, material is spray dried to spray drying tower, old more than 48 hours, extremely
Material water content be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～；
B, under the pressure condition of 180～230MPa, with press, the old material of step A is pressed into base substrate, base substrate through 200～
250 DEG C of temperature drying forming obtains adobe, and control adobe moisture content is 0.5%～1%；
C, glaze water being sprayed on adobe surface, be then placed in roller kilns, after drying, delivers to 1210 in 200～400 DEG C of warm area
Burnt till in～1220 DEG C of warm area, brick body water absorption rate is 1～3%, to obtain final product glazed ceramic exterior wall tile.
In the technical scheme of the manufacture method of above-mentioned glazed ceramic exterior wall tile, more specifically technical scheme can also be：Step
Glaze water in rapid C is added water to grind into by the raw material of following weight percents：Methyl 0.5%, corruption receive 1%, Zirconium orthosilicate. 10%, glaze use
White clay 8%, dry powder 15%, frit 15%, potassium feldspar 50.5%.
Further, it is obtained using the raw material of following percentage by weight：Clay 30%, with good fortune soil 30%, Herba Epigeneii fargesii 20%, potassium sand
20%.
Further, old in step A is carried out in the metal bucket of sealing.
Due to employing technique scheme, the present invention is had the advantages that compared with prior art：
1st, the present invention choose clay, with good fortune soil, Herba Epigeneii fargesii and potassium sand as raw material, and except ferrum sieves after slip is worn into, reduce former
Material impurity, in pressing blank post-drying during preparation, then in glaze spraying post-drying, then carries out high temperature and burns till, i.e., using low temperature twice
Dry, method that high temperature burns till, and combine choose raw material, the equipment from being suitable for, optimizing technology parameters, make to be made to
To glazed ceramic exterior wall tile, there is wear-resistant resistance to compression, anti-water suction, freeze proof cold-resistant, and vivid color and luster can be obtained.
2nd, proportioning raw materials, the strict total aluminum content that control in raw material and total iron-holder are adjusted, to improve the glacing flatness of ceramic tile,
Crack prevention and the generation of surface stain；Total aluminum content of control raw material is 14.5～18%, can improve firing temperature, so as to
Can ensure that base substrate and glaze once-firing, and the generation of crackle can be reduced, improve the glacing flatness of ceramic tile；Total iron content of control raw material
Amount≤2%, advantageously ensures that after sieving except ferrum, only contains micro ferrum, and ferrum can be avoided to aoxidize when burning till not exclusively and in ceramic tile
Surface produces stain.
3rd, appropriate water is added, controls the granularity of ball milling to be 45 μm～50 μm, be conducive to controlling the accurate dimension after burning till.
4th, old more than 48 hours after being spray-dried, material water content can accurately be controlled in the range of 7～7.5%, so as to
Improve compacting quality, it is to avoid during compacting, water content is too low, is easily broken off, and water content is too high, then easily produce the defect of layering.
5th, compressing base substrate controls adobe moisture content for 0.5%～1% through 200～250 DEG C of temperature drying, can
Unnecessary moisture is excluded, strengthens the intensity of base substrate, oven drying at low temperature ensure that product is not easy to crack, not stratified.
6th, after glaze spraying water, adobe is put in roller kilns, the warm area for turning base at 200～400 DEG C is dried, and is excluded and is increased because of glaze water
Plus excessive moisture, delivering in 1210～1220 DEG C of warm area carries out high temperature and burns till, and obtains wear-resistant resistance to compression, anti-water suction, freeze proof resistance to
Cold characteristic.
7th, the formula of glaze water coordinates oven drying at low temperature and high temperature high temperature to burn till so that product has excellent anti-glaze fragility, resistance to
The performance of contaminative, the chemical reagent of resistance to family and swimming pool salt.
Specific embodiment
With reference to embodiment, the invention will be further described：
Embodiment 1
The manufacture method of the glazed ceramic exterior wall tile of the present embodiment is obtained using following raw material：28 tons of clay, with good fortune soil 25 tons, stone
22 tons of rice, potassium are husky 25 tons, wherein, total aluminum content 14.5% of raw material, total iron-holder 2%；
Its manufacture method is comprised the following steps：
A, by the 10% of the raw material of aforementioned proportion amount of calculation and raw material total amount water, add ball mill be milled to granularity for 45 μm～
50 μm, after then the slip for grinding being sieved except ferrum, a material is spray dried to spray drying tower, a material is put into the ferrum of sealing
In bucket, old 48 hours, be 7.5% to a material water content；
B, under the pressure condition of 180MPa, with press, the old material of step A is pressed into base substrate, base substrate is through 200 DEG C of temperature
Degree drying forming obtains adobe, and control adobe moisture content is 1%；
C, glaze water is sprayed on adobe surface, glaze water is made up of the raw material mixing and water adding grinding of following weight percents：Methyl 0.5%,
1%, Zirconium orthosilicate. 10%, glaze white clay 8%, dry powder 15%, frit 15%, potassium feldspar 50.5% are received in corruption；It is then placed in roller kilns,
After drying in 200 DEG C of warm area, burnt till in the warm area of delivering to 1210 DEG C, brick body water absorption rate is 3%, to obtain final product outside glazed ceramic
Wall brick.
Embodiment 2
The manufacture method of the glazed ceramic exterior wall tile of the present embodiment is obtained using following raw material：30 tons of clay, with good fortune soil 30 tons, stone
20 tons of rice, potassium is husky 20 tons, wherein, total aluminum content 16% of raw material, total iron-holder 1.5%；
Its manufacture method is comprised the following steps：
A, by the 10% of the raw material of aforementioned proportion amount of calculation and raw material total amount water, add ball mill be milled to granularity for 45 μm～
50 μm, after then the slip for grinding being sieved except ferrum, a material is spray dried to spray drying tower, a material is put into the ferrum of sealing
In bucket, old 50 hours, be 7% to a material water content；
B, under the pressure condition of 200MPa, with press, the old material of step A is pressed into base substrate, base substrate is through 230 DEG C of temperature
Degree drying forming obtains adobe, and control adobe moisture content is 0.8%；
C, glaze water is sprayed on adobe surface, glaze water is made up of the raw material mixing and water adding grinding of following weight percents：Methyl 0.5%,
1%, Zirconium orthosilicate. 10%, glaze white clay 8%, dry powder 15%, frit 15%, potassium feldspar 50.5% are received in corruption；It is then placed in roller kilns,
After drying in 300 DEG C of warm area, burnt till in the warm area of delivering to 1215 DEG C, brick body water absorption rate is 1.5%, to obtain final product glazed ceramic
Exterior wall tile.
Embodiment 3
The manufacture method of the glazed ceramic exterior wall tile of the present embodiment is obtained using following raw material：25 tons of clay, with good fortune soil 35 tons, stone
20 tons of rice, potassium are husky 20 tons, wherein, total aluminum content 18% of raw material, total iron-holder 1%；
Its manufacture method is comprised the following steps：
A, by the 10% of the raw material of aforementioned proportion amount of calculation and raw material total amount water, add ball mill be milled to granularity for 45 μm～
50 μm, after then the slip for grinding being sieved except ferrum, a material is spray dried to spray drying tower, a material is put into the ferrum of sealing
In bucket, old 50 hours, be 7% to a material water content；
B, under the pressure condition of 230MPa, with press, the old material of step A is pressed into base substrate, base substrate is through 250 DEG C of temperature
Degree drying forming obtains adobe, and control adobe moisture content is 0.5%；
C, glaze water is sprayed on adobe surface, glaze water is made up of the raw material mixing and water adding grinding of following weight percents：Methyl 0.5%,
1%, Zirconium orthosilicate. 10%, glaze white clay 8%, dry powder 15%, frit 15%, potassium feldspar 50.5% are received in corruption；It is then placed in roller kilns,
After drying in 400 DEG C of warm area, burnt till in the warm area of delivering to 1220 DEG C, brick body water absorption rate is 1%, to obtain final product outside glazed ceramic
Wall brick.
Glazed ceramic exterior wall tile prepared by various embodiments of the present invention is made the specification of 100mm × 200mm × 7.4mm,
Test according to GB/T 4100-2015 standard, assay such as following table：
.
Claims (4)
1. a kind of manufacture method of glazed ceramic exterior wall tile, it is characterised in that be obtained using the raw material of following percentage by weight：Viscous
Soil 25～30%, with good fortune soil 25～35%, Herba Epigeneii fargesii 20～22%, potassium sand 20～25%, wherein, total aluminum content of raw material is 14.5～
18%th, total iron-holder≤2%；
Its manufacture method is comprised the following steps：
A, by the 10% of the raw material of aforementioned proportion amount of calculation and raw material total amount water, add ball mill be milled to granularity for 45 μm～
50 μm, after then the slip for grinding being sieved except ferrum, material is spray dried to spray drying tower, old more than 48 hours, extremely
Material water content be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～7.5% be 7～；
B, under the pressure condition of 180～230MPa, with press, the old material of step A is pressed into base substrate, base substrate through 200～
250 DEG C of temperature drying forming obtains adobe, and control adobe moisture content is 0.5%～1%；
C, glaze water being sprayed on adobe surface, be then placed in roller kilns, after drying, delivers to 1210 in 200～400 DEG C of warm area
Burnt till in～1220 DEG C of warm area, brick body water absorption rate is 1～3%, to obtain final product glazed ceramic exterior wall tile.
2. the manufacture method of glazed ceramic exterior wall tile according to claim 1, it is characterised in that：Glaze water in step C by
The raw material of following weight percents is added water to grind into：Methyl 0.5%, corruption receives 1%, Zirconium orthosilicate. 10%, glaze white clay 8%, dry powder
15%th, frit 15%, potassium feldspar 50.5%.
3. the manufacture method of glazed ceramic exterior wall tile according to claim 2, it is characterised in that：Using following weight percent
The raw material of ratio is obtained：Clay 30%, with good fortune soil 30%, Herba Epigeneii fargesii 20%, potassium sand 20%.
4. the manufacture method of the glazed ceramic exterior wall tile according to claim 1 or 2 or 3, it is characterised in that：In step A
Old carried out in the metal bucket of sealing.
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| CN116283216A (en) * | 2023-03-30 | 2023-06-23 | 南安协进建材有限公司 | Old floor tile and production process thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116283216A (en) * | 2023-03-30 | 2023-06-23 | 南安协进建材有限公司 | Old floor tile and production process thereof |
| CN116283216B (en) * | 2023-03-30 | 2023-11-28 | 南安协进建材有限公司 | Old floor tile and production process thereof |
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Application publication date: 20170222 |