CN106344463A - Plant composition having scalp care function and preparation method and application thereof - Google Patents
Plant composition having scalp care function and preparation method and application thereof Download PDFInfo
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- CN106344463A CN106344463A CN201610963549.XA CN201610963549A CN106344463A CN 106344463 A CN106344463 A CN 106344463A CN 201610963549 A CN201610963549 A CN 201610963549A CN 106344463 A CN106344463 A CN 106344463A
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- coarse powder
- scalp
- scalp care
- care function
- extraction
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- OIQJEQLSYJSNDS-UHFFFAOYSA-N piroctone Chemical compound CC(C)(C)CC(C)CC1=CC(C)=CC(=O)N1O OIQJEQLSYJSNDS-UHFFFAOYSA-N 0.000 description 1
- 229950001046 piroctone Drugs 0.000 description 1
- 229920002643 polyglutamic acid Polymers 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 239000013641 positive control Substances 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 208000008742 seborrheic dermatitis Diseases 0.000 description 1
- 210000002374 sebum Anatomy 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 description 1
- 229940048109 sodium methyl cocoyl taurate Drugs 0.000 description 1
- JXKPEJDQGNYQSM-UHFFFAOYSA-M sodium propionate Chemical compound [Na+].CCC([O-])=O JXKPEJDQGNYQSM-UHFFFAOYSA-M 0.000 description 1
- 239000004324 sodium propionate Substances 0.000 description 1
- 229960003212 sodium propionate Drugs 0.000 description 1
- 235000010334 sodium propionate Nutrition 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 150000003431 steroids Chemical class 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 230000035900 sweating Effects 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- NCYCYZXNIZJOKI-UHFFFAOYSA-N vitamin A aldehyde Natural products O=CC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C NCYCYZXNIZJOKI-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the field of skin care products, and in particular relates to a plant composition having a scalp care function, and a preparation method and an application thereof. The plant composition having the scalp care function is prepared from the following raw materials: Polygonum multiflorum, Schisandra chinensis, Portulaca oleracea, Salvia officinalis and/or Salvia japonica, Hippophae rhamnoides, and Ajuga ciliata. The above components are reasonably combined and scientifically compounded, and different extraction methods are adopted to extract the raw materials of the composition, so that different effective active ingredients produce a synergistic effect, which greatly stimulates the medicinal properties of the active ingredients. The composition disclosed by the invention has the effects of improving head skin, promoting metabolism, improving blood circulation of cerebral cortex, enhancing hair quality, protecting scalp and hair follicle, moisturizing and nourishing scalp, soothing scalp, restraining skin pruritus caused by dryness, treating tinea capitis, balancing scalp oil and fat, reducing scurf, treating alopecia, and increasing hair glory. The composition is mild to skin, has no stimulation, and has antibacterial and anti-inflammatory effects.
Description
Technical field
The invention belongs to skin care field is and in particular to a kind of vegetable composition with scalp care function and its preparation
Method and application.
Background technology
The hair hair scale piece of health is proper alignment, and scalp is moist, sebum secretion is normal, and microorganism ecological environment is just
Often.The data display in China's Healthy Education Associations scalp health research center, the scalp of the adult of more than China 60wt% is all
There is different degrees of health problem, the wherein dandruff, or even seborrheic dermatitiss are one of main problems.Microorganism is particularly
Amount reproduction on scalp for the pityrosporum furfur (chlosma) is it is considered to be lead to the hypodermal cell of scalp to divide the master accelerating
Want reason, and hypodermal cell division accelerate to lead to the hyperplasia of scalp epidermal area, thus promote corneocyte with white or
The form of Lycoperdon polymorphum Vitt squama comes off extremely, that is, define the dandruff.In addition the exposing to the weather of hair, naturally-aged, wash comb and blow and scald dye,
Hair drying, bifurcated alopecia will be made, hair scale piece is impaired；The use of inappropriate shampoo, can make hair parasteatosis,
Chemical residual is excessive, leads to that hair is excessively oily, hair quality fragility.
At present, the shampoo kind on market is a lot, and effect is different, but most shampoo, more or less all contain
Harmful chemical composition, life-time service can produce certain side effect to human body.And these are converted using industrial chemicals
The hair product of system, only simple decontamination hair care acts on and lacks alimentary health-care function.With people's consumption concept and
The raising of health perception, people thirst for having more hair-washing hair-cares and alimentary health-care function to come out in the new product of one.
Natural plants, have many active ingredients, such as volatile oil, alkaloid, saponin, flavonoid, organic acid etc., and not
With Chinese medicine, there are different efficacies.The pure natural property of Chinese medicine and its distinctive effect, the cosmetics that its extract is made are in hair washing shield
Originating party face, compared with the product of chemosynthesis, has nontoxic, harmless, not carcinogenic etc. unique and significant advantage.
In recent years, cosmetics, progressively to the trend development of " going back to nature ", have started to study washing containing Chinese medicine additive
Shampoo, but the Chinese medicine ingredients that there is also interpolation are many, effect is not prominent, complex process the problems such as.With people's consumption concept and strong
The raising of Kang Yishi, people thirst for thering is more hair-washing hair-cares, alimentary health-care function and avirulence in the new hair products of one
Come out.
Content of the invention
In order to overcome the deficiencies in the prior art and shortcoming, the primary and foremost purpose of the present invention is to provide one kind to have scalp care
The vegetable composition of function.
Another object of the present invention is to providing the preparation method of the above-mentioned vegetable composition with scalp care function.
It is still another object of the present invention to provide the application of the above-mentioned vegetable composition with scalp care function.
The purpose of the present invention is achieved through the following technical solutions:
A kind of vegetable composition with scalp care function, is prepared by following raw material components in parts by mass:
The described vegetable composition with scalp care function, preferably by following raw material components preparation in parts by mass
Obtain:
The preparation method of the described vegetable composition with scalp care function, comprises the steps of:
(1) Radix Polygoni Multiflori, Fructus Schisandrae Sphenantherae, Herba Portulacae, Salvia japonica Thunb., Fructus Hippophae and Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) are separately dried, pulverize and sieve, obtain
Radix Polygoni Multiflori coarse powder, Fructus Schisandrae Sphenantherae coarse powder, Herba Portulacae coarse powder, Salvia japonica Thunb. coarse powder, Fructus Hippophae coarse powder and Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) coarse powder；
(2) Radix Polygoni Multiflori coarse powder, Fructus Schisandrae Sphenantherae coarse powder, Salvia japonica Thunb. coarse powder and Fructus Hippophae coarse powder are mixed, carry out co2Shooting flow
Body extracts；Wherein, Extracting temperature is 35～45 DEG C, and extraction pressure is 25～30mpa, and extraction time is 1～3h, co2Flow velocity is
15～25l/h, separation temperature is 35～45 DEG C, and separating pressure is 5～10mpa；Collect extract, obtain volatile oil and oils and fatss carry
Take thing 1；
(3) plant residue after step (2) extraction is mixed with Herba Portulacae coarse powder, Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) coarse powder, be then added to water
In, it is 50～60 DEG C in temperature, extract power for carrying out microwave radiation exaraction under conditions of 300～500w, extracting solution concentrates, and obtains
To extract 2；
(4) plant residue after extracting in step (3) is mixed with the ethanol water that volume fraction is 50～90%,
Pressure release after 300～500mpa hyperpressure extraction 10～20min, filters；Filtrate concentrates, and obtains extract 3；
(5) by extract 2 prepared to the prepared volatile oil of step (2) and fat extract 1, step (3) and step (4) system
Extract 3 mix homogeneously obtaining, obtains the vegetable composition with scalp care function；
Fructus Schisandrae Sphenantherae described in step (1) and Fructus Hippophae are preferably Fructus Schisandrae Sphenantherae fruit and sea buckthorn fruit；
Sieving described in step (1) preferably crosses 60～100 mesh sieves；
Co described in step (2)2The condition of supercritical fluid extraction is preferably: Extracting temperature is 40 DEG C, extracts pressure
For 28mpa, extraction time is 2h, co2Flow velocity is 20l/h, and separation temperature is 40 DEG C, and separating pressure is 7mpa；
The solid-to-liquid ratio of the microwave radiation exaraction described in step (3) is preferably 1:(15～20), extraction time is 2～4 times,
5～8min every time；
The condition of the microwave radiation exaraction described in step (3) is preferably: temperature is 55 DEG C, and extraction power is 420w；
The relative density of the extract 2 described in step (3) is preferably 1.10～1.20；
Hyperpressure extraction described in step (4) solid-to-liquid ratio be preferably 1:(10～20)；
The condition of the hyperpressure extraction described in step (4) is preferably: 460mpa hyperpressure extraction 15min；
The relative density of the extract 3 described in step (4) is preferably 1.10～1.20；
Application in hair care product for the described vegetable composition with scalp care function；
Concentration in hair care product for the described vegetable composition with scalp care function is 0.1～10%
(w/w)；
Concentration in hair care product for the described vegetable composition with scalp care function is preferably 0.5～
5% (w/w)；
The form of described hair care product is shampoo, hair cream or hair conditioner etc.；
One kind no silicone oil shampoo, comprises following component: have the vegetable composition of scalp care function, live in gentle surface
Property agent, scalp care agent and water；
Described gentle surfactant is preferably sodium methyl cocoyl taurate, sodium lauroyl sarcosine, lauroyl
Sodium glutamate, cocoamido sodium propionate, cocamido propyl betaine, LAA, decyl glucoside and
At least one in tea saponin；
Described scalp care agent is hydrolysed corn starch, pyrrolidone sodium carboxylate, polyglutamic acid sodium, piroctone ethanol
At least one in amine salt and polyquaternary ammonium salt -7；
The principle of the present invention:
Radix Polygoni Multiflori, slightly warm in nature, bitter but sweet flavor is puckery；Main active be chrysophanol, rheum emodin, chrysophanic acid, physcione,
Fatty oil, starch, saccharide, glycoside and lecithin etc..Radix Polygoni Multiflori has defying age, improves immune system, blood fat reducing and anti-tremulous pulse
Atherosis, protection cardiac muscle and the effects such as antibacterial.Its slow down aging is relevant with antioxidation, because the generation of lipid peroxidation
A series of senile symptoms can be caused with deposition, Radix Polygoni Multiflori extract has clearly to the generation of skin lipid peroxide
Inhibition, can be used as the additive of good skin anti-aging cosmetics.And Radix Polygoni Multiflori is traditional hair caring non-defective unit, because of it
Warm in nature, hair can be nourished, give hair deep layer nutrition, make hair pitch-black beautiful.
Fructus Schisandrae Sphenantherae, warm in nature, sour in the mouth, sweet；Main active is volatile oil, organic acid, protein, terpenoid etc..South five
Taste has astringent or styptic treatment for spontaneous sweating, the supplementing QI for promoting the production of body fluid of convergence, effect of kidney calming, has fine hair care hair care and the work(making medicine for curing poliosis
Effect.
Herba Portulacae, cold in nature, sweet in the mouth acid；Main active be two oxyethylamines, malic acid, glucose, calcium, phosphorus, ferrum and
Vitamin e, carotene, vitamin b, vitamin c etc..Herba Portulacae has the effect of heat-clearing and toxic substances removing, cooling blood for hemostasis.Its extract
Have and releive skin and suppress the skin pruritus because drying causes and antibacterial effect.
Salvia japonica Thunb., mild-natured, bitter in the mouth, pungent；Clearing away heat-damp and promoting diuresis；Main active is quintessence oil, terpenoid, Polyphenols chemical combination
Thing and steroid etc..Salvia japonica Thunb. has promoting blood flow to regulate menstruation, effect of removing toxic substances and promoting subsidence of swelling.Its Salvia japonica Thunb. volatile oil has strong clear
New fragrance, can be used for cosmetic essence, fumigating agent and perfume etc..Sage extract can oil-control and pore refining well, right
Greasy hair has damping effect, also has good auxiliary curative effect to seborrheic alopecia.Contained plant phenols in sage extract
Class can significantly inhibit the infection that funguses and mycete etc. cause, and therefore adds it to can remove dandruff, treatment head in shampoo
Tinea and scalp Pruritus, life-time service can make hair pitch-black beautiful.
Fructus Hippophae, warm in nature, sour in the mouth, puckery；Main active is vitamin, fatty acid, trace element, sub- oil element, Hippophac Rhamnoides Yellow
Ketone, superoxides etc., Fructus Hippophae has eliminating phlegm and stopping cough, relieving dyspepsia, effect of promoting blood circulation to remove blood stasis.Fructus Hippophae extract active component is permissible
Help skin to eliminate sensitive response, play and reduce the effect stimulating, eliminating edema and red blood streak, and correct leatherware nutritious and
Protective effect.
Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.), cold in nature, bitter in the mouth；Main active is ecdysterone, cyasterone, ajugasterone b and c, muscles and bones
Careless lactone, ajugose, flavonoid glycoside, Saponin and alkaloid etc., its extract can promote aquaporin aqp3 to express, and strengthens water
Molecule across membranes permeability, is excellent natural moisture preserving agent.
The present invention by Radix Polygoni Multiflori, Fructus Schisandrae Sphenantherae, Herba Portulacae, Salvia japonica Thunb., Fructus Hippophae and Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) reasonable compatibility, scientific matching,
Using different extracting method, compound raw material is extracted so that the effective skin care ingredient in composition material obtains
Maximized utilization, makes different effective active compositions produce synergistic function, greatly excites effective active matter
The property of medicine, said composition has the work improving skin of head, enhancing metabolism, improve cerebral cortex blood circulation, strengthening hair quality
With scalp and hair follicle, moisturizing and nourishing scalp, scalp of releiving, suppression can be protected because of the dry skin pruritus causing, treatment head
Tinea, balancing head haze wax fat, minimizing dandruff, hair growth, increase hair brilliance, gentle to skin, non-stimulated, antibacterial, antiinflammatory.
The present invention has such advantages as with respect to prior art and effect:
(1) vegetable composition with scalp care function that the present invention provides is prepared from by natural plant raw material, can
It is effectively improved skin of head, the effect enhance metabolism, improve cerebral cortex blood circulation, strengthening hair quality, can also protect
Scalp and hair follicle, moisturizing and nourishing scalp, scalp of releiving, suppression are because of the dry skin pruritus causing, treatment tinea capitis, balancing head haze wax
Fat, correct leatherware has excellent nursing function.
(2) vegetable composition with scalp care function of present invention offer is used in hair-washing hair-care articles for use, can depth
Cleaning hair, plays nourishing, sterilization, oil-control, anti-dandruff, antipruritic effect, makes hair natural gloss soft, soft and smooth easy comb after washing
Reason.Life-time service can prevent pore from blocking, blood circulation promoting, so that hair natural health is grown, pitch-black beautiful submissive.
(3) present invention provide have scalp care function vegetable composition gentle to skin, non-stimulated.
Specific embodiment
With reference to embodiment, the present invention is described in further detail, but embodiments of the present invention not limited to this.
Embodiment 1
The Radix Polygoni Multiflori of (1) 20 mass parts, the Fructus Schisandrae Sphenantherae (fruit) of 8 mass parts, the Herba Portulacae of 7 mass parts, 16 mass parts
Salvia japonica Thunb., the Fructus Hippophae (fruit) of 18 mass parts and the Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) of 8 mass parts be separately dried, pulverized 80 mesh sieves, it is first what obtains
Black coarse powder, Fructus Schisandrae Sphenantherae coarse powder, Herba Portulacae coarse powder, Salvia japonica Thunb. coarse powder, Fructus Hippophae coarse powder and Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) coarse powder；
(2) Radix Polygoni Multiflori coarse powder, Fructus Schisandrae Sphenantherae coarse powder, Salvia japonica Thunb. coarse powder and Fructus Hippophae coarse powder are mixed, carry out co2Shooting flow
Body extracts；Wherein, Extracting temperature is 40 DEG C, and extraction pressure is 28mpa, and extraction time is 2h, co2Flow velocity is 20l/h, separates temperature
Spend for 40 DEG C, separating pressure is 7mpa；Collect extract, obtain volatile oil and fat extract 1；
(3) plant residue after step (2) extraction is mixed with Herba Portulacae coarse powder, Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) coarse powder, then according to solid-liquid
It is added to the water than for 1:16；It is 55 DEG C in temperature, extract power for carrying out microwave radiation exaraction under conditions of 420w, extract secondary
Number is 3 times, each 6min；United extraction liquid, it is 1.15 that extracting solution is concentrated into relative density, obtains extract 2；
(4) by the plant residue after extracting in step (3) be 70% with volume fraction ethanol water according to solid-to-liquid ratio
For 1:15 mixing；Pressure release after 460mpa hyperpressure extraction 15min, filters；It is 1.15 that filtrate is concentrated into relative density, is extracted
Thing 3；
(5) by extract 2 prepared to the prepared volatile oil of step (2) and fat extract 1, step (3) and step (4) system
Extract 3 mix homogeneously obtaining, obtains the vegetable composition with scalp care function.
Embodiment 2
(1) by the Radix Polygoni Multiflori of 15 mass parts, the Fructus Schisandrae Sphenantherae (fruit) of 10 mass parts, the Herba Portulacae of 5 mass parts, 20 mass
The Salvia japonica Thunb. of part, the Fructus Hippophae (fruit) of 12 mass parts and the Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) of 10 mass parts are separately dried, pulverized 60 mesh sieves, and what obtains
Radix Polygoni Multiflori coarse powder, Fructus Schisandrae Sphenantherae coarse powder, Herba Portulacae coarse powder, Salvia japonica Thunb. coarse powder, Fructus Hippophae coarse powder and Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) coarse powder；
(2) Radix Polygoni Multiflori coarse powder, Fructus Schisandrae Sphenantherae coarse powder, Salvia japonica Thunb. coarse powder and Fructus Hippophae coarse powder are mixed, carry out co2Shooting flow
Body extracts；Wherein, Extracting temperature is 35 DEG C, and extraction pressure is 30mpa, and extraction time is 3h, co2Flow velocity is 15l/h, separates temperature
Spend for 35 DEG C, separating pressure is 10mpa；Collect extract, obtain volatile oil and fat extract 1；
(3) plant residue after step (2) extraction is mixed with Herba Portulacae coarse powder, Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) coarse powder, then according to solid-liquid
It is added to the water than for 1:15；It is 50 DEG C in temperature, extract power for carrying out microwave radiation exaraction under conditions of 500w, extract secondary
Number is 4 times, each 5min；United extraction liquid, it is 1.20 that extracting solution is concentrated into relative density, obtains extract 2；
(4) by the plant residue after extracting in step (3) be 50% with volume fraction ethanol water according to solid-to-liquid ratio
For 1:10 mixing；Pressure release after 300mpa hyperpressure extraction 20min, filters；It is 1.20 that filtrate is concentrated into relative density, is extracted
Thing 3；
(5) by extract 2 prepared to the prepared volatile oil of step (2) and fat extract 1, step (3) and step (4) system
Extract 3 mix homogeneously obtaining, obtains the vegetable composition with scalp care function.
Embodiment 3
(1) by the Radix Polygoni Multiflori of 25 mass parts, the Fructus Schisandrae Sphenantherae (fruit) of 5 mass parts, the Herba Portulacae of 8 mass parts, 10 mass
The Salvia japonica Thunb. of part, the Fructus Hippophae (fruit) of 24 mass parts and the Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) of 5 mass parts are separately dried, pulverized 100 mesh sieves, and what obtains
Radix Polygoni Multiflori coarse powder, Fructus Schisandrae Sphenantherae coarse powder, Herba Portulacae coarse powder, Salvia japonica Thunb. coarse powder, Fructus Hippophae coarse powder and Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) coarse powder；
(2) Radix Polygoni Multiflori coarse powder, Fructus Schisandrae Sphenantherae coarse powder, Salvia japonica Thunb. coarse powder and Fructus Hippophae coarse powder are mixed, carry out co2Shooting flow
Body extracts；Wherein, Extracting temperature is 45 DEG C, and extraction pressure is 25mpa, and extraction time is 1h, co2Flow velocity is 25l/h, separates temperature
Spend for 45 DEG C, separating pressure is 5mpa；Collect extract, obtain volatile oil and fat extract 1；
(3) plant residue after step (2) extraction is mixed with Herba Portulacae coarse powder, Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) coarse powder, then according to solid-liquid
It is added to the water than for 1:20；It is 60 DEG C in temperature, extract power for carrying out microwave radiation exaraction under conditions of 300w, extract secondary
Number is 2 times, each 8min；United extraction liquid, it is 1.10 that extracting solution is concentrated into relative density, obtains extract 2；
(4) by the plant residue after extracting in step (3) be 90% with volume fraction ethanol water according to solid-to-liquid ratio
For 1:20 mixing；Pressure release after 500mpa hyperpressure extraction 10min, filters；It is 1.10 that filtrate is concentrated into relative density, is extracted
Thing 3；
(5) by extract 2 prepared to the prepared volatile oil of step (2) and fat extract 1, step (3) and step (4) system
Extract 3 mix homogeneously obtaining, obtains the vegetable composition with scalp care function.
Comparative example
(1) Salvia japonica Thunb. of the Radix Polygoni Multiflori of 20 mass parts, the Fructus Schisandrae Sphenantherae (fruit) of 8 mass parts and 16 mass parts is done respectively
Dry, pulverized 80 mesh sieves, obtain Radix Polygoni Multiflori coarse powder, Fructus Schisandrae Sphenantherae coarse powder and Salvia japonica Thunb. coarse powder；
(2) Radix Polygoni Multiflori coarse powder, Fructus Schisandrae Sphenantherae coarse powder and Salvia japonica Thunb. coarse powder are mixed, carry out co2Supercritical fluid extraction；Its
In, Extracting temperature is 40 DEG C, and extraction pressure is 28mpa, and extraction time is 2h, co2Flow velocity is 20l/h, and separation temperature is 40 DEG C,
Separating pressure is 7mpa；Collect extract, obtain volatile oil and fat extract 1；
(3) plant residue after step (2) extraction is added to the water for 1:16 according to solid-to-liquid ratio；It is 55 DEG C in temperature,
Extract power and carry out microwave radiation exaraction under conditions of 420w, extraction time is 3 times, each 6min；United extraction liquid, extracts
It is 1.15 that liquid is concentrated into relative density, obtains extract 2；
(4) by the plant residue after extracting in step (3) be 70% with volume fraction ethanol water according to solid-to-liquid ratio
For 1:15 mixing；Pressure release after 460mpa hyperpressure extraction 15min, filters；It is 1.15 that filtrate is concentrated into relative density, is extracted
Thing 3；
(5) by extract 2 prepared to the prepared volatile oil of step (2) and fat extract 1, step (3) and step (4) system
Extract 3 mix homogeneously obtaining, obtains vegetable composition.
Effect example
1st, test specimen
What embodiment 1～3 was obtained has a vegetable composition of scalp care function and plant that comparative example is obtained
Compositions are detected, are positive control sample with Ketoconazole.
2nd, test index: minimum inhibitory concentration (mic)
It is now recognized that the generation of the dandruff is relevant in the excessive multiplication hypertrophy of scalp with pityrosporum furfur (chlosma).Can
Measure and more in vitro pityrosporum furfur is had or not with inhibitory action and action intensity to evaluate anti-dandruff effect.With reference to American National
Yeast micro-dilution method in the m27-a scheme that Clinical Laboratory Standard committee (nccls) works out, to Malassezia furfur
(malassezia furfur cbs 1878, Dutch Culture Collection) carries out drug sensitivity testing in vitro.
3rd, experimental result
As shown in table 1 to In vitro culture bacterial strain inhibition assay result:
The minimum inhibitory concentration of the vegetable composition with scalp care function that table 1 embodiment 1～3 is obtained
| Sample ID | Minimum inhibitory concentration (mic) |
| Embodiment 1 | 10.6mg/ml |
| Embodiment 2 | 13.7mg/ml |
| Embodiment 3 | 16.3mg/ml |
| Comparative example | 83mg/ml |
| Ketoconazole | 0.03μg/ml |
Note: the activity of Malassezia furfur (m.furfur cbs 1878) bacterium solution is 5.0 × 105cfu/ml.
Application Example
One kind no silicone oil shampoo, comprises following component by mass percentage:
Said components are mixed, no silicone oil shampoo is obtained and carries out relieving itching and removing dandruff effect assessment and improve hair quality effect and comment
Valency:
(1) relieving itching and removing dandruff effect assessment
Evaluation methodology: the experiment number of every kind of shampoo is 24 people, man 12, female 12 at 20～60 years old age, all has
Head pruritus, the symptom more than dandruff.
Using method: wash weekly shampoo of the present invention twice, according to the dense degree of hair, 20～100ml every time, carry out
2 months.
Curative effect judgment criteria is: 1. effective: head pruritus, and dandruff is many or has the fuel-displaced symptom of scalp concurrently and obtains suitable improvement；
2. effective: head pruritus, the symptom that dandruff is many or scalp is fuel-displaced somewhat reduces；3. invalid: using unchanged in front and back.
The effect assessment of relieving itching and removing dandruff is as shown in table 2, compared with comparative example, the plant societys that embodiment 1～3 is obtained
Thing can effective relieving itching and removing dandruff, wherein, embodiment 1 best results.
The vegetable composition relieving itching and removing dandruff effect assessment effect that table 2 embodiment 1～3 and comparative example are obtained
| Sample ID | Effective | Effectively | Invalid | Total effective rate |
| Embodiment 1 | 21 | 3 | 0 | 100% |
| Embodiment 2 | 18 | 5 | 1 | 95.83% |
| Embodiment 3 | 16 | 7 | 1 | 95.83% |
| Comparative example | 14 | 5 | 5 | 79.17% |
(2) improve hair quality effect assessment
Evaluation methodology: the experiment number of every kind of shampoo is 28 women, and at 20～60 years old age, hair shows as different journeys
The withered damage of degree, fragile easily broken, difficult combing.
Using method: wash weekly shampoo of the present invention twice, according to the dense degree of hair, 20～100ml every time, carry out
2 months.
Curative effect judgment criteria: 1. effective: the cardability of hair, stretching force intensity significantly improve；2. effective: the combing of hair
Property, stretching force intensity somewhat improve；3. invalid: using unchanged in front and back.
Improve the effect assessment of hair quality as shown in table 3, compared with comparative example, the plant societys that embodiment 1～3 is obtained
Thing can be effectively improved hair quality, wherein, embodiment 1 best results.
The vegetable composition that table 3 embodiment 1～3 and comparative example are obtained improves hair quality effect assessment effect
Above-described embodiment is the present invention preferably embodiment, but embodiments of the present invention are not subject to above-described embodiment
Limit, other any spirit without departing from the present invention and the change made under principle, modification, replacement, combine, simplify,
All should be equivalent substitute mode, be included within protection scope of the present invention.
Claims (10)
1. a kind of vegetable composition with scalp care function is it is characterised in that by following raw material components system in parts by mass
Standby obtain:
2. the vegetable composition with scalp care function according to claim 1 is it is characterised in that by following by quality
The raw material components of part meter prepare:
3. the preparation method of the vegetable composition with scalp care function described in claim 1 or 2 is it is characterised in that comprise
Following steps:
(1) Radix Polygoni Multiflori, Fructus Schisandrae Sphenantherae, Herba Portulacae, Salvia japonica Thunb., Fructus Hippophae and Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) are separately dried, pulverize and sieve, it is first what obtains
Black coarse powder, Fructus Schisandrae Sphenantherae coarse powder, Herba Portulacae coarse powder, Salvia japonica Thunb. coarse powder, Fructus Hippophae coarse powder and Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) coarse powder；
(2) Radix Polygoni Multiflori coarse powder, Fructus Schisandrae Sphenantherae coarse powder, Salvia japonica Thunb. coarse powder and Fructus Hippophae coarse powder are mixed, carry out co2Supercritical fluid extracts
Take；Wherein, Extracting temperature is 35～45 DEG C, and extraction pressure is 25～30mpa, and extraction time is 1～3h, co2Flow velocity be 15～
25l/h, separation temperature is 35～45 DEG C, and separating pressure is 5～10mpa；Collect extract, obtain volatile oil and fat extract
1；
(3) plant residue after step (2) extraction is mixed with Herba Portulacae coarse powder, Herba ajugae ciliatae (Herba Ajugae Ajuga ciliata Bge.) coarse powder, be then added in water,
Temperature is 50～60 DEG C, extracts power for carrying out microwave radiation exaraction under conditions of 300～500w, extracting solution concentrates, and is carried
Take thing 2；
(4) plant residue after extracting in step (3) is mixed with the ethanol water that volume fraction is 50～90%, 300～
Pressure release after 500mpa hyperpressure extraction 10～20min, filters；Filtrate concentrates, and obtains extract 3；
(5) extract 2 prepared to the prepared volatile oil of step (2) and fat extract 1, step (3) and step (4) are obtained
Extract 3 mix homogeneously, obtains the vegetable composition with scalp care function.
4. the vegetable composition with scalp care function according to claim 3 preparation method it is characterised in that:
Co described in step (2)2The condition of supercritical fluid extraction is: Extracting temperature is 40 DEG C, and extraction pressure is 28mpa, carries
The time is taken to be 2h, co2Flow velocity is 20l/h, and separation temperature is 40 DEG C, and separating pressure is 7mpa.
5. the vegetable composition with scalp care function according to claim 3 preparation method it is characterised in that:
The solid-to-liquid ratio of the microwave radiation exaraction described in step (3) is 1:(15～20), extraction time is 2～4 times, every time 5～
8min.
6. the vegetable composition with scalp care function according to claim 3 preparation method it is characterised in that:
The condition of the microwave radiation exaraction described in step (3) is: temperature is 55 DEG C, and extraction power is 420w.
7. the vegetable composition with scalp care function according to claim 3 preparation method it is characterised in that:
The condition of the hyperpressure extraction described in step (4) is: 460mpa hyperpressure extraction 15min.
8. described in claim 1 or 2, there is the application in hair care product of the vegetable composition of scalp care function.
9. application in hair care product for the vegetable composition with scalp care function according to claim 8,
It is characterized in that:
Concentration in hair care product for the described vegetable composition with scalp care function is 0.1～10%w/w.
10. one kind no silicone oil shampoo is it is characterised in that comprise following component: has scalp care described in claim 1 or 2
The vegetable composition of function, gentle surfactant, scalp care agent and water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610963549.XA CN106344463A (en) | 2016-11-04 | 2016-11-04 | Plant composition having scalp care function and preparation method and application thereof |
Applications Claiming Priority (1)
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| CN201610963549.XA CN106344463A (en) | 2016-11-04 | 2016-11-04 | Plant composition having scalp care function and preparation method and application thereof |
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| CN201610963549.XA Pending CN106344463A (en) | 2016-11-04 | 2016-11-04 | Plant composition having scalp care function and preparation method and application thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112516032A (en) * | 2020-12-17 | 2021-03-19 | 弘美制药（中国）有限公司 | Composition for moistening scalp and repairing hair quality and preparation method and application thereof |
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| CN112516032A (en) * | 2020-12-17 | 2021-03-19 | 弘美制药（中国）有限公司 | Composition for moistening scalp and repairing hair quality and preparation method and application thereof |
| CN112516032B (en) * | 2020-12-17 | 2023-04-04 | 弘美制药（中国）有限公司 | Composition for moistening scalp and repairing hair quality and preparation method and application thereof |
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Application publication date: 20170125 |