CN106343579A - Fish bladder collagen small peptide chelate calcium and preparing method thereof - Google Patents
Fish bladder collagen small peptide chelate calcium and preparing method thereof Download PDFInfo
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- CN106343579A CN106343579A CN201610759324.2A CN201610759324A CN106343579A CN 106343579 A CN106343579 A CN 106343579A CN 201610759324 A CN201610759324 A CN 201610759324A CN 106343579 A CN106343579 A CN 106343579A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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Abstract
The invention relates to a fish bladder collagen small peptide chelate calcium and preparing method thereof, belongs to the technical field of peptide chelate calcium. Considering poor solubility, low absorptivity and large side effect of traditional calcium supplement solution, the invention provides a preparing method of fish bladder collagen small peptide chelate calcium. The invention takes the waste scallop as the source of calcium. After rinsing and soaking in the acid, surface impurity is removed from the scallop. Then use water flying method to remove high density impurity from the scallop. Hydrochloric acid is then arranged to dissolve the scallop to make soluble calcium liquid.The small biological molecules collagen in the fish bladder is used to chelate the soluble calcium to form fish bladder collagen small peptide chelate calcium.The fish bladder collagen small peptide chelate calcium prepared by the invention has good solubility, high absorptivity and excellent in calcium supplement. Fish bladder collagen small peptide chelate calcium is a comprehensive supplement preparation for the supplement of collagen and calcium.
Description
Technical field
The present invention relates to a kind of chelated calcium preparation method of Air Bladder pseudosciaenae seu Acipenser collagen small peptide, belong to chelating calcium technical field.
Background technology
Flourishing of fishery for many years constantly proposes new requirement to its process technology, but just at present, fresh-water fishes
Process technology is relatively also weaker.Edible part is removed, fish internal organs position is often considered discarded in the fresh-water fishes course of processing
Thing abandons, or is only used as fertilizer, feedstuff, causes the significant wastage of fresh water fish resource.The biological micromolecule collagen egg that Air Bladder pseudosciaenae seu Acipenser contains
White matter, is the raw material that human body supplements synthetic protein.And be easy to absorb and utilize.It is to be stored in human body in form of an aqueous solutions
In tissue, thus improving histotrophic nutrition situation and accelerating metabolism.Have been demonstrated that, the food rich in collagenic protein can pass through
The combination water of collagen protein, goes to affect some particular organizations physiological function, thus enhancing development strengthens resistances against diseases, plays
Slow down aging and the efficiency resisting cancer.There is medicine book " Air Bladder pseudosciaenae seu Acipenser " on the books in Chinese Han dynasty as medicinal；Arrive
As one of tribute, theory of Chinese medical science thinks for the Tang Dynasty: " Air Bladder pseudosciaenae seu Acipenser " and has functions that nourishing；It is Ms's beauty care aesthetic health care
Good merchantable brand, medical research finds, the vitamin group containing magnanimity in " Air Bladder pseudosciaenae seu Acipenser ", and various trace elements, wherein Content of Vitamin A
Exceed other fish products, all very good to improving looks, replenishing the calcium.
In recent years, scallop shell is continuously increased as the important marine products economic shellfish yield of China, and account for its gross weight 80 % with
On scallop shell most of are discarded in soot as solid waste or fill out sea, it has also become the big public hazards of environment one, compel to be essential
New technical meanses are wanted to solve this problem.Further, since the content of Calcium Carbonate is up to 95 %, with scallop shell in scallop shell
Have attracted increasing attention for raw material preparation biological calcium.
Calcium is important mineral element in human body, is not only involved in the composition of skeleton, tooth, also to maintenance osmotic pressure and soda acid
The physiological activities such as balance, heartbeat, the conduction of neural impulse have very important effect.But traditional calcium-supplementing preparation such as phosphorus
Sour calcium, Calcium Carbonate, calcium gluconate, calcium acetate, calcium lactate etc., dissolubility is poor, absorbance is low, large side effects.Therefore, for easy
The research of the calcium-supplementing preparation of solution absorption is particularly important.
Content of the invention
The technical problem to be solved: for traditional calcium-supplementing preparation dissolubility poor, absorbance is low, large side effects
Problem, the invention provides a kind of chelated calcium preparation method of Air Bladder pseudosciaenae seu Acipenser collagen small peptide, the present invention with garbage scallop shell is
Calcium source, removes surface impurity after cleaned acid bubble, then removes high density impurity with elutriation, then with dissolving with hydrochloric acid, prepare solvable
Property calcium liquid, and with biological micromolecule collagenic protein chelating solubility calcium in Air Bladder pseudosciaenae seu Acipenser, prepared Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelates calcium.
The Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating the solubility of calcium of present invention preparation is good, and absorbance is high, and effect of supplemented calcium is notable, is both to have supplemented collagen
Albumen supplements the comprehensive supplementing preparation of calcium again.
For solving above-mentioned technical problem, the technical solution used in the present invention is:
(1) weigh the fresh scallop shell of 600 ~ 800g, be washed with deionized scallop shell 3 ~ 5 times, the fresh scallop shell after cleaning
Being immersed in 1 ~ 2l mass fraction is 1 ~ 2h in 1% hydrochloric acid, subsequently filters, is placed in mortar after natural air drying, add 80 ~
120ml deionized water, grinds 20 ~ 30min, obtains pastel, adds 300 ~ 400ml deionized water, collects top suspension, continues
Continuous grind sinking coarse powder 20 ~ 30min, add 300 ~ 400ml deionized water, repeat to grind and collect suspension 3 ~ 5 times, merge outstanding
Supernatant liquid, after standing 2 ~ 3h, filters, and precipitation is added in drying baker, is dried to constant weight at 105 ~ 110 DEG C, will be dried heavy
Form sediment to add in pulverizer and pulverize, cross 200 mesh sieves, obtain scallop shell fine powder；
(2) weigh 50 ~ 100g above-mentioned scallop shell fine powder to add 1 ~ 2l mass fraction is thermostatted water at 70 ~ 80 DEG C in 5% hydrochloric acid
Under bath, with 300 ~ 400r/min stirring reaction 1 ~ 2h, obtain calcium ion acid hydrolysis solution, subsequently acid hydrolysis solution be placed on Rotary Evaporators,
Be evaporated at 50 ~ 55 DEG C ortho acid solution liquid amass 20 ~ 30%, be cooled to room temperature, obtain calcium ion deacidification liquid；
(3) weigh 30 ~ 50g Channa argus fish glue, cut open from Channa argus fish glue one end, remove Channa argus fish glue medium vessels and mucosa, and deionized water
Washing Channa argus fish glue 3 ~ 5 times, after the Channa argus fish glue after cleaning is drained, pours into 3 ~ 10ml above-mentioned calcium ion deacidification liquid at opening, pricks
It is placed in steamer after tight opening, steaming and decocting 1 ~ 2h at 60 ~ 70 DEG C, open Air Bladder pseudosciaenae seu Acipenser and collect mixed liquor in Air Bladder pseudosciaenae seu Acipenser, then use deionization
Water washing Air Bladder pseudosciaenae seu Acipenser inwall 1 ~ 2 time, merges cleaning mixture and mixed liquor, obtains chelatropic reaction liquid；
(4) above-mentioned chelatropic reaction liquid is carried out sucking filtration, the 10 ~ 15% of filtrate evaporation and concentration to stoste volume, obtain paste, by cream
Shape thing add 100 ~ 200ml mass fraction be 90% ethanol solution in, with 300 ~ 500r/min stir 20 ~ 30min, standing 10 ~
12h, subsequently filters, and it is in 90% ethanol solution that filtering residue adds 80 ~ 150ml mass fraction, with 300 ~ 500r/min stirring 20 ~
30min, centrifugation after standing 10 ~ 12h, collect precipitation, precipitation is proceeded in drying baker, be dried extremely permanent at 110 ~ 120 DEG C
Weight, obtains Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating calcium.
The application process of the present invention is: takes the Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating of 0.1 ~ 0.2g present invention preparation daily
Calcium, after one month, calcium deficiency disease reduces 30 ~ 40%, and the Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating calcium absorptivity of present invention preparation is tradition
3 ~ 4 times of calsium supplement.
The method have the benefit that:
(1) the Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating the solubility of calcium of present invention preparation is good, and absorbance is high, and effect of supplemented calcium is notable, is one
Plant the comprehensive supplementing preparation of not only replenishing collagen but also supplementary calcium；
(2) waste material is turned waste into wealth by the Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating calcium of present invention preparation, environmental protection.
Specific embodiment
Weigh the fresh scallop shell of 600 ~ 800g, be washed with deionized scallop shell 3 ~ 5 times, the fresh scallop shell after cleaning
Being immersed in 1 ~ 2l mass fraction is 1 ~ 2h in 1% hydrochloric acid, subsequently filters, is placed in mortar after natural air drying, add 80 ~
120ml deionized water, grinds 20 ~ 30min, obtains pastel, adds 300 ~ 400ml deionized water, collects top suspension, continues
Continuous grind sinking coarse powder 20 ~ 30min, add 300 ~ 400ml deionized water, repeat to grind and collect suspension 3 ~ 5 times, merge outstanding
Supernatant liquid, after standing 2 ~ 3h, filters, and precipitation is added in drying baker, is dried to constant weight at 105 ~ 110 DEG C, will be dried heavy
Form sediment to add in pulverizer and pulverize, cross 200 mesh sieves, obtain scallop shell fine powder；Weigh 50 ~ 100g above-mentioned scallop shell fine powder and add 1 ~ 2l matter
Amount fraction is in 5% hydrochloric acid, under water bath with thermostatic control at 70 ~ 80 DEG C, with 300 ~ 400r/min stirring reaction 1 ~ 2h, obtains calcium ion acid
Solution liquid, subsequently acid hydrolysis solution is placed on Rotary Evaporators, be evaporated at 50 ~ 55 DEG C ortho acid solution liquid amass 20 ~ 30%, cooling
To room temperature, obtain calcium ion deacidification liquid；Weigh 30 ~ 50g Channa argus fish glue, cut open from Channa argus fish glue one end, remove Channa argus fish glue medium vessels and glue
Film, and it is washed with deionized Channa argus fish glue 3 ~ 5 times, after the Channa argus fish glue after cleaning drains, pour into 3 ~ 10ml at opening above-mentioned
Calcium ion deacidification liquid, is placed in after tightening opening in steamer, steaming and decocting 1 ~ 2h at 60 ~ 70 DEG C, opens Air Bladder pseudosciaenae seu Acipenser and collects mixed in Air Bladder pseudosciaenae seu Acipenser
Close liquid, then be washed with deionized Air Bladder pseudosciaenae seu Acipenser inwall 1 ~ 2 time, merge cleaning mixture and mixed liquor, obtain chelatropic reaction liquid；By above-mentioned chelating
Reactant liquor carries out sucking filtration, and the 10 ~ 15% of filtrate evaporation and concentration to stoste volume, obtain paste, paste is added 100 ~ 200ml
Mass fraction is in 90% ethanol solution, stirs 20 ~ 30min with 300 ~ 500r/min, stands 10 ~ 12h, subsequently filters, filtering residue adds
Entering 80 ~ 150ml mass fraction is in 90% ethanol solution, stirs 20 ~ 30min with 300 ~ 500r/min, is centrifuged after standing 10 ~ 12h
Separate, collect precipitation, precipitation is proceeded in drying baker, be dried to constant weight at 110 ~ 120 DEG C, obtain Air Bladder pseudosciaenae seu Acipenser collagen small peptide chela
Close calcium.
Example 1
Weigh the fresh scallop shell of 600g, be washed with deionized scallop shell 3 times, the fresh scallop shell after cleaning is immersed in 1l matter
Amount fraction is 1h in 1% hydrochloric acid, subsequently filters, is placed in mortar after natural air drying, adds 80ml deionized water, grinds
20min, obtains pastel, adds 300ml deionized water, collects top suspension, continues to grind sinking coarse powder 20min, adds
300ml deionized water, repeats to grind and collects suspension 3 times, merges suspension, after standing 2h, filters, precipitation is added drying
In case, it is dried at 105 DEG C to constant weight, dried precipitation is added in pulverizer and pulverizes, cross 200 mesh sieves, obtain scallop shell thin
Powder；Weigh 50g above-mentioned scallop shell fine powder to add 1l mass fraction is in 5% hydrochloric acid, under water bath with thermostatic control at 70 DEG C, with 300r/
Min stirring reaction 1h, obtains calcium ion acid hydrolysis solution, subsequently acid hydrolysis solution is placed on Rotary Evaporators, is evaporated to ortho acid at 50 DEG C
Solution liquid amass 20%, be cooled to room temperature, obtain calcium ion deacidification liquid；Weigh 30g Channa argus fish glue, cut open from Channa argus fish glue one end, except de-etiolation
Air Bladder pseudosciaenae seu Acipenser medium vessels and mucosa, and it is washed with deionized Channa argus fish glue 3 times, after the Channa argus fish glue after cleaning drains, fill at opening
Enter 3ml above-mentioned calcium ion deacidification liquid, be placed in after tightening opening in steamer, steaming and decocting 1h at 60 DEG C, opens Air Bladder pseudosciaenae seu Acipenser and collects Air Bladder pseudosciaenae seu Acipenser
Interior mixed liquor, then it is washed with deionized Air Bladder pseudosciaenae seu Acipenser inwall 1 time, merge cleaning mixture and mixed liquor, obtain chelatropic reaction liquid；By above-mentioned chela
Close reactant liquor and carry out sucking filtration, the 10% of filtrate evaporation and concentration to stoste volume, obtain paste, paste addition 100ml mass is divided
Number is in 90% ethanol solution, stirs 20min with 300r/min, stands 10h, subsequently filters, and filtering residue addition 80ml mass fraction is
In 90% ethanol solution, 20min, centrifugation after standing 10h are stirred with 300r/min, collects precipitation, precipitation is proceeded to drying baker
In, it is dried to constant weight at 110 DEG C, obtain Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating calcium.
The application process of the present invention is: take daily the 0.1g present invention preparation Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating calcium, one
After individual month, calcium deficiency disease reduces 30%, and the Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating calcium absorptivity of present invention preparation is the 3 of traditional calsium supplement
Times.
Example 2
Weigh the fresh scallop shell of 700g, be washed with deionized scallop shell 4 times, the fresh scallop shell after cleaning is immersed in 1.5l
Mass fraction is 1.5h in 1% hydrochloric acid, subsequently filters, is placed in mortar after natural air drying, adds 100ml deionized water, grinds
Mill 25min, obtains pastel, adds 350ml deionized water, collects top suspension, continues to grind sinking coarse powder 25min, plus
Enter 350ml deionized water, repeat to grind and collect suspension 4 times, merge suspension, after standing 2.5h, filter, precipitation is added
In drying baker, it is dried at 108 DEG C to constant weight, dried precipitation is added in pulverizer and pulverizes, cross 200 mesh sieves, obtain scallop
Shell fine powder；Weigh 80g above-mentioned scallop shell fine powder to add 1.5l mass fraction is in 5% hydrochloric acid, under water bath with thermostatic control at 75 DEG C, with
350r/min stirring reaction 1.5h, obtains calcium ion acid hydrolysis solution, subsequently acid hydrolysis solution is placed on Rotary Evaporators, evaporates at 52 DEG C
To ortho acid solution liquid amass 25%, be cooled to room temperature, obtain calcium ion deacidification liquid；Weigh 40g Channa argus fish glue, cut open from Channa argus fish glue one end,
Remove Channa argus fish glue medium vessels and mucosa, and be washed with deionized Channa argus fish glue 4 times, after the Channa argus fish glue after cleaning drains, from opening
Pour into 5ml above-mentioned calcium ion deacidification liquid at mouthful, be placed in after tightening opening in steamer, steaming and decocting 1 ~ 2h at 65 DEG C, open Air Bladder pseudosciaenae seu Acipenser simultaneously
Collect mixed liquor in Air Bladder pseudosciaenae seu Acipenser, then be washed with deionized Air Bladder pseudosciaenae seu Acipenser inwall 1 time, merge cleaning mixture and mixed liquor, obtain chelatropic reaction liquid；
Above-mentioned chelatropic reaction liquid is carried out sucking filtration, the 12% of filtrate evaporation and concentration to stoste volume, obtain paste, paste is added
150ml mass fraction is in 90% ethanol solution, stirs 25min with 400r/min, stands 11h, subsequently filters, filtering residue adds
120ml mass fraction is in 90% ethanol solution, stirs 25min, centrifugation after standing 11h with 400r/min, collects precipitation,
Precipitation is proceeded in drying baker, is dried to constant weight at 115 DEG C, obtain Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating calcium.
The application process of the present invention is: take daily the 0.15g present invention preparation Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating calcium, one
After individual month, calcium deficiency disease reduces 35%, and the Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating calcium absorptivity of present invention preparation is traditional calsium supplement
3.5 again.
Example 3
Weigh the fresh scallop shell of 800g, be washed with deionized scallop shell 5 times, the fresh scallop shell after cleaning is immersed in 2l matter
Amount fraction is 2h in 1% hydrochloric acid, subsequently filters, is placed in mortar after natural air drying, adds 120ml deionized water, grinds
30min, obtains pastel, adds 400ml deionized water, collects top suspension, continues to grind sinking coarse powder 30min, adds
400ml deionized water, repeats to grind and collects suspension 5 times, merges suspension, after standing 3h, filters, precipitation is added drying
In case, it is dried at 110 DEG C to constant weight, dried precipitation is added in pulverizer and pulverizes, cross 200 mesh sieves, obtain scallop shell thin
Powder；Weigh 100g above-mentioned scallop shell fine powder to add 2l mass fraction is in 5% hydrochloric acid, under water bath with thermostatic control at 80 DEG C, with 400r/
Min stirring reaction 2h, obtains calcium ion acid hydrolysis solution, subsequently acid hydrolysis solution is placed on Rotary Evaporators, is evaporated to ortho acid at 55 DEG C
Solution liquid amass 30%, be cooled to room temperature, obtain calcium ion deacidification liquid；Weigh 50g Channa argus fish glue, cut open from Channa argus fish glue one end, except de-etiolation
Air Bladder pseudosciaenae seu Acipenser medium vessels and mucosa, and it is washed with deionized Channa argus fish glue 5 times, after the Channa argus fish glue after cleaning drains, fill at opening
Enter 10ml above-mentioned calcium ion deacidification liquid, be placed in after tightening opening in steamer, steaming and decocting 2h at 70 DEG C, opens Air Bladder pseudosciaenae seu Acipenser and collects Air Bladder pseudosciaenae seu Acipenser
Interior mixed liquor, then it is washed with deionized Air Bladder pseudosciaenae seu Acipenser inwall 2 times, merge cleaning mixture and mixed liquor, obtain chelatropic reaction liquid；By above-mentioned chela
Close reactant liquor and carry out sucking filtration, the 15% of filtrate evaporation and concentration to stoste volume, obtain paste, paste addition 200ml mass is divided
Number, for, in 90% ethanol solution, stirring 30min with 500r/min, stands 12h, subsequently filters, filtering residue adds 150ml mass fraction
For, in 90% ethanol solution, 30min, centrifugation after standing 12h being stirred with 500r/min, collecting precipitation, precipitation is proceeded to drying
In case, it is dried to constant weight at 120 DEG C, obtain Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating calcium.
The application process of the present invention is: take daily the 0.2g present invention preparation Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating calcium, one
After individual month, calcium deficiency disease reduces 40%, and the Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating calcium absorptivity of present invention preparation is the 4 of traditional calsium supplement
Times.
Claims (1)
1. a kind of chelated calcium preparation method of Air Bladder pseudosciaenae seu Acipenser collagen small peptide is it is characterised in that concrete preparation process is:
(1) weigh the fresh scallop shell of 600 ~ 800g, be washed with deionized scallop shell 3 ~ 5 times, the fresh scallop shell after cleaning
Being immersed in 1 ~ 2l mass fraction is 1 ~ 2h in 1% hydrochloric acid, subsequently filters, is placed in mortar after natural air drying, add 80 ~
120ml deionized water, grinds 20 ~ 30min, obtains pastel, adds 300 ~ 400ml deionized water, collects top suspension, continues
Continuous grind sinking coarse powder 20 ~ 30min, add 300 ~ 400ml deionized water, repeat to grind and collect suspension 3 ~ 5 times, merge outstanding
Supernatant liquid, after standing 2 ~ 3h, filters, and precipitation is added in drying baker, is dried to constant weight at 105 ~ 110 DEG C, will be dried heavy
Form sediment to add in pulverizer and pulverize, cross 200 mesh sieves, obtain scallop shell fine powder；
(2) weigh 50 ~ 100g above-mentioned scallop shell fine powder to add 1 ~ 2l mass fraction is thermostatted water at 70 ~ 80 DEG C in 5% hydrochloric acid
Under bath, with 300 ~ 400r/min stirring reaction 1 ~ 2h, obtain calcium ion acid hydrolysis solution, subsequently acid hydrolysis solution be placed on Rotary Evaporators,
Be evaporated at 50 ~ 55 DEG C ortho acid solution liquid amass 20 ~ 30%, be cooled to room temperature, obtain calcium ion deacidification liquid；
(3) weigh 30 ~ 50g Channa argus fish glue, cut open from Channa argus fish glue one end, remove Channa argus fish glue medium vessels and mucosa, and deionized water
Washing Channa argus fish glue 3 ~ 5 times, after the Channa argus fish glue after cleaning is drained, pours into 3 ~ 10ml above-mentioned calcium ion deacidification liquid at opening, pricks
It is placed in steamer after tight opening, steaming and decocting 1 ~ 2h at 60 ~ 70 DEG C, open Air Bladder pseudosciaenae seu Acipenser and collect mixed liquor in Air Bladder pseudosciaenae seu Acipenser, then use deionization
Water washing Air Bladder pseudosciaenae seu Acipenser inwall 1 ~ 2 time, merges cleaning mixture and mixed liquor, obtains chelatropic reaction liquid；
(4) above-mentioned chelatropic reaction liquid is carried out sucking filtration, the 10 ~ 15% of filtrate evaporation and concentration to stoste volume, obtain paste, by cream
Shape thing add 100 ~ 200ml mass fraction be 90% ethanol solution in, with 300 ~ 500r/min stir 20 ~ 30min, standing 10 ~
12h, subsequently filters, and it is in 90% ethanol solution that filtering residue adds 80 ~ 150ml mass fraction, with 300 ~ 500r/min stirring 20 ~
30min, centrifugation after standing 10 ~ 12h, collect precipitation, precipitation is proceeded in drying baker, be dried extremely permanent at 110 ~ 120 DEG C
Weight, obtains Air Bladder pseudosciaenae seu Acipenser collagen small peptide chelating calcium.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610759324.2A CN106343579A (en) | 2016-08-30 | 2016-08-30 | Fish bladder collagen small peptide chelate calcium and preparing method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610759324.2A CN106343579A (en) | 2016-08-30 | 2016-08-30 | Fish bladder collagen small peptide chelate calcium and preparing method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111481458A (en) * | 2020-04-10 | 2020-08-04 | 上海清冬闻晓电子商务有限公司 | Nutrition restoration composition for enhancing postoperative effect of medical and beauty treatment |
| CN116326782A (en) * | 2023-03-31 | 2023-06-27 | 南京北极光生物科技有限公司 | Protein calcium and preparation method thereof |
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| CN102334690A (en) * | 2010-07-27 | 2012-02-01 | 河北农业大学 | A method for preparing calcium citrate from oyster shells and scallop shells |
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| US20160192689A1 (en) * | 2013-07-31 | 2016-07-07 | Wikifoods, Inc. | Encapsulated functional food compositions |
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| CN111481458A (en) * | 2020-04-10 | 2020-08-04 | 上海清冬闻晓电子商务有限公司 | Nutrition restoration composition for enhancing postoperative effect of medical and beauty treatment |
| CN116326782A (en) * | 2023-03-31 | 2023-06-27 | 南京北极光生物科技有限公司 | Protein calcium and preparation method thereof |
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