CN105754768B - A kind of Baby Care handmade soap containing natural Sasanguasaponin and preparation method thereof - Google Patents
A kind of Baby Care handmade soap containing natural Sasanguasaponin and preparation method thereof Download PDFInfo
- Publication number
- CN105754768B CN105754768B CN201610100337.9A CN201610100337A CN105754768B CN 105754768 B CN105754768 B CN 105754768B CN 201610100337 A CN201610100337 A CN 201610100337A CN 105754768 B CN105754768 B CN 105754768B
- Authority
- CN
- China
- Prior art keywords
- parts
- extract
- preparation
- weight
- phases
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 63
- 239000000344 soap Substances 0.000 title claims abstract description 63
- 241000255789 Bombyx mori Species 0.000 claims abstract description 37
- 244000130592 Hibiscus syriacus Species 0.000 claims abstract description 27
- 235000018081 Hibiscus syriacus Nutrition 0.000 claims abstract description 27
- 210000000496 pancreas Anatomy 0.000 claims abstract description 26
- 241000233855 Orchidaceae Species 0.000 claims abstract description 25
- 241000931143 Gleditsia sinensis Species 0.000 claims abstract description 21
- 239000000203 mixture Substances 0.000 claims abstract description 18
- 244000050510 Cunninghamia lanceolata Species 0.000 claims abstract description 17
- 239000010495 camellia oil Substances 0.000 claims abstract description 14
- 240000000249 Morus alba Species 0.000 claims abstract description 11
- 235000008708 Morus alba Nutrition 0.000 claims abstract description 11
- 241001116389 Aloe Species 0.000 claims abstract description 10
- 244000157790 Buglossoides arvense Species 0.000 claims abstract description 10
- 235000004256 Buglossoides arvense Nutrition 0.000 claims abstract description 10
- 235000006040 Prunus persica var persica Nutrition 0.000 claims abstract description 10
- 235000011399 aloe vera Nutrition 0.000 claims abstract description 10
- 239000011435 rock Substances 0.000 claims abstract description 10
- 244000144730 Amygdalus persica Species 0.000 claims abstract description 9
- 244000241838 Lycium barbarum Species 0.000 claims abstract description 9
- 235000015459 Lycium barbarum Nutrition 0.000 claims abstract description 9
- 238000005238 degreasing Methods 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 4
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 51
- 239000007788 liquid Substances 0.000 claims description 48
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 46
- 239000000706 filtrate Substances 0.000 claims description 43
- 238000001914 filtration Methods 0.000 claims description 39
- 238000000108 ultra-filtration Methods 0.000 claims description 28
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 26
- 239000000463 material Substances 0.000 claims description 25
- 238000002390 rotary evaporation Methods 0.000 claims description 20
- 230000002829 reductive effect Effects 0.000 claims description 18
- 239000000843 powder Substances 0.000 claims description 16
- 241000628997 Flos Species 0.000 claims description 15
- 241000533849 Gleditsia Species 0.000 claims description 15
- 229940069521 aloe extract Drugs 0.000 claims description 15
- 235000013399 edible fruits Nutrition 0.000 claims description 15
- 239000003921 oil Substances 0.000 claims description 15
- 238000003809 water extraction Methods 0.000 claims description 15
- 238000001223 reverse osmosis Methods 0.000 claims description 13
- 239000012535 impurity Substances 0.000 claims description 11
- 238000001816 cooling Methods 0.000 claims description 10
- 238000000605 extraction Methods 0.000 claims description 10
- 235000015099 wheat brans Nutrition 0.000 claims description 10
- 235000015911 Amorpha canescens Nutrition 0.000 claims description 8
- 235000013629 Lippia javanica Nutrition 0.000 claims description 8
- 244000107780 Capraria biflora Species 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 239000008280 blood Substances 0.000 claims description 6
- 210000004369 blood Anatomy 0.000 claims description 6
- 238000000151 deposition Methods 0.000 claims description 6
- 238000005266 casting Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000003303 reheating Methods 0.000 claims description 5
- 238000002604 ultrasonography Methods 0.000 claims description 5
- 238000005119 centrifugation Methods 0.000 claims description 4
- 239000003643 water by type Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 22
- 238000005406 washing Methods 0.000 abstract description 9
- 238000004140 cleaning Methods 0.000 abstract description 7
- 241000196324 Embryophyta Species 0.000 abstract description 4
- 238000013329 compounding Methods 0.000 abstract description 2
- 241001465754 Metazoa Species 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 12
- 230000000844 anti-bacterial effect Effects 0.000 description 10
- 239000002956 ash Substances 0.000 description 10
- 238000002156 mixing Methods 0.000 description 8
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 5
- 230000001954 sterilising effect Effects 0.000 description 5
- 238000004659 sterilization and disinfection Methods 0.000 description 5
- 208000001840 Dandruff Diseases 0.000 description 4
- 201000010099 disease Diseases 0.000 description 4
- 239000008233 hard water Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 235000002918 Fraxinus excelsior Nutrition 0.000 description 3
- 241000233866 Fungi Species 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- 230000003110 anti-inflammatory effect Effects 0.000 description 3
- 230000001139 anti-pruritic effect Effects 0.000 description 3
- 239000003908 antipruritic agent Substances 0.000 description 3
- 230000036651 mood Effects 0.000 description 3
- 239000008213 purified water Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 201000004384 Alopecia Diseases 0.000 description 2
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 2
- 208000003351 Melanosis Diseases 0.000 description 2
- PVNIIMVLHYAWGP-UHFFFAOYSA-N Niacin Chemical compound OC(=O)C1=CC=CN=C1 PVNIIMVLHYAWGP-UHFFFAOYSA-N 0.000 description 2
- 102000011759 adducin Human genes 0.000 description 2
- 108010076723 adducin Proteins 0.000 description 2
- 231100000360 alopecia Toxicity 0.000 description 2
- 230000003656 anti-hair-loss Effects 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 238000005202 decontamination Methods 0.000 description 2
- 230000003588 decontaminative effect Effects 0.000 description 2
- 239000006260 foam Substances 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 230000005764 inhibitory process Effects 0.000 description 2
- IYRMWMYZSQPJKC-UHFFFAOYSA-N kaempferol Chemical compound C1=CC(O)=CC=C1C1=C(O)C(=O)C2=C(O)C=C(O)C=C2O1 IYRMWMYZSQPJKC-UHFFFAOYSA-N 0.000 description 2
- 238000002386 leaching Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000003020 moisturizing effect Effects 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 231100000241 scar Toxicity 0.000 description 2
- 208000017520 skin disease Diseases 0.000 description 2
- 239000002689 soil Substances 0.000 description 2
- FTVWIRXFELQLPI-ZDUSSCGKSA-N (S)-naringenin Chemical compound C1=CC(O)=CC=C1[C@H]1OC2=CC(O)=CC(O)=C2C(=O)C1 FTVWIRXFELQLPI-ZDUSSCGKSA-N 0.000 description 1
- HGUVPEBGCAVWID-KETMJRJWSA-N 7-O-(beta-D-glucosyl)isovitexin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC(C(=C1O)[C@H]2[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)O)=CC2=C1C(=O)C=C(C=1C=CC(O)=CC=1)O2 HGUVPEBGCAVWID-KETMJRJWSA-N 0.000 description 1
- 229920001817 Agar Polymers 0.000 description 1
- NEZONWMXZKDMKF-JTQLQIEISA-N Alkannin Chemical group C1=CC(O)=C2C(=O)C([C@@H](O)CC=C(C)C)=CC(=O)C2=C1O NEZONWMXZKDMKF-JTQLQIEISA-N 0.000 description 1
- 239000004229 Alkannin Substances 0.000 description 1
- AFHJQYHRLPMKHU-XXWVOBANSA-N Aloin Natural products O=C1c2c(O)cc(CO)cc2[C@H]([C@H]2[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O2)c2c1c(O)ccc2 AFHJQYHRLPMKHU-XXWVOBANSA-N 0.000 description 1
- 240000001426 Amorpha canescens Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 208000032544 Cicatrix Diseases 0.000 description 1
- UBSCDKPKWHYZNX-UHFFFAOYSA-N Demethoxycapillarisin Natural products C1=CC(O)=CC=C1OC1=CC(=O)C2=C(O)C=C(O)C=C2O1 UBSCDKPKWHYZNX-UHFFFAOYSA-N 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000371 Esterases Proteins 0.000 description 1
- SQUHHTBVTRBESD-UHFFFAOYSA-N Hexa-Ac-myo-Inositol Natural products CC(=O)OC1C(OC(C)=O)C(OC(C)=O)C(OC(C)=O)C(OC(C)=O)C1OC(C)=O SQUHHTBVTRBESD-UHFFFAOYSA-N 0.000 description 1
- 108090000604 Hydrolases Proteins 0.000 description 1
- 102000004157 Hydrolases Human genes 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 108091005804 Peptidases Proteins 0.000 description 1
- 239000001888 Peptone Substances 0.000 description 1
- 108010080698 Peptones Proteins 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 239000004365 Protease Substances 0.000 description 1
- 240000005809 Prunus persica Species 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 1
- 206010067130 Spastic diplegia Diseases 0.000 description 1
- 206010053615 Thermal burn Diseases 0.000 description 1
- 241000130764 Tinea Species 0.000 description 1
- 208000002474 Tinea Diseases 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000008272 agar Substances 0.000 description 1
- 235000019232 alkannin Nutrition 0.000 description 1
- UNNKKUDWEASWDN-UHFFFAOYSA-N alkannin Natural products CC(=CCC(O)c1cc(O)c2C(=O)C=CC(=O)c2c1O)C UNNKKUDWEASWDN-UHFFFAOYSA-N 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 229940006091 aloe polysaccharide Drugs 0.000 description 1
- CPUHNROBVJNNPW-UHFFFAOYSA-N aloin A Natural products OC1C(O)C(O)C(CO)OC1OC1C2=CC(CO)=CC(O)=C2C(=O)C2=C(O)C=CC=C21 CPUHNROBVJNNPW-UHFFFAOYSA-N 0.000 description 1
- AFHJQYHRLPMKHU-WEZNYRQKSA-N aloin B Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1[C@H]1C2=CC(CO)=CC(O)=C2C(=O)C2=C(O)C=CC=C21 AFHJQYHRLPMKHU-WEZNYRQKSA-N 0.000 description 1
- VBIXEXWLHSRNKB-UHFFFAOYSA-N ammonium oxalate Chemical compound [NH4+].[NH4+].[O-]C(=O)C([O-])=O VBIXEXWLHSRNKB-UHFFFAOYSA-N 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000001754 anti-pyretic effect Effects 0.000 description 1
- 239000002221 antipyretic Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 235000015278 beef Nutrition 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 229960003237 betaine Drugs 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 239000007853 buffer solution Substances 0.000 description 1
- QNEFNFIKZWUAEQ-UHFFFAOYSA-N carbonic acid;potassium Chemical compound [K].OC(O)=O QNEFNFIKZWUAEQ-UHFFFAOYSA-N 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 230000010261 cell growth Effects 0.000 description 1
- 206010008129 cerebral palsy Diseases 0.000 description 1
- -1 ceryl alcohols Chemical class 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000010612 desalination reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 230000001079 digestive effect Effects 0.000 description 1
- 230000037336 dry skin Effects 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000010336 energy treatment Methods 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 150000002240 furans Chemical class 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000002779 inactivation Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 150000007529 inorganic bases Chemical class 0.000 description 1
- CDAISMWEOUEBRE-GPIVLXJGSA-N inositol Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@H](O)[C@@H]1O CDAISMWEOUEBRE-GPIVLXJGSA-N 0.000 description 1
- 229960000367 inositol Drugs 0.000 description 1
- AFHJQYHRLPMKHU-UHFFFAOYSA-N isobarbaloin Natural products OC1C(O)C(O)C(CO)OC1C1C2=CC(CO)=CC(O)=C2C(=O)C2=C(O)C=CC=C21 AFHJQYHRLPMKHU-UHFFFAOYSA-N 0.000 description 1
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 description 1
- 235000008777 kaempferol Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- UXOUKMQIEVGVLY-UHFFFAOYSA-N morin Natural products OC1=CC(O)=CC(C2=C(C(=O)C3=C(O)C=C(O)C=C3O2)O)=C1 UXOUKMQIEVGVLY-UHFFFAOYSA-N 0.000 description 1
- 229940117954 naringenin Drugs 0.000 description 1
- WGEYAGZBLYNDFV-UHFFFAOYSA-N naringenin Natural products C1(=O)C2=C(O)C=C(O)C=C2OC(C1)C1=CC=C(CC1)O WGEYAGZBLYNDFV-UHFFFAOYSA-N 0.000 description 1
- 235000007625 naringenin Nutrition 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 229960003512 nicotinic acid Drugs 0.000 description 1
- 235000001968 nicotinic acid Nutrition 0.000 description 1
- 239000011664 nicotinic acid Substances 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 150000007530 organic bases Chemical class 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 235000019319 peptone Nutrition 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 229920001184 polypeptide Polymers 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 102000004196 processed proteins & peptides Human genes 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- HGUVPEBGCAVWID-UHFFFAOYSA-N saponarin Natural products OC1C(O)C(O)C(CO)OC1OC(C(=C1O)C2C(C(O)C(O)C(CO)O2)O)=CC2=C1C(=O)C=C(C=1C=CC(O)=CC=1)O2 HGUVPEBGCAVWID-UHFFFAOYSA-N 0.000 description 1
- 230000037387 scars Effects 0.000 description 1
- CDAISMWEOUEBRE-UHFFFAOYSA-N scyllo-inosotol Natural products OC1C(O)C(O)C(O)C(O)C1O CDAISMWEOUEBRE-UHFFFAOYSA-N 0.000 description 1
- 210000002374 sebum Anatomy 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000000271 synthetic detergent Substances 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 230000017423 tissue regeneration Effects 0.000 description 1
- 230000001256 tonic effect Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 229930182493 triterpene saponin Natural products 0.000 description 1
- 150000008130 triterpenoid saponins Chemical class 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
- 230000029663 wound healing Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/045—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on non-ionic surface-active compounds and soap
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of Baby Care handmade soap containing natural Sasanguasaponin and preparation method thereof, its is raw materials used to include by weight：Wild 10 ~ 30 parts of tea oil, 10 ~ 20 parts of Oil-tea-cake, 5 ~ 10 parts of Chinese honey locust, 5 ~ 15 parts of pig pancreas, 5 ~ 10 parts of China fir ash, 5 ~ 10 parts of the rose of Sharon, 1 ~ 5 part of aloe, 3 ~ 5 parts of the root bark of white mulberry, 5 ~ 10 parts of Asian puccoon, 2 ~ 5 parts of matrimony vine, 1 ~ 3 part of stiff silkworm, 3 ~ 5 parts of peach blossom, 3 ~ 5 parts of orchid, 3 ~ 8 parts of KOH, 1 part of rock sugar.The present invention is based on a variety of animals and plants degreasing compositions, natural plant component of the compounding with cosmetology effect, develops a kind of natural Manual perfumed soap, and it collects a variety of functions such as hair washing, face cleaning, shower, washing, there are stronger washing cleaning capacity and good security, be adapted to baby to use.
Description
Technical field
The invention belongs to daily chemical product technical field, and in particular to a kind of Baby Care handmade soap containing natural Sasanguasaponin
And preparation method thereof.
Background technology
Perfumed soap is the articles for washing for being usually used in deterging skin day, as the quick more new development of scientific level and people are lived
Horizontal continuous improvement, people are no longer only limitted to most basic washing cleaning action for the requirement that perfumed soap acts on, and start to arrange
Denounce the perfumed soap as made from chemical composition, simultaneously as perfumed soap neutral and alkali is too strong to wash away a large amount of sebums of skin surface, make skin mistake
It is even red and swollen in drying, allergy, decline the protective effect of skin, be susceptible to suffer from disease of skin.Therefore, it is raw material by natural animal-plant
What exploitation formed not only turns into people with very strong cleaning function and with preferable skin care effect, Manual perfumed soap safe to use
New pursuit, and its degradability is better than synthetic detergent, the more research and development focus as soap production field.
The content of the invention
It is an object of the invention to provide a kind of Baby Care handmade soap containing natural Sasanguasaponin and preparation method thereof, its
Soap base is mixed to prepare by organic base, inorganic base and grease, compounded with the vegetalitas soil release component such as Sasanguasaponin, Chinese honey locust, rose of Sharon, pole
Big overcomes the shortcomings that soap base is hard water resistance poor, then attaches natural plant component to reach skin care water retention, institute well
Obtaining Manual perfumed soap has hair washing, has a bath, washs a variety of functions such as clothing, has a variety of protrusions such as beauty, health care, sterilization, sterilization concurrently
Effect.
To achieve the above object, the present invention adopts the following technical scheme that：
A kind of Baby Care handmade soap containing natural Sasanguasaponin, its is raw materials used to include by weight：Wild tea oil 10 ~
30 parts, 10 ~ 20 parts of Oil-tea-cake, 5 ~ 10 parts of Chinese honey locust, 5 ~ 15 parts of pig pancreas, 5 ~ 10 parts of China fir ash, shrub althea flower and 5 ~ 10 parts of leaf, aloe
1 ~ 5 part, 3 ~ 5 parts of the root bark of white mulberry, 5 ~ 10 parts of Asian puccoon, 2 ~ 5 parts of matrimony vine, 1 ~ 3 part of stiff silkworm, 3 ~ 5 parts of peach blossom, 3 ~ 5 parts of orchid, KOH 3 ~ 8
Part, 1 part of rock sugar.
The China fir ash is will to dry to crush after China fir leaf fully burns to be made.
The preparation method of the Baby Care handmade soap containing natural Sasanguasaponin comprises the following steps：
1）The preparation of stiff silkworm powder：0.5-1 times of wheat bran of stiff silkworm weight is roasted in pot to 50% charing, then added stiff
Silkworm, roast untill stiff silkworm becomes yellowish-brown, wheat bran is screened out after cooling, the abundant crushed after being dried of stiff silkworm to 300 ~ 400 mesh obtains stiff
Silkworm powder；
2）The preparation of Sasanguasaponin：Two parts will be divided into after the complete degreasing of Oil-tea-cake, crushing, by feed liquid weight than 1:15
95 ~ 100 DEG C of hot water is added in a copy of it Oil-tea-cake crushed material, 38min is extracted, filters out residue；Added in gained filtrate
Another Oil-tea-cake crushed material, the hot water of 3 times of crushed material weight is added, continue to extract 38min, filtering；Filtrate through dish-style from
The heart, ultrafiltration, rotary evaporation to paste, obtain Sasanguasaponin；
3）The preparation of Fructus Gleditsia extract：Two parts will be divided into after Chinese honey locust drying, crushing, a copy of it Chinese honey locust crushed material is existed
With 85 ~ 95 DEG C, feed liquid weight than 1 in Ultrasound Instrument:Hot water extraction 25min under the conditions of 12, filtering, remove residue；In gained filtrate
Middle another Chinese honey locust crushed material of addition, in 85 ~ 95 DEG C, feed liquid weight than 1:Hot water extraction 15min under the conditions of 6, filtering；Filtrate passes through
Disk centrifugal, ultrafiltration, rotary evaporation to paste, obtain Fructus Gleditsia extract；
4）The preparation of pig pancreas stamping：Fresh pig pancreas is washed away into watery blood, is cut into small pieces, finely ground rock sugar is added, fills
Divide after smashing to pieces to add and mixed with heavy purified waters such as rock sugar, obtain pig pancreas stamping；
5）The preparation of aloe extract：Fresh aloe is taken, washes away surface dirt impurity, by feed liquid weight than 1:1 adds water,
Fully smashed to pieces in juice extractor, leach fresh juice；Filter residue is by feed liquid weight than 1:6 add the ethanol solution that mass concentration is 45%, in 75
~ 80 DEG C extraction 35min, filtering, filtrate through disk centrifugal, ultrafiltration, it is reverse osmosis concentrated be reduced to 25 ~ 30 Brix after, with first time gained
Fresh juice mixing, obtains aloe extract；
6）The preparation of rose of Sharon extract：Shrub althea flower and leaf are washed away into surface dirt impurity respectively, by feed liquid weight than 1:1 adds
Enter water, fully smashed to pieces in juice extractor, juice is leached；Filter residue is by feed liquid weight than 1:After 8 add water, in 65 ~ 70 DEG C of extractions
24h, filtering；Filtrate mixes after disk centrifugal, rotary evaporation to paste with first time gained juice, obtains rose of Sharon extract；
7）The preparation of Flos persicae extract or orchid extract：Add water in peach blossom or orchid, squeezed the juice in juice extractor,
Then 5 times of water weight, the ethanol solution that mass concentration is 65%, are extracted under the conditions of 65 ~ 70 DEG C used in being added in juice
25min, filtering, filtrate through disk centrifugal, ultrafiltration, it is reverse osmosis concentrated be reduced to 25 ~ 30 Brix, obtain Flos persicae extract or orchid extraction
Thing；
8）The preparation of the root bark of white mulberry-wolfberry fruit extract：By the root bark of white mulberry it is dry, be crushed to 10 ~ 20 mesh after add matrimony vine, 95 ~
100 DEG C, feed liquid weight ratio be 1:Hot water extraction 75min under the conditions of 25, filtering；Filter residue is in 95 ~ 100 DEG C, feed liquid weight than 1:10
Under the conditions of reheating flooding 15min, filtering；Merge filter liquor twice, through disk centrifugal, ultrafiltration, rotary evaporation to paste, obtain mulberry
Bai Pi-wolfberry fruit extract；
9）The preparation of Groomwell root oil：Asian puccoon is immersed in the wild tea oil of its 1-2 times of weight, soaked under the conditions of normal temperature darkness
21d, filtering；The remaining wild tea oil of filter residue soaks 1.5 h, then heating extraction 25min, and the h of diacolation 12 is stood after cooling fills it
Divide filtering, merge filtrate twice, obtain Groomwell root oil；
10）The preparation of Manual perfumed soap：KOH is configured to the KOH solution that mass concentration is 30%, is then added into and adds
In the Groomwell root oil of heat to 60 DEG C and the mixture of Sasanguasaponin, it is stirred continuously using 500 r/min to paste and is used as A phases；By China fir
Ash is slowly added into pig pancreas stamping and constantly stirred evenly as B phases；Fructus Gleditsia extract and rose of Sharon extract are mixed and mixed thoroughly
As C phases；The root bark of white mulberry-wolfberry fruit extract, stiff silkworm powder, aloe extract are mixed and mixed thoroughly as D phases；By Flos persicae extract and
Orchid extract is mixed and mixed thoroughly as E phases；By A heat phases to 60 DEG C, add B phases, C phases and constantly stir evenly, treat temperature reduction
D phases are added to 55 DEG C to stir evenly, and are finally cooled to 50 DEG C of addition E phases and are mixed simultaneously casting thoroughly, are produced after depositing 28 ~ 31 d.
Sasanguasaponin is pentacyclic triterpene saponins, HLB value 16, has emulsification well, scattered and foamability, has simultaneously
Good bactericidal properties, so there is very strong degreasing bactericidal action, and there is no excitant to skin；Peach blossom contains Kaempferol, three
The main components such as leaf beans glycosides, naringenin, vitamin, can expand capillary, improve blood circulation, so as to promote skin-nourishing and
The supply of oxygen, skin care, the deposition for preventing melanin in skin, it has the function that to refresh oneself, adjusts mood with orchid compounding；
Matrimony vine contains glycine betaine, multivitamin（VB1, VB2 etc.）, the composition such as nicotinic acid, have good anti-aging, skin nutrition, preventing and treating
Alopecia and white hair etc. acts on；Asian puccoon main component is alkannin, has antipruritic, antipyretic, anti-inflammatory, convergence, the function of antibacterial, can nurse one's health
Skin and hair, there is the effect of fine to skin diseases such as pachylosis, scars；Aloe contains aloin, aloe polysaccharide, amino
The compositions such as acid, organic acid, enzyme, it is nutritious to skin, moisten moisturizing, be nti-freckle, crease-resistant, antibacterial（Predominantly fungi）, antiultraviolet,
Promote the effect such as cell growth, be advantageous to tissue repair and wound healing, while it has good hair tonic, black hair effect；Pig pancreas
Dirty similar fat, also containing compositions such as pancreas fat digestive ferment, elastoser, polypeptides, China fir ash mainly contains carbonic acid potassium composition, will
Pig pancreas and China fir ash form the main component of perfumed soap, can form that quality is fine and smooth, gentle to skin, ability of cleaning greasy dirt is strong, and energy
Dry skin, chap are prevented, there is the Natural toilet soap for moistening the effects such as foster skin, if there is the effect of anti-dandruff and itching-relieving for hair,
And China fir ash also has the function that preferable soil pick-up decontamination；The root bark of white mulberry contains the compositions such as abundant flavonoids, mulberry furans, polysaccharide,
There are very strong anti-inflammatory, antibacterial, repair tissue cell, desalination scar etc. to skin, its manufactured perfumed soap has in hair washing
The effect of anti-dandruff, Anti-hair loss, dark hair；Stiff silkworm contains the compositions such as abundant protein, esterase, protease, hydrolase, ammonium oxalate,
Being used in perfumed soap has good nutrition skin hair, anti-inflammatory, antibacterial（In particular pathomycete）, whitening, the effect such as nti-freckle；Shrub althea flower
Contain the important components such as protein, reduced sugar, saponarin, inositol, mucilaginous substance with shrubalthea leaf, its antibacterial having, heat-clearing are cool
The effects such as blood, removing toxicity for detumescence can make perfumed soap have preferably washing decontamination, skin care, anti-dandruff, the soft hair of dark hair and treatment skin disease
Disease（Skin tinea, scald）Deng effect；Chinese honey locust has stronger washing degreasing energy containing compositions such as triterpenoid saponin, tannin, ceryl alcohols
Power, its antibacterial action can prevent the generation of scurf, while play the role of Anti-hair loss and black hair.
The remarkable advantage of the present invention is：Gained Baby Care handmade soap of the invention have skin care, nourishes rough skin, it is antipruritic,
The effect of freeze proof sore, fatigue of refreshing oneself, regulation mood, anti-drying furfur, preventing and treating alopecia, dark hair, anti-harm ray etc..Its component
Both from the extract of natural animal-plant, without any hormone, have no side effect, there is higher safety in utilization, do not only have
Stronger cleaning function, also skin care effect, or even energy treatment part disease of skin, and its alkalescence is small, its delicate fragrance is naturally spent
People can refresh oneself after, adjust mood for perfume (or spice).
Embodiment
In order that content of the present invention easily facilitates understanding, with reference to embodiment to of the present invention
Technical scheme is described further, but the present invention is not limited only to this.
It will dry to crush after China fir leaf fully burns and required China fir ash is made.
Embodiment 1
The preparation method of Baby Care handmade soap containing natural Sasanguasaponin, comprises the following steps：
1）The preparation of stiff silkworm powder：1 parts by weight wheat bran is roasted in pot to 50% charing, then adds 1 parts by weight stiff silkworm,
Roast untill stiff silkworm becomes yellowish-brown, wheat bran is screened out after cooling, by the abundant crushed after being dried of stiff silkworm to 400 mesh, obtains stiff silkworm powder；
2）The preparation of Sasanguasaponin：Two parts will be divided into after the complete degreasing of 20 parts by weight Oil-tea-cakes, crushing, by feed liquid weight
Than 1:15 add 95 DEG C of hot water in wherein a Oil-tea-cake crushed material, extract 38min, filter out residue；In gained filtrate
Another Oil-tea-cake crushed material is added, adds the hot water of 3 times of crushed material weight, continues to extract 38min, filtering；Filtrate is through dish
Formula centrifugation, ultrafiltration, rotary evaporation to paste, obtain Sasanguasaponin；
3）The preparation of Fructus Gleditsia extract：Two parts will be divided into after the drying of 10 parts by weight Chinese honey locusts, crushing, by a copy of it Chinese honey locust
Crushed material is in Ultrasound Instrument with 95 DEG C, feed liquid weight than 1:Hot water extraction 25min under the conditions of 12, filtering, remove residue；In gained
Another Chinese honey locust crushed material is added in filtrate, in 85 DEG C, feed liquid weight than 1:Hot water extraction 15min under the conditions of 6, filtering；Filtrate
Through disk centrifugal, ultrafiltration, rotary evaporation to paste, Fructus Gleditsia extract is obtained；
4）The preparation of pig pancreas stamping：The fresh pig pancreas of 10 parts by weight is washed away into watery blood, is cut into small pieces, adds 1 weight
The finely ground rock sugar of part, the mixing of 1 parts by weight purified water is added after fully smashing to pieces, obtains pig pancreas stamping；
5）The preparation of aloe extract：The fresh parts by weight of aloe 2 are taken, surface dirt impurity are washed away, by feed liquid weight than 1:1 adds
Enter water, fully smashed to pieces in juice extractor, leach fresh juice；Filter residue is by feed liquid weight than 1:The ethanol that 6 addition mass concentrations are 45% is molten
Liquid, in 78 DEG C extract 35min, filtering, filtrate through disk centrifugal, ultrafiltration, it is reverse osmosis concentrated be reduced to 26 Brix after, with first time institute
Fresh juice mixing is obtained, obtains aloe extract；
6）The preparation of rose of Sharon extract：5 parts by weight shrub althea flowers and leaf are washed away into surface dirt impurity respectively, by feed liquid weight
Than 1:1 adds water, is fully smashed to pieces in juice extractor, juice is leached；Filter residue is by feed liquid weight than 1:After 8 add water, in 70 DEG C of leachings
24h is carried, is filtered；Filtrate mixes after disk centrifugal, rotary evaporation to paste with first time gained juice, obtains rose of Sharon extract；
7）The preparation of Flos persicae extract：Add 1 parts by weight water in 3 parts by weight peach blossoms, squeezed the juice in juice extractor, then
5 times of water weight, the ethanol solution that mass concentration is 65%, 25min is extracted under the conditions of 65 DEG C, is filtered used in being added in juice,
Filtrate through disk centrifugal, ultrafiltration, it is reverse osmosis concentrated be reduced to 25 Brix, obtain Flos persicae extract；
8）The preparation of orchid extract：Add 1 parts by weight water in 5 parts by weight orchids, squeezed the juice in juice extractor, then
5 times of water weight, the ethanol solution that mass concentration is 65%, 25min is extracted under the conditions of 68 DEG C, is filtered used in being added in juice,
Filtrate through disk centrifugal, ultrafiltration, it is reverse osmosis concentrated be reduced to 28 Brix, obtain orchid extract；
9）The preparation of the root bark of white mulberry-wolfberry fruit extract：By the 3 parts by weight root barks of white mulberry it is dry, be crushed to after 10 mesh and add 2 parts by weight
Matrimony vine, it is 1 in 95 DEG C, feed liquid weight ratio:Hot water extraction 75min under the conditions of 25, filtering；Filter residue is in 95 DEG C, feed liquid weight than 1:
Reheating flooding 15min under the conditions of 10, filtering；Merge filter liquor twice, through disk centrifugal, ultrafiltration, rotary evaporation to paste, obtain
The root bark of white mulberry-wolfberry fruit extract；
10）The preparation of Groomwell root oil：5 parts by weight Asian puccoons are immersed in 5 parts by weight open country tea oil, soaked under the conditions of normal temperature darkness
Steep 21d, filtering；Filter residue soaks 1.5 h with 5 parts by weight open country tea oil again, then heating extraction 25min, and diacolation 12 is stood after cooling
H makes it fully filter, and merges filtrate twice, obtains Groomwell root oil；
11）The preparation of Manual perfumed soap：3 parts by weight KOH are configured to the KOH solution that mass concentration is 30%, then added
Enter into the Groomwell root oil and the mixture of Sasanguasaponin for being heated to 60 DEG C, be stirred continuously using 500 r/min to paste and be used as A phases；
10 parts by weight China fir ashes are slowly added into pig pancreas stamping and constantly stirred evenly as B phases；Fructus Gleditsia extract and the rose of Sharon are carried
Take thing to mix and mix thoroughly as C phases；The root bark of white mulberry-wolfberry fruit extract, stiff silkworm powder, aloe extract are mixed and mixed thoroughly as D phases；
Flos persicae extract and orchid extract are mixed and mixed thoroughly as E phases；By A heat phases to 60 DEG C, add B phases, C phases and constantly stir
It is even, treat that temperature is reduced to 55 DEG C of addition D phases and stirred evenly, be finally cooled to 50 DEG C of addition E phases and mix simultaneously casting thoroughly, after depositing 28 d
Produce.
Embodiment 2
The preparation method of Baby Care handmade soap containing natural Sasanguasaponin, comprises the following steps：
1）The preparation of stiff silkworm powder：1 parts by weight wheat bran is roasted in pot to 50% charing, then adds 2 parts by weight stiff silkworms,
Roast untill stiff silkworm becomes yellowish-brown, wheat bran is screened out after cooling, by the abundant crushed after being dried of stiff silkworm to 300 mesh, obtains stiff silkworm powder；
2）The preparation of Sasanguasaponin：Two parts will be divided into after the complete degreasing of 15 parts by weight Oil-tea-cakes, crushing, by feed liquid weight
Than 1:15 add 98 DEG C of hot water in wherein a Oil-tea-cake crushed material, extract 38min, filter out residue；In gained filtrate
Another Oil-tea-cake crushed material is added, adds the hot water of 3 times of crushed material weight, continues to extract 38min, filtering；Filtrate is through dish
Formula centrifugation, ultrafiltration, rotary evaporation to paste, obtain Sasanguasaponin；
3）The preparation of Fructus Gleditsia extract：Two parts will be divided into after the drying of 8 parts by weight Chinese honey locusts, crushing, by a copy of it Chinese honey locust
Crushed material is in Ultrasound Instrument with 90 DEG C, feed liquid weight than 1:Hot water extraction 25min under the conditions of 6, filtering, remove residue；In gained
Another Chinese honey locust crushed material is added in filtrate, in 90 DEG C, feed liquid weight than 1:Hot water extraction 15min under the conditions of 6, filtering；Filtrate
Through disk centrifugal, ultrafiltration, rotary evaporation to paste, Fructus Gleditsia extract is obtained；
4）The preparation of pig pancreas stamping：The fresh pig pancreas of 5 parts by weight is washed away into watery blood, is cut into small pieces, adds 1 parts by weight
Finely ground rock sugar, the mixing of 1 parts by weight purified water is added after fully smashing to pieces, obtains pig pancreas stamping；
5）The preparation of aloe extract：The fresh parts by weight of aloe 1 are taken, surface dirt impurity are washed away, by feed liquid weight than 1:1 adds
Enter water, fully smashed to pieces in juice extractor, leach fresh juice；Filter residue is by feed liquid weight than 1:The ethanol that 6 addition mass concentrations are 45% is molten
Liquid, in 75 DEG C extract 35min, filtering, filtrate through disk centrifugal, ultrafiltration, it is reverse osmosis concentrated be reduced to 25 Brix after, with first time institute
Fresh juice mixing is obtained, obtains aloe extract；
6）The preparation of rose of Sharon extract：8 parts by weight shrub althea flowers and leaf are washed away into surface dirt impurity respectively, by feed liquid weight
Than 1:1 adds water, is fully smashed to pieces in juice extractor, juice is leached；Filter residue is by feed liquid weight than 1:After 8 add water, in 68 DEG C of leachings
24h is carried, is filtered；Filtrate mixes after disk centrifugal, rotary evaporation to paste with first time gained juice, obtains rose of Sharon extract；
7）The preparation of Flos persicae extract：Add 1 parts by weight water in 4 parts by weight peach blossoms, squeezed the juice in juice extractor, then
5 times of water weight, the ethanol solution that mass concentration is 65%, 25min is extracted under the conditions of 68 DEG C, is filtered used in being added in juice,
Filtrate through disk centrifugal, ultrafiltration, it is reverse osmosis concentrated be reduced to 28 Brix, obtain Flos persicae extract；
8）The preparation of orchid extract：Add 1 parts by weight water in 3 parts by weight orchids, squeezed the juice in juice extractor, then
5 times of water weight, the ethanol solution that mass concentration is 65%, 25min is extracted under the conditions of 65 DEG C, is filtered used in being added in juice,
Filtrate through disk centrifugal, ultrafiltration, it is reverse osmosis concentrated be reduced to 25 Brix, obtain orchid extract；
9）The preparation of the root bark of white mulberry-wolfberry fruit extract：By the 4 parts by weight root barks of white mulberry it is dry, be crushed to after 10 mesh and add 3 parts by weight
Matrimony vine, it is 1 in 98 DEG C, feed liquid weight ratio:Hot water extraction 75min under the conditions of 25, filtering；Filter residue is in 98 DEG C, feed liquid weight than 1:
Reheating flooding 15min under the conditions of 10, filtering；Merge filter liquor twice, through disk centrifugal, ultrafiltration, rotary evaporation to paste, obtain
The root bark of white mulberry-wolfberry fruit extract；
10）The preparation of Groomwell root oil：8 parts by weight Asian puccoons are immersed in the wild tea oil of its 2 times of weight, in normal temperature darkness condition
Lower immersion 21d, filtering；Filter residue soaks 1.5 h with 6 parts by weight open country tea oil again, then heating extraction 25min, stands and oozes after cooling
12 h that filter make it fully filter, and merge filtrate twice, obtain Groomwell root oil；
11）The preparation of Manual perfumed soap：4 parts by weight KOH are configured to the KOH solution that mass concentration is 30%, then added
Enter into the Groomwell root oil and the mixture of Sasanguasaponin for being heated to 60 DEG C, be stirred continuously using 500 r/min to paste and be used as A phases；
8 parts by weight China fir ashes are slowly added into pig pancreas stamping and constantly stirred evenly as B phases；Fructus Gleditsia extract and the rose of Sharon are extracted
Thing is mixed and mixed thoroughly as C phases；The root bark of white mulberry-wolfberry fruit extract, stiff silkworm powder, aloe extract are mixed and mixed thoroughly as D phases；Will
Flos persicae extract and orchid extract are mixed and mixed thoroughly as E phases；By A heat phases to 60 DEG C, add B phases, C phases and constantly stir
It is even, treat that temperature is reduced to 55 DEG C of addition D phases and stirred evenly, be finally cooled to 50 DEG C of addition E phases and mix simultaneously casting thoroughly, after depositing 30d
Produce.
Embodiment 3
The preparation method of Baby Care handmade soap containing natural Sasanguasaponin, comprises the following steps：
1）The preparation of stiff silkworm powder：3 parts by weight wheat brans are roasted in pot to 50% charing, then add 3 parts by weight stiff silkworms,
Roast untill stiff silkworm becomes yellowish-brown, wheat bran is screened out after cooling, by the abundant crushed after being dried of stiff silkworm to 300 mesh, obtains stiff silkworm powder；
2）The preparation of Sasanguasaponin：Two parts will be divided into after the complete degreasing of 10 parts by weight Oil-tea-cakes, crushing, by feed liquid weight
Than 1:15 add 95 DEG C of hot water in wherein a Oil-tea-cake crushed material, extract 38min, filter out residue；In gained filtrate
Another Oil-tea-cake crushed material is added, adds the hot water of 3 times of crushed material weight, continues to extract 38min, filtering；Filtrate is through dish
Formula centrifugation, ultrafiltration, rotary evaporation to paste, obtain Sasanguasaponin；
3）The preparation of Fructus Gleditsia extract：Two parts will be divided into after the drying of 5 parts by weight Chinese honey locusts, crushing, by a copy of it Chinese honey locust
Crushed material is in Ultrasound Instrument with 85 DEG C, feed liquid weight than 1:Hot water extraction 25min under the conditions of 12, filtering, remove residue；In gained
Another Chinese honey locust crushed material is added in filtrate, in 95 DEG C, feed liquid weight than 1:Hot water extraction 15min under the conditions of 6, filtering；Filtrate
Through disk centrifugal, ultrafiltration, rotary evaporation to paste, Fructus Gleditsia extract is obtained；
4）The preparation of pig pancreas stamping：The fresh pig pancreas of 15 parts by weight is washed away into watery blood, is cut into small pieces, adds 1 weight
The finely ground rock sugar of part, the mixing of 1 parts by weight purified water is added after fully smashing to pieces, obtains pig pancreas stamping；
5）The preparation of aloe extract：The fresh parts by weight of aloe 5 are taken, surface dirt impurity are washed away, by feed liquid weight than 1:1 adds
Enter water, fully smashed to pieces in juice extractor, leach fresh juice；Filter residue is by feed liquid weight than 1:The ethanol that 6 addition mass concentrations are 45% is molten
Liquid, in 80 DEG C extract 35min, filtering, filtrate through disk centrifugal, ultrafiltration, it is reverse osmosis concentrated be reduced to 30 Brix after, with first time institute
Fresh juice mixing is obtained, obtains aloe extract；
6）The preparation of rose of Sharon extract：10 parts by weight shrub althea flowers and leaf are washed away into surface dirt impurity respectively, by feed liquid weight
Measure ratio 1:1 adds water, is fully smashed to pieces in juice extractor, juice is leached；Filter residue is by feed liquid weight than 1:After 8 add water, in 65 DEG C
Extract 24h, filtering；Filtrate mixes after disk centrifugal, rotary evaporation to paste with first time gained juice, obtains rose of Sharon extraction
Thing；
7）The preparation of Flos persicae extract：Add 1 parts by weight water in 5 parts by weight peach blossoms, squeezed the juice in juice extractor, then
5 times of water weight, the ethanol solution that mass concentration is 65%, 25min is extracted under the conditions of 70 DEG C, is filtered used in being added in juice,
Filtrate through disk centrifugal, ultrafiltration, it is reverse osmosis concentrated be reduced to 30 Brix, obtain Flos persicae extract；
8）The preparation of orchid extract：Add 1 parts by weight water in 4 parts by weight orchids, squeezed the juice in juice extractor, then
5 times of water weight, the ethanol solution that mass concentration is 65%, 25min is extracted under the conditions of 70 DEG C, is filtered used in being added in juice,
Filtrate through disk centrifugal, ultrafiltration, it is reverse osmosis concentrated be reduced to 30 Brix, obtain orchid extract；
9）The preparation of the root bark of white mulberry-wolfberry fruit extract：By the 5 parts by weight root barks of white mulberry it is dry, be crushed to after 20 mesh and add 5 parts by weight
Matrimony vine, it is 1 in 100 DEG C, feed liquid weight ratio:Hot water extraction 75min under the conditions of 25, filtering；Filter residue is in 100 DEG C, feed liquid weight ratio
1:Reheating flooding 15min under the conditions of 10, filtering；Merge filter liquor twice, through disk centrifugal, ultrafiltration, rotary evaporation to paste,
Obtain the root bark of white mulberry-wolfberry fruit extract；
10）The preparation of Groomwell root oil：10 parts by weight Asian puccoons are immersed in the wild tea oil of its 2 times of weight, in normal temperature darkness bar
21d is soaked under part, is filtered；Filter residue soaks 1.5 h with 10 parts by weight open country tea oil again, and then heating extraction 25min, stands after cooling
The h of diacolation 12 makes it fully filter, and merges filtrate twice, obtains Groomwell root oil；
11）The preparation of Manual perfumed soap：8 parts by weight KOH are configured to the KOH solution that mass concentration is 30%, then added
Enter into the Groomwell root oil and the mixture of Sasanguasaponin for being heated to 60 DEG C, be stirred continuously using 500 r/min to paste and be used as A phases；
5 parts by weight China fir ashes are slowly added into pig pancreas stamping and constantly stirred evenly as B phases；Fructus Gleditsia extract and the rose of Sharon are extracted
Thing is mixed and mixed thoroughly as C phases；The root bark of white mulberry-wolfberry fruit extract, stiff silkworm powder, aloe extract are mixed and mixed thoroughly as D phases；Will
Flos persicae extract and orchid extract are mixed and mixed thoroughly as E phases；By A heat phases to 60 DEG C, add B phases, C phases and constantly stir
It is even, treat that temperature is reduced to 55 DEG C of addition D phases and stirred evenly, be finally cooled to 50 DEG C of addition E phases and mix simultaneously casting thoroughly, after depositing 31 d
Produce.
First, Manual perfumed soap measure of different nature is according to QB/T 2485-2008
1st, physicochemical property：Natural Manual perfumed soap of the invention belongs to compound perfumed soap, and total effective content is that dry soap content is 75%
~85%（QB/T 2487-2008）, moisture and volatile matter are 5% ~ 25%（QB/T 2623.4-2003）, total free alkali is 0.2%
（QB/T 2623.2-2003）, the caustic alkali that dissociates is 0.05%（QB/T 2623.1-2003）, meet the requirements of the standard.
2nd, soap body outward appearance：Soap body rectifies, uniform color, has not seen cracking, smooth exquisiteness, without macroscopic impurity and
Stain.
3rd, smell：There is the fragrant and indistinct peach blossom fragrance of stable orchid, become sour without wild tea oil and other obvious peculiar smell.
4th, resistance to hard water：The resistance to hard water of Manual perfumed soap is respectively 4.1 ml, 3.9 ml, 4.0 obtained by 3 embodiments
Ml, illustrate there is stronger resistance to hard water（QB/T 2487-2008）.
5th, solubility：The solubility of Manual perfumed soap is respectively 0.8341 mg/cm obtained by 3 embodiments2、0.8581mg/
cm2、0.8434mg/cm2 , show that it is respectively provided with higher solubility, it is easy to use.
6th, stability：Perfumed soap is respectively placed in 42 DEG C of 7d, -4 DEG C of 7d, with water logging 1d, as a result shows perfumed soap soap body without bright
It is aobvious to melt, ftracture, pasting the bad phenomenon that the conventional toilet soaps such as rotten under equal conditions easily occur.
2nd, using effect
Manual perfumed soap obtained by 3 embodiments is tried out, foam of the display with certain richness, wherein embodiment
1 foaming power is most strong, is adapted to like the people more than foam to use, has extraordinary cleaning effect, and will not be to skin after use
Skin, which produces, stimulates and tightens sense.
Overall using effect is compared with commercially available magic soap prevailing, as a result such as table 1.
1 magic soap of table uses result with perfumed soap of the present invention
As a result show, present invention gained Manual perfumed soap can compare favourably in terms of part with magic soap, even more than magic soap
Effect, it can bring to user and wash well with effect and enjoyment.Wherein, the Manual perfumed soap of embodiment 1 lays particular emphasis on moisturizing, moistened
Effect, embodiment 2,3 lay particular emphasis on sterilization, antipruritic etc. effect.
3rd, sterilization test
The present invention is prepared fragrant by hand using natural plant formulas such as Sasanguasaponin, Asian puccoon, aloe, stiff silkworm, the rose of Sharon, Chinese honey locusts
Soap has stronger sterilization（Particularly skin pathomycete）, antibacterial and skin care effect, using commercially available magic soap as control group, embodiment
Manual perfumed soap prepared by 1-3 is test group, uses several children's common skin pathomycetes to be determined to test strain with cylinder-plate method
Magic soap and Manual perfumed soap of the present invention are cured the disease the inactivation inhibition of fungi to skin, and its specific method is：By peptone 5g, beef
Leach powder 3g, agar 15g, buffer solution 3g and be diluted to 1L bacterium culture mediums, sterilize, be classified as when being cooled to 35 DEG C -45 DEG C
60 dish, per dish 20mL, the mixing of equivalent different strain being separately added into, every kind of strain repeats 3 dish, four Oxford cups is added in every dish,
Four kinds of each 1g of perfumed soap separately are taken, are fully dissolved with 100 mL, 60 DEG C of warm water, every kind of perfumed soap draws 200 μ L, is added drop-wise to every dish four respectively
In individual Oxford cup, cultivated under the conditions of 37 DEG C, observe and measure the size of inhibition zone, the results are shown in Table 2.
The test result of the different perfumed soap bactericidal effects of table 2（Unit：cm2）
Shown by the result of table 2, Manual perfumed soap of the present invention fungi of being cured the disease to skin has stronger inhibitory action, can prevent one
The generation of a little disease of skin, so as to reach more preferable skin effect.
The foregoing is only presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with
Modification, it should all belong to the covering scope of the present invention.
Claims (3)
- A kind of 1. Baby Care handmade soap containing natural Sasanguasaponin, it is characterised in that：Its is raw materials used to wrap by weight Include：Wild 10 ~ 30 parts of tea oil, 10 ~ 20 parts of Oil-tea-cake, 5 ~ 10 parts of Chinese honey locust, 5 ~ 15 parts of pig pancreas, 5 ~ 10 parts of China fir ash, shrub althea flower and 5 ~ 10 parts of leaf, 1 ~ 5 part of aloe, 3 ~ 5 parts of the root bark of white mulberry, 5 ~ 10 parts of Asian puccoon, 2 ~ 5 parts of matrimony vine, 1 ~ 3 part of stiff silkworm, 3 ~ 5 parts of peach blossom, orchid 3 ~ 5 parts, 3 ~ 8 parts of KOH, 1 part of rock sugar.
- 2. the Baby Care handmade soap containing natural Sasanguasaponin according to claim 1, it is characterised in that：The China fir ash is It will dry to crush after China fir leaf fully burns and be made.
- A kind of 3. preparation method of the Baby Care handmade soap containing natural Sasanguasaponin as claimed in claim 1, it is characterised in that： Comprise the following steps：1）The preparation of stiff silkworm powder：0.5-1 times of wheat bran of stiff silkworm weight is roasted in pot to 50% charing, then adds stiff silkworm, is roasted Fry untill stiff silkworm becomes yellowish-brown, wheat bran is screened out after cooling, by the abundant crushed after being dried of stiff silkworm to 300 ~ 400 mesh, obtains stiff silkworm powder；2）The preparation of Sasanguasaponin：Two parts will be divided into after the complete degreasing of Oil-tea-cake, crushing, by feed liquid weight than 1:15 wherein 95 ~ 100 DEG C of hot water is added in a Oil-tea-cake crushed material, 38min is extracted, filters out residue；Added in gained filtrate another Part Oil-tea-cake crushed material, the hot water of 3 times of the crushed material weight is added, continue to extract 38min, filtering；Filtrate through disk centrifugal, Ultrafiltration, rotary evaporation to paste, obtain Sasanguasaponin；3）The preparation of Fructus Gleditsia extract：Two parts will be divided into after Chinese honey locust drying, crushing, by a copy of it Chinese honey locust crushed material in ultrasound With 85 ~ 95 DEG C, feed liquid weight than 1 in instrument:Hot water extraction 25min under the conditions of 12, filtering, remove residue；Add in gained filtrate Enter another Chinese honey locust crushed material, in 85 ~ 95 DEG C, feed liquid weight than 1:Hot water extraction 15min under the conditions of 6, filtering；Filtrate is through dish-style Centrifugation, ultrafiltration, rotary evaporation to paste, obtain Fructus Gleditsia extract；4）The preparation of pig pancreas stamping：Fresh pig pancreas is washed away into watery blood, is cut into small pieces, finely ground rock sugar is added, fully smashes Add after broken and mixed with heavy purified waters such as rock sugar, obtain pig pancreas stamping；5）The preparation of aloe extract：Fresh aloe is taken, washes away surface dirt impurity, by feed liquid weight than 1:1 adds water, fully smashes Fresh juice is leached after broken；Filter residue is by feed liquid weight than 1:6 add the ethanol solution that mass concentration is 45%, in 75 ~ 80 DEG C of extractions 35min, filtering, filtrate through disk centrifugal, ultrafiltration, it is reverse osmosis concentrated be reduced to 25 ~ 30 ° of Brix after, mixed with the first time fresh juice of gained Close, obtain aloe extract；6）The preparation of rose of Sharon extract：Shrub althea flower and leaf are washed away into surface dirt impurity respectively, by feed liquid weight than 1:1 adds Water, juice is leached after fully smashing to pieces；Filter residue is by feed liquid weight than 1:After 8 add water, 24h, filtering are extracted in 65 ~ 70 DEG C；Filtrate Mixed after disk centrifugal, rotary evaporation to paste with first time gained juice, obtain rose of Sharon extract；7）The preparation of Flos persicae extract or orchid extract：After adding water to squeeze the juice in peach blossom or orchid, in juice used in addition 5 times of water weight, mass concentration be 65% ethanol solution, 25min is extracted under the conditions of 65 ~ 70 DEG C, filter, filtrate through dish-style from The heart, ultrafiltration, it is reverse osmosis concentrated be reduced to 25 ~ 30 ° of Brix, obtain Flos persicae extract or orchid extract；8）The preparation of the root bark of white mulberry-wolfberry fruit extract：By the root bark of white mulberry it is dry, be crushed to 10 ~ 20 mesh after add matrimony vine, 95 ~ 100 DEG C, feed liquid weight ratio be 1:Hot water extraction 75min under the conditions of 25, filtering；Filter residue is in 95 ~ 100 DEG C, feed liquid weight than 1:10 conditions Lower reheating flooding 15min, filtering；Merge filter liquor twice, through disk centrifugal, ultrafiltration, rotary evaporation to paste, get Sang Bai Skin-wolfberry fruit extract；9）The preparation of Groomwell root oil：Asian puccoon is immersed in the wild tea oil of its 1-2 times of weight, soaks 21d under the conditions of normal temperature darkness, Filtering；The remaining wild tea oil of filter residue soaks 1.5 h, then heating extraction 25min, and the h of diacolation 12 is stood after cooling makes its fully mistake Filter, merge filtrate twice, obtain Groomwell root oil；10）The preparation of Manual perfumed soap：KOH is configured to the KOH solution that mass concentration is 30%, is then added into and is heated to In 60 DEG C of Groomwell root oil and the mixture of Sasanguasaponin, it is stirred continuously using 500 r/min to paste and is used as A phases；China fir ash is slow Slow be added in pig pancreas stamping is constantly stirred evenly as B phases；Fructus Gleditsia extract and rose of Sharon extract are mixed and mixed thoroughly as C Phase；The root bark of white mulberry-wolfberry fruit extract, stiff silkworm powder, aloe extract are mixed and mixed thoroughly as D phases；By Flos persicae extract and orchid Extract is mixed and mixed thoroughly as E phases；By A heat phases to 60 DEG C, add B phases, C phases and constantly stir evenly, treat that temperature is reduced to 55 DEG C adding D phases stirs evenly, and is finally cooled to 50 DEG C and adds E phases to mix thoroughly and casting, is produced after depositing 28 ~ 31 d.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610100337.9A CN105754768B (en) | 2016-02-24 | 2016-02-24 | A kind of Baby Care handmade soap containing natural Sasanguasaponin and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610100337.9A CN105754768B (en) | 2016-02-24 | 2016-02-24 | A kind of Baby Care handmade soap containing natural Sasanguasaponin and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105754768A CN105754768A (en) | 2016-07-13 |
| CN105754768B true CN105754768B (en) | 2018-03-23 |
Family
ID=56329746
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610100337.9A Active CN105754768B (en) | 2016-02-24 | 2016-02-24 | A kind of Baby Care handmade soap containing natural Sasanguasaponin and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105754768B (en) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106214734A (en) * | 2016-07-27 | 2016-12-14 | 南京正宽医药科技有限公司 | The extracting method of a kind of Fructus Gleditsia extract and bar soap |
| CN106038421B (en) * | 2016-07-27 | 2019-03-12 | 福建春辉生物工程有限公司 | A kind of itching-relieving lotion and preparation method thereof containing old wild tea oil |
| CN106318715A (en) * | 2016-08-03 | 2017-01-11 | 南安辰光日用化工品有限公司 | Sterilization soap with antibacterial activity |
| CN106833973A (en) * | 2017-01-18 | 2017-06-13 | 广西南宁博智生物科技有限公司 | A kind of cold process soap for acne of dispelling and preparation method thereof |
| CN107213081A (en) * | 2017-05-22 | 2017-09-29 | 邵洁明 | It is a kind of to improve hair washing gel of oily hair and preparation method thereof |
| CN107354038A (en) * | 2017-07-13 | 2017-11-17 | 罗平县腊峰蜂业科技有限公司 | A kind of honey nourishes soap and preparation method thereof |
| CN108839165A (en) * | 2018-06-08 | 2018-11-20 | 阜南县星光工艺品有限公司 | A method of reducing wood color difference before and after highland hook leaf rattan thermal softening |
| CN109568182B (en) * | 2018-12-14 | 2021-11-05 | 江西绿海油脂有限公司 | Tea oil soothing cream for children |
| CN111378540A (en) * | 2020-03-30 | 2020-07-07 | 山西大学 | Preparation method of novel porcine pancreas soap |
| CN112111342A (en) * | 2020-09-08 | 2020-12-22 | 杭州耕欣农林科技开发有限公司 | Handmade soap and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1534087A (en) * | 2003-04-01 | 2004-10-06 | 王保迎 | Skin protection soap and its making method |
| CN103333752A (en) * | 2013-07-10 | 2013-10-02 | 福建农林大学 | Preparation method of camellia oil skin care soap |
| CN105296232A (en) * | 2015-11-25 | 2016-02-03 | 王晓伟 | Arnebia root handmade soap and production method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20160089325A1 (en) * | 2013-04-29 | 2016-03-31 | Insight Institute Of Neurosurgery & Neuroscience | Soap composition |
-
2016
- 2016-02-24 CN CN201610100337.9A patent/CN105754768B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1534087A (en) * | 2003-04-01 | 2004-10-06 | 王保迎 | Skin protection soap and its making method |
| CN103333752A (en) * | 2013-07-10 | 2013-10-02 | 福建农林大学 | Preparation method of camellia oil skin care soap |
| CN105296232A (en) * | 2015-11-25 | 2016-02-03 | 王晓伟 | Arnebia root handmade soap and production method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105754768A (en) | 2016-07-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105754768B (en) | A kind of Baby Care handmade soap containing natural Sasanguasaponin and preparation method thereof | |
| CN105062722A (en) | Handmade soap containing mulberry and derivatives, and making method thereof | |
| CN105012224A (en) | Natural shampoo and preparation method thereof | |
| JP7315985B2 (en) | Soap composition using mountain ginseng and soap containing the same | |
| CN106434028A (en) | Fruit and vegetable washing salt for removing pesticide residues and preparation method thereof | |
| CN109221558A (en) | A kind of jasmine coffee for beauty and beauty and preparation method thereof | |
| CN107802547A (en) | A kind of rosemary shampoo | |
| KR101138411B1 (en) | Manufacturing method of shampoo composition using fermented liquid and shampoo composition thereof | |
| CN107281085A (en) | Face mask for eliminating macula and whitening skin slurries, facial mask and the preparation method of a kind of essential oil containing pear flower | |
| CN104068183A (en) | Aroma rich type tea leaves and preparation method thereof | |
| CN103892011B (en) | Peony coffee as well as preparation method and application thereof | |
| CN107625691A (en) | Rose wate | |
| CN111110574A (en) | A kind of wet wipes with three-in-one functions of cleaning, sterilization and moisturizing and preparation method thereof | |
| KR20140111364A (en) | My skin health and beauty using the functional bio-ceramic and 107 kinds of native grasses | |
| CN102604750A (en) | Method for preparing forest herbaceous plant biomass detergent | |
| KR101606381B1 (en) | Manufacture method of complex beauty Salt using solar salt processing environmentally friendly | |
| KR101478784B1 (en) | Manufacturing method of functional salt using chamaecyparis obtusa | |
| CN107184467A (en) | A kind of hair care exterior-applied article being made of Lignum Xanthoceratis extract and preparation method thereof | |
| CN109793085B (en) | Preparation method of fermented mulberry leaf tea | |
| KR101554598B1 (en) | Manufacturing method of body cleanser using herb and body cleanser made by that manufacturing method | |
| CN106261422A (en) | A kind of Liquor Rosae Rugosae Distillata and preparation method thereof | |
| CN108542850A (en) | A kind of antibacterial preserving moisture and protecting skin hand cleanser of addition indocalamus leaf flavones-soapberry pericarp total saposins | |
| CN107594013A (en) | A kind of dandelion black tea and its production method | |
| KR102291229B1 (en) | Cleaning composition comprising coffee by-products and uses thereof | |
| CN107712142A (en) | A kind of dandelion oolong tea and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |