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CN106333880B - Toner with thin emulsion base and preparation method thereof - Google Patents

Toner with thin emulsion base and preparation method thereof Download PDF

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CN106333880B
CN106333880B CN201610917268.0A CN201610917268A CN106333880B CN 106333880 B CN106333880 B CN 106333880B CN 201610917268 A CN201610917268 A CN 201610917268A CN 106333880 B CN106333880 B CN 106333880B
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CN106333880A (en
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孙淑萍
陈滢俐
王露
王玲玲
金鑫
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Wannan Medical College
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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Abstract

本发明提供了一种稀薄乳液基质的爽肤水及其制备方法,含有:薏苡仁提取液、金缕梅提取液、甘草提取液、雪莲果榨取液,黄秋葵榨取液,芦荟油,玫瑰果油,小麦胚芽油,海藻酸钠,阳离子瓜尔胶,1%透明质酸钠溶液、聚乙二醇400、1,2‑丙二醇、尼泊金甲脂,自乳化复合型乳化剂AC‑402,香精,柠檬酸、75%乙醇和蒸馏水。与现有技术相比,本发明制备的稀薄乳液基质的爽肤水为淡淡的乳白色,粘度适宜,稠度适宜,稳定性好,气味芬芳,质感清爽,能保持肌肤水分,减轻皱纹,改善粗糙,美白嫩肤,永葆肌肤柔软嫩滑白皙。The invention provides a toner with a thin emulsion matrix and a preparation method thereof, which contains: coix seed extract, witch hazel extract, licorice extract, yacon extract, okra extract, aloe vera oil, rosehip oil, wheat Germ oil, sodium alginate, cationic guar gum, 1% sodium hyaluronate solution, polyethylene glycol 400, 1,2-propylene glycol, methylparaben, self-emulsifying compound emulsifier AC‑402, essence, Citric acid, 75% ethanol and distilled water. Compared with the prior art, the toner of the thin emulsion base prepared by the present invention is light milky white, with suitable viscosity, suitable consistency, good stability, fragrant smell and refreshing texture, which can maintain skin moisture, reduce wrinkles, improve roughness, whiten and tender Keep skin soft, smooth and white forever.

Description

一种稀薄乳液基质的爽肤水及其制备方法Toner with thin emulsion base and preparation method thereof

技术领域technical field

本发明属于化妆品领域,具体涉及一种稀薄乳液基质的爽肤水及其制备方法。The invention belongs to the field of cosmetics, and in particular relates to a toner with a thin emulsion base and a preparation method thereof.

背景技术Background technique

现代生活中的人们长期经历着高强度工作、暴露于电脑手机等高辐射以及紫外线照射环境,使得原本随年龄增长日渐暗淡的皮肤衰老的更加明显,形成小细纹、皱纹。皱纹是皮肤老化的一种显著标志,老化的皮肤对于每个爱美之人是不能忍受的,所以皮肤的抗皱美白对于每一个爱美之人来说都至关重要。People in modern life have experienced high-intensity work for a long time, exposure to high radiation such as computers and mobile phones, and ultraviolet radiation environments, which makes the aging of the skin that is getting darker with age more obvious, forming small fine lines and wrinkles. Wrinkles are a significant sign of skin aging, and aging skin is unbearable for everyone who loves beauty, so anti-wrinkle and whitening of skin is very important for everyone who loves beauty.

而皱纹的产生归结起来有四方面原因:自然老化、地心引力、光老化与光损伤、面部表情肌过多的收缩。其中最为关键的因素是自然老化和光老化两种形式,前者主要指随着年龄的增长,机体内存在的不可抗拒因素,如遗传、重力、内分泌以及免疫功能等引起的老化;后者主要由于紫外线的作用,加重了自然衰老的进程。皮肤日渐变现出松弛、变薄、含水量下降,显得干燥,有鳞屑,失去光泽;弹性和坚实度也随之下降;皱纹形成,并逐渐增多,加深。此外,皮肤的敏感性增加,色素也增多。皮肤衰老的内在表现为皮肤细胞增殖能力下降,表皮更新速度减慢,皮肤重建能力减弱,皮肤胶原合成减慢,皮肤免疫力下降,色素分布不均匀等。There are four reasons for the generation of wrinkles: natural aging, gravity, photoaging and photodamage, and excessive contraction of facial expression muscles. The most critical factors are two forms of natural aging and photoaging. The former mainly refers to aging caused by irresistible factors in the body with age, such as genetics, gravity, endocrine and immune functions; the latter is mainly caused by ultraviolet rays. The effect of aggravating the natural aging process. The skin gradually becomes slack, thinner, water content decreases, dry, scaly, and loses luster; elasticity and firmness also decrease; wrinkles form, and gradually increase and deepen. In addition, the sensitivity of the skin increases and pigmentation increases. The internal manifestations of skin aging are the decline of skin cell proliferation, the slowdown of epidermal renewal, the weakening of skin reconstruction ability, the slowdown of skin collagen synthesis, the decline of skin immunity, and the uneven distribution of pigment.

随着社会的发展、伴随人们物质生活的日益增加,护肤品行业是越做越大,供给女性的选择也越来越多,但是若没有选择好适合自己肌肤的护肤品或者这些产品中甚至有不安全的化学物质,会造成更为严重肌肤问题,人们都在乞求安全有效的护肤产品的问世。With the development of society and the increase of people's material life, the skin care industry is getting bigger and bigger, and there are more and more choices for women, but if you don't choose the skin care products that suit your skin or there are even some Unsafe chemicals can cause more serious skin problems, and people are begging for safe and effective skin care products.

目前天然植物类护肤品成为了国内外护肤品研发的最主要趋势,而“中草药”则是功能性护肤品的最好原料,若选用合适的中草药加入,既能改善肌肤问题,使皮肤白皙嫩滑,如婴儿的肌肤般滑嫩。又能避免使用化学物质的影响。所以用天然植物提取物来开发新的护肤品必将是前途光明的一条新道路。At present, natural plant skin care products have become the most important trend in the research and development of skin care products at home and abroad, and "Chinese herbal medicine" is the best raw material for functional skin care products. If the appropriate Chinese herbal medicine is added, it can improve skin problems and make the skin fair and tender Smooth, as smooth and tender as a baby's skin. Can avoid the influence of using chemical substance again. So using natural plant extracts to develop new skin care products will be a new path with a bright future.

发明内容Contents of the invention

本发明的目的在于提供一种稀薄乳液基质的爽肤水及其制备方法,含有中药提取物,可以有效的锁住肌肤中的水分,能减少皱纹,使肌肤更加水润透白,呈现水感透白的美丽。The purpose of the present invention is to provide a toner with a thin emulsion base and its preparation method, which contains Chinese medicine extracts, can effectively lock the moisture in the skin, reduce wrinkles, make the skin more moist and white, and present a watery and white skin beauty of.

本发明提供的一种稀薄乳液基质的爽肤水,含有以下重量份的原料:A skin toner with a thin emulsion matrix provided by the invention contains the following raw materials in parts by weight:

所述的甘草提取液通过以下方法制备:Described licorice extract is prepared by the following method:

称取甘草粗粉适量,浸泡0.25-0.75h,加热至90-100℃,煎煮提取3次,第1次加甘草12-15倍重量的水,提取0.5-2h,第2次加10-12倍重量的水,提取0.5-1.5h,第3次加6-8倍重量的水,提取0.5-1.5h,每次四层纱布滤过,合并滤液,滤液的体积浓缩至甘草重量的10-12倍g/ml,过滤,滤液水浴加热到80℃,加入1-5%活性炭和0.5-3%滑石粉,边加热边搅拌,持续时间30-60min,趁热抽滤,取滤液即得。Weigh an appropriate amount of licorice coarse powder, soak for 0.25-0.75h, heat to 90-100°C, decoct and extract 3 times, add 12-15 times the weight of licorice in water for the first time, extract for 0.5-2h, and add 10- 12 times the weight of water, extract 0.5-1.5h, add 6-8 times the weight of water for the third time, extract 0.5-1.5h, filter each time with four layers of gauze, combine the filtrate, and concentrate the volume of the filtrate to 10% of the weight of licorice -12 times g/ml, filter, heat the filtrate in a water bath to 80°C, add 1-5% activated carbon and 0.5-3% talcum powder, stir while heating for 30-60min, suction filter while it is hot, and get the filtrate .

所述的薏苡仁提取液通过以下方法制备:The coix seed extract is prepared by the following method:

称取薏苡仁适量,用1-2倍量自来水冲洗,冲洗液倒掉,加薏苡仁12-16倍重量的水煎煮提取1-1.5h,四层纱布过滤;滤渣再加薏苡仁10-12倍重量的水提取0.5-1.5h,四层纱布过滤;滤渣再加薏苡仁8-10倍重量的水提取0.5-1.5h,四层纱布过滤,滤渣弃掉,合并三次滤液,浓缩至薏苡仁重量的8-12倍g/ml,趁热抽滤,取滤液即得。Weigh an appropriate amount of coix seed, wash it with 1-2 times the amount of tap water, pour off the washing liquid, add 12-16 times the weight of coix seed, decoct it for 1-1.5 hours, filter it with four layers of gauze; add coix seed 10- Extract with 12 times the weight of water for 0.5-1.5 hours, filter with four layers of gauze; add 8-10 times the weight of coix seed to the filter residue, extract with water for 0.5-1.5 hours, filter with four layers of gauze, discard the filter residue, combine the three filtrates, and concentrate to Coix. Kernel weight 8-12 times g/ml, while hot suction filtration, take the filtrate.

所述的金缕梅提取液通过以下方法制备:Described witch hazel extract is prepared by the following method:

称取金缕梅适量,加金缕梅14-18倍重量的水煎煮提取0.5-1.5h,四层纱布过滤;滤渣再加金缕梅12-14倍重量的水提取0.5-1.5h,四层纱布过滤;滤渣再加金缕梅10-12倍重量的水提取0.5-1.5h,四层纱布过滤,滤渣弃掉,合并三次滤液,浓缩至金缕梅重量的6-9倍g/ml,过滤,滤液水浴加热到80℃,加入1-5%活性炭和0.5-3%滑石粉,边加热边搅拌,持续时间30-60min,趁热抽滤,取滤液即得。Weigh an appropriate amount of hamamelis, add 14-18 times the weight of hamamelis to decoct for 0.5-1.5 hours, filter through four layers of gauze; add water 12-14 times the weight of hamamelis to extract for 0.5-1.5 hours, Filter with four layers of gauze; extract the residue with 10-12 times the weight of witch hazel for 0.5-1.5h, filter with four layers of gauze, discard the filter residue, combine three filtrates, concentrate to 6-9 times the weight of witch hazel g/ ml, filter, heat the filtrate to 80°C in a water bath, add 1-5% activated carbon and 0.5-3% talcum powder, stir while heating for 30-60min, suction filter while it is hot, and take the filtrate.

所述的雪莲果榨取液通过以下方法制备:Described Yacon fruit extract is prepared by the following method:

称取一定重量的雪莲果,洗净切成块状,加雪莲果3-5倍重量的蒸馏水,用榨汁机榨取后,用四层纱布过滤,取滤液备用。Weigh a certain weight of yacon, wash and cut into blocks, add distilled water 3-5 times the weight of yacon, squeeze it with a juicer, filter it with four layers of gauze, and take the filtrate for later use.

所述的黄秋葵榨取液通过以下方法制备:Described okra extract is prepared by the following method:

称取一定重量新鲜的黄秋葵,用清水冲洗后,切成块状,加黄秋葵3-5倍重量蒸馏水,用榨汁机榨取后,用四层纱布过滤,取滤液备用即可。Weigh a certain weight of fresh okra, wash it with water, cut it into pieces, add 3-5 times the weight of okra in distilled water, squeeze it with a juicer, filter it with four layers of gauze, and take the filtrate for later use.

所述的香精为柠檬香精、百合香精、桂花香精、玫瑰香精、黄瓜香精、菠萝香精或水蜜桃香精任一种。The essence is any one of lemon essence, lily essence, osmanthus essence, rose essence, cucumber essence, pineapple essence or peach essence.

本发明提供的一种稀薄乳液基质的爽肤水的制备方法,包括以下步骤:A kind of preparation method of the toner of thin emulsion matrix provided by the invention comprises the following steps:

a)将0.01-0.05份海藻酸钠加入到10-30份蒸馏水中自然溶胀,等溶胀完全形成晶莹透明的海藻酸钠凝胶液,待用;a) Add 0.01-0.05 parts of sodium alginate to 10-30 parts of distilled water to swell naturally, and wait until the swelling is complete to form a crystal clear sodium alginate gel solution, which is ready for use;

b)将0.01-0.03份阳离子瓜尔胶加入到10-30份蒸馏水中自然溶胀,等溶胀完全形成晶莹透明的阳离子瓜尔胶凝胶液,待用;b) Add 0.01-0.03 parts of cationic guar gum to 10-30 parts of distilled water to swell naturally, wait for the swelling to completely form a crystal clear cationic guar gum gel, and set aside;

c)量取1-3份75%乙醇溶解0.003-0.009份尼泊金甲脂作为防腐剂溶液,待用;c) Measure 1-3 parts of 75% ethanol and dissolve 0.003-0.009 parts of methylparaben as a preservative solution, and set aside;

d)分别称取玫瑰果油0.5-1份、小麦胚芽油0.5-1份、芦荟油0.5-1份,将三者搅拌混合均匀,再加入自乳化复合型乳化剂AC-4021-2.5份,于70-80℃中水浴加热,边加热边搅拌使其混合均匀,得到O/W型乳液的油相;d) Weigh 0.5-1 part of rosehip oil, 0.5-1 part of wheat germ oil, and 0.5-1 part of aloe vera oil, stir and mix the three, and then add self-emulsifying compound emulsifier AC-4021-2.5 parts, Heat in a water bath at 70-80°C, stir while heating to mix evenly, and obtain the oil phase of the O/W emulsion;

e)量取10-30份蒸馏水放在70-80℃水浴中,加热得到O/W型乳液的水相;e) Take 10-30 parts of distilled water and place it in a water bath at 70-80°C, and heat to obtain the water phase of the O/W emulsion;

f)等油相、水相达到相同温度时,将上述的水相呈细流状缓慢加入到油相中,边加热边沿同一方匀速搅拌,约15-30min后,乳化完成,即得到O/W型稀薄乳液基质;f) When the oil phase and the water phase reach the same temperature, slowly add the above-mentioned water phase into the oil phase in a thin stream, and stir at a constant speed along the same side while heating. After about 15-30min, the emulsification is completed, and O/ W-type thin emulsion base;

g)待乳液基质搅拌冷却至室温后,再向其加入聚乙二醇400 1-3份、1,2-丙二醇1-3份、1%透明质酸钠溶液0.5-2份、海藻酸钠凝胶、阳离子瓜尔胶凝胶液、金缕梅提取液1-3份、薏苡仁提取液1-3份、甘草提取液1-3份、黄秋葵榨取液1-3份、雪莲果榨取液1-3份、防腐剂溶液,加入0.01-0.25份柠檬酸调pH值为6.5-7.2,再加入0.1-0.25份香精,混合搅拌均匀,即得稀薄乳液基质的爽肤水。g) After stirring and cooling the emulsion matrix to room temperature, add 1-3 parts of polyethylene glycol 400, 1-3 parts of 1,2-propylene glycol, 0.5-2 parts of 1% sodium hyaluronate solution, sodium alginate Gel, cationic guar gum gel, 1-3 parts of witch hazel extract, 1-3 parts of coix seed extract, 1-3 parts of licorice extract, 1-3 parts of okra extract, yacon fruit extract 1-3 parts, preservative solution, add 0.01-0.25 parts of citric acid to adjust the pH value to 6.5-7.2, then add 0.1-0.25 parts of essence, mix and stir evenly, and obtain the toner with thin emulsion matrix.

本发明中的各种成分如下:Various compositions among the present invention are as follows:

薏苡仁具有利水、健脾、除痹、清热排脓的功效。薏苡仁中含有多种维生素和矿物质能够保持人体皮肤光泽细腻,减少皱纹。所含的维他命B群能够抗发炎、控油、保湿锁水。而且,能够消除粉刺、雀斑、老年斑,改善皮肤的粗糙等。并且它对于由病毒感染引起的赘疣等有一定的治疗作用。另外,它还对紫外线有吸收能力,其提炼物加入护肤品或化妆品中还可达到防晒和防紫外线的效果。因为这些功效,长期坚持在脸上使用,皮肤自然会比原来光泽细腻很多,变得白嫩光滑。Coix seed has the effects of benefiting water, invigorating the spleen, eliminating numbness, clearing away heat and discharging pus. Coix seed contains a variety of vitamins and minerals, which can keep human skin shiny and delicate, and reduce wrinkles. The vitamin B complex contained in it can resist inflammation, control oil, moisturize and lock water. Moreover, it can eliminate acne, freckles, age spots, and improve skin roughness. And it has a certain therapeutic effect on warts caused by viral infections. In addition, it also has the ability to absorb ultraviolet rays, and its extracts can be added to skin care products or cosmetics to achieve sunscreen and anti-ultraviolet effects. Because of these effects, if you keep using it on the face for a long time, the skin will naturally become more radiant and smoother than before, and become white, tender and smooth.

金缕梅可以调节皮脂分泌,具有保湿及嫩白作用。能促进淋巴血液循环,专门克服早晨眼脬和黑眼圈,对龟裂、晒伤、粉刺有改善效果。可有效帮助肌肤夜间的再生能力。去除眼袋、放松以及缓和对于油性肌肤或是过敏的肌肤都有很优异的效果。有舒缓、收敛、抗菌的效果,因有收敛控油、杀菌的显著疗效。能够迅速渗入皮肤,由内而外全面调节肌肤,平衡皮肤PH值及油脂分泌,净化毛孔,修复受损的肌肤,有效调节舒张的毛孔,明显收敛粗毛孔,防止黑头、粉刺产生,使肌肤快速呈现细腻、光滑、紧致状态。金缕梅具有深层清洁和对抗自由基的功效,可使肌肤抗老。一般在护肤品和化妆品中,用来消炎和缓和受刺激的皮肤但不会造成皮肤干燥,且具愈合伤口的功效。Witch hazel can regulate sebum secretion, and has moisturizing and whitening effects. It can promote lymphatic blood circulation, and it can specifically overcome morning sores and dark circles, and can improve cracks, sunburn, and acne. Can effectively help the skin's ability to regenerate at night. It is excellent for removing bags under the eyes, relaxing and calming oily skin or sensitive skin. It has soothing, astringent, and antibacterial effects, because it has significant curative effects of astringent, oil control, and sterilization. It can quickly penetrate into the skin, fully regulate the skin from the inside out, balance the PH value and oil secretion of the skin, purify pores, repair damaged skin, effectively regulate dilated pores, significantly shrink coarse pores, prevent blackheads and acne, and make skin fast Reveals a delicate, smooth and firm state. Witch Hazel works to age-defying skin with its deep cleansing and free-radical-fighting properties. Generally used in skin care products and cosmetics to reduce inflammation and soothe irritated skin without drying the skin, and has the effect of healing wounds.

雪莲果对痘痘肌肤有很好的效果。由于雪莲果中含有大量的挥发油、生物碱、黄酮类、酚类、糖类、鞣质等营养成份。能加快皮肤的新陈代谢,减少皱纹,使皮肤保持光泽、丰满、延缓衰老,对面部雀斑、肝斑等有良好的疗效,同时有较强的美白嫩肤的效果。Yacon is very good for acne-prone skin. Because yacon contains a large amount of volatile oils, alkaloids, flavonoids, phenols, sugars, tannins and other nutrients. It can speed up the metabolism of the skin, reduce wrinkles, keep the skin shiny and plump, and delay aging.

黄秋葵相对于其他蔬菜比较特殊的地方在于黄秋葵的内部含有的粘液。这种稀有的黏性物质(糖聚合体)中主要成分含有果胶、粘性糖蛋白、维生素A和维生素C。维生素C和可溶性纤维可以促进消化和美容,这两者结合作用对皮肤有一定温和的保护效应。What makes okra special compared to other vegetables is the mucus contained inside the okra. This rare viscous substance (sugar polymer) contains pectin, viscous glycoprotein, vitamin A and vitamin C as the main components. Vitamin C and soluble fiber can promote digestion and beauty, and the combination of the two has a mild protective effect on the skin.

甘草被誉为“植物美白皇后”,因为甘草中含有蛋白质和多种氨基酸,脂类、多糖类、果酸、维生素和微量元素等。多种物质的协调作用对皮肤有营养保湿作用。可以消除黑斑、防止皮肤粗糙。甘草中所含有的黄酮类成分有明显的抗氧化作用,其主要是对酪氨酸活性的抑制及对DOPA色素互变异构酶活性的抑制和INDOLE5.6quinone聚合的阻碍,从而有效抑制黑色素的生成,使肌肤变白。甘草的抗氧化能力与维生素E比较接近,能清除多种自由基和抑制脂褐素生成,促进抗氧化防御系统等多种功能。具有延缓衰老、减轻色素沉着的作用等。甘草美白效果好、作用温和、安全无毒副作用,作为美白剂广泛用于各种护肤品中。Licorice is known as the "Queen of Whitening Plants" because licorice contains protein, a variety of amino acids, lipids, polysaccharides, fruit acids, vitamins and trace elements. The coordinated effect of various substances has a nourishing and moisturizing effect on the skin. Can eliminate dark spots and prevent rough skin. The flavonoids contained in licorice have obvious antioxidant effects, which mainly inhibit the activity of tyrosine, the activity of DOPA pigment tautomerase and the polymerization of INDOLE5.6quinone, thereby effectively inhibiting the formation of melanin. Generate, whiten the skin. The antioxidant capacity of licorice is similar to that of vitamin E. It can scavenge a variety of free radicals, inhibit the production of lipofuscin, and promote the antioxidant defense system and other functions. It has the effects of delaying aging and reducing pigmentation. Licorice has good whitening effect, mild effect, safety and no side effects, and is widely used in various skin care products as a whitening agent.

小麦胚芽油被称为“皮肤的维他命”。其中富含维他命E、B、蛋白质、矿物质,新鲜椰子油、还有亚麻酸、亚油酸等多种不饱和脂肪酸。可补充维生素E以及具有改善皮肤上色素沉淀、皮肤干燥的作用,保护皮肤免受紫外线的干扰。同时它还是一种天然的且性能好的防腐剂。Wheat Germ Oil has been called the "vitamin for the skin". It is rich in vitamin E, B, protein, minerals, fresh coconut oil, and various unsaturated fatty acids such as linolenic acid and linoleic acid. It can supplement vitamin E, improve skin pigmentation and dry skin, and protect skin from ultraviolet rays. At the same time, it is a natural and good preservative.

玫瑰果油中富含有γ-亚麻油酸、不饱和脂肪酸、棕榈酸、柠檬酸、维生素A、C、类胡萝卜素等。玫瑰果油对因痤疮、手术、烧伤、水痘、伤口和切口导致的皮肤损伤疤痕都有效。溶解黑头、收缩毛孔、消除红肿红斑。玫瑰果油强有力的细胞再生和伤口愈合功能有助于健康、正常皮肤的生长,替代疤痕组织。它不仅能重新构造损坏了的皮肤结构,而且还能改善皮肤的颜色和弹性。玫瑰果油能通过促进表皮细胞的活性来提高皮肤再生和更新能力,从而停止和扭转皮肤老化产生的典型症状如皱纹、眼角皱纹和松弛。随着老化现象的消失,面部皮肤就会变得紧实和光滑些。玫瑰果油能修复和替代被撕扯了的皮肤组织,有效地减少萎缩纹的出现。长期坚持使用玫瑰果油,色素沉着斑点就会逐渐减轻还能修复晒伤皮肤、淡化黑斑雀斑、恢复嫩白面孔。Rosehip oil is rich in gamma-linolenic acid, unsaturated fatty acids, palmitic acid, citric acid, vitamins A, C, carotenoids, etc. Rosehip oil is effective for scarring of skin damage from acne, surgery, burns, chickenpox, wounds and cuts. Dissolve blackheads, shrink pores, eliminate redness and redness. Rosehip Oil's potent cell regeneration and wound healing properties support the growth of healthy, normal skin and replace scar tissue. It not only restructures the damaged skin structure, but also improves the skin's color and elasticity. Rosehip oil can improve skin regeneration and renewal by promoting the activity of epidermal cells, thereby stopping and reversing the typical symptoms of skin aging such as wrinkles, eye wrinkles and sagging. As signs of aging fade away, facial skin becomes firmer and smoother. Rosehip oil repairs and replaces torn skin tissue, effectively reducing the appearance of stretch marks. Long-term use of rosehip oil will gradually reduce pigmentation spots and repair sun-damaged skin, dilute dark spots and freckles, and restore a whiter face.

透明质酸钠又名玻璃酸钠、玻尿酸钠,是一种酸性粘多糖。透明质酸是从牛眼、鸡冠、人的脐带等特殊原料中提取,近来也有从某些细菌如放线菌中提取。透明质酸钠本身是人体皮肤的构成之一,是人体内分布最广的一种酸性粘多糖,存在于结缔组织的基质中,具有良好的保湿作用。透明质酸分子中含有大量的羧基和羟基,在水溶液中形成分子内和分子间的氢键,这使其具有强大的保水作用,可结合自身400倍以上的水,是目前发现的自然界中保湿性最好的物质,被称为理想的天然保湿因子。2%的纯透明质酸水溶液能牢固地保持98%水分。Sodium hyaluronate, also known as sodium hyaluronate and sodium hyaluronate, is an acidic mucopolysaccharide. Hyaluronic acid is extracted from special raw materials such as ox eyes, cockscombs, and human umbilical cords. Recently, it is also extracted from certain bacteria such as actinomycetes. Sodium hyaluronate itself is one of the components of human skin. It is the most widely distributed acidic mucopolysaccharide in the human body. It exists in the matrix of connective tissue and has a good moisturizing effect. Hyaluronic acid molecules contain a large number of carboxyl groups and hydroxyl groups, which form intramolecular and intermolecular hydrogen bonds in aqueous solution, which makes it have a strong water retention effect, and can bind more than 400 times its own water. It is currently found in nature. The most effective substance is known as the ideal natural moisturizing factor. A 2% aqueous solution of pure hyaluronic acid firmly holds 98% of moisture.

海藻酸钠又名褐藻酸钠、海带胶、褐藻胶、藻酸盐,是由海带中提取的天然多糖碳水化合物。海藻酸钠具有天然保湿作用,同时也是一种性能良好的增稠剂。Sodium alginate, also known as sodium alginate, kelp gum, alginate, and alginate, is a natural polysaccharide carbohydrate extracted from kelp. Sodium alginate is naturally moisturizing and also acts as a good thickening agent.

阳离子瓜尔胶在护肤产品中,可降低化学物质对皮肤的刺激性和保护角质蛋白不受损伤。使皮肤平滑、减少皮肤中天然脂质的损失,增加皮肤的柔软度。同时能与阴离子、非离子和两面性离子相结合,是一种性能较好的表面活性剂。In skin care products, cationic guar gum can reduce the irritation of chemicals to the skin and protect keratin from damage. Smoothes the skin, reduces the loss of natural lipids in the skin, and increases the suppleness of the skin. At the same time, it can be combined with anion, non-ion and amphoteric ion, and it is a kind of surfactant with better performance.

经实验验证,薏苡仁提取液、金缕梅提取液、甘草提取液、雪莲果榨取液、黄秋葵榨取液、小麦胚芽油、玫瑰果油、芦荟油等在美白、祛斑、抗皱、保湿、滋润、嫩肤等方面有很好的协同效果,肌肤白皙嫩滑。It has been verified by experiments that coix seed extract, witch hazel extract, licorice extract, yacon fruit extract, okra extract, wheat germ oil, rosehip oil, aloe vera oil, etc. are effective in whitening, freckle removal, anti-wrinkle, moisturizing, moisturizing, Skin rejuvenation and other aspects have a good synergistic effect, making the skin fair and smooth.

与现有技术相比,本发明制备的爽肤水呈淡淡的乳白色,粘度适宜、稠度适宜、稳定性好、安全性强气味芳香、质感清爽、能保持肌肤水分。能够减少皱纹、改善粗糙肌肤、美白嫩肤、永葆肌肤柔软弹滑,使皮肤如同婴儿肌肤般嫩滑白皙。多种天然中药材的加入,一方面可以避免加入过多化学物质对肌肤的刺激和伤害;另一方面可以有效的锁住肌肤中的水分,能减少皱纹,使肌肤更加水润透白,呈现水感透白的美丽。同时利用稀薄乳液基质的做法,能够更好的被肌肤所吸收,有较强的美白保湿效果。淡雅的香气,沁人心脾,更让人充分享受护肤的无穷乐趣。Compared with the prior art, the toner prepared by the invention is light milky white, suitable in viscosity, suitable in consistency, good in stability, strong in safety, fragrant in smell, refreshing in texture and capable of maintaining skin moisture. It can reduce wrinkles, improve rough skin, whiten and rejuvenate the skin, keep the skin soft and smooth forever, and make the skin as tender and white as a baby's skin. The addition of a variety of natural Chinese medicinal materials, on the one hand, can avoid the stimulation and damage of the skin by adding too many chemical substances; Watery white beauty. At the same time, the method of using a thin emulsion base can be better absorbed by the skin, and has a strong whitening and moisturizing effect. The elegant aroma is refreshing and makes people fully enjoy the endless fun of skin care.

具体实施方式Detailed ways

下面结合实施例对本发明做进一步的描述。The present invention will be further described below in conjunction with the examples.

本发明的小麦胚芽油、玫瑰果油、芦荟油等为市售;乙醇的浓度为体积浓度。The wheat germ oil, rosehip oil, aloe oil etc. of the present invention are commercially available; the concentration of ethanol is volume concentration.

实施例1Example 1

一种稀薄乳液基质的爽肤水,含有以下原料:A thin emulsion-based toner containing the following ingredients:

一种稀薄乳液基质的爽肤水的制备方法,包括以下步骤:A preparation method of a toner with a thin emulsion base, comprising the following steps:

1.1甘草提取液的制备:1.1 Preparation of licorice extract:

称取甘草粗粉20g,浸泡0.5h,加热至90℃,煎煮提取3次,第1次加甘草12倍重量的水,提取1.5h,第2次加甘草10倍重量的水,提取1h,第3次加甘草6倍重量的水,提取1h,每次四层纱布滤过,合并滤液,滤液的体积浓缩至甘草重量的12倍(g/ml),过滤,滤液水浴加热到80℃,加入滤液重量2.5%活性炭和1%滑石粉,边加热边搅拌,持续时间40min,趁热抽滤,取滤液即得。Weigh 20g of licorice coarse powder, soak for 0.5h, heat to 90°C, decoct and extract 3 times, add water 12 times the weight of licorice for the first time, extract for 1.5h, add water 10 times the weight of licorice for the second time, extract for 1h For the third time, add water with 6 times the weight of licorice, extract for 1 hour, filter each time with four layers of gauze, combine the filtrate, concentrate the volume of the filtrate to 12 times the weight of licorice (g/ml), filter, and heat the filtrate to 80°C in a water bath , add 2.5% activated carbon and 1% talcum powder by weight of the filtrate, stir while heating for 40 minutes, suction filter while it is hot, and take the filtrate.

1.2薏苡仁提取液的制备:1.2 Preparation of coix seed extract:

称取薏苡仁25g,用1倍重量的自来水冲洗,冲洗液倒掉,加薏苡仁12倍重量的水煎煮提取1.5h,四层纱布过滤;滤渣再加薏苡仁10倍重量的水提取1h,四层纱布过滤;滤渣再加薏苡仁8倍重量的水提取1h,四层纱布过滤,滤渣弃掉,合并三次滤液,浓缩至薏苡仁重量的12倍(g/ml),过滤即得。Weigh 25g of coix seed, wash it with 1 times the weight of tap water, pour off the washing liquid, add 12 times the weight of coix seed, decoct and extract for 1.5h, filter with four layers of gauze; add 10 times the weight of coix seed with water, extract for 1 hour , filtered through four layers of gauze; the filter residue was extracted with 8 times the weight of coix seed with water for 1 hour, filtered through four layers of gauze, discarded the filter residue, combined three filtrates, concentrated to 12 times the weight of coix seed (g/ml), and filtered to obtain.

1.3金缕梅提取液的制备:1.3 Preparation of witch hazel extract:

称取金缕梅20g,加金缕梅14倍重量的水煎煮提取1.5h,四层纱布过滤;滤渣再加金缕梅12倍重量的水提取1h,四层纱布过滤;滤渣再加金缕梅10倍重量的水提取1h,四层纱布过滤,滤渣弃掉,合并三次滤液,浓缩至金缕梅重量的9倍(g/ml),过滤,滤液水浴加热到80℃,加入滤液重量2.5%活性炭和1%滑石粉,边加热边搅拌,持续时间40min,趁热抽滤,取滤液即得。Weigh 20g of witch hazel, add 14 times the weight of witch hazel, decoct and extract for 1.5h, filter with four layers of gauze; Extract 10 times the weight of hazel with water for 1 hour, filter with four layers of gauze, discard the filter residue, combine the three filtrates, concentrate to 9 times the weight of witch hazel (g/ml), filter, heat the filtrate to 80 ° C in a water bath, add the weight of the filtrate 2.5% activated carbon and 1% talcum powder, stir while heating for 40 minutes, suction filter while hot, and get the filtrate.

1.4雪莲果榨取液的制备1.4 Preparation of yacon extract

称取雪莲果20g,洗净切成块状,加入100ml的蒸馏水。用榨汁机榨取后,用四层纱布过滤,取滤液备用。Weigh 20g of yacon, wash and cut into pieces, and add 100ml of distilled water. After extracting with a juicer, filter with four layers of gauze, and take the filtrate for later use.

1.5黄秋葵榨取液的制备1.5 Preparation of okra extract

称取新鲜的黄秋葵20g,用清水冲洗后,切成块状,加入100ml的蒸馏水。用榨汁机榨取后,用四层纱布过滤,取滤液备用即可。Weigh 20g of fresh okra, wash it with clear water, cut it into pieces, and add 100ml of distilled water. After extracting with a juicer, filter it with four layers of gauze, and take the filtrate for later use.

1.6稀薄乳液基质的爽肤水制备1.6 Preparation of Toner with Thin Emulsion Base

a)将0.01g海藻酸钠加入到10g蒸馏水中自然溶胀,等溶胀完全形成晶莹透明的海藻酸钠凝胶液,待用;a) Add 0.01g of sodium alginate to 10g of distilled water to swell naturally, wait for the swelling to completely form a crystal clear sodium alginate gel, and set aside;

b)将0.01g阳离子瓜尔胶加入到15g蒸馏水中自然溶胀,等溶胀完全形成晶莹透明的阳离子瓜尔胶凝胶液,待用;b) 0.01g cationic guar gum is added to 15g distilled water to swell naturally, wait for the swelling to completely form crystal clear cationic guar gum gel liquid, stand-by;

c)量取1g 75%乙醇溶解0.003g尼泊金甲脂作为防腐剂溶液,待用;c) measure 1g of 75% ethanol and dissolve 0.003g of paraben as preservative solution, and set aside;

d)分别称取玫瑰果油0.5g、小麦胚芽油0.5g、芦荟油0.5g,将三者搅拌混合均匀,再加入自乳化复合型乳化剂AC-402 1.5g,于70℃中水浴加热,边加热边搅拌使其混合均匀,得到O/W型乳液的油相;d) Weigh 0.5g of rosehip oil, 0.5g of wheat germ oil, and 0.5g of aloe vera oil, stir and mix them evenly, then add 1.5g of self-emulsifying compound emulsifier AC-402, and heat in a water bath at 70°C, Stir while heating to make it evenly mixed to obtain the oil phase of the O/W emulsion;

e)量取10g蒸馏水放在水浴锅中加热得到O/W型乳液的水相;e) Measure 10g of distilled water and place it in a water bath to heat to obtain the water phase of the O/W type emulsion;

f)于70℃水浴中,等油相、水相达到相同温度时,将上述的水相呈细流状沿烧杯壁缓慢加入到油相中,边加热边沿同一方匀速搅拌,约15min后,乳化完成,即得到O/W型稀薄乳液基质;f) In a water bath at 70°C, when the oil phase and the water phase reach the same temperature, slowly add the above water phase into the oil phase in a thin stream along the beaker wall, stir at the same speed while heating, and after about 15 minutes, After the emulsification is completed, the O/W type thin emulsion matrix is obtained;

g)待乳液搅拌冷却至室温后再向其加入聚乙二醇400 1g、1,2-丙二醇1g、1%透明质酸钠1.5g、海藻酸钠凝胶、阳离子瓜尔胶凝胶液、金缕梅提取液1g、薏苡仁提取液1g、甘草提取液1g、黄秋葵榨取液1g、雪莲果榨取液1g、防腐剂溶液,加入0.1g柠檬酸调pH值为7.2,再加入0.1g香精,混合搅拌均匀,即得稀薄乳液基质的爽肤水。g) Add polyethylene glycol 400 1g, 1,2-propanediol 1g, 1% sodium hyaluronate 1.5g, sodium alginate gel, cationic guar gum gel, Add 1g of witch hazel extract, 1g of coix seed extract, 1g of licorice extract, 1g of okra extract, 1g of yacon fruit extract, preservative solution, add 0.1g of citric acid to adjust the pH value to 7.2, then add 0.1g of essence, Mix and stir evenly to obtain a toner with a thin emulsion base.

实施例2Example 2

一种稀薄乳液基质的爽肤水,含有以下原料:A thin emulsion-based toner containing the following ingredients:

一种稀薄乳液基质的爽肤水的制备方法,包括以下步骤:A preparation method of a toner with a thin emulsion base, comprising the following steps:

2.1甘草提取液的制备:2.1 Preparation of licorice extract:

称取甘草25g适量,浸泡0.5h,加热至100℃,煎煮提取3次,第1次加甘草13倍重量的水,提取1.5h,第2次加甘草11倍重量的水,提取1h,第3次加甘草7倍重量的水,提取1h,每次四层纱布滤过,合并滤液,滤液的体积浓缩至甘草重量的11倍(g/ml),过滤,滤液水浴加热到80℃,加入滤液重量4%活性炭和2%滑石粉,边加热边搅拌,持续时间50min,趁热抽滤,取滤液即得。Weigh an appropriate amount of licorice 25g, soak for 0.5h, heat to 100°C, decoct and extract 3 times, add water 13 times the weight of licorice for the first time, extract for 1.5h, add water 11 times the weight of licorice for the second time, extract for 1h, For the third time, add water with 7 times the weight of licorice, extract for 1 hour, filter each time with four layers of gauze, combine the filtrate, concentrate the volume of the filtrate to 11 times the weight of licorice (g/ml), filter, and heat the filtrate to 80 ° C in a water bath. Add 4% activated carbon and 2% talcum powder by weight of the filtrate, stir while heating for 50 minutes, suction filter while it is hot, and take the filtrate.

2.2薏苡仁提取液的制备:2.2 Preparation of coix seed extract:

称取薏苡仁30g,用1.5倍重量的自来水冲洗,冲洗液倒掉,加薏苡仁14倍重量的水煎煮提取1.5h,四层纱布过滤;滤渣再加薏苡仁11倍重量的水提取1h,四层纱布过滤;滤渣再加薏苡仁9倍重量的水提取1h,四层纱布过滤,滤渣弃掉,合并三次滤液,浓缩至薏苡仁重量的10倍(g/ml),过滤即得。Weigh 30g of coix seed, wash it with 1.5 times the weight of tap water, pour off the washing liquid, add 14 times the weight of coix seed, decoct and extract for 1.5 hours, filter with four layers of gauze; add 11 times the weight of coix seed to the filter residue, and extract for 1 hour , filter with four layers of gauze; extract the filter residue with 9 times the weight of coix seed with water for 1 hour, filter with four layers of gauze, discard the filter residue, combine the three filtrates, concentrate to 10 times the weight of coix seed (g/ml), and filter to obtain.

2.3金缕梅提取液的制备:2.3 Preparation of witch hazel extract:

称取金缕梅25g,加金缕梅16倍重量的水煎煮提取1.5h,四层纱布过滤;滤渣再加金缕梅13倍重量的水提取1h,四层纱布过滤;滤渣再加金缕梅11倍重量的水提取1h,四层纱布过滤,滤渣弃掉,合并三次滤液,浓缩至金缕梅重量的8倍(g/ml),过滤,滤液水浴加热到80℃,加入4%活性炭和2%滑石粉,边加热边搅拌,持续时间50min,趁热抽滤,取滤液即得。Weigh 25g of witch hazel, add 16 times the weight of witch hazel, decoct and extract for 1.5h, filter with four layers of gauze; Extract 1 hour of water with 11 times the weight of Hamamelis, filter through four layers of gauze, discard the filter residue, combine the three filtrates, concentrate to 8 times the weight of Hamamelis (g/ml), filter, heat the filtrate to 80°C in a water bath, add 4% Activated carbon and 2% talcum powder are stirred while heating for 50 minutes, suction filtered while hot, and the filtrate is obtained.

2.4雪莲果榨取液的制备:2.4 Preparation of yacon extract:

称取雪莲果25g,洗净切成块状,加入100ml的蒸馏水,用榨汁机榨取后,用四层纱布过滤,取滤液备用。Weigh 25g of yacon fruit, wash and cut into pieces, add 100ml of distilled water, extract it with a juicer, filter it with four layers of gauze, and take the filtrate for later use.

2.5黄秋葵榨取液的制备:2.5 Preparation of okra extract:

称取一定新鲜的黄秋葵25g,用清水冲洗后,切成块状,加入100ml的蒸馏水,用榨汁机榨取后,用四层纱布过滤,取滤液备用即可。Weigh 25g of fresh okra, wash it with water, cut it into pieces, add 100ml of distilled water, extract it with a juicer, filter it with four layers of gauze, and take the filtrate for later use.

2.6稀薄乳液基质的爽肤水制备2.6 Preparation of Toner with Thin Emulsion Base

a)将0.03g海藻酸钠加入到20g蒸馏水中自然溶胀,等溶胀完全形成晶莹透明的海藻酸钠凝胶液,待用;a) Add 0.03g of sodium alginate to 20g of distilled water to swell naturally, wait for the swelling to completely form a crystal clear sodium alginate gel, and set aside;

b)将0.02g阳离子瓜尔胶加入到20g蒸馏水中自然溶胀,等溶胀完全形成晶莹透明的阳离子瓜尔胶凝胶液,待用;b) 0.02g of cationic guar gum is added to 20g of distilled water to swell naturally, wait for the swelling to completely form crystal clear cationic guar gum gel, and set aside;

c)量取3g 75%乙醇溶解0.009g尼泊金甲脂作为防腐剂溶液,待用;c) measure 3g of 75% ethanol and dissolve 0.009g of paraben as preservative solution, and set aside;

d)分别称取玫瑰果油0.8g、小麦胚芽油0.8g、芦荟油0.8g,将三者搅拌混合均匀,再加入自乳化复合型乳化剂AC-402 2g,于70℃中水浴加热,边加热边搅拌使其混合均匀,得到O/W型乳液的油相;d) Weigh 0.8g of rosehip oil, 0.8g of wheat germ oil, and 0.8g of aloe vera oil respectively, stir and mix them evenly, then add 2g of self-emulsifying compound emulsifier AC-402, and heat in a water bath at 70°C while Stir while heating to mix evenly to obtain the oil phase of the O/W emulsion;

e)量取20g蒸馏水放在水浴锅中加热得到O/W型乳液的水相;e) Measure 20g of distilled water and place it in a water bath to heat to obtain the water phase of the O/W type emulsion;

f)于70-80℃水浴中,等油相、水相达到相同温度时,将上述的水相呈细流状沿烧杯壁缓慢加入到油相中,边加热边沿同一方匀速搅拌,约20min后,乳化完成,即得到O/W型稀薄乳液基质;f) In a water bath at 70-80°C, when the oil phase and the water phase reach the same temperature, slowly add the above water phase into the oil phase in a thin stream along the beaker wall, and stir at a constant speed on the same side while heating, about 20min Finally, the emulsification is completed, and the O/W type thin emulsion matrix is obtained;

g)待乳液搅拌冷却至室温后再向其加入聚乙二醇400 2g、1,2-丙二醇2g、1%透明质酸钠1g、海藻酸钠凝胶、阳离子瓜尔胶凝胶液、金缕梅提取液2g、薏苡仁提取液2g、甘草提取液2g、黄秋葵榨取液2g、雪莲果榨取液2g、防腐剂溶液,加入0.18g柠檬酸调pH值为6.8,再加入0.18g香精,混合搅拌均匀,即得稀薄乳液基质的爽肤水。g) Add polyethylene glycol 400 2g, 1,2-propanediol 2g, 1% sodium hyaluronate 1g, sodium alginate gel, cationic guar gum gel, gold to it after the emulsion is stirred and cooled to room temperature. Hammer hazel extract 2g, coix seed extract 2g, licorice extract 2g, okra extract 2g, yacon fruit extract 2g, preservative solution, add 0.18g citric acid to adjust the pH value to 6.8, then add 0.18g essence, mix Stir evenly to obtain a toner with a thin emulsion base.

实施例3Example 3

一种稀薄乳液基质的爽肤水,含有以下原料:A thin emulsion-based toner containing the following ingredients:

一种稀薄乳液基质的爽肤水的制备方法,包括以下步骤:A preparation method of a toner with a thin emulsion base, comprising the following steps:

3.1甘草提取液的制备:3.1 Preparation of licorice extract:

称取甘草30g适量,浸泡0.75h,加热至100℃,煎煮提取3次,第1次加甘草15倍重量的水,提取2h,第2次加甘草12倍重量的水,提取1.5h,第3次加甘草8倍重量的水,提取1h,每次四层纱布滤过,合并滤液,滤液的体积浓缩至甘草重量的10倍(g/ml),过滤,滤液水浴加热到80℃,加入滤液重量5%活性炭和3%滑石粉,边加热边搅拌,持续时间60min,趁热抽滤,取滤液即得。Weigh an appropriate amount of licorice 30g, soak for 0.75h, heat to 100°C, decoct and extract 3 times, add water 15 times the weight of licorice for the first time, extract for 2 hours, add water 12 times the weight of licorice for the second time, extract for 1.5h, For the third time, add water with 8 times the weight of licorice, extract for 1 hour, filter each time with four layers of gauze, combine the filtrate, concentrate the volume of the filtrate to 10 times the weight of licorice (g/ml), filter, and heat the filtrate to 80 ° C in a water bath. Add 5% activated carbon and 3% talcum powder by weight of the filtrate, stir while heating for 60 minutes, suction filter while it is hot, and take the filtrate.

3.2薏苡仁提取液的制备:3.2 Preparation of coix seed extract:

称取薏苡仁35g,用2倍重量的自来水冲洗,冲洗液倒掉,加薏苡仁16倍重量的水煎煮提取1.5h,四层纱布过滤;滤渣再加薏苡仁12倍重量的水提取1h,四层纱布过滤;滤渣再加薏苡仁10倍重量的水提取1h,四层纱布过滤,滤渣弃掉,合并三次滤液,浓缩至薏苡仁重量的8倍(g/ml),过滤即得。Weigh 35g of coix seed, wash it with 2 times the weight of tap water, pour off the washing liquid, add 16 times the weight of coix seed, decoct and extract for 1.5h, filter with four layers of gauze; add 12 times the weight of coix seed with water, extract for 1 hour , filter with four layers of gauze; extract the filter residue with 10 times the weight of coix seed with water for 1 hour, filter with four layers of gauze, discard the filter residue, combine the three filtrates, concentrate to 8 times the weight of coix seed (g/ml), and filter to obtain.

3.3金缕梅提取液的制备:3.3 Preparation of witch hazel extract:

称取金缕梅30g,加金缕梅18倍重量的水煎煮提取1.5h,四层纱布过滤;滤渣再加金缕梅14倍重量的水提取1.5h,四层纱布过滤;滤渣再加金缕梅12倍重量的水提取1.5h,四层纱布过滤,滤渣弃掉,合并三次滤液,浓缩至金缕梅重量的6倍(g/ml),过滤,滤液水浴加热到80℃,加入滤液重量5%活性炭和3%滑石粉,边加热边搅拌,持续时间60min,趁热抽滤,取滤液即得。Weigh 30g of witch hazel, add 18 times the weight of witch hazel, decoct and extract for 1.5h, filter with four layers of gauze; Extract 12 times the weight of witch hazel with water for 1.5 hours, filter through four layers of gauze, discard the filter residue, combine the three filtrates, concentrate to 6 times the weight of witch hazel (g/ml), filter, heat the filtrate to 80°C in a water bath, add The weight of the filtrate is 5% activated carbon and 3% talcum powder, heated and stirred for 60 minutes, suction filtered while hot, and the filtrate is obtained.

2.4雪莲果榨取液的制备:2.4 Preparation of yacon extract:

称取雪莲果30g,洗净切成块状,加入90ml蒸馏水,用榨汁机榨取后,用四层纱布过滤,取滤液备用。Weigh 30g of yacon fruit, wash and cut into pieces, add 90ml of distilled water, extract it with a juicer, filter it with four layers of gauze, and take the filtrate for later use.

2.5黄秋葵榨取液的制备:2.5 Preparation of okra extract:

称取一定新鲜的黄秋葵30g,用清水冲洗后,切成块状,加入90ml蒸馏水,用榨汁机榨取后,用四层纱布过滤,取滤液备用即可。Weigh 30g of fresh okra, wash it with water, cut it into pieces, add 90ml of distilled water, extract it with a juicer, filter it with four layers of gauze, and take the filtrate for later use.

2.6稀薄乳液基质的爽肤水制备2.6 Preparation of Toner with Thin Emulsion Base

a)将0.05g海藻酸钠加入到30g蒸馏水中自然溶胀,等溶胀完全形成晶莹透明的海藻酸钠凝胶液,待用;a) Add 0.05 g of sodium alginate to 30 g of distilled water to swell naturally, wait for the swelling to completely form a crystal clear sodium alginate gel, and set aside;

b)将0.03g阳离子瓜尔胶加入到30g蒸馏水中自然溶胀,等溶胀完全形成晶莹透明的阳离子瓜尔胶凝胶液,待用;b) 0.03g cationic guar gum is added to 30g distilled water to swell naturally, wait for the swelling to completely form crystal clear cationic guar gum gel, stand-by;

c)量取3g75%乙醇溶解0.009g尼泊金甲脂作为防腐剂溶液,待用;c) Measure 3g of 75% ethanol to dissolve 0.009g of methylparaben as a preservative solution, and set aside;

d)分别称取玫瑰果油1g、小麦胚芽油1g、芦荟油1g,将三者搅拌混合均匀,再加入自乳化复合型乳化剂AC-402 2.5g,于80℃中水浴加热,边加热边搅拌使其混合均匀,得到O/W型乳液的油相;d) Weigh 1g of rosehip oil, 1g of wheat germ oil, and 1g of aloe vera oil, stir and mix them evenly, then add 2.5g of self-emulsifying compound emulsifier AC-402, and heat in a water bath at 80°C, while heating Stir to make it evenly mixed to obtain the oil phase of the O/W emulsion;

e)量取30g蒸馏水放在水浴锅中加热得到O/W型乳液的水相;e) Measure 30g of distilled water and place it in a water bath to heat to obtain the water phase of the O/W type emulsion;

f)于80℃水浴中,等油相、水相达到相同温度时,将上述的水相呈细流状沿烧杯壁缓慢加入到油相中,边加热边沿同一方匀速搅拌,约30min后,乳化完成,即得到O/W型稀薄乳液基质;f) In a water bath at 80°C, when the oil phase and the water phase reach the same temperature, slowly add the above water phase into the oil phase in a thin stream along the beaker wall, stir at the same speed while heating, and after about 30 minutes, After the emulsification is completed, the O/W type thin emulsion matrix is obtained;

g)待乳液搅拌冷却至室温后再向其加入聚乙二醇400 3g、1,2-丙二醇3g、1%透明质酸钠溶液2g、海藻酸钠凝胶、阳离子瓜尔胶凝胶液、金缕梅提取液3g、薏苡仁提取液3g、甘草提取液3g、黄秋葵榨取液3g、雪莲果榨取液3g、防腐剂溶液,加入0.25g柠檬酸调pH值为6.5,再加入0.25g香精,混合搅拌均匀,即得稀薄乳液基质的爽肤水。g) After stirring and cooling the emulsion to room temperature, add 3 g of polyethylene glycol 400, 3 g of 1,2-propylene glycol, 2 g of 1% sodium hyaluronate solution, sodium alginate gel, cationic guar gum gel, Add 3g of witch hazel extract, 3g of coix seed extract, 3g of licorice extract, 3g of okra extract, 3g of yacon fruit extract, preservative solution, add 0.25g of citric acid to adjust the pH value to 6.5, then add 0.25g of essence, Mix and stir evenly to obtain a toner with a thin emulsion base.

实施例4Example 4

实施例1、2、3的理化指标如下:The physicochemical index of embodiment 1,2,3 is as follows:

1、性状1. Characters

本品为粘稠度适宜,稳定性好,均匀性好,质感清爽,呈淡淡乳白色,气味清新淡雅的稀薄乳液基质的溶液。This product is a thin emulsion base solution with suitable viscosity, good stability, good uniformity, refreshing texture, light milky white, fresh and elegant smell.

2、pH值检查2. pH check

取本品测得pH值为6.5-7.2。The measured pH value of this product is 6.5-7.2.

3、冷热试验3. Hot and cold test

将爽肤水封装于透明化妆品瓶中,于4℃的冰箱冷藏一个月观察无变质现象。于55℃的恒温箱内24h,爽肤水无变味、变质等现象。Package the toner in a transparent cosmetic bottle and refrigerate it in a refrigerator at 4°C for one month to observe no deterioration. In a constant temperature box at 55°C for 24 hours, the toner has no odor or deterioration.

4、室温放置实验4. Placement experiment at room temperature

将实施例1、2、3所制的爽肤水置于化妆品瓶中,室温静置考察6个月,无分层现象,用后感觉无变化,气味无变化,无变质现象。The toner prepared in Examples 1, 2, and 3 was placed in a cosmetic bottle, and left standing at room temperature for 6 months, no delamination phenomenon, no change in feeling after use, no change in smell, and no deterioration.

5、刺激性试验5. Irritation test

小白鼠背部剪去毛,取实施例1、2、3爽肤水适量涂于剪去毛的部位,和没涂部位进行比较,结果没有刺激性和过敏反应。The back hair of the mouse was cut off, and the toners of Examples 1, 2, and 3 were applied to the cut hair in an appropriate amount, and compared with the uncoated part, the results showed no irritation and allergic reaction.

取实施例1、2、3爽肤水适量涂于志愿者(16-65岁,100人)手面上,过30分钟后观察无发红、发疹、起泡现象。用后感觉皮肤比较水润,柔软,细腻,有比较舒服的感觉。Take Example 1, 2, 3 toner and apply it on the hands and faces of volunteers (16-65 years old, 100 people), and observe no redness, rash, and blistering after 30 minutes. After using it, the skin feels more hydrated, soft, delicate, and has a more comfortable feeling.

6、稀薄乳液基质的爽肤水综合效果考察6. Investigation on the comprehensive effect of toner with thin emulsion base

以下利用试用感觉来评价实施例1、2、3制造出的稀薄乳液基质的爽肤水的功效。采用民意调查评分法,选取90名25-55岁年龄段的女性作为试用对象,任意等分成三组,分别用实施例1、2、3制备的爽肤水搽胳膊。每天使用两次,使用时间两个月。各项使用效果总分为5分:五分为最高分,表示很好,非常满意;4分为较好;3分为可以接受;3分以下为不好,不能接受。以下为各项平均得分。结The efficacy of the toners with thin emulsion bases produced in Examples 1, 2, and 3 will be evaluated by using the trial experience below. Adopt the public opinion survey scoring method, select 90 women in the age group of 25-55 as trial objects, divide them into three groups arbitrarily, and paint their arms with the toner prepared in Examples 1, 2, and 3 respectively. Use twice a day for two months. The total score of each use effect is 5 points: 5 points are the highest score, which means very good and very satisfied; 4 points are good; 3 points are acceptable; below 3 points are bad and unacceptable. Below are the average scores for each category. Knot

果见表:The results are shown in the table:

综上所述,本发明所制的稀薄乳液基质的爽肤水有良好的美白嫩肤、保湿、滋养及抗细纹的效果。To sum up, the thin emulsion-based toner prepared by the present invention has good effects of whitening and rejuvenating the skin, moisturizing, nourishing and anti-fine lines.

Claims (3)

1.一种稀薄乳液基质的爽肤水,其特征在于,所述的稀薄乳液基质的爽肤水含有以下重量份的原料:1. a skin toner of thin emulsion matrix, is characterized in that, the toner of described thin emulsion matrix contains the raw material of following weight portion: 小麦胚芽油 0.5-1份0.5-1 parts of wheat germ oil 芦荟油 0.5-1份Aloe vera oil 0.5-1 parts 玫瑰果油 0.5-1份Rosehip oil 0.5-1 part 自乳化复合型乳化剂AC-402 1-2.5份Self-emulsifying compound emulsifier AC-402 1-2.5 parts 薏苡仁提取液 1-3份Coix seed extract 1-3 parts 金缕梅提取液 1-3份1-3 parts of witch hazel extract 甘草提取液 1-3份1-3 parts of licorice extract 雪莲果榨取液 1-3份Yacon extract 1-3 parts 黄秋葵榨取液 1-3份1-3 parts of okra extract 阳离子瓜尔胶 0.01-0.03份Cationic guar gum 0.01-0.03 parts 海藻酸钠 0.01-0.05份Sodium alginate 0.01-0.05 parts 1%透明质酸钠溶液 0.5-2份0.5-2 parts of 1% sodium hyaluronate solution 聚乙二醇400 1-3份Polyethylene glycol 400 1-3 parts 1,2-丙二醇 1-3份1,2-propanediol 1-3 parts 尼泊金甲酯 0.003-0.009份Methylparaben 0.003-0.009 parts 75%乙醇 1-3份75% ethanol 1-3 parts 香精 0.1-0.25份Flavor 0.1-0.25 parts 柠檬酸 0.01-0.25份Citric acid 0.01-0.25 parts 蒸馏水 30-90份;30-90 parts of distilled water; 所述的甘草提取液通过以下方法制备:Described licorice extract is prepared by the following method: 称取甘草粗粉适量,浸泡0.25-0.75h,加热至90-100℃,煎煮提取3次,第1次加甘草12-15倍重量的水,提取0.5-2h,第2次加10-12倍重量的水,提取0.5-1.5h,第3次加6-8倍重量的水,提取0.5-1.5h,每次四层纱布滤过,合并滤液,滤液的体积浓缩至甘草重量的10-12倍,滤液体积以ml计,甘草重量以g计;过滤,滤液水浴加热到80℃,加入1-5%活性炭和0.5-3%滑石粉,边加热边搅拌,持续时间30-60min,趁热抽滤,取滤液即得;Weigh an appropriate amount of licorice coarse powder, soak for 0.25-0.75h, heat to 90-100°C, decoct and extract 3 times, add 12-15 times the weight of licorice in water for the first time, extract for 0.5-2h, and add 10- 12 times the weight of water, extract 0.5-1.5h, add 6-8 times the weight of water for the third time, extract 0.5-1.5h, filter each time with four layers of gauze, combine the filtrate, and concentrate the volume of the filtrate to 10% of the weight of licorice -12 times, the volume of the filtrate is measured in ml, and the weight of licorice is measured in g; filter, heat the filtrate in a water bath to 80°C, add 1-5% activated carbon and 0.5-3% talcum powder, and stir while heating for 30-60 minutes. Suction filtration while hot, and get the filtrate; 所述的薏苡仁提取液通过以下方法制备:The coix seed extract is prepared by the following method: 称取薏苡仁适量,用1-2倍量自来水冲洗,冲洗液倒掉,加薏苡仁12-16倍重量的水煎煮提取1-1.5h,四层纱布过滤;滤渣再加薏苡仁10-12倍重量的水提取0.5-1.5h,四层纱布过滤;滤渣再加薏苡仁8-10倍重量的水提取0.5-1.5h,四层纱布过滤,滤渣弃掉,合并三次滤液,浓缩至薏苡仁重量的8-12倍 ,滤液体积以ml计,薏苡仁重量以g计,趁热抽滤,取滤液即得;Weigh an appropriate amount of coix seed, wash it with 1-2 times the amount of tap water, pour off the washing liquid, add 12-16 times the weight of coix seed, decoct it for 1-1.5 hours, filter it with four layers of gauze; add coix seed 10- Extract with 12 times the weight of water for 0.5-1.5 hours, filter with four layers of gauze; add 8-10 times the weight of coix seed to the filter residue, extract with water for 0.5-1.5 hours, filter with four layers of gauze, discard the filter residue, combine the three filtrates, and concentrate to Coix. 8-12 times the weight of the kernels, the volume of the filtrate is measured in ml, the weight of coix seed is measured in g, suction filtered while it is hot, and the filtrate is obtained; 所述的金缕梅提取液通过以下方法制备:Described witch hazel extract is prepared by the following method: 称取金缕梅适量,加金缕梅14-18倍重量的水煎煮提取0.5-1.5h,四层纱布过滤;滤渣再加金缕梅12-14倍重量的水提取0.5-1.5h,四层纱布过滤;滤渣再加金缕梅10-12倍重量的水提取0.5-1.5h,四层纱布过滤,滤渣弃掉,合并三次滤液,浓缩至金缕梅重量的6-9倍,滤液体积以ml计,金缕梅重量以g计,过滤,滤液水浴加热到80℃,加入1-5%活性炭和0.5-3%滑石粉,边加热边搅拌,持续时间30-60min,趁热抽滤,取滤液即得;Weigh an appropriate amount of hamamelis, add 14-18 times the weight of hamamelis to decoct for 0.5-1.5 hours, filter through four layers of gauze; add water 12-14 times the weight of hamamelis to extract for 0.5-1.5 hours, Filter with four layers of gauze; add 10-12 times the weight of witch hazel to the filter residue and extract with water for 0.5-1.5h, filter with four layers of gauze, discard the filter residue, combine three filtrates, concentrate to 6-9 times the weight of witch hazel, and filtrate The volume is in ml, the weight of witch hazel is in g, filter, heat the filtrate in a water bath to 80°C, add 1-5% activated carbon and 0.5-3% talcum powder, stir while heating for 30-60min, and pump while it is hot Filter and get the filtrate; 所述的雪莲果榨取液通过以下方法制备:Described Yacon fruit extract is prepared by the following method: 称取一定重量的雪莲果,洗净切成块状,加雪莲果3-5倍重量的蒸馏水,用榨汁机榨取后,用四层纱布过滤,取滤液备用;Weigh a certain weight of yacon, wash and cut into blocks, add distilled water 3-5 times the weight of yacon, squeeze it with a juicer, filter it with four layers of gauze, and take the filtrate for later use; 所述的黄秋葵榨取液通过以下方法制备:Described okra extract is prepared by the following method: 称取一定重量新鲜的黄秋葵,用清水冲洗后,切成块状,加黄秋葵3-5倍重量蒸馏水,用榨汁机榨取后,用四层纱布过滤,取滤液备用即可。Weigh a certain weight of fresh okra, wash it with water, cut it into pieces, add 3-5 times the weight of okra in distilled water, squeeze it with a juicer, filter it with four layers of gauze, and take the filtrate for later use. 2.根据权利要求1所述的稀薄乳液基质的爽肤水,其特征在于,所述的香精为柠檬香精、百合香精、桂花香精、玫瑰香精、黄瓜香精、菠萝香精或水蜜桃香精任一种。2. The skin toner with a thin emulsion matrix according to claim 1, wherein the essence is any one of lemon essence, lily essence, sweet-scented osmanthus essence, rose essence, cucumber essence, pineapple essence or peach essence. 3.一种权利要求1或2所述的稀薄乳液基质的爽肤水的制备方法,其特征在于,所述制备方法包括以下步骤:3. a preparation method of the toning water of the thin emulsion matrix described in claim 1 or 2, is characterized in that, described preparation method comprises the following steps: a)将0.01-0.05份海藻酸钠加入到10-30份蒸馏水中自然溶胀,等溶胀完全形成晶莹透明的海藻酸钠凝胶液,待用;a) Add 0.01-0.05 parts of sodium alginate to 10-30 parts of distilled water to swell naturally, and wait until the swelling is complete to form a crystal clear sodium alginate gel, which is ready for use; b)将0.01-0.03份阳离子瓜尔胶加入到10-30份蒸馏水中自然溶胀,等溶胀完全形成晶莹透明的阳离子瓜尔胶凝胶液,待用;b) Add 0.01-0.03 parts of cationic guar gum to 10-30 parts of distilled water to swell naturally, and wait until the swelling is complete to form a crystal clear cationic guar gum gel, which is ready for use; c)量取1-3份 75%乙醇溶解0.003-0.009份尼泊金甲酯作为防腐剂溶液,待用;c) Measure 1-3 parts of 75% ethanol and dissolve 0.003-0.009 parts of methyl paraben as a preservative solution, and set aside; d)分别称取玫瑰果油0.5-1份、小麦胚芽油0.5-1份、芦荟油0.5-1份,将三者搅拌混合均匀,再加入自乳化复合型乳化剂AC-402 1-2.5份,于70-80℃中水浴加热,边加热边搅拌使其混合均匀,得到O/W型乳液的油相;d) Weigh 0.5-1 part of rosehip oil, 0.5-1 part of wheat germ oil, and 0.5-1 part of aloe vera oil, stir and mix them evenly, and then add 1-2.5 parts of self-emulsifying compound emulsifier AC-402 , heated in a water bath at 70-80°C, stirred while heating to mix evenly, and obtained the oil phase of the O/W emulsion; e)量取10-30份蒸馏水放在70-80℃水浴中,加热得到O/W型乳液的水相;e) Take 10-30 parts of distilled water and place it in a water bath at 70-80°C, and heat to obtain the water phase of the O/W emulsion; f)等油相、水相达到相同温度时,将上述的水相呈细流状缓慢加入到油相中,边加热边沿同一方向匀速搅拌,15-30min后,乳化完成,即得到O/W型稀薄乳液基质;f) When the oil phase and water phase reach the same temperature, slowly add the above water phase into the oil phase in a thin stream, and stir at a constant speed in the same direction while heating. After 15-30 minutes, the emulsification is completed, and O/W is obtained Type thin emulsion base; g)待乳液基质搅拌冷却至室温后,再向其加入聚乙二醇400 1-3份、1,2-丙二醇1-3份、1%透明质酸钠溶液0.5-2份、海藻酸钠凝胶液、阳离子瓜尔胶凝胶液、金缕梅提取液1-3份、薏苡仁提取液1-3份、甘草提取液1-3份、黄秋葵榨取液1-3份、雪莲果榨取液1-3份、防腐剂溶液,加入0.01-0.25份柠檬酸调pH值为6.5-7.2,再加入0.1-0.25份香精,混合搅拌均匀,即得稀薄乳液基质的爽肤水。g) After stirring and cooling the emulsion base to room temperature, add 1-3 parts of polyethylene glycol 400, 1-3 parts of 1,2-propylene glycol, 0.5-2 parts of 1% sodium hyaluronate solution, sodium alginate Gel solution, cationic guar gum gel solution, 1-3 parts of witch hazel extract, 1-3 parts of coix seed extract, 1-3 parts of licorice extract, 1-3 parts of okra extract, yacon extract Add 0.01-0.25 parts of citric acid to adjust the pH value to 6.5-7.2, and then add 0.1-0.25 parts of essence, and mix and stir evenly to obtain a toner with a thin emulsion matrix.
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