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CN106116138A - A kind of wire drawing coating processes of minor diameter low-loss bend-insensitive single-mode optical fiber - Google Patents

A kind of wire drawing coating processes of minor diameter low-loss bend-insensitive single-mode optical fiber Download PDF

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CN106116138A
CN106116138A CN201610328402.3A CN201610328402A CN106116138A CN 106116138 A CN106116138 A CN 106116138A CN 201610328402 A CN201610328402 A CN 201610328402A CN 106116138 A CN106116138 A CN 106116138A
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optical fiber
coating
diameter
loss
fiber
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曹珊珊
刘志忠
徐海涛
王震
张海涛
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Zhongtian Technologies Fibre Optics Co Ltd
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Zhongtian Technologies Fibre Optics Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/02Manufacture of glass fibres or filaments by drawing or extruding, e.g. direct drawing of molten glass from nozzles; Cooling fins therefor
    • C03B37/025Manufacture of glass fibres or filaments by drawing or extruding, e.g. direct drawing of molten glass from nozzles; Cooling fins therefor from reheated softened tubes, rods, fibres or filaments, e.g. drawing fibres from preforms
    • C03B37/0253Controlling or regulating
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C25/00Surface treatment of fibres or filaments made from glass, minerals or slags
    • C03C25/10Coating
    • C03C25/104Coating to obtain optical fibres
    • C03C25/105Organic claddings
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C25/00Surface treatment of fibres or filaments made from glass, minerals or slags
    • C03C25/10Coating
    • C03C25/12General methods of coating; Devices therefor
    • C03C25/16Dipping

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Surface Treatment Of Glass Fibres Or Filaments (AREA)
  • Optical Fibers, Optical Fiber Cores, And Optical Fiber Bundles (AREA)

Abstract

本发明涉及一种小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺,该小直径弯曲不敏感单模光纤的拉丝涂覆工艺步骤如下:熔融拉丝、退火、测径、涂覆以及筛选。本发明的优点在于:玻璃预制棒在拉丝过程中注意张力控制,改善光纤的弯曲损耗;采用PLC控制,实测玻璃光纤的外径大小,将测量结果反馈给PLC控制单元,通过调整预制棒进料速度和拉丝速度进行动态控制,实现加工过程的自动控制;采用改进的涂覆模具在光纤上涂覆聚丙烯酸树脂,不但减小了光纤的涂覆层厚度,而且保护了内部光纤,且对光纤的性能影响很小;由于涂层变薄,在固化单元调整固化功率,节能降耗,获得最优的固化功率匹配,减少光纤固化过程产生的附件损耗。

The invention relates to a wire drawing coating process of a small-diameter, low-loss, bend-insensitive single-mode optical fiber. The steps of the wire-drawing coating process of the small-diameter bend-insensitive single-mode optical fiber are as follows: melting wire drawing, annealing, diameter measurement, coating and screening . The advantages of the present invention are: attention should be paid to the tension control of the glass preform during the wire drawing process to improve the bending loss of the optical fiber; PLC control is adopted to measure the outer diameter of the glass optical fiber, and the measurement result is fed back to the PLC control unit. The speed and drawing speed are dynamically controlled to realize the automatic control of the processing process; the improved coating mold is used to coat polyacrylic resin on the optical fiber, which not only reduces the coating thickness of the optical fiber, but also protects the internal optical fiber, and the optical fiber The effect on the performance of the optical fiber is very small; due to the thinning of the coating, the curing power is adjusted in the curing unit to save energy and reduce consumption, obtain the best matching of curing power, and reduce the loss of accessories caused by the fiber curing process.

Description

一种小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺A drawing coating process for small-diameter low-loss bend-insensitive single-mode optical fiber

技术领域technical field

本发明涉及一种光纤制造领域,特别涉及一种小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺。The invention relates to the field of optical fiber manufacturing, in particular to a wire drawing coating process for a small-diameter low-loss bending-insensitive single-mode optical fiber.

背景技术Background technique

中国“ 十二五” 规划中,将新一代信息通信纳入七大新兴战略产业, 要求加快泛在、宽带融合的信息网络基础设施建设、加快推进三网融合、加快重要基础设施的智能化改造, 推动新一代移动通信和下一代互联网设备,促进物联网、云计算的研发和示范应用。光纤光缆的应用热点是宽带中国和智能电网建设。In China's "Twelfth Five-Year Plan", the new generation of information and communication is included in the seven emerging strategic industries, and it is required to accelerate the construction of ubiquitous and broadband-integrated information network infrastructure, accelerate the integration of three networks, and accelerate the intelligent transformation of important infrastructure. Promote the new generation of mobile communications and next-generation Internet devices, and promote the research and development and demonstration applications of the Internet of Things and cloud computing. The application hotspots of optical fiber and cable are broadband China and smart grid construction.

城域网通信建设促进了光缆的大规模敷设。对于运营商而言, 城市中敷设通信光缆用的地下管道及槽道路由资源逐渐稀缺。新建路由会引发拆迁、资金、时间进度、城市密集区域管道资源无法拓展、与其他基础设施抢路由的情况。若能够充分利用稀缺路由资源敷设更大量的光纤,无疑是对城市建设的促进。在这种尺寸受限的环境下,采用更小尺寸的单模光纤,可以在有限的空间资源中,引入更多芯数的光缆,以节省空间、管道资源。将单模光纤涂层直径电常规下降到小尺寸的研究就是满足此种新型光缆应用模式。The communication construction of the metropolitan area network has promoted the large-scale laying of optical cables. For operators, underground pipelines and channel routing resources for laying communication optical cables in cities are gradually scarce. New routes will lead to demolition, capital, time schedule, failure to expand pipeline resources in urban dense areas, and competition with other infrastructure for routing. If we can make full use of scarce routing resources to lay more optical fibers, it will undoubtedly promote urban construction. In this size-constrained environment, the use of smaller-sized single-mode optical fibers can introduce more fiber optic cables in limited space resources to save space and pipe resources. The research on reducing the coating diameter of single-mode optical fiber to a small size is to meet the application mode of this new type of optical fiber cable.

随着国家“宽带中国”、“互联网+”等技术不断发展,城市中敷设通信光缆用的地下管道及槽道路由资源逐渐稀缺,这就对当前的光纤、光缆提出了新的要求。单模光纤涂层直径由常规降到小尺寸的需求应运而生,即在保证当前性能的前提下,缩小光缆尺寸。而光纤作为光缆的核心材料,其尺寸的缩小,尤其是多芯数光缆,如96芯、128芯、256芯等,可以有效减小光缆尺寸;由于涂层变薄,对光纤性能带来严重影响,因此,需要通过对预制棒折射率剖面结构调整、拉丝设备和拉丝工艺条件改进,能够生产出涂层直径稳定的小尺寸光纤。With the continuous development of national technologies such as "Broadband China" and "Internet+", the underground pipelines and channel routing resources for laying communication optical cables in cities are gradually scarce, which puts forward new requirements for current optical fibers and optical cables. The need to reduce the coating diameter of single-mode optical fiber from conventional to small size arises at the historic moment, that is, to reduce the size of the optical cable under the premise of ensuring the current performance. As the core material of the optical fiber cable, the size reduction of the optical fiber, especially the multi-core optical cable, such as 96 cores, 128 cores, 256 cores, etc., can effectively reduce the size of the optical cable; due to the thinning of the coating, it will seriously affect the performance of the optical fiber. Therefore, it is necessary to adjust the refractive index profile structure of the preform, improve the drawing equipment and drawing process conditions, and be able to produce small-sized optical fibers with stable coating diameters.

发明内容Contents of the invention

本发明要解决的技术问题是提供一种明显地减小光缆结构尺寸,而光缆性能不会出现下降的小直径弯曲不敏感单模光纤的拉丝涂覆工艺。The technical problem to be solved by the present invention is to provide a wire drawing coating process for small-diameter bend-insensitive single-mode optical fibers that significantly reduces the structural size of the optical cable without degrading the performance of the optical cable.

为解决上述技术问题,本发明的技术方案为:一种小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺,其创新点在于:该小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺步骤如下:In order to solve the above technical problems, the technical solution of the present invention is: a small-diameter low-loss bend-insensitive single-mode optical fiber drawing coating process, the innovation of which is: the small-diameter low-loss bending-insensitive single-mode optical fiber drawing coating process The covering process steps are as follows:

(1)熔融拉丝:将前期加工好的预制棒放入加热炉内,预制棒融化,在拉丝张力为100~190g的作用下以一定的速度被抽细成为玻璃光纤;(1) Fusion drawing: put the preformed rod processed in the previous stage into the heating furnace, the preform is melted, and is thinned into a glass optical fiber at a certain speed under the action of the drawing tension of 100~190g;

(2)退火:抽拉成丝后的光纤进入退火程序,退火程序依次包括退火高温炉、加热炉以及保温管三个部分,通过三级退火工序,光纤已缓慢冷却至表面假定温度,有效的消除了光纤残余内应力,且降低了光纤的衰减;(2) Annealing: The fiber drawn into filaments enters the annealing process. The annealing process includes three parts: the annealing high temperature furnace, the heating furnace and the heat preservation tube. After the three-stage annealing process, the optical fiber has been slowly cooled to the assumed surface temperature, effectively The residual internal stress of the optical fiber is eliminated, and the attenuation of the optical fiber is reduced;

(3)测径:玻璃光纤的外径通过纤经测量仪进行测量,测量结果反馈给PLC控制单元,PLC控制单元根据光纤直径数据对预制棒进料速度和拉丝速度进行调整,起到光纤拉丝过程的整体控制作用;(3) Diameter measurement: the outer diameter of the glass optical fiber is measured by a fiber warp measuring instrument, and the measurement result is fed back to the PLC control unit. The PLC control unit adjusts the feeding speed and drawing speed of the preform rod according to the fiber diameter data, which plays a role in fiber drawing. overall control of the process;

(4)涂覆:光纤进入涂覆工序,涂覆模具为一中空的柱状结构,中空内腔内盛有丙烯酸树脂涂料,在光纤的运动过程中,中空内腔中的涂料均匀的粘覆在光纤外表面上,形成一定厚度的涂覆层,涂覆层包括低模量内涂层以及高模量外涂层,内涂层与外涂层的尺寸比例为0.8~1.2:1;(4) Coating: The optical fiber enters the coating process. The coating mold is a hollow columnar structure, and the hollow cavity is filled with acrylic resin coating. During the movement of the optical fiber, the coating in the hollow cavity is evenly adhered to the surface. On the outer surface of the optical fiber, a coating layer with a certain thickness is formed. The coating layer includes a low modulus inner coating and a high modulus outer coating. The size ratio of the inner coating to the outer coating is 0.8~1.2:1;

(5)固化:光纤进入固化灯照射范围,根据涂覆层厚度变薄的情况,固化灯固化功率调整为1800~3000W;(5) Curing: The optical fiber enters the irradiation range of the curing lamp. According to the thinning of the coating layer, the curing power of the curing lamp is adjusted to 1800~3000W;

(6)筛选:由于光纤尺寸的减小,调整筛选复绕机的导轮速度,为牵引光纤提供0.35~0.85g的收线拉力。(6) Screening: Due to the reduction in the size of the optical fiber, adjust the speed of the guide wheel of the screening rewinding machine to provide a take-up pulling force of 0.35~0.85g for pulling the optical fiber.

进一步的,所述步骤(1)中加热炉内温度控制在1800℃~2200℃。Further, the temperature in the heating furnace in the step (1) is controlled at 1800°C to 2200°C.

进一步的,所述步骤(2)中加热炉温度在900℃~1200℃。Further, the temperature of the heating furnace in the step (2) is between 900°C and 1200°C.

进一步的,所述步骤(2)中,加热炉位于退火高温炉下方15cm处,保温管位于加热炉下方20~25cm处。Further, in the step (2), the heating furnace is located 15 cm below the high-temperature annealing furnace, and the insulation pipe is located 20-25 cm below the heating furnace.

进一步的,所述步骤(4)中,涂覆模具内部包括上大下小设置的圆锥状内腔以及连接在圆锥状内腔下端的涂覆孔,圆锥状内腔的锥度为3~25°,涂覆孔长度为0.8~5mm。Further, in the step (4), the interior of the coating mold includes a conical inner cavity with a large top and a small bottom and a coating hole connected to the lower end of the conical inner cavity. The taper of the conical inner cavity is 3-25° , The coating hole length is 0.8~5mm.

本发明的优点在于:The advantages of the present invention are:

(1)玻璃预制棒在拉丝过程中注意张力控制,改善光纤的弯曲损耗;采用PLC控制,实测玻璃光纤的外径大小,将测量结果反馈给PLC控制单元,通过调整预制棒进料速度和拉丝速度进行动态控制,实现加工过程的自动控制;采用改进的涂覆模具在光纤上涂覆聚丙烯酸树脂,且采用试验过的最佳的涂层比例,不但减小了光纤的涂覆层厚度,而且保护了内部光纤,且对光纤的性能影响很小;由于涂层变薄,在固化单元调整固化功率,节能降耗,获得最优的固化功率匹配,减少光纤固化过程产生的附件损耗。(1) Pay attention to the tension control of the glass preform during the drawing process to improve the bending loss of the optical fiber; use PLC control to measure the outer diameter of the glass optical fiber, and feed back the measurement results to the PLC control unit. By adjusting the feeding speed of the preform and drawing The speed is dynamically controlled to realize the automatic control of the processing process; the improved coating mold is used to coat polyacrylic resin on the optical fiber, and the best coating ratio tested is adopted, which not only reduces the coating thickness of the optical fiber, Moreover, the internal optical fiber is protected and has little impact on the performance of the optical fiber; due to the thinning of the coating, the curing power is adjusted in the curing unit to save energy and reduce consumption, obtain the optimal curing power matching, and reduce the accessory loss caused by the optical fiber curing process.

(2)采用改进的涂覆模具,调整了模具的锥度和长度,获得了适合小尺寸光纤用压力梯度范围,保证了涂覆质量和同心度要求。(2) Adopting an improved coating mold, adjusting the taper and length of the mold, obtaining a pressure gradient range suitable for small-sized optical fibers, and ensuring the coating quality and concentricity requirements.

附图说明Description of drawings

图1为本发明一种小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺的小直径弯曲不敏感单模光纤截面图。Fig. 1 is a cross-sectional view of a small-diameter bend-insensitive single-mode optical fiber in a drawing coating process of a small-diameter low-loss bend-insensitive single-mode optical fiber according to the present invention.

图2为本发明一种小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺的流程图。Fig. 2 is a flow chart of a drawing coating process for a small-diameter, low-loss, bend-insensitive single-mode optical fiber of the present invention.

图3为本发明一种小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺的涂覆模具示意图。Fig. 3 is a schematic diagram of a coating die for a wire drawing coating process of a small-diameter, low-loss, bend-insensitive single-mode optical fiber according to the present invention.

具体实施方式detailed description

如图1所示,小直径弯曲不敏感单模光纤的标称直径为200mm,从内部到外部依次包括纤芯1、包层以及涂覆层,纤芯1层为掺锗二氧化硅玻璃层,包层包括内包层2以及外包层3,内包层2为掺F的下陷内包层,在制备该光纤的预制棒中减少锗掺量以降低芯层内的瑞利散射,同时包层采用深掺氟使折射率剖面的内包层2形成下陷,并控制径向折射率均匀分布和折射率剖面斜率。As shown in Figure 1, the nominal diameter of the small-diameter bend-insensitive single-mode optical fiber is 200mm, which includes the core 1, cladding and coating layers from the inside to the outside, and the core 1 layer is a germanium-doped silica glass layer , the cladding includes an inner cladding 2 and an outer cladding 3, the inner cladding 2 is a sunken inner cladding doped with F, the germanium doping amount is reduced in the preform for preparing the optical fiber to reduce the Rayleigh scattering in the core layer, and the cladding adopts a deep Doping with fluorine makes the inner cladding layer 2 of the refractive index section form a depression, and controls the uniform distribution of the radial refractive index and the slope of the refractive index section.

如图2所示,该小直径弯曲不敏感单模光纤的拉丝涂覆工艺步骤如下:As shown in Figure 2, the drawing coating process steps of the small-diameter bend-insensitive single-mode fiber are as follows:

(1)熔融拉丝:将前期加工好的预制棒放入加热炉内,预制棒融化,在拉丝张力为100~190g的作用下以一定的速度被抽细成为玻璃光纤;(1) Fusion drawing: put the preformed rod processed in the previous stage into the heating furnace, the preform is melted, and is thinned into a glass optical fiber at a certain speed under the action of the drawing tension of 100~190g;

(2)退火:抽拉成丝后的光纤进入退火程序,退火程序依次包括退火高温炉、加热炉以及保温管三个部分,通过三级退火工序,光纤已缓慢冷却至表面假定温度,有效的消除了光纤残余内应力,且降低了光纤的衰减;(2) Annealing: The fiber drawn into filaments enters the annealing process. The annealing process includes three parts: the annealing high temperature furnace, the heating furnace and the heat preservation tube. After the three-stage annealing process, the optical fiber has been slowly cooled to the assumed surface temperature, effectively The residual internal stress of the optical fiber is eliminated, and the attenuation of the optical fiber is reduced;

(3)测径:玻璃光纤的外径通过纤经测量仪进行测量,测量结果反馈给PLC控制单元,PLC控制单元根据光纤直径数据对预制棒进料速度和拉丝速度进行调整,起到光纤拉丝过程的整体控制作用;(3) Diameter measurement: the outer diameter of the glass optical fiber is measured by a fiber warp measuring instrument, and the measurement result is fed back to the PLC control unit. The PLC control unit adjusts the feeding speed and drawing speed of the preform rod according to the fiber diameter data, which plays a role in fiber drawing. overall control of the process;

(4)涂覆:光纤进入涂覆工序,如图3所示,涂覆模具6为一中空的柱状结构,涂覆模具6内部包括上大下小设置的圆锥状内腔7以及连接在圆锥状内腔7下端的涂覆孔9,圆锥状内腔7的锥度为3~25°,涂覆孔9长度为0.8~5mm;圆锥状空腔7内盛有丙烯酸树脂涂料,光纤依次穿过涂覆模具7的圆锥状内腔以及涂覆孔9,在光纤的运动过程中,圆锥状的内腔7中的涂料均匀的粘覆在光纤8外表面上,通过下端的涂覆孔9,形成一定厚度的涂覆层,涂覆层包括低模量内涂层以及高模量外涂层,内涂层与外涂层的尺寸比例为0.8~1.2:1;(4) Coating: The optical fiber enters the coating process. As shown in Figure 3, the coating mold 6 is a hollow columnar structure. The inside of the coating mold 6 includes a conical inner cavity 7 with a large top and a small bottom and a conical cavity connected to the The coating hole 9 at the lower end of the conical cavity 7, the taper of the conical cavity 7 is 3~25°, the length of the coating hole 9 is 0.8~5mm; the conical cavity 7 is filled with acrylic resin paint, and the optical fiber passes through it in turn Coating the conical inner cavity of the mold 7 and the coating hole 9, during the movement of the optical fiber, the coating in the conical inner cavity 7 is uniformly coated on the outer surface of the optical fiber 8, and passes through the coating hole 9 at the lower end, Form a coating layer with a certain thickness, the coating layer includes a low modulus inner coating and a high modulus outer coating, and the size ratio of the inner coating to the outer coating is 0.8~1.2:1;

(5)固化:光纤进入固化灯照射范围,根据涂覆层厚度变薄的情况,固化灯固化功率调整为1800~3000W;(5) Curing: The optical fiber enters the irradiation range of the curing lamp. According to the thinning of the coating layer, the curing power of the curing lamp is adjusted to 1800~3000W;

(6)筛选:由于光纤尺寸的减小,调整筛选复绕机的导轮速度,为牵引光纤提供0.35~0.85g的收线拉力。(6) Screening: Due to the reduction in the size of the optical fiber, adjust the speed of the guide wheel of the screening rewinding machine to provide a take-up pulling force of 0.35~0.85g for pulling the optical fiber.

在拉丝过程中,注意拉丝张力的控制。光纤损耗和弯曲损耗均受到拉丝张力的影响,拉丝张力增大将增加光纤的损耗,但同时可以改善弯曲损耗,因此,在拉丝过程中,需要摸索合适的拉丝张力,从而可以解决光纤损耗和弯曲损耗的平衡控制,经过实验验证,当张力在100~190g范围内时,该产品的光纤损耗和弯曲损耗可达到最优值。During the wire drawing process, pay attention to the control of the wire drawing tension. Fiber loss and bending loss are both affected by the drawing tension. Increasing the drawing tension will increase the loss of the fiber, but at the same time it can improve the bending loss. Therefore, in the drawing process, it is necessary to find the appropriate drawing tension to solve the fiber loss and bending loss. The balance control of the product has been verified by experiments. When the tension is in the range of 100~190g, the fiber loss and bending loss of this product can reach the optimal value.

光纤弯曲损耗可以通过无量纲参数来表示:Fiber bending loss can be expressed by a dimensionless parameter:

MAC=MFD/λMAC=MFD/λ

其中,MFD为光纤的模场直径,λ为光纤的截止波长。从研究结果来看,MAC越小,光纤的弯曲损耗越小。在拉丝过程中,通过MAC值的有效控制,保证光纤的宏弯损耗不随涂层直径明显降低。Among them, MFD is the mode field diameter of the fiber, and λ is the cut-off wavelength of the fiber. From the research results, the smaller the MAC, the smaller the bending loss of the fiber. During the drawing process, through the effective control of the MAC value, it is ensured that the macrobending loss of the optical fiber does not decrease significantly with the diameter of the coating.

在退火过程中,光纤经过三次退火,第一次在拉丝炉退火高温炉中,光纤在退火高温炉中缓缓降温,下降到1500度,第二次退火在高温退火炉下方15cm处的加热炉中退火,保证光纤在加热炉内的温度在1000~1200度,第三次退火在加热炉下方20~50cm处的保温管内,对光纤进行保温退火,通过上述三次退火,使得光纤的温度呈梯度变化,当光纤暴露在车间冷空气环境中时,已经低于表面假定温度,起到了很好的退火效果。During the annealing process, the optical fiber is annealed three times. The first time is annealed in the high-temperature annealing furnace of the drawing furnace. The temperature of the optical fiber is slowly lowered in the annealing high-temperature furnace to 1500 degrees. The second annealing is in the heating furnace 15cm below the high-temperature annealing furnace. Middle annealing, to ensure that the temperature of the optical fiber in the heating furnace is 1000~1200 degrees, the third annealing is carried out in the insulation tube 20~50cm below the heating furnace, and the optical fiber is thermally annealed. Through the above three annealing, the temperature of the optical fiber is gradient When the optical fiber is exposed to the cold air environment in the workshop, it is already lower than the assumed temperature of the surface, which has a good annealing effect.

在涂覆过程中考虑内外涂层厚度的匹配性,高模量外涂层承受光纤的径向和侧向压力,低模量内涂层吸收施加于光纤上的外力,起缓冲作用。涂覆树脂本身的性能,如粘度、模量、玻璃化转变温度等影响光纤弯曲损耗。因此,这款200μm小尺寸光纤选择不同性能涂覆树脂以及研究内外涂层的厚度比较关键。结合理论分析,通过设计不同涂料、内涂层厚度、外涂层厚度三因数的DOE试验设计分析,选取两层丙烯酸树脂涂层,且内外两层涂层的厚度比为0.8~1.2:1的比例关系,能够保证内外涂层的厚度足够起到保护光纤作用,稳定光纤性能。In the coating process, the matching of the thickness of the inner and outer coatings is considered. The high-modulus outer coating bears the radial and lateral pressure of the optical fiber, and the low-modulus inner coating absorbs the external force applied to the optical fiber and acts as a buffer. The properties of the coating resin itself, such as viscosity, modulus, glass transition temperature, etc., affect the bending loss of the optical fiber. Therefore, it is critical to select different performance coating resins and study the thickness of the inner and outer coatings for this 200 μm small-size optical fiber. Combined with theoretical analysis, through the design and analysis of DOE experiment design with three factors of different coatings, inner coating thickness and outer coating thickness, two acrylic resin coatings are selected, and the thickness ratio of the inner and outer coatings is 0.8~1.2:1 The proportional relationship can ensure that the thickness of the inner and outer coatings is sufficient to protect the optical fiber and stabilize the performance of the optical fiber.

在固化过程中,由于涂层变薄,涂覆层固化速度相比常规尺寸光纤有显著提高,原有固化工艺已不适用。从节能降耗考虑,通过调整固化功率调整为1800~3000W,达到满足外观、固化度及相关机械性能要求,获得最优的固化功率匹配,减少光纤固化过程产生的附加损耗。During the curing process, due to the thinning of the coating, the curing speed of the coating layer is significantly improved compared with conventional size optical fibers, and the original curing process is no longer applicable. From the perspective of energy saving and consumption reduction, by adjusting the curing power to 1800~3000W, it can meet the requirements of appearance, curing degree and related mechanical properties, obtain the optimal curing power matching, and reduce the additional loss caused by the fiber curing process.

在筛选工序中,光纤由筛选机施加一定拉力进行缠绕,过程中所受的张力会引起光纤的附加损耗,张力较大时光纤发生断裂。同时,由于光纤尺寸的减小,原来的筛选工艺以不能满足要求,将排线节距调整为0.38~0.44mm。排线节距不佳易造成光纤弯曲损耗,缠绕密度不佳。调节筛选机收线张力为0.35~0.85g,控制线速度保持张力稳定以及排线节距的调整,减少附加衰减,降低弯曲损耗。In the screening process, the optical fiber is wound with a certain tension applied by the screening machine. The tension in the process will cause additional loss of the optical fiber, and the optical fiber will break when the tension is high. At the same time, due to the reduction of the size of the optical fiber, the original screening process cannot meet the requirements, so the cable pitch is adjusted to 0.38~0.44mm. Poor cable pitch can easily cause fiber bending loss and poor winding density. Adjust the take-up tension of the screening machine to 0.35~0.85g, control the line speed to keep the tension stable and adjust the line pitch to reduce additional attenuation and bending loss.

通过200μm低损耗弯曲不敏感单模光纤的生产研制,突破了光纤涂覆模具设计、小尺寸光纤固化工艺、微弯性能改善等关键技术和制造工艺,填补了国内空白。Through the production and development of 200μm low-loss bend-insensitive single-mode optical fiber, breakthroughs have been made in key technologies and manufacturing processes such as optical fiber coating mold design, small-size optical fiber curing process, and microbending performance improvement, filling the domestic gap.

以上显示和描述了本发明的基本原理和主要特征。本行业的技术人员应该了解,本发明不受上述实施例的限制,上述实施例和说明书中描述的只是说明本发明的原理,在不脱离本发明精神和范围的前提下,本发明还会有各种变化和改进,这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。The basic principles and main features of the present invention have been shown and described above. Those skilled in the industry should understand that the present invention is not limited by the above-mentioned embodiments. What are described in the above-mentioned embodiments and the description only illustrate the principle of the present invention. Without departing from the spirit and scope of the present invention, the present invention will also have Variations and improvements are possible, which fall within the scope of the claimed invention. The protection scope of the present invention is defined by the appended claims and their equivalents.

Claims (5)

1.一种小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺,所述小直径弯曲不敏感单模光纤的标称直径为200mm,从内部到外部依次包括纤芯、包层以及涂覆层,所述纤芯层为掺锗二氧化硅玻璃层,所述包层包括内包层以及外包层,所述内包层为掺氟的下陷内包层,其特征在于:该小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺步骤如下:1. A wire drawing coating process for a small-diameter low-loss bend-insensitive single-mode optical fiber. The nominal diameter of the small-diameter bend-insensitive single-mode optical fiber is 200 mm, which includes a core, a cladding, and a coating from the inside to the outside. The cladding layer, the core layer is a germanium-doped silica glass layer, the cladding layer includes an inner cladding layer and an outer cladding layer, and the inner cladding layer is a depressed inner cladding layer doped with fluorine, which is characterized in that: the small-diameter low-loss bending The drawing and coating process steps of insensitive single-mode fiber are as follows: 熔融拉丝:将前期加工好的预制棒放入加热炉内,预制棒融化,在拉丝张力为100~190g的作用下以一定的速度被抽细成为玻璃光纤;Fusion drawing: Put the preform processed in the early stage into the heating furnace, the preform is melted, and is thinned at a certain speed under the action of the drawing tension of 100~190g to become a glass optical fiber; 退火:抽拉成丝后的光纤进入退火程序,退火程序依次包括退火高温炉、加热炉以及保温管三个部分,通过三级退火工序,光纤已缓慢冷却至表面假定温度,有效的消除了光纤残余内应力,且降低了光纤的衰减;Annealing: The fiber drawn into filaments enters the annealing process. The annealing process includes three parts: an annealing high temperature furnace, a heating furnace, and a heat preservation tube. Through the three-stage annealing process, the fiber has been slowly cooled to the assumed surface temperature, effectively eliminating the fiber Residual internal stress, and reduce the attenuation of optical fiber; 测径:玻璃光纤的外径通过纤经测量仪进行测量,测量结果反馈给PLC控制单元,PLC控制单元根据光纤直径数据对预制棒进料速度和拉丝速度进行调整,起到光纤拉丝过程的整体控制作用;Diameter measurement: The outer diameter of the glass optical fiber is measured by a fiber warp measuring instrument, and the measurement result is fed back to the PLC control unit. The PLC control unit adjusts the feeding speed and drawing speed of the preform according to the fiber diameter data, which plays an integral role in the fiber drawing process. control effect; 涂覆:光纤进入涂覆工序,涂覆模具为一中空的柱状结构,中空内腔内盛有丙烯酸树脂涂料,在光纤的运动过程中,中空内腔中的涂料均匀的粘覆在光纤外表面上,形成一定厚度的涂覆层,涂覆层包括低模量内涂层以及高模量外涂层,内涂层与外涂层的尺寸比例为0.8~1.2:1;Coating: The optical fiber enters the coating process. The coating mold is a hollow columnar structure, and the hollow cavity is filled with acrylic resin coating. During the movement of the optical fiber, the coating in the hollow cavity is evenly adhered to the outer surface of the optical fiber. On top, a coating layer with a certain thickness is formed, the coating layer includes a low modulus inner coating and a high modulus outer coating, and the size ratio of the inner coating to the outer coating is 0.8~1.2:1; 固化:光纤进入固化灯照射范围,根据涂覆层厚度变薄的情况,固化灯固化功率调整为1800~3000W;Curing: The optical fiber enters the irradiation range of the curing lamp. According to the thinning of the coating layer, the curing power of the curing lamp is adjusted to 1800~3000W; 筛选:由于光纤尺寸的减小,调整筛选复绕机的导轮速度,为牵引光纤提供0.35~0.85g的收线拉力。Screening: Due to the reduction in the size of the optical fiber, adjust the speed of the guide wheel of the screening and rewinding machine to provide a take-up pulling force of 0.35~0.85g for pulling the optical fiber. 2.根据权利要求1所述的一种小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺,其特征在于:所述步骤(1)中加热炉内温度控制在1800℃~2200℃。2. The wire drawing coating process for small-diameter, low-loss, bend-insensitive single-mode optical fiber according to claim 1, wherein the temperature in the heating furnace in the step (1) is controlled at 1800°C~2200°C. 3.根据权利要求1所述的一种小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺,其特征在于:所述步骤(2)中加热炉温度在900℃~1200℃。3. The wire drawing coating process for small-diameter, low-loss, bend-insensitive single-mode optical fiber according to claim 1, wherein the temperature of the heating furnace in the step (2) is 900°C-1200°C. 4.根据权利要求1所述的一种小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺:其特征在于:所述步骤(2)中,加热炉位于退火高温炉下方15cm处,保温管位于加热炉下方20~25cm处。4. The drawing coating process of a small-diameter, low-loss, bend-insensitive single-mode optical fiber according to claim 1: characterized in that: in the step (2), the heating furnace is located 15 cm below the annealing high-temperature furnace, and the heat preservation The tube is located 20-25 cm below the furnace. 5.根据权利要求1所述的一种小直径低损耗弯曲不敏感单模光纤的拉丝涂覆工艺,其特征在于:所述步骤(4)中,涂覆模具内部包括上大下小设置的圆锥状内腔以及连接在圆锥状内腔下端的涂覆孔,圆锥状内腔的锥度为3~25°,涂覆孔长度为0.8~5mm。5. The wire-drawing coating process for small-diameter, low-loss, bend-insensitive single-mode optical fiber according to claim 1, characterized in that: in the step (4), the interior of the coating mold includes upper, lower, and lower The conical inner cavity and the coating hole connected to the lower end of the conical inner cavity, the taper of the conical inner cavity is 3-25°, and the length of the coating hole is 0.8-5mm.
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CN109116466A (en) * 2018-08-24 2019-01-01 长飞光纤光缆股份有限公司 A kind of thin footpath small-bend radius single mode optical fiber
CN111362572A (en) * 2018-12-26 2020-07-03 深圳特发信息光纤有限公司 Optical fiber preparation method and optical fiber
WO2022121259A1 (en) * 2020-12-07 2022-06-16 中天科技光纤有限公司 Optical fiber and preparation method therefor
CN114371530A (en) * 2020-12-24 2022-04-19 中天电力光缆有限公司 Optical fiber structure, production method of optical fiber structure and optical cable structure
CN112897874A (en) * 2021-05-07 2021-06-04 中天科技光纤有限公司 Control method and control device for optical fiber drawing speed and optical fiber drawing system
CN112897874B (en) * 2021-05-07 2021-11-16 中天科技光纤有限公司 Optical fiber drawing speed control method, control device and optical fiber drawing system
CN113582534A (en) * 2021-09-01 2021-11-02 中天科技光纤有限公司 Method and apparatus for manufacturing optical fiber
CN113716862A (en) * 2021-09-01 2021-11-30 中天科技光纤有限公司 Method and apparatus for manufacturing optical fiber

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