CN106109316A - A kind of face water alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E and preparation method thereof - Google Patents
A kind of face water alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E and preparation method thereof Download PDFInfo
- Publication number
- CN106109316A CN106109316A CN201610593932.0A CN201610593932A CN106109316A CN 106109316 A CN106109316 A CN 106109316A CN 201610593932 A CN201610593932 A CN 201610593932A CN 106109316 A CN106109316 A CN 106109316A
- Authority
- CN
- China
- Prior art keywords
- extract
- semen coicis
- aurantii immaturus
- phase
- chest nut
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of face water alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E and preparation method thereof.It is made up of the raw material of following percentage by weight: glycerol: 2.0 5.0, butanediol: 4.0 8.0, methyl hydroxybenzoate: 0.05 0.2, allantoin: 0.05 0.2, hydroxyethyl cellulose: 0.2 0.5, glycine betaine: 0.5 1.5,2% acrylic acid (ester) class/C10 30 alkylol acrylamide acid esters cross linked polymer: 2.0 4.0, hyaluronate sodium: 0.04 0.16, deionized water: 70.0 90.0；Triethanolamine: 0.02 0.1, reed fragrant plant oil: 2.0 5.0；GPL:0.3 0.5, PEG 14 polydimethylsiloxane: 0.5 1.5；HPS:0.01 0.015, essence: 0.001 0.002, Semen Coicis extract: 0.05 0.2, Fructus Aurantii Immaturus berry extract: 0.05 0.2, Horse chest Nut P.E: 0.05 0.2.The formula of the present invention is simple, has the effect of antiallergic moisturizing, and manufacture method is simple, is suitable for a large amount of production, cost-effective.
Description
Technical field
The invention belongs to cosmetic technical field, particularly to one containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Semen Aesculi
Pole oxygen face water alive of extract and preparation method thereof.
Background technology
Along with the development of modern society, what all kinds of chemicals used be continuously increased, increasing environmental pollution
Etc. causing skin to be often dried, intensely dark pool, the crowd of sensitive skin are also continuously increased.At present, cosmetics are people's
Occupying considerable status in daily life, China is populous, especially cosmetics consumption big country.Advocate nature, return certainly
Right theory is increasingly by the most well-established.China's plant resources is numerous, therefore for development plant extract be effective ingredient
Cosmetics there is inborn advantage.
Semen Coicis is the kernel of grass Semen Coicis.Humid region is born in happiness, but can be waterlogging drought-enduring.The most all there is cultivation
Training, various places, the Changjiang river areas to the south have wild.In China's medical book ancient books the most on the books, Semen Coicis is splendid beauty treatment food materials, has
Control the flat pox of wart, light speckles, beautification and white, enhance metabolism, the maintaining beauty and keeping young, especially institute such as thinning face, skin moistening smoothing wrinkle, Glycerin
The proteolytic enzyme contained can make skin keratin soften, and vitamin E has antioxidation and enhancing immunity and promotion cell regeneration
Effect, strengthens blood circulation, promotes skin tissue regeneration.
Fructus Aurantii Immaturus is rutaceae Citrus aurantium Linn. and variety thereof or the dry young fruit of Fructus Citri sinensis, and extract contains higher flavone
Constituents, accounts for 5%-28%, and flavones ingredient is mainly Hesperidin, hesperetin, naringin, naringenin, neohesperidin, Pericarpium Citri grandis rue
Fragrant glycosides, tangeritin, isosakuranetin, neohesperidoside, 8-tetramethoxy flavones, Radix seu Folium Tosicodendri Delavayi glucoside, xylostein etc..Research finds Fructus Aurantii Immaturus
Extract has antiallergic, antiinflammatory, antioxidation, reduction vascular permeability and effect of fragility.
Semen Aesculi is the dry mature seed of Hippocastanaceae plant Aesculus chinensis Bunge, and Aesculus chinensis Bunge is deciduous tree, up to 25m, many
Cultivation, rare wild, for " Chinese Pharmacopoeia " conventional Chinese medicine recorded.Semen Aesculi fatty oily 31.8%, starch 36%, fiber
L4.7%, crude protein 1.1%, separately containing Aescin.Fatty oil is mainly oleic acid and stearic glyceride.Its main component seven leaf
The energy such as saponin, flavone compound, the tannic acid of concentration, sterol and phytosterol play synergism with phospholipid, promote skin
Microcirculation, smooth the vestige of asthenia, be used for alleviate diffusivity red blood streak, have be effectively improved face blood capillary expansion
Zhang Xianxiang, safeguards the integrity of blood vessel wall, and in lowering vascular permeability and pre-preventing tissue, moisture stockpiles, eliminates rapidly local edema
The heavy sensation caused and pressure, make skin histology closely knit and high resilience.
Carry out above-mentioned effective ingredients in plant extracting the extract obtained, arrange in pairs or groups through different proportion, make an addition to cosmetics
In, both can effectively solve the various problems that skin exists, can effectively overcome again the zest of synthetics, dependence
Property, market potential is huge.
Summary of the invention
It is an object of the invention to provide including Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E is gentle
Plant extract application in cosmetics, not only can effectively realize the effects such as whitening, antiinflammatory sterilization, moisturizing but also overcomes chemistry
The untoward reaction such as the zest of synthetic, dependency.
Add Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E to Yan Shuizhong alive, prepare one and carry containing Semen Coicis
Taking the pole oxygen face water alive of thing, Furctus Aurantii Immaturus extract and Horse chest Nut P.E, preparation technology is simple and reliable, gentle non-stimulated, to skin
Dry, rubescent, pruritus etc. has improves effect.
A kind of face water alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E, by following weight percent
The component of ratio prepares:
A phase:
Glycerol: 2.0-5.0,
Butanediol: 4.0-8.0,
Methyl hydroxybenzoate: 0.05-0.2,
Allantoin: 0.05-0.2,
Hydroxyethyl cellulose: 0.2-0.5,
Glycine betaine: 0.5-1.5,
2% acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer: 2.0-4.0,
Hyaluronate sodium: 0.04-0.16,
Deionized water: 70.0-90.0；
B phase:
Triethanolamine: 0.02-0.1,
Reed fragrant plant oil: 2.0-5.0；
C phase:
Preservative: 0.3-0.5,
PEG-14 polydimethylsiloxane: 0.5-1.5；
D phase:
Cocos nucifera oil alcohol ether-7/PPG-1-PEG-9 lauryl glycol ether/PEG-40 castor oil hydrogenated (trade name HPS): 0.01-
0.015,
Essence: 0.001-0.002,
Semen Coicis extract: 0.05-0.2,
Fructus Aurantii Immaturus berry extract: 0.05-0.2,
Horse chest Nut P.E: 0.05-0.2.
Preferably, described preservative is purchased from Long Sha company of the U.S., trade name GPL.
Preferably, described Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E are to use with use ethanol as entrainer
Semen Coicis after cleaning, Fructus Aurantii Immaturus and Semen Aesculi are extracted gained by supercritical carbon dioxide method for extracting.
It is highly preferred that described supercritical carbon dioxide extraction condition is: extracting pressure 30-40 MPa, extraction temperature 45-
55 DEG C, extract 4-6 hour, CO2 flow 10-12 mL/min.
Preferably, the density relative to water of described Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E is
0.9-1.1。
Preferably, described essence is that cosmetic field commonly uses raw material, including in vanillin, Flos Jasmini Sambac quintessence oil or Flos Rosae Rugosae quintessence oil
One.
The preparation side of described a kind of face water alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E
Method, comprises the following steps:
(1) equipment cleaning process, then heat hot water to 80-90 DEG C, sterilize more than ten minutes；
(2) accurately weighing each material of A phase, 15-30r/min stirring is warming up to 85-87 DEG C and is uniformly dissolved, and is incubated 5 minutes, starts
Cooling；
(3) it is sequentially added into B phase when being cooled to 58-60 DEG C in order every, and 15-30r/min stirring and dissolving is uniform；
(4) D phase is pre-mixed and is uniformly dissolved；
(5) it is cooled to 45-50 DEG C, each for C phase material is sequentially added in order, add the D phase that mixed dissolution is good, 15-30r/
Min stirs 15 minutes；
(6) self-inspection is through after the assay was approved with discharging after filter-cloth filtering.
Beneficial effects of the present invention is as follows:
The Furctus Aurantii Immaturus extract, the Horse chest Nut P.E that add in the cosmetic composition of the present invention have excellent antiinflammatory antiallergic and make
With, can neutralize or lower the noxious substance of cosmetics, prevent anaphylaxis.
The face water formula alive letter of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E that the present invention provides
Single, promote skin to permeate moisturizing, regulate water and oil balance, have preferable antiinflammatory antiallergic effect；Do not stimulate skin of face simultaneously, described
Manufacture method simple, be suitable for a large amount of production, cost-effective.
Accompanying drawing explanation
Fig. 1 is the radar map using sense evaluation result of the product that embodiment prepares with comparative example；
Fig. 2 is the evaluation result schematic diagram of the moistening effect of the product that embodiment prepares with comparative example.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described further, and described embodiment is served only for explaining the present invention, not
For limiting the scope of the present invention.
The part material source used in following example is as follows: HPS(cocos nucifera oil alcohol ether-7/PPG-1-PEG-9 lauryl
Glycol ether/PEG-40 castor oil hydrogenated) purchased from Kening Co., Ltd of Germany；Reed fragrant plant oil (polyglycerolmethacrylate/propylene glycol/
PVM/MA) purchased from American I SP company；GPL(dimethyloldimethylhydantoin), purchased from Long Sha company of the U.S..
Table 1 embodiment 1-3 and the formula of comparative example 1-4
Embodiment 1
(1) equipment cleaning process, then heat hot water to 90 DEG C, sterilize more than ten minutes；
(2) accurately weighing each material of A phase, 15r/min stirring is warming up to 85 DEG C and is uniformly dissolved, and is incubated 5 minutes, starts cooling；
(3) it is cooled to addition B phase when 60 DEG C every, and 15r/min stirring and dissolving is uniform；
(4) D phase is uniformly dissolved in advance；
(5) being cooled to 45 DEG C and be separately added into each material of C phase and the D phase dissolved, 15r/min stirs 15 minutes；
(6) self-inspection is through after the assay was approved with discharging after 400 mesh filter-cloth filterings.
Embodiment 2
(1) equipment cleaning process, then heat hot water to 85 DEG C, sterilize more than ten minutes；
(2) accurately weighing each material of A phase, 30r/min stirring is warming up to 86 DEG C and is uniformly dissolved, and is incubated 5 minutes, starts cooling；
(3) it is cooled to addition B phase when 58 DEG C every, and 30r/min stirring and dissolving is uniform；
(4) D phase is uniformly dissolved in advance；
(5) being cooled to 50 DEG C and be separately added into each material of C phase and the D phase dissolved, 30r/min stirs 15 minutes；
(6) self-inspection is through after the assay was approved with discharging after 400 mesh filter-cloth filterings.
Embodiment 3
(1) equipment cleaning process, then heat hot water to 80 DEG C, sterilize more than ten minutes；
(2) accurately weighing each material of A phase, 22.5r/min stirring is warming up to 87 DEG C and is uniformly dissolved, and is incubated 5 minutes, starts fall
Temperature；
(3) it is cooled to addition B phase when 59 DEG C every, and 22.5r/min stirring and dissolving is uniform；
(4) D phase is uniformly dissolved in advance；
(5) being cooled to 47.5 DEG C and be separately added into each material of C phase and the D phase dissolved, 22.5r/min stirs 15 minutes；
(6) self-inspection is through after the assay was approved with discharging after 400 mesh filter-cloth filterings.
Comparative example 1
(1) equipment cleaning process, then heat hot water to 90 DEG C, sterilize more than ten minutes；
(2) accurately weighing each material of A phase, 15r/min stirring is warming up to 85 DEG C and is uniformly dissolved, and is incubated 5 minutes, starts cooling；
(3) it is cooled to addition B phase when 60 DEG C every, and 15r/min stirring and dissolving is uniform；
(4) D phase is uniformly dissolved in advance；
(5) being cooled to 45 DEG C and be separately added into each material of C phase and the D phase dissolved, 15r/min stirs 15 minutes；
(6) self-inspection is through after the assay was approved with discharging after 400 mesh filter-cloth filterings.
Comparative example 2
(1) equipment cleaning process, then heat hot water to 85 DEG C, sterilize more than ten minutes；
(2) accurately weighing each material of A phase, 30r/min stirring is warming up to 86 DEG C and is uniformly dissolved, and is incubated 5 minutes, starts cooling；
(3) it is cooled to addition B phase when 58 DEG C every, and 30r/min stirring and dissolving is uniform；
(4) D phase is uniformly dissolved in advance；
(5) being cooled to 50 DEG C and be separately added into each material of C phase and the D phase dissolved, 30r/min stirs 15 minutes；
(6) self-inspection is through after the assay was approved with discharging after 400 mesh filter-cloth filterings.
Comparative example 3
(1) equipment cleaning process, then heat hot water to 80 DEG C, sterilize more than ten minutes；
(2) accurately weighing each material of A phase, 22.5r/min stirring is warming up to 87 DEG C and is uniformly dissolved, and is incubated 5 minutes, starts fall
Temperature；
(3) it is cooled to addition B phase when 59 DEG C every, and 22.5r/min stirring and dissolving is uniform；
(4) D phase is uniformly dissolved in advance；
(5) being cooled to 47.5 DEG C and be separately added into each material of C phase and the D phase dissolved, 22.5r/min stirs 15 minutes；
(6) self-inspection is through after the assay was approved with discharging after 400 mesh filter-cloth filterings.
Comparative example 4
(1) equipment cleaning process, then heat hot water to 85 DEG C, sterilize more than ten minutes；
(2) accurately weighing each material of A phase, 25r/min stirring is warming up to 85 DEG C and is uniformly dissolved, and is incubated 5 minutes, starts cooling；
(3) it is cooled to addition B phase when 60 DEG C every, and 25r/min stirring and dissolving is uniform；
(4) D phase is uniformly dissolved in advance；
(5) being cooled to 50 DEG C and be separately added into each material of C phase and the D phase dissolved, 25r/min stirs 15 minutes；
(6) self-inspection is through after the assay was approved with discharging after 400 mesh filter-cloth filterings.
The sample prepared in above example and comparative example, all through stability test, will expect that body is respectively-15 DEG C, 4 DEG C, room
Temperature, 45 DEG C, place one month under the conditions of natural lighting and fluorescent lamp ,-15 DEG C, 4 DEG C, 25 DEG C, 45 DEG C of circulating temperatures (follow
Ring incubator is arranged each temperature hold-time be 4h, 16h be a circulation) under the conditions of place one week, respectively expect the color of body, abnormal smells from the patient and
Form all keeps stable.
Use skinfeel is evaluated
Carried out using the evaluation test of sense by the specialty evaluation person of 20 cosmetic evaluations, be used for evaluating by each test sample 0.5g
Following 6 projects are evaluated: 1 by person) denseness；2) smoothness；3) salubrious property；4) water moisture feeling；5) absorbability；6) residual
Stay film；7) sticky sense.
The marking result of each specialty evaluation person will be averaged, using institute's value as the evaluation result using sense, make
Go out the radar map being illustrated in fig. 1 shown below.In evaluating at this, professional group member marks, every item rating 1 ~ 5 point, and score value is the highest,
This result obtained is the highest or the best, such as in denseness is evaluated, the denseness of the product of 5 must be divided into be higher than to be divided into the product of 3
Product denseness.The scoring of each embodiment and comparative example product use skinfeel is as shown in table 2.
The each embodiment of table 2 and comparative example product use skinfeel scoring
As shown in Table 2, each embodiment without large change, is evaluated at smoothness, salubrious property, water moisture feeling, absorbability etc. in denseness
In project, add Semen Coicis extract, Furctus Aurantii Immaturus extract and three kinds of active component products (embodiment 1-3) of Horse chest Nut P.E simultaneously
Scoring higher than add single-activity component product (comparative example 2-4), the comparative example 1 being not added with any active matter is marked minimum.
Antiallergic effect is evaluated
Antiallergic effect by the cosmetics obtained by relative analysis evaluation the various embodiments described above and comparative example.
The cosmetics that above-described embodiment and comparative example prepare, 30 personnel through 25～50 years old try out respectively, person on probation
Healthy, without dermatosis and allergy medical history, non-sensitive skin, it is possible to by Normalization rule cosmetics, and cooperating personnel press
Requirement completes appraisal, has certain expressive faculty, the impression after energy actual response use.
Using face cheek, lip as test zone, smear the lactic acid of 10% at test zone, when tester feels thorn
When swashing, smear test product.Experimenter, according to pain, carries out recording antianaphylactic effect and (divides: without effect, gently when the 4th minute
Micro-effect, partial action and obvious effect)；Antiallergic test statistics the results are shown in Table 3.
Table 3 antiallergic test result
As known from Table 3, the antiallergic effect of the cosmetics obtained by embodiment 1～3 is good, is better than comparative example 1～4；Embodiment 1
～3 compare with comparative example 2～4 and to understand, add Semen Coicis extract, Furctus Aurantii Immaturus extract and three kinds of active component energy of Horse chest Nut P.E
Further enhance the antiallergic effect of product, after three kinds of active adding ingredients are compounding, there is collaborative antiallergic effect；Comparative example 1
Compare with comparative example 2～4 and understand, do not add arbitrary composition in Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E
Cosmetics antiallergic effect is poor；Knowable to comparative example 2 compares with comparative example 3,4, individually add Furctus Aurantii Immaturus extract or Semen Aesculi carries
The product taking thing is better than the antiallergic effect of individually interpolation Semen Coicis extract product.
Moistening effect is evaluated
Carried out product beta test by 10 triers and carry out keratodermatitis water cut test: by skin before and after measurement use product
The change of water content of stratum corneum is weighed in the change of skin horny layer capacitance, thus evaluates the moisture-keeping efficacy of makeup removal products, this
The method of kind carries out quantification to the moisture of keratodermatitis, it is possible to react the change of skin moisture content delicately.
Experimental technique: bend side at candidate left and right forearm and mark 3 × 3cm2The square Experimental Area of size, makees with left arm
For the test zone of embodiment, right arm test zone as a comparison case, then with Corneometer CM825, (moisture content is tested
Probe) detect the moisture at each test position, it is repeated 3 times and draws stationary value.
Moisture content is calculated: moisture content=(test value-blank value)/blank value × 100% with following formula.
Above evaluation result is shown in Fig. 2, obtains 20 bit test persons change of different time skin moisture content in 6h
Percentage ratio, before the data of 0h record are for using product.As seen from Figure 2, the pole oxygen of the present invention face water moisturizing to skin alive
Effect is obvious, the most after a procedure in the time range of 1h；Prolongation over time, moistening effect decreases, but is surveying
In examination time range, the moisture content of (6h) skin is still significantly improved, and illustrates that oxygen face water alive in pole has obvious moisturizing effect
Really.
The above, be only presently preferred embodiments of the present invention, and the present invention not does any pro forma restriction, thus all not
Depart from technical solution of the present invention content, according to the present invention technical spirit to any simple modification made for any of the above embodiments,
Equivalent variations and modification, all still fall within the scope of technical solution of the present invention.
Claims (7)
1. the face water alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E, it is characterised in that by following
The component of percentage by weight prepares:
A phase:
Glycerol: 2.0-5.0,
Butanediol: 4.0-8.0,
Methyl hydroxybenzoate: 0.05-0.2,
Allantoin: 0.05-0.2,
Hydroxyethyl cellulose: 0.2-0.5,
Glycine betaine: 0.5-1.5,
2% acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer: 2.0-4.0,
Hyaluronate sodium: 0.04-0.16,
Deionized water: 70.0-90.0；
B phase:
Triethanolamine: 0.02-0.1,
Reed fragrant plant oil: 2.0-5.0；
C phase:
Preservative: 0.3-0.5,
PEG-14 polydimethylsiloxane: 0.5-1.5；
D phase:
Cocos nucifera oil alcohol ether-7/PPG-1-PEG-9 lauryl glycol ether/PEG-40 castor oil hydrogenated: 0.01-0.015,
Essence: 0.001-0.002,
Semen Coicis extract: 0.05-0.2,
Fructus Aurantii Immaturus berry extract: 0.05-0.2,
Horse chest Nut P.E: 0.05-0.2.
A kind of face alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E the most according to claim 1
Water, it is characterised in that described preservative is purchased from Long Sha company of the U.S., trade name GPL.
A kind of face alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E the most according to claim 1
Water, it is characterised in that described Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E are with super with use ethanol as entrainer
Semen Coicis after cleaning, Fructus Aurantii Immaturus and Semen Aesculi are extracted gained by critical carbon dioxide extracting process.
A kind of face alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E the most according to claim 3
Water, it is characterised in that described supercritical carbon dioxide extraction condition is: extracting pressure 30-40MPa, extraction temperature 45-55 DEG C,
Extract 4-6 hour, CO2Flow 10-12mL/min.
A kind of face alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E the most according to claim 1
Water, it is characterised in that the density relative to water of described Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E is
0.9-1.1。
A kind of face alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E the most according to claim 1
Water, it is characterised in that described essence is that cosmetic field commonly uses raw material, including in vanillin, Flos Jasmini Sambac quintessence oil or Flos Rosae Rugosae quintessence oil
One.
7. a kind of face alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E described in preparation claim 1
The method of water, it is characterised in that comprise the following steps:
(1) equipment cleaning process, then heat hot water to 80-90 DEG C, sterilize more than ten minutes；
(2) accurately weighing each material of A phase, 15-30r/min stirring is warming up to 85-87 DEG C and is uniformly dissolved, and is incubated 5 minutes, starts
Cooling；
(3) it is sequentially added into B phase when being cooled to 58-60 DEG C in order every, and 15-30r/min stirring and dissolving is uniform；
(4) D phase is pre-mixed and is uniformly dissolved；
(5) it is cooled to 45-50 DEG C, each for C phase material is sequentially added in order, add the D phase that mixed dissolution is good, 15-30r/
Min stirs 15 minutes；
(6) self-inspection is through after the assay was approved with discharging after filter-cloth filtering.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610593932.0A CN106109316A (en) | 2016-07-26 | 2016-07-26 | A kind of face water alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610593932.0A CN106109316A (en) | 2016-07-26 | 2016-07-26 | A kind of face water alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106109316A true CN106109316A (en) | 2016-11-16 |
Family
ID=57289677
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610593932.0A Pending CN106109316A (en) | 2016-07-26 | 2016-07-26 | A kind of face water alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106109316A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106924110A (en) * | 2017-02-15 | 2017-07-07 | 广东华夏友美生物科技有限公司 | A kind of preparation of Ganodenna Lucidum P.E and its application process |
| ES2685002A1 (en) * | 2017-03-31 | 2018-10-05 | Itf Research Pharma, S.L.U. | Lubricant formulations (Machine-translation by Google Translate, not legally binding) |
| CN112569148A (en) * | 2019-09-28 | 2021-03-30 | 广州市中通生化制品有限公司 | Traditional Chinese medicine composition with allergy-relieving and anti-allergy effects and preparation method and application thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102258436A (en) * | 2011-08-29 | 2011-11-30 | 广州市白云联佳精细化工厂 | Refreshing hydrating and beautifying lotion with moisture function |
| CN104622740A (en) * | 2015-01-14 | 2015-05-20 | 武汉爱民制药有限公司 | Application of semen aesculi extract in preparation of pharmaceutical cosmetic |
| CN105769741A (en) * | 2016-05-19 | 2016-07-20 | 覃政强 | Whitening mask lotion suitable for sensitive skins and preparation method thereof |
-
2016
- 2016-07-26 CN CN201610593932.0A patent/CN106109316A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102258436A (en) * | 2011-08-29 | 2011-11-30 | 广州市白云联佳精细化工厂 | Refreshing hydrating and beautifying lotion with moisture function |
| CN104622740A (en) * | 2015-01-14 | 2015-05-20 | 武汉爱民制药有限公司 | Application of semen aesculi extract in preparation of pharmaceutical cosmetic |
| CN105769741A (en) * | 2016-05-19 | 2016-07-20 | 覃政强 | Whitening mask lotion suitable for sensitive skins and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 光华养生堂: "《100种美容食物排行榜》", 31 October 2011, 广东经济出版社 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106924110A (en) * | 2017-02-15 | 2017-07-07 | 广东华夏友美生物科技有限公司 | A kind of preparation of Ganodenna Lucidum P.E and its application process |
| ES2685002A1 (en) * | 2017-03-31 | 2018-10-05 | Itf Research Pharma, S.L.U. | Lubricant formulations (Machine-translation by Google Translate, not legally binding) |
| WO2018178478A3 (en) * | 2017-03-31 | 2018-11-22 | Itf Research Pharma, S.L.U. | Lubricant formulations |
| CN112569148A (en) * | 2019-09-28 | 2021-03-30 | 广州市中通生化制品有限公司 | Traditional Chinese medicine composition with allergy-relieving and anti-allergy effects and preparation method and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103284940B (en) | Saccharomycetes fermented traditional Chinese medicine composition, as well as preparation method and application thereof | |
| CN105434323B (en) | Saccharomycetes to make fermentation compound and its application in skin whitening, moisturizing skin care item | |
| JP2021020887A (en) | Enhanced anti-aging cosmetic composition | |
| JP2022059604A (en) | Anti-aging cosmetic composition | |
| CN102258442B (en) | Compound traditional Chinese medicine extract and application thereof to whitening, moisturizing and anti-aging skin care product | |
| CN105411951B (en) | Application of the Xylaria nigripes extract in skin whitening, moisturizing cosmetics | |
| CN101873847A (en) | Composition for skin external application containing complex of herbal extracts | |
| CN108670943A (en) | A kind of moisturizing, whitening, light spot composition of plant extracts | |
| KR101964809B1 (en) | Inhibitor for NO activator, Anit-inflammation agent containing of the same, Revitalizing cosmetics containing the same and Manufacturing method thereof | |
| CN109453087B (en) | Whitening skin-penetrating lotion, preparation method thereof and whitening cosmetic additive | |
| TW200423961A (en) | Composition for promoting production of type I collagen and/or elastin | |
| CN104188857B (en) | Traditional Chinese medicine skin-whitening fleck-banishing cream and preparation method thereof | |
| CN109662904A (en) | It is a kind of to have effects that the skin care compositions of whitening antioxidation and its application and preparation method | |
| CN106176511A (en) | A kind of propolis pore cleanser nose film and its preparation method and application | |
| CN103099774B (en) | Chinese medicine composition and application thereof | |
| CN105998195A (en) | Cannabis extract with anti-sensitive and moisture retention functions and application thereof | |
| CN106420459B (en) | A kind of ginseng water Essence living and preparation method thereof and the facial mask comprising it | |
| KR101638832B1 (en) | A cosmetic composition for improving the refreshing and elasticity of skin comprising medicinal herbs | |
| CN108309923A (en) | Whitening spot-eliminating composition and preparation method thereof | |
| CN106109316A (en) | A kind of face water alive of the pole oxygen containing Semen Coicis extract, Furctus Aurantii Immaturus extract and Horse chest Nut P.E and preparation method thereof | |
| Talreja et al. | Formulation and evaluation of herbal soap by using Moringa oleifera as main active constituents | |
| CN106511218A (en) | Emulsion capable of removing acne | |
| CN110313898A (en) | A kind of evaluation method of Shu Min substance used for cosmetic | |
| CN103816083B (en) | A kind of pox-dispelling function transparency emulsion containing basic fibroblast growth factor and preparation method thereof | |
| CN108836904A (en) | A kind of skin care compositions of wrinkle reduction and the preparation method and application thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161116 |