CN106009604A - Inorganic vitrification-modified nano environment-friendly rubber material and preparation method thereof - Google Patents
Inorganic vitrification-modified nano environment-friendly rubber material and preparation method thereof Download PDFInfo
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- CN106009604A CN106009604A CN201610617285.2A CN201610617285A CN106009604A CN 106009604 A CN106009604 A CN 106009604A CN 201610617285 A CN201610617285 A CN 201610617285A CN 106009604 A CN106009604 A CN 106009604A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L71/00—Compositions of polyethers obtained by reactions forming an ether link in the main chain; Compositions of derivatives of such polymers
- C08L71/02—Polyalkylene oxides
- C08L71/03—Polyepihalohydrins
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/001—Conductive additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
- C08L2205/16—Fibres; Fibrils
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Abstract
The invention discloses an inorganic vitrification-modified nano environment-friendly rubber material and a preparation method thereof. The inorganic vitrification-modified nano environment-friendly rubber material is prepared from epichlorohydrin rubber, acrylonitrile-butadiene copolymer rubber, diene rubber, styrene-butadiene rubber, regenerated rubber, light calcium carbonate, high-water-retentivity resin polyvinyl alcohol, a dispersing agent, a thickener, a whitener, zinc sulfide, foamed aluminum, hydroxypropyl methylcellulose, nano silicon dioxide, an adhesive, cobalt naphthenate, molybdenum, nickel, propanediol and chromium. The inorganic vitrification-modified nano environment-friendly rubber material is specially used for building external walls, and effectively enhances various properties of the building external wall. The combination of the butadiene-acrylonitrile rubber, acrylonitrile-butadiene copolymer rubber, diene rubber, styrene-butadiene rubber and regenerated rubber used as main materials greatly enhances the toughness of the inorganic vitrification-modified nano environment-friendly rubber material and effectively solves the problem of high cracking rupture tendency of the conveyer belt. The inorganic vitrification-modified nano environment-friendly rubber material can not generate harmful gases to the human body, has a perfect combination of high temperature resistance, tear resistance and other properties, and thus, is applicable to various severe working conditions. The asphalt-base carbon fibers are adopted to enhance the mechanical properties of the material, and can greatly adsorb and remove harmful gases and dust substances in the tail gas.
Description
Technical field
The present invention relates to technical field of construction and decoration materials, particularly relate to a kind of inorganic vitreous modified Nano environment-friendly rubber material
Material and preparation method.
Background technology
Base material is typically by four kinds of bases: film forming matter (resin), pigment (including extender pigment), solvent and interpolation
Agent.
1 film forming matter is the main component of film, including oils and fats, fats and oils processing product, cellulose derivative, natural tree
Fat and synthetic resin.Film forming matter also includes the nonvolatile reactive diluent of part, and it is to make base material be firmly attached to coated article
Form the main matter of continuous film on face, be the basis constituting base material, decide the fundamental characteristics of base material.
2 auxiliary agents such as defoamer, levelling agent etc., also have some special function additives, such as ground wetting agent etc..These help
Agent typically can not film forming, but process and durability that base material is formed film play considerable effect.
3 pigment typically divide two kinds, and one is coloring pigment, common titanium dioxide, chrome yellow etc., and also planting is extender pigment,
The filler namely often said, such as calcium carbonate, Pulvis Talci.
4 solvents include varsol (mineral spirits, kerosene, gasoline, benzene,toluene,xylene etc.), alcohols, ethers, ketone
Class and Ester.The Main Function of solvent and water is to make film forming binder dispersion form thick liquid.It contributes to construction
With some performance improving film.
Substrate performance of the prior art is not sufficiently stable, and the especially heat-insulating property of base material is the highest.
Summary of the invention
For overcoming above-mentioned deficiency, the present invention provides a kind of inorganic vitreous modified Nano environment-protective rubber material and preparation side
Method.
The present invention takes techniques below scheme to realize: a kind of inorganic vitreous modified Nano environment-protective rubber material, it
Including constitutive material be: nitrile rubber modified phenolic resin 8-10 part, hexamethylenamine 15-20 part, decompression residuum 5-10 part, drip
Blue or green base carbon fibre powder 6-8 part, non-halogenated organophosphinate 5-7 part, hexamethylenetetramine 8-10 part, tri-methyl-amyl three second
TMOS 2-4 part, conductive mica powder 0.3-0.5 weight portion, conductive nano graphite powder 0.2-0.4 weight portion, polyisocyanates
Trimer 0.8-1 weight portion, polytetrafluoroethylene fibre 1-2 weight portion, glass bead 20-30 weight portion, titanium dioxide 1-10
Part, quartz sand 1-5 weight portion, silicon carbide micro-powder 2-6 weight portion, nano-cerium oxide 1-5 weight portion, ethanedioic acid polyester 1-5 weight
Part, precipitated calcium carbonate 4-10 weight portion, high-moisture-retention resin polyvinyl alcohol 10-14 weight portion, dispersant 6-10 weight portion, thickening
Agent 1-5 weight portion, brightening agent 2-6 weight portion, zinc sulfide 3-7 weight portion, foamed aluminium 0.8-2.8 weight portion, hydroxypropyl methyl are fine
Dimension element 8-12 weight portion, nano silicon 10-14 weight portion, binding agent 8-14 weight portion.
The present invention also provides for the preparation method of a kind of inorganic vitreous modified Nano environment-protective rubber material, by following steps group
Become:
(1) pulverize after organic siliconresin, glass bead, titanium dioxide, quartz sand mixing, cross 100-200 mesh sieve, as component
A is standby；
(2) by silicon carbide micro-powder, nano-cerium oxide, ethanedioic acid polyester, precipitated calcium carbonate, high-moisture-retention resin polyvinyl alcohol, sulfur
Change zinc, foamed aluminium, hydroxypropyl methyl cellulose are placed in pulverizer pulverizing, cross 100-200 mesh sieve, prepare component B standby；
(3) under vacuum, after component A, the mixing of component B, mixing 3-4min in mixing roll is poured into；Regulation mixing roll temperature
To 140-160 DEG C,
(4) plasticate, by chlorohydrin rubber, nitrile rubber, acrylonitrile-butadiene copolymer rubber, diene rubber part, butadiene-styrene rubber,
Mix and blend 30min in the plasticator that internal temperature is 120 DEG C put into by reclaimed rubber, obtains component C,
(5) mixing, by component A, it is to add other component, mix and blend 20min in 120 DEG C of mixing rolls that B, C put into internal temperature；
And under conditions of 100 DEG C, vulcanizing 30min, it is thus achieved that product places 3h；
(6) molding, puts in forming machine by the product of previous step, it is thus achieved that product.
The method have the advantages that invention is with chlorohydrin rubber, nitrile rubber, propylene in sum
Nitrile-butadiene copolymer rubber, diene rubber, butadiene-styrene rubber, reclaimed rubber are that major ingredient is with the use of substantially increasing material
Toughness, effectively solves the situation that conveyer belt is easily broken off, also will not produce harmful gas simultaneously under higher temperature
The performances such as body is high temperature resistant, tear-resistant perfectly merge so that the present invention can apply to work under various mal-condition.Offer group
Assignment system is reasonable, by the raw material components of composition, such as: pulverize after the mixing of organic siliconresin, glass bead, titanium dioxide, quartz sand,
Especially by part material component therein, the thermal and insulating performance with excellence and the fire prevention that effectively increase this base material are resistance to
Ageing properties, not hollowing cracking, intensity are high, and environment-protecting asepsis, free from extraneous odour, light weight, heat conductivity is low, and heat-insulating property is stable, good
Good freeze-thaw resistance and water resistance, Fire retardant grade is high, and good cohesive force and shearing force have outstanding cracking resistance anti-wind pressure
Can, not hollowing cracking, the performances, especially heat-insulating property such as intensity is high significantly improve；.Add rock gangue, conductive mica powder,
The reinforcing agents such as conductive nano graphite powder can improve resistant to thermal aging cracking performance, thus improves casting efficiency, reduces casting cost.
The present invention uses asphalt base carbon fiber to enhance harmful gas that the mechanical property of material can adsorb and remove in tail gas greatly
Body and dust material.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and be easy to understand with effect, below in conjunction with
Detailed description of the invention, is expanded on further the present invention.
Embodiment 1 one kinds inorganic vitreous modified Nano environment-protective rubber material and preparation method
A kind of inorganic vitreous modified Nano environment-protective rubber material, the constitutive material that it includes is: chlorohydrin rubber 90 parts, nitrile rubber
30 parts, acrylonitrile-butadiene copolymer rubber 55 parts, diene rubber 50 parts, 20 parts of butadiene-styrene rubber, reclaimed rubber 25 parts, Colophonium
6 parts of base carbon fibre powder, non-halogenated organophosphinate 5 parts, hexamethylenetetramine 8 parts, tri-methyl-amyl triethoxysilane 2
Part, trimer 0.8 weight portion of conductive mica powder 0.3 weight portion, conductive nano graphite powder 0.2 weight portion, polyisocyanates, poly-
Tetrafluoroethylene fiber 1 weight portion, glass bead 20 weight portion, titanium dioxide 1 part, quartz sand 1 weight portion, silicon carbide micro-powder 2 weight
Amount part, nano-cerium oxide 1 weight portion, ethanedioic acid polyester 1 weight portion, precipitated calcium carbonate 4 weight portion, high-moisture-retention resin polyethylene
Alcohol 10 weight portion, dispersant 6 weight portion, thickening agent 1 weight portion, brightening agent 2 weight portion, zinc sulfide 3 weight portion, foamed aluminium 0.8
Weight portion, hydroxypropyl methyl cellulose 8 weight portion, nano silicon 10 weight portion, binding agent 8 weight portion.
The present invention also provides for the preparation method of a kind of inorganic vitreous modified Nano environment-protective rubber material, by following steps group
Become:
(1) pulverize after organic siliconresin, glass bead, titanium dioxide, quartz sand mixing, cross 100-200 mesh sieve, as component
A is standby；
(2) by silicon carbide micro-powder, nano-cerium oxide, ethanedioic acid polyester, precipitated calcium carbonate, high-moisture-retention resin polyvinyl alcohol, sulfur
Change zinc, foamed aluminium, hydroxypropyl methyl cellulose are placed in pulverizer pulverizing, cross 100-200 mesh sieve, prepare component B standby；
(3) under vacuum, after component A, the mixing of component B, mixing 3-4min in mixing roll is poured into；Regulation mixing roll temperature
To 140-160 DEG C,
(4) plasticate, by chlorohydrin rubber, nitrile rubber, acrylonitrile-butadiene copolymer rubber, diene rubber part, butadiene-styrene rubber,
Mix and blend 30min in the plasticator that internal temperature is 120 DEG C put into by reclaimed rubber, obtains component C,
(5) mixing, by component A, it is to add other component, mix and blend 20min in 120 DEG C of mixing rolls that B, C put into internal temperature；
And under conditions of 100 DEG C, vulcanizing 30min, it is thus achieved that product places 3h；
(6) molding, puts in forming machine by the product of previous step, it is thus achieved that product.
Embodiment 2 one kinds inorganic vitreous modified Nano environment-protective rubber material and preparation method method
A kind of inorganic vitreous modified Nano environment-protective rubber material, the constitutive material that it includes is: chlorohydrin rubber 100 parts, the fine rubber of fourth
50 parts of glue, acrylonitrile-butadiene copolymer rubber 60 parts, diene rubber 60 parts, 40 parts of butadiene-styrene rubber, reclaimed rubber 40 parts, drip
Blue or green 8 parts of base carbon fibre powder, non-halogenated organophosphinate 7 parts, hexamethylenetetramine 10 parts, tri-methyl-amyl triethoxysilicane
4 parts of alkane, conductive mica powder 0.5 weight portion, conductive nano graphite powder 0.4 weight portion, trimer 1 weight portion of polyisocyanates,
Polytetrafluoroethylene fibre 2 weight portion, glass bead 30 weight portion, titanium dioxide 10 parts, quartz sand 5 weight portion, silicon carbide micro-powder 6
Weight portion, nano-cerium oxide 5 weight portion, ethanedioic acid polyester 5 weight portion, precipitated calcium carbonate 10 weight portion, high-moisture-retention resin are poly-
Vinyl alcohol 14 weight portion, dispersant 10 weight portion, thickening agent 5 weight portion, brightening agent 6 weight portion, zinc sulfide 7 weight portion, foam
Aluminum 2.8 weight portion, hydroxypropyl methyl cellulose 12 weight portion, nano silicon 14 weight portion, binding agent 14 weight portion.
The present invention also provides for the preparation method of a kind of inorganic vitreous modified Nano environment-protective rubber material, by following steps group
Become:
(1) pulverize after organic siliconresin, glass bead, titanium dioxide, quartz sand mixing, cross 100-200 mesh sieve, as component
A is standby；
(2) by silicon carbide micro-powder, nano-cerium oxide, ethanedioic acid polyester, precipitated calcium carbonate, high-moisture-retention resin polyvinyl alcohol, sulfur
Change zinc, foamed aluminium, hydroxypropyl methyl cellulose are placed in pulverizer pulverizing, cross 100-200 mesh sieve, prepare component B standby；
(3) under vacuum, after component A, the mixing of component B, mixing 3-4min in mixing roll is poured into；Regulation mixing roll temperature
To 140-160 DEG C,
(4) plasticate, by chlorohydrin rubber, nitrile rubber, acrylonitrile-butadiene copolymer rubber, diene rubber part, butadiene-styrene rubber,
Mix and blend 30min in the plasticator that internal temperature is 120 DEG C put into by reclaimed rubber, obtains component C,
(5) mixing, by component A, it is to add other component, mix and blend 20min in 120 DEG C of mixing rolls that B, C put into internal temperature；
And under conditions of 100 DEG C, vulcanizing 30min, it is thus achieved that product places 3h；
(6) molding, puts in forming machine by the product of previous step, it is thus achieved that product.
The above is embodiments of the invention, therefore all according to the structure described in the present patent application scope, feature and principle institute
The equivalence change done or modification, in the range of being all included in present patent application.
Claims (2)
1. an inorganic vitreous modified Nano environment-protective rubber material, it is characterised in that the constitutive material that it includes is: chlorohydrin rubber
90-100 part, nitrile rubber 30-50 part, acrylonitrile-butadiene copolymer rubber 55-60 part, diene rubber 50-60 part, butylbenzene
Rubber 20-40 part, reclaimed rubber 25-40 part, asphalt base carbon fiber powder 6-8 part, non-halogenated organophosphinate 5-7 part, six
Methine tetramine 8-10 part, tri-methyl-amyl triethoxysilane 2-4 part, conductive mica powder 0.3-0.5 weight portion, conductive nano
Graphite powder 0.2-0.4 weight portion, the trimer 0.8-1 weight portion of polyisocyanates, polytetrafluoroethylene fibre 1-2 weight portion, glass
Change microballon 20-30 weight portion, titanium dioxide 1-10 part, quartz sand 1-5 weight portion, silicon carbide micro-powder 2-6 weight portion, nano oxidized
Cerium 1-5 weight portion, ethanedioic acid polyester 1-5 weight portion, precipitated calcium carbonate 4-10 weight portion, high-moisture-retention resin polyvinyl alcohol 10-
14 weight portions, dispersant 6-10 weight portion, thickening agent 1-5 weight portion, brightening agent 2-6 weight portion, zinc sulfide 3-7 weight portion, bubble
Foam aluminum 0.8-2.8 weight portion, hydroxypropyl methyl cellulose 8-12 weight portion, nano silicon 10-14 weight portion, binding agent 8-
14 weight portions.
2. according to the preparation method of the arbitrary described a kind of inorganic vitreous modified Nano environment-protective rubber material of claim 1-3, its
It is characterised by: comprise the steps of:
(1) pulverize after organic siliconresin, glass bead, titanium dioxide, quartz sand mixing, cross 100-200 mesh sieve, as component
A is standby；
(2) by silicon carbide micro-powder, nano-cerium oxide, ethanedioic acid polyester, precipitated calcium carbonate, high-moisture-retention resin polyvinyl alcohol, sulfur
Change zinc, foamed aluminium, hydroxypropyl methyl cellulose are placed in pulverizer pulverizing, cross 100-200 mesh sieve, prepare component B standby；
(3) under vacuum, after component A, the mixing of component B, mixing 3-4min in mixing roll is poured into；Regulation mixing roll temperature
To 140-160 DEG C,
(4) plasticate, by chlorohydrin rubber, nitrile rubber, acrylonitrile-butadiene copolymer rubber, diene rubber part, butadiene-styrene rubber,
Mix and blend 30min in the plasticator that internal temperature is 120 DEG C put into by reclaimed rubber, obtains component C,
(5) mixing, by component A, it is to add other component, mix and blend 20min in 120 DEG C of mixing rolls that B, C put into internal temperature；
And under conditions of 100 DEG C, vulcanizing 30min, it is thus achieved that product places 3h；
(6) molding, puts in forming machine by the product of previous step, it is thus achieved that product.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108035511A (en) * | 2018-01-18 | 2018-05-15 | 金亿源(江苏)新材料有限公司 | A kind of nitrile rubber and PVC mixing vulcanization floor |
| CN109097688A (en) * | 2018-09-10 | 2018-12-28 | 江苏天泽教育咨询有限公司 | A kind of environment protection type high-strength metal material and its production technology |
| CN109320806A (en) * | 2018-11-06 | 2019-02-12 | 盐城神瑞胶带有限公司 | A kind of PVG whole belt core fire retarding conveying band |
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| CN102378834A (en) * | 2009-01-30 | 2012-03-14 | 帝人株式会社 | Graphitized short fibers and composition thereof |
| CN105164193A (en) * | 2013-05-03 | 2015-12-16 | 埃克森美孚化学专利公司 | Filled elastomeric composite and process to control composite crumb size |
| CN105462177A (en) * | 2016-01-07 | 2016-04-06 | 苏州法斯特信息科技有限公司 | High-temperature resistance inflaming retarding bamboo-plastic composite material and preparation method thereof |
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| CN101778903A (en) * | 2007-07-06 | 2010-07-14 | 独立行政法人产业技术综合研究所 | Structural body comprising filler and incompatible resin or elastomer, and production process or use thereof |
| CN102378834A (en) * | 2009-01-30 | 2012-03-14 | 帝人株式会社 | Graphitized short fibers and composition thereof |
| CN105164193A (en) * | 2013-05-03 | 2015-12-16 | 埃克森美孚化学专利公司 | Filled elastomeric composite and process to control composite crumb size |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108035511A (en) * | 2018-01-18 | 2018-05-15 | 金亿源(江苏)新材料有限公司 | A kind of nitrile rubber and PVC mixing vulcanization floor |
| CN109097688A (en) * | 2018-09-10 | 2018-12-28 | 江苏天泽教育咨询有限公司 | A kind of environment protection type high-strength metal material and its production technology |
| CN109320806A (en) * | 2018-11-06 | 2019-02-12 | 盐城神瑞胶带有限公司 | A kind of PVG whole belt core fire retarding conveying band |
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