CN105916221A - Graphene electrical heating body preparation method - Google Patents
Graphene electrical heating body preparation method Download PDFInfo
- Publication number
- CN105916221A CN105916221A CN201610302390.7A CN201610302390A CN105916221A CN 105916221 A CN105916221 A CN 105916221A CN 201610302390 A CN201610302390 A CN 201610302390A CN 105916221 A CN105916221 A CN 105916221A
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- Prior art keywords
- electrical heating
- incubated
- minutes
- room temperature
- graphene
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 33
- 229910021389 graphene Inorganic materials 0.000 title claims abstract description 31
- 238000010438 heat treatment Methods 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 238000005485 electric heating Methods 0.000 claims abstract description 15
- 239000002002 slurry Substances 0.000 claims abstract description 13
- 238000000034 method Methods 0.000 claims abstract description 6
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims abstract description 3
- 229910052709 silver Inorganic materials 0.000 claims abstract description 3
- 239000004332 silver Substances 0.000 claims abstract description 3
- 238000001816 cooling Methods 0.000 claims description 12
- 239000003085 diluting agent Substances 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 230000005540 biological transmission Effects 0.000 claims description 8
- 229910052799 carbon Inorganic materials 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 238000007650 screen-printing Methods 0.000 claims description 8
- 239000000758 substrate Substances 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 5
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 239000005011 phenolic resin Substances 0.000 claims description 4
- 229920001568 phenolic resin Polymers 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 238000007639 printing Methods 0.000 abstract description 6
- 238000006243 chemical reaction Methods 0.000 abstract description 4
- 238000005245 sintering Methods 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 239000010410 layer Substances 0.000 description 7
- 238000001755 magnetron sputter deposition Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 238000005118 spray pyrolysis Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- XMWRBQBLMFGWIX-UHFFFAOYSA-N C60 fullerene Chemical compound C12=C3C(C4=C56)=C7C8=C5C5=C9C%10=C6C6=C4C1=C1C4=C6C6=C%10C%10=C9C9=C%11C5=C8C5=C8C7=C3C3=C7C2=C1C1=C2C4=C6C4=C%10C6=C9C9=C%11C5=C5C8=C3C3=C7C1=C1C2=C4C6=C2C9=C5C3=C12 XMWRBQBLMFGWIX-UHFFFAOYSA-N 0.000 description 1
- 239000002041 carbon nanotube Substances 0.000 description 1
- 229910021393 carbon nanotube Inorganic materials 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000004146 energy storage Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229910003472 fullerene Inorganic materials 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000010257 thawing Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B3/00—Ohmic-resistance heating
- H05B3/10—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor
- H05B3/12—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor characterised by the composition or nature of the conductive material
- H05B3/14—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor characterised by the composition or nature of the conductive material the material being non-metallic
- H05B3/145—Carbon only, e.g. carbon black, graphite
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B3/00—Ohmic-resistance heating
- H05B3/84—Heating arrangements specially adapted for transparent or reflecting areas, e.g. for demisting or de-icing windows, mirrors or vehicle windshields
Landscapes
- Carbon And Carbon Compounds (AREA)
Abstract
The present invention discloses a graphene electrical heating body preparation method. The method comprises the following steps: (1) preparing electrical heating body slurry; (2) preparing silver electrode; (3) preparing an electric heating layer; and (4) preparing an encapsulated layer. The electrical heating body prepared by the graphene electrical heating body preparation method employs the graphene electrical heating slurry, and because the minimal current can activate a grapheme far-infrared electrothermal portion, the graphene electrical heating body preparation method only save 60% of energy compared with a traditional electrothermal mode, and therefore, the electric energy utilization rate is improved, the heat transfer resistance is small, and the chemical stability, the heat stability and the electrothermal conversion efficiency are high. The number of the printing silk screens, the number of times of printing sintering and the number of times of continuous printing are combined to realize the changing of the total resistance value of a fixed figure so as to reach an object restistance.
Description
Technical field
The present invention relates to household electrical appliances and manufacture field, be specifically related to the preparation method of a kind of Graphene electric heating body.
Background technology
It is little that traditional method using resistance wire to carry out heating service also exists electrical heating area, and electrical heating efficiency is low, and resistance wire uses easily oxidation, the shortcoming that the life-span is short for a long time.Therefore, increasing electric heating film initially enters the visual field of people.
Semiconductor conducting film has been widely used in the glass defrosting of the equipment such as automobile, aircraft, refrigerator.But mainly use the mode of magnetron sputtering and spray pyrolysis to prepare.But the equipment used in this preparation process is much more expensive, additionally, due to the shape of household electrical appliance is the most extremely complex, the mode of magnetron sputtering and spray pyrolysis is used to be difficult to be compound on electrical heating utensil semiconductor conducting film.
Graphene (Graphene) was caused the extensive concern of scientist by the report such as the professor Geim of Univ Manchester UK with its peculiar performance from 2004 and great interest is predicted probably causes revolutionary variation in a lot of fields.Single-layer graphene with two dimensional crystal structure exist thickness 0.1334nm it be construct other dimension carbonaceous material elementary cell it can wrap up and form the fullerene of zero dimension and roll and form one-dimensional carbon nanotube layer layer stack and amass and form three-dimensional graphite.Graphene is that a kind of quasiconductor not having energy gap has the carrier mobility (2 × 10cm/v) of high 100 times than silicon and at room temperature has a micron order free path and big coherence length therefore Graphene is the ideal material of nanometric circuit.Graphene has good heat conductivity [3000W/ (m K)], high intensity (110GPa) and the specific surface area (2630m/g) of super large.The performance of these excellences makes Graphene have the application prospect of light in fields such as nano electron device, gas sensor, energy storage and composites.
Existing heater is inconvenient when making, and Production Time is long, and heater heating efficiency is low.
Summary of the invention
The present invention provides the preparation method of a kind of Graphene electric heating body, electric heating body prepared by this technique, has the electrical heating conversion performance of excellence and longer service life.
To achieve these goals, it is achieved above-mentioned purpose, the invention provides the preparation method of a kind of Graphene electric heating body, the method comprises the steps:
(1) electrical heating slurry is prepared
Weigh the graphene powder of 6-7 weight portion, the far infrared transmission agent of 0.5-2 weight portion, the bonding diluent of 3-5 weight portion, stir after first graphene powder being mixed with far infrared transmission agent, after being subsequently adding bonding diluent mixing, form slurry；Described bonding diluent is resistant to elevated temperatures phenolic resin, and the particle diameter of graphene powder is: 30-60nm；
(2) silver electrode is made
Substrate is printed 250 mesh silk screens, room temperature levelling 10-15min, in 110-150 DEG C of temperature range, is dried 10-15min；It is sintered at conventional, electric-resistance stove: room temperature 150 DEG C, is incubated 10 minutes, is then heated to 450 DEG C-600 DEG C, about 5-10 DEG C per minute of programming rate, it is incubated 10 minutes；Open fire door, take out cooling；
(3) electric heating layer is made
Above-mentioned electrical heating slurry is being done in substrate 100 mesh or 150 mesh silk screen printings, room temperature levelling 10-15min, in 150-180 DEG C of temperature range, it is dried 10-15min；It is sintered at conventional, electric-resistance stove: room temperature 150 DEG C, is incubated 10 minutes, is then heated to 650 DEG C-750 DEG C, about 10-15 DEG C per minute of programming rate, it is incubated 15 minutes；Open fire door, take out cooling；
(4) encapsulated layer is made
Encapsulating material is carried out on electric heating layer 200 mesh silk screen printings, room temperature levelling 5-10min；After drying, sinter at continuous tunnel furnace: during continuous tunnel furnace room temperature 150 DEG C, be incubated 10 minutes；It is then heated to 600 DEG C, 15-20 DEG C per minute of programming rate, it is incubated 10 minutes after arriving 600 DEG C；Opening fire door, temperature is down to less than 500 DEG C, i.e. takes out cooling.
Electric heating element prepared by the present invention, use above-mentioned Graphene electrical heating slurry, Graphene far-infrared electric part just can be activated due to small electric current, than traditional electrothermal method saving energy 60%, improve the utilization rate of electric energy, heat transfer resistance is little, chemical stability and heat stability, electric-thermal conversion efficiency is high, and being combined by the pass of continuous printing when the mesh number of printing screen, the number of times of printing-sintering and printing reaches the change of total resistance value under set figure, reaches target resistance.
Detailed description of the invention
Embodiment one
Weigh the graphene powder of 6 weight portions, the far infrared transmission agent of 0.5 weight portion, the bonding diluent of 3 weight portions, stir after first graphene powder being mixed with far infrared transmission agent, after being subsequently adding bonding diluent mixing, form slurry；Described bonding diluent is resistant to elevated temperatures phenolic resin, and the particle diameter of graphene powder is: 30-60nm.
Substrate is printed 250 mesh silk screens, room temperature levelling 10min, in 110 DEG C of temperature ranges, is dried 10-15min；It is sintered at conventional, electric-resistance stove: room temperature 150 DEG C, is incubated 10 minutes, is then heated to 450 DEG C DEG C, about 5 DEG C per minute of programming rate, it is incubated 10 minutes；Open fire door, take out cooling.
Above-mentioned electrical heating slurry is being done in substrate 100 mesh silk screen printings, room temperature levelling 10min, in 150 DEG C of temperature ranges, it is dried 10min；It is sintered at conventional, electric-resistance stove: room temperature 150 DEG C, is incubated 10 minutes, is then heated to 650 DEG C, about 10 DEG C per minute of programming rate, it is incubated 15 minutes；Open fire door, take out cooling.
Encapsulating material is carried out on electric heating layer 200 mesh silk screen printings, room temperature levelling 5min；After drying, sinter at continuous tunnel furnace: during continuous tunnel furnace room temperature 150 DEG C, be incubated 10 minutes；It is then heated to 600 DEG C, 15 DEG C per minute of programming rate, it is incubated 10 minutes after arriving 600 DEG C；Opening fire door, temperature is down to less than 500 DEG C, i.e. takes out cooling.
Embodiment two
Weigh the graphene powder of 7 weight portions, the far infrared transmission agent of 2 weight portions, the bonding diluent of 5 weight portions, stir after first graphene powder being mixed with far infrared transmission agent, after being subsequently adding bonding diluent mixing, form slurry；Described bonding diluent is resistant to elevated temperatures phenolic resin, and the particle diameter of graphene powder is: 30-60nm.
Substrate is printed 250 mesh silk screens, room temperature levelling 15min, in 150 DEG C of temperature ranges, is dried 15min；It is sintered at conventional, electric-resistance stove: room temperature 150 DEG C, is incubated 10 minutes, is then heated to 600 DEG C, about 10 DEG C per minute of programming rate, it is incubated 10 minutes；Open fire door, take out cooling.
Above-mentioned electrical heating slurry is being done in substrate 150 mesh silk screen printings, room temperature levelling 15min, in 180 DEG C of temperature ranges, it is dried 15min；It is sintered at conventional, electric-resistance stove: room temperature 150 DEG C, is incubated 10 minutes, is then heated to 750 DEG C, about-15 DEG C per minute of programming rate, it is incubated 15 minutes；Open fire door, take out cooling.
Encapsulating material is carried out on electric heating layer 200 mesh silk screen printings, room temperature levelling 10min；After drying, sinter at continuous tunnel furnace: during continuous tunnel furnace room temperature 150 DEG C, be incubated 10 minutes；It is then heated to 600 DEG C, 20 DEG C per minute of programming rate, it is incubated 10 minutes after arriving 600 DEG C；Opening fire door, temperature is down to less than 500 DEG C, i.e. takes out cooling.
Testing embodiment 1-2, test result shows: the electrical heating conversion efficiency of embodiment 1-2 is up to more than 9%.
The foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, for a person skilled in the art, the present invention can have various modifications and variations.All within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included within the scope of the present invention.
Claims (1)
1. a preparation method for Graphene electric heating body, the method comprises the steps:
(1) electrical heating slurry is prepared
Weigh the graphene powder of 6-7 weight portion, the far infrared transmission agent of 0.5-2 weight portion, the bonding diluent of 3-5 weight portion, stir after first graphene powder being mixed with far infrared transmission agent, after being subsequently adding bonding diluent mixing, form slurry；Described bonding diluent is resistant to elevated temperatures phenolic resin, and the particle diameter of graphene powder is: 30-60nm；
(2) silver electrode is made
Substrate is printed 250 mesh silk screens, room temperature levelling 10-15min, in 110-150 DEG C of temperature range, is dried 10-15min；It is sintered at conventional, electric-resistance stove: room temperature 150 DEG C, is incubated 10 minutes, is then heated to 450 DEG C-600 DEG C, about 5-10 DEG C per minute of programming rate, it is incubated 10 minutes；Open fire door, take out cooling；
(3) electric heating layer is made
Above-mentioned electrical heating slurry is being done in substrate 100 mesh or 150 mesh silk screen printings, room temperature levelling 10-15min, in 150-180 DEG C of temperature range, it is dried 10-15min；It is sintered at conventional, electric-resistance stove: room temperature 150 DEG C, is incubated 10 minutes, is then heated to 650 DEG C-750 DEG C, about 10-15 DEG C per minute of programming rate, it is incubated 15 minutes；Open fire door, take out cooling；
(4) encapsulated layer is made
Encapsulating material is carried out on electric heating layer 200 mesh silk screen printings, room temperature levelling 5-10min；After drying, sinter at continuous tunnel furnace: during continuous tunnel furnace room temperature 150 DEG C, be incubated 10 minutes；It is then heated to 600 DEG C, 15-20 DEG C per minute of programming rate, it is incubated 10 minutes after arriving 600 DEG C；Opening fire door, temperature is down to less than 500 DEG C, i.e. takes out cooling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610302390.7A CN105916221A (en) | 2016-05-09 | 2016-05-09 | Graphene electrical heating body preparation method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610302390.7A CN105916221A (en) | 2016-05-09 | 2016-05-09 | Graphene electrical heating body preparation method |
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| CN105916221A true CN105916221A (en) | 2016-08-31 |
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| CN201610302390.7A Pending CN105916221A (en) | 2016-05-09 | 2016-05-09 | Graphene electrical heating body preparation method |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106604423A (en) * | 2015-10-19 | 2017-04-26 | 中山市乾元高科电子有限公司 | Processing technology of heating body |
| CN107454699A (en) * | 2017-08-14 | 2017-12-08 | 戴承萍 | A kind of electromagnetic induction heating film production method and electromagnetic induction heating film |
| CN108248120A (en) * | 2017-12-29 | 2018-07-06 | 无锡格菲电子薄膜科技有限公司 | Graphene composite heating film |
| CN110470720A (en) * | 2019-09-20 | 2019-11-19 | 贵州申科生物科技有限公司 | A kind of device in temperature for capillary electrophoresis |
| CN110798915A (en) * | 2019-11-09 | 2020-02-14 | 王成斌 | A high temperature resistant graphene heating plate |
| CN110845148A (en) * | 2019-12-06 | 2020-02-28 | 山东国启新能源科技有限公司 | Heating body with quartz glass and graphene coating and preparation process |
| CN110996410A (en) * | 2019-11-09 | 2020-04-10 | 王成斌 | Manufacturing process of high-temperature-resistant graphene heating plate |
| CN111132395A (en) * | 2019-12-31 | 2020-05-08 | 陆建华 | Heating body with mica sheet and graphene coating and preparation process thereof |
| CN111417222A (en) * | 2020-05-07 | 2020-07-14 | 佛山市新豪瑞科技有限公司 | Laser sintering film forming production line and production method of graphene electric heating body |
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| CN101005719A (en) * | 2006-01-17 | 2007-07-25 | 宁波市塞纳电热电器有限公司 | Metal base printed circuit heater and its preparing technology |
| CN101277555A (en) * | 2007-03-29 | 2008-10-01 | 宁波市塞纳电热电器有限公司 | Printing electric heating membrane calandria based on vitrified enamel plate and preparation technique thereof |
| CN103338538A (en) * | 2013-07-19 | 2013-10-02 | 南京中脉科技控股有限公司 | Graphene radiation heating film and preparation method and application thereof |
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2016
- 2016-05-09 CN CN201610302390.7A patent/CN105916221A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101005719A (en) * | 2006-01-17 | 2007-07-25 | 宁波市塞纳电热电器有限公司 | Metal base printed circuit heater and its preparing technology |
| CN101277555A (en) * | 2007-03-29 | 2008-10-01 | 宁波市塞纳电热电器有限公司 | Printing electric heating membrane calandria based on vitrified enamel plate and preparation technique thereof |
| CN103338538A (en) * | 2013-07-19 | 2013-10-02 | 南京中脉科技控股有限公司 | Graphene radiation heating film and preparation method and application thereof |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106604423A (en) * | 2015-10-19 | 2017-04-26 | 中山市乾元高科电子有限公司 | Processing technology of heating body |
| CN107454699A (en) * | 2017-08-14 | 2017-12-08 | 戴承萍 | A kind of electromagnetic induction heating film production method and electromagnetic induction heating film |
| CN108248120A (en) * | 2017-12-29 | 2018-07-06 | 无锡格菲电子薄膜科技有限公司 | Graphene composite heating film |
| CN110470720A (en) * | 2019-09-20 | 2019-11-19 | 贵州申科生物科技有限公司 | A kind of device in temperature for capillary electrophoresis |
| CN110470720B (en) * | 2019-09-20 | 2022-05-13 | 贵州申科生物科技有限公司 | Temperature standing device for capillary electrophoresis apparatus |
| CN110798915A (en) * | 2019-11-09 | 2020-02-14 | 王成斌 | A high temperature resistant graphene heating plate |
| CN110996410A (en) * | 2019-11-09 | 2020-04-10 | 王成斌 | Manufacturing process of high-temperature-resistant graphene heating plate |
| CN110798915B (en) * | 2019-11-09 | 2025-02-07 | 王成斌 | A high temperature resistant graphene heating plate |
| CN110845148A (en) * | 2019-12-06 | 2020-02-28 | 山东国启新能源科技有限公司 | Heating body with quartz glass and graphene coating and preparation process |
| CN111132395A (en) * | 2019-12-31 | 2020-05-08 | 陆建华 | Heating body with mica sheet and graphene coating and preparation process thereof |
| CN111417222A (en) * | 2020-05-07 | 2020-07-14 | 佛山市新豪瑞科技有限公司 | Laser sintering film forming production line and production method of graphene electric heating body |
| CN111417222B (en) * | 2020-05-07 | 2024-04-09 | 佛山市新豪瑞科技有限公司 | Laser sintering film forming assembly line of graphene electric heating body and production method |
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Application publication date: 20160831 |