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CN1057997C - 对硝基芳香酰胺的制备方法及其产物 - Google Patents

对硝基芳香酰胺的制备方法及其产物 Download PDF

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Publication number
CN1057997C
CN1057997C CN93117658A CN93117658A CN1057997C CN 1057997 C CN1057997 C CN 1057997C CN 93117658 A CN93117658 A CN 93117658A CN 93117658 A CN93117658 A CN 93117658A CN 1057997 C CN1057997 C CN 1057997C
Authority
CN
China
Prior art keywords
acid amides
alkali
mirbane
oil
amides
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN93117658A
Other languages
English (en)
Chinese (zh)
Other versions
CN1098402A (zh
Inventor
M·K·施特恩
郑启明
J·K·巴什金
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Solutia Inc
Original Assignee
Solutia Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to US08/045,309 priority Critical patent/US5331099A/en
Priority to JP50053194A priority patent/JP3339859B2/ja
Priority to AT93910797T priority patent/ATE158274T1/de
Priority to EP93910797A priority patent/EP0662074B1/de
Priority to DE69314045T priority patent/DE69314045T2/de
Priority to PCT/US1993/003892 priority patent/WO1993024447A1/en
Application filed by Solutia Inc filed Critical Solutia Inc
Priority to CN93117658A priority patent/CN1057997C/zh
Publication of CN1098402A publication Critical patent/CN1098402A/zh
Application granted granted Critical
Publication of CN1057997C publication Critical patent/CN1057997C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/08—Preparation of carboxylic acid amides from amides by reaction at nitrogen atoms of carboxamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/62—Preparation of compounds containing amino groups bound to a carbon skeleton by cleaving carbon-to-nitrogen, sulfur-to-nitrogen, or phosphorus-to-nitrogen bonds, e.g. hydrolysis of amides, N-dealkylation of amines or quaternary ammonium compounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN93117658A 1992-05-22 1993-08-06 对硝基芳香酰胺的制备方法及其产物 Expired - Fee Related CN1057997C (zh)

Priority Applications (7)

Application Number Priority Date Filing Date Title
US08/045,309 US5331099A (en) 1992-05-22 1993-04-16 Process for preparing p-nitroaromatic amides and products thereof
AT93910797T ATE158274T1 (de) 1992-05-22 1993-04-26 Prozess zur herstellung von p-nitroaromatischen aminen und aus diesen hergestellte produkte
EP93910797A EP0662074B1 (de) 1992-05-22 1993-04-26 Prozess zur herstellung von p-nitroaromatischen aminen und aus diesen hergestellte produkte
DE69314045T DE69314045T2 (de) 1992-05-22 1993-04-26 Prozess zur herstellung von p-nitroaromatischen aminen und aus diesen hergestellte produkte
JP50053194A JP3339859B2 (ja) 1992-05-22 1993-04-26 ｐ−ニトロ芳香族アミドの製造方法およびその生成物
PCT/US1993/003892 WO1993024447A1 (en) 1992-05-22 1993-04-26 Process for preparing p-nitroaromatic amides and products thereof
CN93117658A CN1057997C (zh) 1992-05-22 1993-08-06 对硝基芳香酰胺的制备方法及其产物

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US88899992A 1992-05-22 1992-05-22
CN93117658A CN1057997C (zh) 1992-05-22 1993-08-06 对硝基芳香酰胺的制备方法及其产物

Publications (2)

Publication Number Publication Date
CN1098402A CN1098402A (zh) 1995-02-08
CN1057997C true CN1057997C (zh) 2000-11-01

Family

ID=36843296

Family Applications (1)

Application Number Title Priority Date Filing Date
CN93117658A Expired - Fee Related CN1057997C (zh) 1992-05-22 1993-08-06 对硝基芳香酰胺的制备方法及其产物

Country Status (7)

Country Link
US (1) US5331099A (de)
EP (1) EP0662074B1 (de)
JP (1) JP3339859B2 (de)
CN (1) CN1057997C (de)
AT (1) ATE158274T1 (de)
DE (1) DE69314045T2 (de)
WO (1) WO1993024447A1 (de)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5552531A (en) * 1992-05-22 1996-09-03 Monsanto Company Process for preparing substituted aromatic azo compounds
US5352705A (en) * 1992-06-26 1994-10-04 Merck & Co., Inc. Inhibitors of farnesyl protein transferase
US5380946A (en) * 1993-07-30 1995-01-10 Monsanto Company Process for preparing p-nitroaromatic amides and products thereof
DE4427249A1 (de) 1994-08-02 1996-02-08 Bayer Ag Verfahren zur Herstellung nitrosubstituierter Arylamine
DE4427248A1 (de) * 1994-08-02 1996-02-08 Bayer Ag Verfahren zur Herstellung nitrosubstituierter Arylamide und Arylamine
DE4432556A1 (de) * 1994-09-13 1996-03-14 Bayer Ag Verfahren zur Herstellung nitrosubstituierter Arylamine
US6140538A (en) 1998-05-18 2000-10-31 Flexsys America L.P. Process for preparing 4-aminodiphenylamines
KR100294125B1 (ko) * 1999-11-16 2001-06-15 박찬구 요소와 니트로벤젠으로부터 4-니트로소아닐린을 제조하는방법
KR100362772B1 (ko) * 2000-07-07 2002-12-11 금호석유화학 주식회사 파라페닐렌디아민의 제조방법
CN1276530C (zh) * 2001-07-31 2006-09-20 株式会社德山 新型鎓盐、包含新型鎓盐的非水电池电解液及利用包含鎓盐的电解液优化负极的方法
KR20030035343A (ko) 2001-10-31 2003-05-09 금호석유화학 주식회사 4-니트로소 치환 방향족아민 화합물의 제조방법
US20040039181A1 (en) * 2002-07-29 2004-02-26 Rains Roger Keranen Process for preparing aromatic azo and hydrazo compounds, aromatic amides and aromatic amines
BRPI0412101A (pt) * 2003-07-04 2006-08-15 Nongyue Wang processo para a preparação da 4-aminodifenilamina
US8686188B2 (en) 2003-07-04 2014-04-01 Jiangsu Sinorgchem Technology Co., Ltd. Process for preparing 4-aminodiphenylamine
US8486223B2 (en) * 2003-07-04 2013-07-16 Jiangsu Sinorgchem Technology Co., Ltd. Falling film evaporator
CN102259029B (zh) 2010-05-24 2014-12-10 江苏圣奥化学科技有限公司 固体碱催化剂
KR101358605B1 (ko) 2010-12-21 2014-02-04 금호석유화학 주식회사 4-니트로아닐린을　이용한 4,4'-디니트로디페닐아민 및 4,4'-비스(알킬아미노)디페닐아민의 제조방법
KR101358519B1 (ko) 2010-12-21 2014-02-05 금호석유화학 주식회사 복합염기촉매를　이용한 4,4'-디니트로디페닐아민 및 4,4'-비스(알킬아미노)디페닐아민의 제조방법
CN102796011A (zh) * 2012-08-25 2012-11-28 山西翔宇化工有限公司 一种对氨基二苯胺的制备方法
CN110773144A (zh) * 2019-10-28 2020-02-11 湖南科技学院 一种用于氰基水解制备酰胺的催化体系及其应用

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5117063A (en) * 1991-06-21 1992-05-26 Monsanto Company Method of preparing 4-aminodiphenylamine

Family Cites Families (23)

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Publication number Priority date Publication date Assignee Title
FR1456497A (fr) * 1964-05-25 1966-10-28 Monsanto Co Condensation catalytique de composés carbonyliques avec des amines
US3481983A (en) * 1965-12-09 1969-12-02 Monsanto Co N,n'-di(1,3,3-trimethylbutyl)-p-phenylenediamine
BE789273A (fr) * 1971-09-28 1973-03-26 Bayer Ag Procede de preparation de derives de nitrodiphenylamine
GB1440767A (en) * 1972-11-24 1976-06-23 Ici Ltd Oxidation process for the manufacture of 4-aminodiphenylamine and related higher amines
DE2633811C2 (de) * 1976-07-28 1983-11-10 Bayer Ag, 5090 Leverkusen Verfahren zur Herstellung von Nitrodiphenylaminen
DE2713602C3 (de) * 1977-03-28 1980-03-20 Akzo Gmbh, 5600 Wuppertal Verfahren zur Herstellung von Nitrosobenzol
US4187248A (en) * 1977-11-23 1980-02-05 Monsanto Company Making a nitrodiarylamine by reacting an alkali metal salt of a formamide with a nitrohaloarene
US4209463A (en) * 1977-12-27 1980-06-24 Monsanto Company Promoting the formation of nitrodiarylamines from nitrohaloarenes, activated aryl amines and sodium carbonates
US4187249A (en) * 1977-12-27 1980-02-05 Monsanto Company Promoting the reaction of sodium salts of formyl derivatives of aromatic amines to form nitrodiarylamines
US4140716A (en) * 1978-01-05 1979-02-20 Monsanto Company Process for making an amide of formic acid and forming nitrodiarylamine therefrom
US4155936A (en) * 1978-03-08 1979-05-22 The Goodyear Tire & Rubber Company Para-nitrodiphenylamines synthesis using Polyethers and macrocyclic esters as solubilizing agents
US4196146A (en) * 1978-03-13 1980-04-01 Monsanto Company Making nitrodiarylamines from formyl derivatives of aromatic amines and nitrohaloarenes by admixing with certain aqueous salt solutions
US4404401A (en) * 1979-02-23 1983-09-13 Akzona Incorporated Process for the preparation of para-amino-diphenylamine
US4900868A (en) * 1982-01-18 1990-02-13 Monsanto Company Process for producing N,N'-disubstituted paraphenylene diamine mixtures by sequential reductive alkylation
US4479008A (en) * 1982-09-30 1984-10-23 Uniroyal, Inc. Preparation of p-nitrosodiphenylamine
US4518803A (en) * 1982-09-30 1985-05-21 Uniroyal, Inc. Process for the preparation of p-nitrosodiphenylamine
US4463191A (en) * 1983-09-26 1984-07-31 The Goodyear Tire & Rubber Company Process for the reductive alkylation of aromatic nitro-containing compounds with ketones or aldehydes
US4614817A (en) * 1983-12-19 1986-09-30 Monsanto Company Making nitrodiarylamines
DE3504479A1 (de) * 1985-02-09 1986-08-14 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von 4-nitrodiphenylaminen
US4683332A (en) * 1985-05-20 1987-07-28 The Goodyear Tire & Rubber Company Para-nitrodiphenylamine synthesis
US4760186A (en) * 1986-09-15 1988-07-26 Monsanto Company Preparation of substituted aromatic amines
GB8712879D0 (en) * 1987-06-02 1987-07-08 Shell Int Research Coproduction of anilines & oxamides
PL163080B1 (pl) * 1990-04-23 1994-02-28 Inst Chemii Organicznej Pan Sposób wytwarzania amin aromatycznych PL

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5117063A (en) * 1991-06-21 1992-05-26 Monsanto Company Method of preparing 4-aminodiphenylamine

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
CHEMICAL ABSTRACTS V01.109,NO.23,2107299 1988.12.5 I.V.A.HAVEIK"METHOD OF PREPARATION OF 4-AMINO-4-NITROBENZANILIDE" *

Also Published As

Publication number Publication date
US5331099A (en) 1994-07-19
DE69314045D1 (de) 1997-10-23
DE69314045T2 (de) 1998-04-16
CN1098402A (zh) 1995-02-08
WO1993024447A1 (en) 1993-12-09
JPH07507301A (ja) 1995-08-10
EP0662074B1 (de) 1997-09-17
JP3339859B2 (ja) 2002-10-28
EP0662074A1 (de) 1995-07-12
ATE158274T1 (de) 1997-10-15

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Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C53 Correction of patent of invention or patent application
CB02 Change of applicant information

Applicant after: Sorotia Co.

Applicant before: Monsanto, Co.

COR Change of bibliographic data

Free format text: CORRECT: APPLICANT; FROM: MONSANTO CO. TO: SOLUTIA CORP.

C14 Grant of patent or utility model
GR01 Patent grant
C19 Lapse of patent right due to non-payment of the annual fee
CF01 Termination of patent right due to non-payment of annual fee