CN105566006A - Compound fertilizer with castor oil residues and method for preparing compound fertilizer - Google Patents
Compound fertilizer with castor oil residues and method for preparing compound fertilizer Download PDFInfo
- Publication number
- CN105566006A CN105566006A CN201510960656.2A CN201510960656A CN105566006A CN 105566006 A CN105566006 A CN 105566006A CN 201510960656 A CN201510960656 A CN 201510960656A CN 105566006 A CN105566006 A CN 105566006A
- Authority
- CN
- China
- Prior art keywords
- fertilizer
- compound fertilizer
- phosphate
- fertilizers
- castor oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000003337 fertilizer Substances 0.000 title claims abstract description 53
- 238000000034 method Methods 0.000 title abstract description 10
- 150000001875 compounds Chemical class 0.000 title abstract description 8
- 239000004359 castor oil Substances 0.000 title abstract 5
- 235000019438 castor oil Nutrition 0.000 title abstract 5
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 title abstract 5
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims abstract description 10
- 229940072033 potash Drugs 0.000 claims abstract description 10
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims abstract description 10
- 235000015320 potassium carbonate Nutrition 0.000 claims abstract description 10
- 239000011573 trace mineral Substances 0.000 claims abstract description 9
- 235000013619 trace mineral Nutrition 0.000 claims abstract description 9
- 239000005696 Diammonium phosphate Substances 0.000 claims abstract description 5
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 5
- YYRMJZQKEFZXMX-UHFFFAOYSA-L calcium bis(dihydrogenphosphate) Chemical compound [Ca+2].OP(O)([O-])=O.OP(O)([O-])=O YYRMJZQKEFZXMX-UHFFFAOYSA-L 0.000 claims abstract description 5
- 229910000389 calcium phosphate Inorganic materials 0.000 claims abstract description 5
- 239000004202 carbamide Substances 0.000 claims abstract description 5
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229910000388 diammonium phosphate Inorganic materials 0.000 claims abstract description 5
- 235000019838 diammonium phosphate Nutrition 0.000 claims abstract description 5
- 235000019691 monocalcium phosphate Nutrition 0.000 claims abstract description 5
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims abstract description 5
- 229910052939 potassium sulfate Inorganic materials 0.000 claims abstract description 5
- DPLVEEXVKBWGHE-UHFFFAOYSA-N potassium sulfide Chemical compound [S-2].[K+].[K+] DPLVEEXVKBWGHE-UHFFFAOYSA-N 0.000 claims abstract description 5
- 235000011151 potassium sulphates Nutrition 0.000 claims abstract description 5
- 235000004443 Ricinus communis Nutrition 0.000 claims description 25
- 239000002131 composite material Substances 0.000 claims description 15
- 239000000618 nitrogen fertilizer Substances 0.000 claims description 8
- 239000002686 phosphate fertilizer Substances 0.000 claims description 8
- 238000002360 preparation method Methods 0.000 claims description 7
- 238000005469 granulation Methods 0.000 claims description 6
- 230000003179 granulation Effects 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- 238000012216 screening Methods 0.000 claims description 5
- MPNNOLHYOHFJKL-UHFFFAOYSA-N peroxyphosphoric acid Chemical group OOP(O)(O)=O MPNNOLHYOHFJKL-UHFFFAOYSA-N 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 3
- 238000007689 inspection Methods 0.000 claims description 3
- 238000004806 packaging method and process Methods 0.000 claims description 3
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 2
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 2
- 229910052796 boron Inorganic materials 0.000 claims description 2
- 229910052802 copper Inorganic materials 0.000 claims description 2
- 239000010949 copper Substances 0.000 claims description 2
- 239000011777 magnesium Substances 0.000 claims description 2
- 229910052749 magnesium Inorganic materials 0.000 claims description 2
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims description 2
- 229910052750 molybdenum Inorganic materials 0.000 claims description 2
- 239000011733 molybdenum Substances 0.000 claims description 2
- 239000002994 raw material Substances 0.000 claims description 2
- 239000011701 zinc Substances 0.000 claims description 2
- 229910052725 zinc Inorganic materials 0.000 claims description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 10
- 235000015097 nutrients Nutrition 0.000 abstract description 6
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract description 5
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 abstract description 5
- 229910052757 nitrogen Inorganic materials 0.000 abstract description 5
- 239000011574 phosphorus Substances 0.000 abstract description 5
- 229910052698 phosphorus Inorganic materials 0.000 abstract description 5
- 239000011591 potassium Substances 0.000 abstract description 5
- 229910052700 potassium Inorganic materials 0.000 abstract description 5
- 230000012010 growth Effects 0.000 abstract description 4
- 229910019142 PO4 Inorganic materials 0.000 abstract 2
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 abstract 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract 2
- 239000010452 phosphate Substances 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 description 9
- 239000002689 soil Substances 0.000 description 9
- 241000196324 Embryophyta Species 0.000 description 5
- 238000011161 development Methods 0.000 description 4
- 230000018109 developmental process Effects 0.000 description 4
- 239000003895 organic fertilizer Substances 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- 229910052793 cadmium Inorganic materials 0.000 description 3
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 3
- 230000002708 enhancing effect Effects 0.000 description 3
- 230000035558 fertility Effects 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 230000008635 plant growth Effects 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 210000003608 fece Anatomy 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000010871 livestock manure Substances 0.000 description 2
- 235000021049 nutrient content Nutrition 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 230000002787 reinforcement Effects 0.000 description 2
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 240000007049 Juglans regia Species 0.000 description 1
- 235000009496 Juglans regia Nutrition 0.000 description 1
- 241000220225 Malus Species 0.000 description 1
- 235000011430 Malus pumila Nutrition 0.000 description 1
- 235000015103 Malus silvestris Nutrition 0.000 description 1
- 244000061456 Solanum tuberosum Species 0.000 description 1
- 235000002595 Solanum tuberosum Nutrition 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- -1 mountain region Substances 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 230000007226 seed germination Effects 0.000 description 1
- 235000020234 walnut Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/02—Superphosphates
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Soil Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a compound fertilizer with castor oil residues and a method for preparing the compound fertilizer. The compound fertilizer comprises, by weight, 58%-84% of the castor oil residues, 3%-14% of nitrogenous fertilizers, 10%-24% of phosphate fertilizers, 0%-8% of potash fertilizers and 0.3%-3% of micro-element fertilizers. The nitrogenous fertilizers are made of urea, the phosphate fertilizers are made of calcium superphosphate or diammonium phosphate, and the potash fertilizers are made of potassium sulfide or potassium sulfate. The compound fertilizer with the castor oil residues and the method have the advantages that large quantities of nutrient elements such as nitrogen, phosphorus and potassium which are required by plants can be provided for different crops, and accordingly vigorous growth of the plants can be promoted; the castor oil residues contain large quantities of organic matters and trace elements, and accordingly requirements of the different crops on different trace elements can be met.
Description
[technical field]
The present invention relates to composite fertilizer's technical field, particularly a kind of castor pomace composite fertilizer and preparation method thereof.
[background technology]
Castor pomace can produce high temperature during the fermentation, belongs to the hot source of manure, as improper use in tradition application, can cause and burns root or affect seed germination, reduce the utility value of castor pomace.In order to solve this shortcoming, the existing processing through science and good formula comprehensive utilization castor pomace, overcome this shortcoming.
[summary of the invention]
For solving the Problems existing of prior art, a kind of castor pomace composite fertilizer of the present invention and preparation method thereof, this castor pomace composite fertilizer can meet the demand of crop to Different Nutrients, enhancing development, increase yield, oil recovery enhancement.This fertilizer has certain repair to cadmium pollution soil in addition.
For achieving the above object, the present invention is by the following technical solutions:
A kind of castor pomace composite fertilizer, is prepared from by the raw material of following mass percent:
Castor pomace 58% ~ 84%, nitrogenous fertilizer 3% ~ 14%, phosphate fertilizer 10% ~ 24%, potash fertilizer 0 ~ 8%, micro-fertile 0.3% ~ 3%; Wherein, described nitrogenous fertilizer is urea, and phosphate fertilizer is peroxophosphoric acid acid calcium or diammonium phosphate, and potash fertilizer is potassium sulphide or potassium sulfate.
Described micro-fertilizer is at least one in trace element zinc, magnesium, boron, manganese, copper and molybdenum
A preparation method for castor pomace composite fertilizer, comprises the following steps:
1) first castor pomace is carried out drying, broken after dry;
2) add nitrogenous fertilizer, phosphate fertilizer, potash fertilizer and trace element to mix;
3) mixing granulation, enters intermediate bin through screening;
4) pack after inspection meets recipe requirements, after packaging, check warehouse-in;
5) delivery is dispatched from the factory.
The present invention, relative to prior art, has following beneficial effect:
Castor pomace composite fertilizer prepared by the present invention, can provide the plant desired nutritional elements such as a large amount of nitrogen, phosphorus, potassium for different crops, promote the growth of plant advantage; Castor pomace itself containing a large amount of organic and micro-, then according to the demand of Different Crop to different trace element, be equipped with corresponding micro-fertilizer, can improve soil, culture fertility; Can regulate and make nutrient balance in object, growth promoting effects, strengthen resistance; The demand of crop to Different Nutrients can be met, enhancing development, increase yield, oil recovery enhancement.This castor pomace fertilizer has certain repair to cadmium pollution soil in addition.
In addition, the present invention can improve the industrialization production efficiency of fertilizer and ensure the commercial quality of fertilizer, the fundamental research of further reinforcement fertilizer and applied research, with the actual needs of satisfied production, solve the technical problem faced in industrialization process, and adopt vigorous measures in following several respects: (1) adopts advanced granulation fertilize preparation craft, the product that production physical behavior is good, to overcome appearance poor, shortcoming that level is low, improve commodity quality; (2) develop compound organic and inorganic fertilizer, improve nutrient content, strengthen quick-acting, play the feature that rapid long-acting combines; (3) strict implement organic fertilizer products quality standard, Branding is realized, and forms scale effect.
[accompanying drawing explanation]
Fig. 1 castor pomace composite organic-inorganic fertilizer production technological process.
[embodiment]
Below in conjunction with the drawings and specific embodiments, the present invention will be further described, the invention is not restricted to following examples.
A formula for castor pomace and inorganic nutritive element, the manufacturing process of castor pomace composite fertilizer.The present invention is the growth characteristic desired nutritional characteristic according to different plants such as the soil such as mountain region, sand ground actual state, characteristics of soil fertility and corn, soybean, potato, apple, walnut, red date and flowers, the different castor pomace consumption of common development and the formula of different mineral manure, produce the composite organic-inorganic fertilizer proposing to be adapted to different plant.And study its corresponding production technique.
The inventive method entire protocol:
1) first castor pomace is carried out drying, broken after dry;
2) fertilizer such as nitrogen, phosphorus, potassium and trace element are added by formula (different plant different ingredients) mixing, (nitrogenous fertilizer is urea, phosphate fertilizer is peroxophosphoric acid acid calcium or diammonium phosphate, and potash fertilizer selects potassium sulphide or potassium sulfate);
3) mixing granulation, enters intermediate bin through screening;
4) again dry, broken to the particle entering intermediate bin after screening, add the fertilizer such as nitrogen, phosphorus, potassium, (nitrogenous fertilizer is urea, phosphate fertilizer is peroxophosphoric acid acid calcium or diammonium phosphate, and potash fertilizer selects potassium sulphide or potassium sulfate);
5) mixing granulation enters intermediate bin through screening;
6) pack after inspection meets recipe requirements, after packaging, check warehouse-in;
7) delivery is dispatched from the factory.
Using method: adopt soil application method, concrete fertilising consumption is specifically used according to different crops and is formulated separately.Proportioning different ingredients is carried out according to Different Crop, different soils administration.Optimum embodiment specifically for the composite fertilizer of different crop dispositions 100 jin is as follows:
The present invention can improve the industrialization production efficiency of fertilizer and ensure the commercial quality of fertilizer, the fundamental research of further reinforcement fertilizer and applied research, with the actual needs of satisfied production, solve the technical problem faced in industrialization process, and adopt vigorous measures in following several respects: (1) adopts advanced granulation fertilize preparation craft, the product that production physical behavior is good, to overcome appearance poor, shortcoming that level is low, improves commodity quality; (2) develop compound organic and inorganic fertilizer, improve nutrient content, strengthen quick-acting, play the feature that rapid long-acting combines; (3) strict implement organic fertilizer products quality standard, Branding is realized, and forms scale effect.
Shown by agricultural experiment, this product has clear superiority to plant growth: provide the plant desired nutritional elements such as a large amount of nitrogen, phosphorus, potassium for crop, promotes the growth of plant advantage; Castor pomace itself containing a large amount of organic and micro-, then according to the demand of Different Crop to different trace element, be equipped with corresponding micro-fertilizer, can improve soil, culture fertility; Can regulate and make nutrient balance in object, growth promoting effects, strengthen resistance; The demand of crop to Different Nutrients can be met, enhancing development, increase yield, oil recovery enhancement.This fertilizer has certain repair to cadmium pollution soil in addition.
Claims (3)
1. a castor pomace composite fertilizer, is characterized in that, is prepared from by the raw material of following mass percent:
Castor pomace 58% ~ 84%, nitrogenous fertilizer 3% ~ 14%, phosphate fertilizer 10% ~ 24%, potash fertilizer 0 ~ 8%; Micro-fertile 0.3% ~ 3%; Wherein, described nitrogenous fertilizer is urea, and phosphate fertilizer is peroxophosphoric acid acid calcium or diammonium phosphate, and potash fertilizer is potassium sulphide or potassium sulfate.
2. a kind of castor pomace composite fertilizer according to claim 2, is characterized in that, described micro-fertilizer is at least one in trace element zinc, magnesium, boron, manganese, copper and molybdenum.
3. the preparation method of a kind of castor pomace composite fertilizer according to claim 1, is characterized in that, comprise the following steps:
1) first castor pomace is carried out drying, broken after dry;
2) add nitrogenous fertilizer, phosphate fertilizer, potash fertilizer and trace element to mix;
3) mixing granulation, enters intermediate bin through screening;
4) pack after inspection meets recipe requirements, after packaging, check warehouse-in;
5) delivery is dispatched from the factory.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510960656.2A CN105566006A (en) | 2015-12-19 | 2015-12-19 | Compound fertilizer with castor oil residues and method for preparing compound fertilizer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510960656.2A CN105566006A (en) | 2015-12-19 | 2015-12-19 | Compound fertilizer with castor oil residues and method for preparing compound fertilizer |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105566006A true CN105566006A (en) | 2016-05-11 |
Family
ID=55876722
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510960656.2A Pending CN105566006A (en) | 2015-12-19 | 2015-12-19 | Compound fertilizer with castor oil residues and method for preparing compound fertilizer |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105566006A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110818469A (en) * | 2019-11-22 | 2020-02-21 | 陕西佳上肥料科技有限公司 | Special vegetable fertilizer produced by using castor oil meal and preparation process thereof |
| CN111517886A (en) * | 2020-04-25 | 2020-08-11 | 陕西汉唐环保农业有限公司 | Special fruit tree fertilizer produced by using castor oil meal and preparation process thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1093075A (en) * | 1993-03-29 | 1994-10-05 | 田永豪 | A kind of polyelement composite fertilizer and method for making thereof |
| CN1287108A (en) * | 2000-09-22 | 2001-03-14 | 海南神龙氨基酸肥料有限公司 | Preparation and product of water-retaining amino acid fertilizer |
-
2015
- 2015-12-19 CN CN201510960656.2A patent/CN105566006A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1093075A (en) * | 1993-03-29 | 1994-10-05 | 田永豪 | A kind of polyelement composite fertilizer and method for making thereof |
| CN1287108A (en) * | 2000-09-22 | 2001-03-14 | 海南神龙氨基酸肥料有限公司 | Preparation and product of water-retaining amino acid fertilizer |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110818469A (en) * | 2019-11-22 | 2020-02-21 | 陕西佳上肥料科技有限公司 | Special vegetable fertilizer produced by using castor oil meal and preparation process thereof |
| CN111517886A (en) * | 2020-04-25 | 2020-08-11 | 陕西汉唐环保农业有限公司 | Special fruit tree fertilizer produced by using castor oil meal and preparation process thereof |
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| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160511 |