CN105267124A - Whitening and hydrating cleansing milk and method for manufacturing same - Google Patents
Whitening and hydrating cleansing milk and method for manufacturing same Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q19/00—Preparations for care of the skin
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- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to whitening and hydrating cleansing milk and a method for manufacturing the same. The whitening and hydrating cleansing milk comprises, by weight, 5-25 parts of surfactants, 15-35 parts of humectants, 5-25 parts of traditional Chinese medicine extract, 0.5-1.5 parts of thickeners, 30-40 parts of water, 0.05-0.25 part of vitamin E and 1-3 parts of propolis. The traditional Chinese medicine extract comprises eucommia ulmoides extract, aloe extract and mixed extract, the mixed extract comprises pearl barley and radix asparagi according to a weight ratio of 2-5:2-5. The whitening and hydrating cleansing milk and the method have the advantages that the whitening and hydrating cleansing milk is mild, skin friendly and safe and is free of irritation, the skins of users can be deeply cleansed, and obvious water supplementing and whitening effects can be realized.
Description
Technical field
The present invention relates to cosmetic technical field, be specifically related to a kind of whitening skin and preserving moisture face breast and preparation method thereof.
Background technology
Skin is divided into epidermal area, skin corium and subcutaneous tissue three layers.Epidermal area is divided into again horny layer, clear layer, granular layer, prickle cell layer and basal layer, and the horny layer of epidermal area is the first barrier of human body skin protection, and basal layer is melanic main source.Along with the metabolism of skin, basal layer cell constantly divides and promotes its metabolite to horny layer, forms aging cutin layer, as cleaned not in time, aging, obscure, the pore of skin can be caused to increase or block, metabolism weakens.
Facial milk cleanser is the skin care item of a kind of clean face dirt, protection skin, is one of indispensable article of everyday use in our daily life.It is the milky product be made up of oil phase thing, aqueous-phase material, surfactant, nutrient etc.Mainly play the effect of the residuals of cleaning skin oils and fats, dirt, aging cutin layer, skin care item cosmetics etc.
Chinese patent application 201210370932.6 discloses a kind of whitening skin and preserving moisture face cleaning milk, and it is made up of following raw material: white mineral oil, methyl hydroxybenzoate, Polyethylene Glycol, sad glycerinate, Cera Flava, bamboo charcoal powder, Viaminate, potassium alkyl phosphate, lactic acid, compound vitamin, acetylated lanolin, spice and deionized water.This invention has certain whitening, moistening effect, but in this invention, chemical composition is more, and life-time service can bring very large harm.In sum, in order to overcome the deficiencies in the prior art, provide more products to enrich the selection in market simultaneously, meet the demand of people to high-quality cosmetics, be necessary that research and development one has whitening skin and preserving moisture effect, simultaneously can effective clean skin, gentle non-stimulated whitening skin and preserving moisture facial milk cleanser.
Summary of the invention
In order to overcome the deficiencies in the prior art, the object of the present invention is to provide a kind of whitening skin and preserving moisture facial milk cleanser, which are added Chinese medicine ingredients, gentle pro-skin, safe and non-stimulating, the multiple dirt of energy deep layer cleaning, excess oil and aging cutin, moisturizing while purification whitening, effectively auxiliary desalination pigment, improves skin gloss and brightness.
To achieve these goals, technical scheme of the present invention is as follows:
A kind of whitening skin and preserving moisture facial milk cleanser, comprise the raw materials of following parts by weight: 5 ~ 25 parts, surfactant, wetting agent 15 ~ 35 parts, Chinese medicine extract 5 ~ 25 parts, thickening agent 0.5 ~ 1.5 part, 30 ~ 40 parts, water, vitamin E 0.05 ~ 0.25 part and propolis 1 ~ 3 part, described Chinese medicine extract comprises Cortex Eucommiae extract, Aloe extract and mixed extract, and the raw materials of described mixed extract is made up of according to the weight ratio of 2 ~ 5:2 ~ 5 Semen Coicis and Radix Asparagi.
Preferably, described Chinese medicine extract is made up of according to the weight ratio of 2 ~ 5:2 ~ 5:4 ~ 10 Cortex Eucommiae extract, Aloe extract, mixture extract.
Preferably, described surfactant is made up of dodecyl alanine, sodium cocoyl glycinate and the sodium lauroyl glutamate weight ratio by 1:2:1, described wetting agent comprises hyaluronic acid, glycerol, squalane and butanediol, and described thickening agent is selected from propylene glycol alginate.
Preferably, described whitening skin and preserving moisture facial milk cleanser also comprises antiseptic 0.1 ~ 1 part, and described antiseptic is made up of by the weight ratio of 1:1 methyl hydroxybenzoate and propyl hydroxybenzoate.
Preferably, described whitening skin and preserving moisture facial milk cleanser comprises the raw materials of following parts by weight: 10 parts, surfactant, wetting agent 20 parts, Cortex Eucommiae extract 3 parts, Aloe extract 3 parts, mixed extract 6 parts, thickening agent 1 part, vitamin E 0.1 part, propolis 2 parts and 35 parts, water.
Preferably, described Aloe extract is obtained by following steps:
S1: get Aloe, cleans, and after drying, is squeezed obtain Aloe mixing juice with squeezer;
S2: the Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice;
S3: put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 1 ~ 3 time of circulation, obtains Aloe extract.
Preferably, described Cortex Eucommiae extract is obtained by following steps:
S1: get the Cortex Eucommiae, pulverizes mixing after cleaning, drying, and add the water soaking 30 ~ 60 minutes of medical material gross weight 5 ~ 8 times amount, reflux, extract, 1 ~ 2 time, each 3 ~ 6h, filters and retain filtering residue, merging filtrate, obtaining Aqueous extracts;
S2: adding medical material gross weight 5 ~ 8 times amount volume fraction in filtering residue is the ethanol of 65 ~ 90%, reflux, extract, 1 ~ 2 time, each 3 ~ 6h, filter, merging filtrate, obtains alcohol extract;
S3: merge Aqueous extracts and alcohol extract, after stirring, leaves standstill 12 ~ 24h, centrifugal 10 ~ 25 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 30 ~ 45 DEG C, and material liquid pH is 6 ~ 8, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.1 ~ 0.2MPa, when feed liquid stock solution reduces 1/10 ~ 1/4, then the ultrafiltration 2 ~ 3 times that adds water, merge ultrafiltrate, obtain Cortex Eucommiae extract.
Preferably, described mixed extract is obtained by following steps:
Get Semen Coicis and Radix Asparagi, coarse powder is ground into after mixing, be placed in supercritical carbon dioxide extraction apparatus, the volume fraction adding 10 ~ 25 parts by weight is the alcoholic solution of 70 ~ 85%, regulation and control carbon dioxide flow is 10 ~ 15L/h, and extracting pressure is 10 ~ 15MPa, and extraction temperature is 45 ~ 60 DEG C, extraction time is 3 ~ 5h, and decompression separation obtains described mixed extract.
Cortex Eucommiae extract of the present invention is rich in the unsaturated fatty acid such as linolenic acid, linoleic acid, wherein the content of alpha-linolenic acid is more up to 61%, alpha-linolenic acid belongs to Omega-3 class fatty acid, it is the base structure of composition cell membrane, the nutritive equilibrium of cell membrane can be safeguarded, resist the infringement of external environment to skin, make skin present efficient regeneration, moisturizing, the daily life function such as penetrating; The natural preventive of skin can also be protected and strengthen to Omega-3 fatty acid, increases cell membrane elasticity and activating cell, improve the quality of epidermal area, and reduce the deposition of pigment, skin care, improves coarse, the obscure skin without light quality; In addition, eucommia ulmoides seed oil is also containing the functional component such as aucubin, chlorogenic acid, and it has good non-oxidizability and the ability of scavenging activated oxygen.
Barbaloin energy regulation of skin contained by described Aloe extract, has the effect of obvious skin care and Palmitoleic Acid, can promote skin metabolism, be conducive to living again of outer skin tissue, have Promotive union effect to wound.
Described Semen Coicis contains rich in protein and vitamin, and skin can be made delicate fine and smooth, eliminating mottle with reducing wrinkle, eliminating pigment, having obvious curative effect to face acne and pachylosis.
Aspartic acid contained by described Radix Asparagi has non-oxidizability, can stop the oxidation of unsaturated fatty acid, delays and treat the keratinization of skin, keeps the soft and smooth and moistening of skin, makes skin water tender flexible.
Described propolis includes more than 50 kind of flavonoid composition, subcutaneous tissue blood circulation can be promoted, the generation strengthening skin elasticity, decompose pigment, suppress senile plaque, and the composition such as lecithin, mineral, terpenes in propolis can soften cuticle, make that skin is delicate, not coarse, high resilience, there is anti-aging effects.
Described vitamin E has antioxidation, protects the moisture in sebum and cell membrane protein and skin, suppresses the peroxidating of unsaturated fatty acid, thus effectively resists the deposition of melanin on skin, makes skin keep pale.
Described Cortex Eucommiae extract, Aloe extract, Semen Coicis extract, Radix Asparagi extract, propolis and vitamin E work in coordination with dodecyl alanine, sodium cocoyl glycinate and sodium lauroyl glutamate, can effective antioxidation, improve the quality of epidermal area, reduce the deposition of pigment, timely replenishing water and preserving moisture simultaneously, supply skin desired nutritional, effective delaying skin aging, skin is compacted, and water is tender adds glycerol again, hyaluronic acid, squalane, butanediol is as wetting agent, can effectively assist to pin moisture of skin, prevent from cleaning rear skin water loss, further collocation propylene glycol alginate, EDETATE SODIUM, ring five polydimethylsiloxane, essence, methyl hydroxybenzoate, the basic material such as propyl hydroxybenzoate and water obtains whitening skin and preserving moisture facial milk cleanser of the present invention, each component is worked in coordination with, make stable system safety, gentle non-stimulated, bubble abundant, easy flushing, noresidue, can life-time service.
Present invention also offers the preparation method of above-mentioned whitening skin and preserving moisture facial milk cleanser, specifically comprise the following steps:
S1: the preparation of oil phase: add thickening agent 0.5 ~ 1.5 part in oil phase pot, be heated with stirring to 70 ~ 75 DEG C, be stirred to material and dissolve completely, obtain material A, stand-by;
S2: the preparation of aqueous phase: add wetting agent 15 ~ 35 parts, 30 ~ 40 parts, water in aqueous phase pot, be heated with stirring to 90 ~ 100 DEG C, be stirred to material and dissolve completely, maintains sterilizing in 20 minutes, is then cooled to 70 ~ 80 DEG C, obtains material B, stand-by;
S3: emulsifying: above-mentioned material A and material B are added in emulsifying pot according to the order of water after first oil, carries out high-speed stirred under the condition of 75 ~ 85 DEG C, treat material A and material B mix homogeneously, obtain material C;
S4; Cooling: material C above-mentioned steps obtained is cooled to 50 ~ 60 DEG C, adds 5 ~ 25 parts, surfactant, stirs;
S5: when system being cooled to 45 DEG C, adds Chinese medicine extract, 0 ~ 1 part, essence, vitamin E 0 ~ 1 part and propolis 1 ~ 3 part, is stirred to evenly; Be cooled to 35 ~ 40 DEG C, discharging;
S6: homogenizing process: make material particular diameter between 100 ~ 200nm through the process of extra-high-pressure nano homogenizer homogenizing after discharging, through carrying out fill after the assay was approved, obtains whitening skin and preserving moisture facial milk cleanser of the present invention.
Preferably, described Chinese medicine extract is obtained by following steps:
S1: get the Cortex Eucommiae, pulverizes mixing after cleaning, drying, and add the water soaking 30 ~ 60 minutes of medical material gross weight 5 ~ 8 times amount, reflux, extract, 1 ~ 2 time, each 3 ~ 6h, filters and retain filtering residue, merging filtrate, obtaining Aqueous extracts; In filtering residue, add medical material gross weight 5 ~ 8 times amount volume fraction is the ethanol of 65 ~ 90%, reflux, extract, 1 ~ 2 time, each 3 ~ 6h, and filter, merging filtrate, obtains alcohol extract; Merge Aqueous extracts and alcohol extract, after stirring, leave standstill 12 ~ 24h, centrifugal 10 ~ 25 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 30 ~ 45 DEG C, and material liquid pH is 6 ~ 8, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.1 ~ 0.2MPa, when feed liquid stock solution reduces 1/10 ~ 1/4, then the ultrafiltration 2 ~ 3 times that adds water, merge ultrafiltrate, obtain Cortex Eucommiae extract;
S2: get Semen Coicis and Radix Asparagi, coarse powder is ground into after mixing, be placed in supercritical carbon dioxide extraction apparatus, the volume fraction adding 10 ~ 25 parts by weight is the alcoholic solution of 70 ~ 85%, regulation and control carbon dioxide flow is 10 ~ 15L/h, and extracting pressure is 10 ~ 15MPa, and extraction temperature is 45 ~ 60 DEG C, extraction time is 3 ~ 5h, and decompression separation obtains described mixed extract;
S3: get Aloe, cleans, and after drying, is squeezed obtain Aloe mixing juice with squeezer; The Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice; Put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 1 ~ 3 time of circulation, obtains Aloe extract;
S4: Cortex Eucommiae extract, mixed extract and Aloe extract are merged and obtains described Chinese medicine extract.
Containing dodecyl alanine, sodium cocoyl glycinate and sodium lauroyl glutamate three seed amino acid class surfactant in whitening skin and preserving moisture facial milk cleanser of the present invention, three's character is gentle, soft to skin, do not cause allergy, also there is excellent wettability, foaming characteristic, water solublity, anti-water hardness tolerance and antibiotic property, its faintly acid same with skin makes skin feel comfortable, soft and moist simultaneously, the all low stimulation of what is more important three, low toxicity, have good biodegradability properties; And three works in coordination with, reach the effect of gentle non-stimulated, safe and effective cleaning skin.
Therefore, compared with prior art, advantage of the present invention is:
(1) whitening skin and preserving moisture facial milk cleanser of the present invention contains dodecyl alanine, sodium cocoyl glycinate and sodium lauroyl glutamate cleansing, the excess oil of the safe and effective clean skin surface of energy and pore depths and dust dirt, natural faintly acid is close with skin PH, skin-friendly is good, cause any burden and injury to tender skin, keep skin moisture, the sebum film that face skin is natural can not be destroyed.
(2) whitening skin and preserving moisture facial milk cleanser of the present invention adds Cortex Eucommiae extract, Aloe extract, Semen Coicis extract, Radix Asparagi extract, propolis, vitamin E, timely whitening and moisturizing moisturizing while clean skin, and whitening composition is effectively sent to skin deep layer, repair impaired or innutritive cell, reduce the deposition of pigment, desalination mottle, make skin water moisten water tender, flexible.
(3) the gentle pro-skin of whitening skin and preserving moisture facial milk cleanser of the present invention, bubble abundant, easily rinse, heavy metal free, without foaming agent etc., containing aminoacid cleaning gene and multiple active skull cap components, non-stimulated to skin; Can deep layer cleaning, replenishing water and preserving moisture, whitening skin and preserving moisture, whitening skin and preserving moisture facial milk cleanser cost of material of the present invention is low simultaneously, and preparation method is simple, and process stabilizing, can be applicable.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following examples.Within the scope of the invention or not departing from content of the present invention, spirit and scope, whitening skin and preserving moisture facial milk cleanser of the present invention is suitably improved, replaces the identical component of effect, will become apparent to those skilled in the art that they are all deemed to be included within scope of the present invention.
embodiment 1, whitening skin and preserving moisture facial milk cleanser of the present invention and preparation thereof
formula:be prepared from by the raw material of following parts by weight: dodecyl alanine 2 parts, sodium cocoyl glycinate 3 parts, sodium lauroyl glutamate 2 parts, hyaluronic acid 10 parts, glycerol 5 parts, squalane 3 parts, butanediol 0.2 part, Cortex Eucommiae extract 2 parts, Aloe extract 2 parts, mixed extract 4 parts, propylene glycol alginate 1 part, 0.5 part, essence, vitamin E 0.5 part, propolis 1 part, methyl hydroxybenzoate 0.5 part, propyl hydroxybenzoate 0.5 part and 30 parts, water.
preparation method:
S1: the Cortex Eucommiae of getting 2 parts by weight, pulverizes mixing after cleaning, drying, and add the water soaking 30 minutes of medical material gross weight 5 ~ 8 times amount, reflux, extract, 1 time, each 3h, filters and retain filtering residue, merging filtrate, obtaining Aqueous extracts; In filtering residue, add medical material gross weight 6 times amount volume fraction is the ethanol of 75%, reflux, extract, 1 time, each 4h, and filter, merging filtrate, obtains alcohol extract; Merge Aqueous extracts and alcohol extract, after stirring, leave standstill 12h, centrifugal 10 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 30 DEG C, and material liquid pH is 6, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.1MPa, when feed liquid stock solution reduces 1/10, then the ultrafiltration 2 times that adds water, merge ultrafiltrate, obtain Cortex Eucommiae extract;
S2: the Aloe of getting 2 parts by weight, cleans, and after drying, is squeezed obtain Aloe mixing juice with squeezer; The Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice; Put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 1 time of circulation, obtains Aloe extract;
S3: Semen Coicis and the 2 parts by weight Radix Asparagi of getting 2 parts by weight, coarse powder is ground into after mixing, be placed in supercritical carbon dioxide extraction apparatus, the volume fraction adding 10 parts by weight is the alcoholic solution of 70%, regulation and control carbon dioxide flow is 10L/h, and extracting pressure is 10MPa, and extraction temperature is 45 DEG C, extraction time is 3h, and decompression separation obtains mixed extract;
S4: described Cortex Eucommiae extract and described Aloe extract, mixed extract are mixed, obtains Chinese medicine extract;
S5: the preparation of oil phase: add squalane 3 parts, propylene glycol alginate 1 part, methyl hydroxybenzoate 0.5 part and propyl hydroxybenzoate 0.5 part and be heated with stirring to 70 DEG C in oil phase pot, be stirred to material and dissolve completely, obtain material A, stand-by;
S6: the preparation of aqueous phase: add 30 parts, water, glycerol 5 parts, hyaluronic acid 10 parts and butanediol 0.2 part in aqueous phase pot, be heated with stirring to 90 DEG C, be stirred to material and dissolve completely, maintains sterilizing in 20 minutes, is then cooled to 70 DEG C, obtains material B, stand-by;
S7: emulsifying: above-mentioned material A and material B are added in emulsifying pot according to the order of water after first oil, carries out high-speed stirred under the condition of 75 DEG C, treat material A and material B mix homogeneously, obtain material C;
S8: cooling: material C above-mentioned steps obtained is cooled to 50 DEG C, adds dodecyl alanine 2 parts, sodium cocoyl glycinate 3 parts and sodium lauroyl glutamate 2 parts, stirs;
S9: when system being cooled to 45 DEG C, adds above-mentioned Chinese medicine extract, 0.5 part, essence, vitamin E 0.5 part and propolis 1 part, is stirred to evenly; Be cooled to 35 DEG C, discharging;
S10: homogenizing process: make material particular diameter between 100 through the process of extra-high-pressure nano homogenizer homogenizing after discharging, through carrying out fill after the assay was approved, obtains whitening skin and preserving moisture facial milk cleanser of the present invention.
embodiment 2, whitening skin and preserving moisture facial milk cleanser of the present invention and preparation thereof
formula:be prepared from by the raw material of following parts by weight: dodecyl alanine 5 parts, sodium cocoyl glycinate 9 parts, sodium lauroyl glutamate 5 parts, hyaluronic acid 15 parts, glycerol 10 parts, squalane 8 parts, butanediol 1 part, Cortex Eucommiae extract 5 parts, Aloe extract 5 parts, mixed extract 10 parts, propylene glycol alginate 2 parts, 1 part, essence, vitamin e1 part, propolis 3 parts, methyl hydroxybenzoate 1 part, propyl hydroxybenzoate 1 part and 40 parts, water.
preparation method:
S1: the Cortex Eucommiae of getting 5 parts by weight, pulverizes mixing after cleaning, drying, and add the water soaking 45 minutes of medical material gross weight 8 times amount, reflux, extract, 2 times, each 5h, filters and retain filtering residue, merging filtrate, obtaining Aqueous extracts; In filtering residue, add medical material gross weight 8 times amount volume fraction is the ethanol of 85%, reflux, extract, 1 time, each 5h, and filter, merging filtrate, obtains alcohol extract; Merge Aqueous extracts and alcohol extract, after stirring, leave standstill 12h, centrifugal 20 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 45 DEG C, and material liquid pH is 8, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.2MPa, when feed liquid stock solution reduces 1/4, then the ultrafiltration 2 times that adds water, merge ultrafiltrate, obtain Cortex Eucommiae extract;
S2: the Aloe of getting 5 parts by weight, cleans, and after drying, is squeezed obtain Aloe mixing juice with squeezer; The Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice; Put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 2 times of circulation, obtains Aloe extract;
S3: Semen Coicis and the 5 parts by weight Radix Asparagi of getting 5 parts by weight, coarse powder is ground into after mixing, be placed in supercritical carbon dioxide extraction apparatus, the volume fraction adding 15 parts by weight is the alcoholic solution of 75%, regulation and control carbon dioxide flow is 15L/h, and extracting pressure is 15MPa, and extraction temperature is 50 DEG C, extraction time is 4h, and decompression separation obtains mixed extract;
S4: described Cortex Eucommiae extract and described Aloe extract, described mixed extract are mixed, obtains Chinese medicine extract;
S5: the preparation of oil phase: add squalane 8 parts, propylene glycol alginate 2 parts, methyl hydroxybenzoate 1 part and propyl hydroxybenzoate 1 part in oil phase pot, be heated with stirring to 75 DEG C, be stirred to material and dissolve completely, obtain material A, stand-by;
S6: the preparation of aqueous phase: add 40 parts, water, glycerol 10 parts, hyaluronic acid 15 parts and butanediol 1 part in aqueous phase pot, be heated with stirring to 100 DEG C, be stirred to material and dissolve completely, maintains sterilizing in 20 minutes, is then cooled to 80 DEG C, obtains material B, stand-by;
S7: emulsifying: above-mentioned material A and material B are added in emulsifying pot according to the order of water after first oil, carries out high-speed stirred under the condition of 85 DEG C, treat material A and material B mix homogeneously, obtain material C;
S8: cooling: material C above-mentioned steps obtained is cooled to 60 DEG C, adds dodecyl alanine 5 parts, sodium cocoyl glycinate 9 parts and sodium lauroyl glutamate 5 parts, stirs;
S9: when system being cooled to 45 DEG C, adds above-mentioned Chinese medicine extract, 1 part, essence, vitamin e1 part and propolis 3 parts, is stirred to evenly; Be cooled to 40 DEG C, discharging;
S10: homogenizing process: make material particular diameter between 200nm through the process of extra-high-pressure nano homogenizer homogenizing after discharging, through carrying out fill after the assay was approved, obtains whitening skin and preserving moisture facial milk cleanser of the present invention.
embodiment 3, whitening skin and preserving moisture facial milk cleanser of the present invention and preparation thereof
formula:be prepared from by the raw material of following parts by weight: dodecyl alanine 3 parts, sodium cocoyl glycinate 6 parts, sodium lauroyl glutamate 3 parts, hyaluronic acid 12 parts, glycerol 8 parts, squalane 6 parts, butanediol 0.5 part, Cortex Eucommiae extract 3 parts, Aloe extract 3 parts, mixed extract 6 parts, propylene glycol alginate 1 part, 0.5 part, essence, vitamin E 0.5 part, propolis 2 parts, methyl hydroxybenzoate 0.5 part, propyl hydroxybenzoate 0.5 part and 35 parts, water.
Preparation method:
S1: the Cortex Eucommiae of getting 3 parts by weight, pulverizes mixing after cleaning, drying, and add the water soaking 45 minutes of medical material gross weight 7 times amount, reflux, extract, 2 times, each 6h, filters and retain filtering residue, merging filtrate, obtaining Aqueous extracts; In filtering residue, add medical material gross weight 7 times amount volume fraction is the ethanol of 85%, reflux, extract, 1 time, each 6h, and filter, merging filtrate, obtains alcohol extract; Merge Aqueous extracts and alcohol extract, after stirring, leave standstill 24h, centrifugal 10 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 40 DEG C, and material liquid pH is 7, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.15MPa, when feed liquid stock solution reduces 1/6, then the ultrafiltration 2 times that adds water, merge ultrafiltrate, obtain Cortex Eucommiae extract;
S2: the Aloe of getting 3 parts by weight, cleans, and after drying, is squeezed obtain Aloe mixing juice with squeezer; The Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice; Put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 2 times of circulation, obtains Aloe extract;
S3: Semen Coicis and the 3 parts by weight Radix Asparagi of getting 3 parts by weight, coarse powder is ground into after mixing, be placed in supercritical carbon dioxide extraction apparatus, the volume fraction adding 15 parts by weight is the alcoholic solution of 80%, regulation and control carbon dioxide flow is 12L/h, and extracting pressure is 12MPa, and extraction temperature is 50 DEG C, extraction time is 4h, and decompression separation obtains mixed extract;
S4: described Cortex Eucommiae extract and described Aloe extract, described mixed extract are mixed, obtains Chinese medicine extract;
S5: the preparation of oil phase: add squalane 6 parts, propylene glycol alginate 1 part, methyl hydroxybenzoate 0.5 part and propyl hydroxybenzoate 0.5 part in oil phase pot, be heated with stirring to 70 DEG C, be stirred to material and dissolve completely, obtain material A, stand-by;
S6: the preparation of aqueous phase: add 35 parts, water, glycerol 8 parts, hyaluronic acid 12 parts and butanediol 0.5 part in aqueous phase pot, be heated with stirring to 95 DEG C, be stirred to material and dissolve completely, maintains sterilizing in 20 minutes, is then cooled to 75 DEG C, obtains material B, stand-by;
S7: emulsifying: above-mentioned material A and material B are added in emulsifying pot according to the order of water after first oil, carries out high-speed stirred under the condition of 80 DEG C, treat material A and material B mix homogeneously, obtain material C;
S8: cooling: material C above-mentioned steps obtained is cooled to 50 ~ 60 DEG C, adds dodecyl alanine 3 parts, sodium cocoyl glycinate 6 parts and sodium lauroyl glutamate 3 parts, stirs;
S9: when system being cooled to 45 DEG C, adds above-mentioned Chinese medicine extract, 0.5 part, essence, vitamin E 0.5 part and propolis 2 parts, is stirred to evenly; Be cooled to 40 DEG C, discharging;
S10: homogenizing process: make material particular diameter between 150nm through the process of extra-high-pressure nano homogenizer homogenizing after discharging, through carrying out fill after the assay was approved, obtains whitening skin and preserving moisture facial milk cleanser of the present invention.
Do testing performance index to the whitening skin and preserving moisture facial milk cleanser of embodiment 1 ~ 3, its test result is as follows:
1, outward appearance: white mastic; 2, pH value: 5.5 ~ 7.0; 3, viscosity: 5 ~ 100,000; 4, heat-resistant stability investigates (45 DEG C × 24h): qualified; 5, cold-resistant study on the stability (-15 DEG C × 24h): qualified.
comparative example 1
formula:be prepared from by the raw material of following parts by weight: dodecyl alanine 2 parts, sodium cocoyl glycinate 3 parts, sodium lauroyl glutamate 2 parts, hyaluronic acid 10 parts, glycerol 5 parts, squalane 3 parts, butanediol 0.2 part, Cortex Eucommiae extract 2 parts, Aloe extract 2 parts, propylene glycol alginate 1 part, 0.5 part, essence, vitamin E 0.5 part, propolis 1 part, methyl hydroxybenzoate 0.5 part, propyl hydroxybenzoate 0.5 part, 30 parts, water.
Preparation method is with reference to embodiment 1.
comparative example 2
formula:be prepared from by the raw material of following parts by weight: sodium cocoyl glycinate 3 parts, sodium lauroyl glutamate 2 parts, hyaluronic acid 10 parts, glycerol 5 parts, squalane 3 parts, butanediol 0.2 part, Cortex Eucommiae extract 2 parts, Aloe extract 2 parts, mixed extract 4 parts, propylene glycol alginate 1 part, 0.5 part, essence, vitamin E 0.5 part, propolis 1 part, methyl hydroxybenzoate 0.5 part, propyl hydroxybenzoate 0.5 part and 30 parts, water.
Preparation method is with reference to embodiment 1.
test example one, Product Safety evaluation (experiment of human body skin patch)
One, trial target: the whitening skin and preserving moisture facial milk cleanser that embodiment 1 ~ 3, comparative example 1 ~ 2 prepare.
Tested crowd's number: 100 people, women.
Age: between 22 ~ 50 years old.
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: 5 groups, often organize 20 people, 27 ± 2 years old mean age.
Two, patch method: select qualified speckle examination device, with closed patch experiment method, tested material being about 0.015g ~ 0.03g drips in speckle examination device, external special adhesive tape is covered on experimenter back, tested material is removed after 24 hours, within after removing respectively 1,6,12,24,48 hour, observe dermoreaction, according to its result of dermoreaction grade scale record in " cosmetics health specification ".
Three, experimental result: human skin patch result shows: each group experimenter is by the patch test of the whitening skin and preserving moisture facial milk cleanser of embodiment 1 ~ 3, comparative example 1 ~ 2, dermoreaction is observed at 1,6,12,24,48 hour, wherein there is skin adverse reaction in 0 example, the whitening skin and preserving moisture facial milk cleanser use safety described in explanation.
test example two, product effect assessment
part I: the moisturizing effect of whitening skin and preserving moisture facial milk cleanser of the present invention.
One, trial target: the whitening skin and preserving moisture facial milk cleanser that embodiment 1 ~ 3, comparative example 1 ~ 2 prepare.
Two, tested crowd:
Sex number: female, 100 people.
Age: between 22 ~ 45 years old.
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: be divided into 5 groups, often organize 20 people.
Three, method of testing: experimenter uses Fes Kai Er SK-I skin moisture detector to test the moisture of forehead, left face, right face and chin skin respectively after using clean water face, and get arithmetic mean of instantaneous value, experimenter re-uses the moistening face of warm water, then the clean face of above-mentioned whitening skin and preserving moisture facial milk cleanser is used, by clean water, again by the skin moisture content of skin moisture tester test forehead, left face, right face and the same position of chin, and get arithmetic mean of instantaneous value.Often organize 20 experimenters and tested result is got arithmetic mean of instantaneous value.
Four, test result is as following table 1:
Table 1 skin moisture content table with test results
| Project | Skin average moisture before use whitening skin and preserving moisture facial milk cleanser | Skin average moisture after use whitening skin and preserving moisture facial milk cleanser | Skin moisture content gradient |
| Embodiment 1 | 21.25% | 26.29% | +5.24% |
| Embodiment 2 | 22.54% | 26.81% | +4.37% |
| Embodiment 3 | 20.72% | 25.23% | +4.64% |
| Comparative example 1 | 21.69% | 21.44% | -0.46% |
| Comparative example 2 | 21.45% | 21.64% | +0.24% |
From upper table 1, after using clean of the embodiment of the present invention 1 ~ 3 whitening skin and preserving moisture facial milk cleanser, moisture of skin can not only be kept not run off, the sebum film that face skin is natural can not be destroyed, also can replenishing water and preserving moisture in time, skin beauty water is moistened, wherein best with the moistening effect of embodiment 1 whitening skin and preserving moisture facial milk cleanser.Comparative example 1 all lacks some component with comparative example 2 compared with embodiment 1, and its moisturizing effect, not as good as embodiment 1 ~ 3, illustrates that plant extract of the present invention is worked in coordination with.
part II: the whitening effect of whitening skin and preserving moisture facial milk cleanser of the present invention
One, trial target: the whitening skin and preserving moisture facial milk cleanser that embodiment 1,2,3 prepares.
Two, test philosophy and standard: whitening skin and preserving moisture facial milk cleanser of the present invention is active by restraint of tyrosinase or blocks and generate melanic oxidation reaction from tyrosine, reduce melanic generation thus reach the effect of skin whitening, detect its whitening effect by measuring the suppression ratio of whitening skin and preserving moisture facial milk cleanser of the present invention to tryrosinase, the higher whitening effect of suppression ratio is better.
Three, method of testing:
Matched group: commercial whitening agent arbutin;
Test group 1: the whitening skin and preserving moisture facial milk cleanser that the embodiment of the present invention 1 is obtained;
Test group 2: the whitening skin and preserving moisture facial milk cleanser that the embodiment of the present invention 2 is obtained;
Test group 3: the whitening skin and preserving moisture facial milk cleanser that the embodiment of the present invention 3 is obtained.
1) preparation of matched group solution to be measured: get commercial whitening agent arbutin 0.5g in 10ml beaker, add a small amount of distilled water, be stirred to arbutin and fully dissolve, continues to add distilled water to 5ml.
2) preparation of test group solution to be measured: get the present embodiment 1,2,3 whitening skin and preserving moisture facial milk cleanser 0.5g respectively in 3 10ml beakers, respectively add a small amount of distilled water, be stirred to facial milk cleanser and fully dissolve, continues to add distilled water to 5ml.
3) preparation of base soln: the 0.2mol/lPBS(phosphate buffer preparing 100u/ml tyrosinase solution, 2.0mmol/lL-tyrosine solution and pH=6.8 respectively) solution based on solution.
4) get 4 test tube accordings to the form below and quantitatively add each base soln and test group solution to be measured, shake up;
| Test tube number | 1 | 2 | 3 | 4 |
| L-tyrosine solution (ml) | 0.50 | 0 | 0.50 | 0 |
| Test group solution to be measured (ml) | 0 | 0 | 0.50 | 0.5 |
| PBS solution (ml) | 2.00 | 2.50 | 2.00 | 2.50 |
| Tyrosinase solution (ml) | 0.50 | 0.50 | 0.50 | 0.50 |
| Absorbance | A 1 | A 2 | A 3 | A 4 |
5) 1,2,3, No. 4 test tube is placed in the heating of 310K water-bath after 60 minutes, adopts visible spectrophotometric instrument to measure its absorbance under wavelength 475nm respectively, according to following computing formula:
Tyrosinase inhibition rate (%)=[1-(A3-A4)/(A1-A2)] × 100%
Calculate the solution to be measured of this concentration to the suppression ratio of tryrosinase;
6) step 4) and 5 is repeated), measure matched group solution to be measured to the suppression ratio of tryrosinase.
Four, test result is as table 2
Table 2 whitening skin and preserving moisture facial milk cleanser whitening effect table with test results
| Group | Test group 1 | Test group 2 | Test group 3 | Matched group |
| Tyrosinase inhibition rate (%) | 77.2 | 69.3 | 67.2 | 65 |
TYR (analytical pure), purchased from Solarbio company; Tryrosinase (analytical pure), available from Sigma; Sodium hydrogen phosphate (analytical pure), purchased from Chemical Reagent Co., Ltd., Sinopharm Group; Sodium dihydrogen phosphate (analytical pure), purchased from Chemical Reagent Co., Ltd., Sinopharm Group.
As seen from the above table: the embodiment of the present invention 1,2,3 is under visible spectrophotometric instrument wavelength 475nm, record absorbance as calculated the suppression ratio of whitening skin and preserving moisture facial milk cleanser to tryrosinase of the embodiment of the present invention 1,2,3 is respectively 77.2%, 69.3%, 67.2%, wherein best with the whitening effect of embodiment 1 whitening skin and preserving moisture facial milk cleanser, and the suppression ratio of commercial arbutin to tryrosinase is only 65.0%, visible whitening skin and preserving moisture facial milk cleanser of the present invention has more significant whitening effect compared with commercial arbutin.
part III: the result of use of whitening skin and preserving moisture facial milk cleanser of the present invention
One, trial target: embodiment 1 ~ 3, whitening skin and preserving moisture facial milk cleanser prepared by comparative example 1 ~ 2.
Two, tested crowd:
Sex number: female, 100 people.
Age: between 22 ~ 50 years old.
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: be divided into 5 groups, often organize 20 people.
Three, method of testing: use the clean face of example 1 ~ 3, whitening skin and preserving moisture facial milk cleanser prepared by comparative example 1 ~ 2 respectively, observe and experience result of use.Using method: experimenter directly uses tested products, every day is sooner or later each to be used once, face is drenched with warm water, extrude appropriate facial milk cleanser in the centre of the palm before using, and adds a small amount of clear water and has rubbed and enrich foam, rinse well in a moment at face message with clear water.Adhere to use one month, at least check weekly once to understand with or without whole body and local untoward reaction, and itemized record result.
Four, testing evaluation result is as follows:
(one month) on probation feedback conclusive table of table 3 embodiment 1 whitening skin and preserving moisture facial milk cleanser
(one month) on probation feedback conclusive table of table 4 embodiment 2 whitening skin and preserving moisture facial milk cleanser
(one month) on probation feedback conclusive table of table 5 embodiment 3 whitening skin and preserving moisture facial milk cleanser
(one month) on probation feedback conclusive table of table 6 comparative example 1 facial milk cleanser
(one month) on probation feedback conclusive table of table 7 comparative example 2 facial milk cleanser
(1) from upper table 2 ~ 5, the whitening skin and preserving moisture facial milk cleanser of embodiment 1 ~ 3 almost obtains the accreditation of all experimenters, illustrate that whitening skin and preserving moisture facial milk cleanser gentleness of the present invention does not stimulate, bubble abundant, easy flushing, the excess oil of effectively clean skin surface and pore depths and dust dirt, use the salubrious non-greasy of rear face, without tight sense, skin moisture can be kept, timely moisturizing and simultaneously whitening composition is effectively sent to skin deep layer, repair impaired or innutritive cell, reduce color element, desalination mottle, skin is made to reach the effect of whitening, skin keeps water profit smooth, flexible.In embodiment 1 ~ 3, the degree of recognition of embodiment 1 is the highest, and therefore embodiment 1 is most preferred embodiment.
(2) from upper table 6 ~ 7, the result of use of comparative example 1 and comparative example 2 facial milk cleanser, all not as embodiment 1 ~ 3, illustrates that whitening skin and preserving moisture facial milk cleanser formula of the present invention is not obtained by the simple combination of each component.
There is not people to occur allergic phenomena in whole experimenter simultaneously, all do not occur the situations such as skin pruritus, twinge, redness yet.Therefore, the gentle safety of whitening skin and preserving moisture facial milk cleanser of the present invention, can life-time service.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.
Claims (10)
1. a whitening skin and preserving moisture facial milk cleanser, it is characterized in that, comprise the raw materials of following parts by weight: 5 ~ 25 parts, surfactant, wetting agent 15 ~ 35 parts, Chinese medicine extract 5 ~ 25 parts, thickening agent 0.5 ~ 1.5 part, 30 ~ 40 parts, water, vitamin E 0.05 ~ 0.25 part and propolis 1 ~ 3 part, described Chinese medicine extract comprises Cortex Eucommiae extract, Aloe extract and mixed extract, and the raw materials of described mixed extract is made up of according to the weight ratio of 2 ~ 5:2 ~ 5 Semen Coicis and Radix Asparagi.
2. whitening skin and preserving moisture facial milk cleanser as claimed in claim 1, it is characterized in that, described Chinese medicine extract is made up of according to the weight ratio of 2 ~ 5:2 ~ 5:4 ~ 10 Cortex Eucommiae extract, Aloe extract, mixture extract.
3. whitening skin and preserving moisture facial milk cleanser as claimed in claim 1, it is characterized in that, described surfactant is made up of dodecyl alanine, sodium cocoyl glycinate and the sodium lauroyl glutamate weight ratio by 1:2:1, described wetting agent comprises hyaluronic acid, glycerol, squalane and butanediol, and described thickening agent is selected from propylene glycol alginate.
4. whitening skin and preserving moisture facial milk cleanser as claimed in claim 1, it is characterized in that, described whitening skin and preserving moisture facial milk cleanser also comprises antiseptic 0.1 ~ 1 part, and described antiseptic is made up of by the weight ratio of 1:1 methyl hydroxybenzoate and propyl hydroxybenzoate.
5. whitening skin and preserving moisture facial milk cleanser as claimed in claim 1, it is characterized in that, comprise the raw materials of following parts by weight: 10 parts, surfactant, wetting agent 20 parts, Cortex Eucommiae extract 3 parts, Aloe extract 3 parts, mixed extract 6 parts, thickening agent 1 part, vitamin E 0.1 part, propolis 2 parts and 35 parts, water.
6. whitening skin and preserving moisture facial milk cleanser as claimed in claim 1, it is characterized in that, described Aloe extract is obtained by following steps:
S1: get Aloe, cleans, and after drying, is squeezed obtain Aloe mixing juice with squeezer;
S2: the Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice;
S3: put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 1 ~ 3 time of circulation, obtains Aloe extract.
7. whitening skin and preserving moisture facial milk cleanser as claimed in claim 1, it is characterized in that, described Cortex Eucommiae extract is obtained by following steps:
S1: get the Cortex Eucommiae, pulverizes mixing after cleaning, drying, and add the water soaking 30 ~ 60 minutes of medical material gross weight 5 ~ 8 times amount, reflux, extract, 1 ~ 2 time, each 3 ~ 6h, filters and retain filtering residue, merging filtrate, obtaining Aqueous extracts;
S2: adding medical material gross weight 5 ~ 8 times amount volume fraction in filtering residue is the ethanol of 65 ~ 90%, reflux, extract, 1 ~ 2 time, each 3 ~ 6h, filter, merging filtrate, obtains alcohol extract;
S3: merge Aqueous extracts and alcohol extract, after stirring, leaves standstill 12 ~ 24h, centrifugal 10 ~ 25 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 30 ~ 45 DEG C, and material liquid pH is 6 ~ 8, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.1 ~ 0.2MPa, when feed liquid stock solution reduces 1/10 ~ 1/4, then the ultrafiltration 2 ~ 3 times that adds water, merge ultrafiltrate, obtain Cortex Eucommiae extract.
8. whitening skin and preserving moisture facial milk cleanser as claimed in claim 1, it is characterized in that, described mixed extract is obtained by following steps:
Get Semen Coicis and 2 ~ 5 parts by weight Radix Asparagi of 2 ~ 5 parts by weight, coarse powder is ground into after mixing, be placed in supercritical carbon dioxide extraction apparatus, the volume fraction adding 10 ~ 25 parts by weight is the alcoholic solution of 70 ~ 85%, regulation and control carbon dioxide flow is 10 ~ 15L/h, and extracting pressure is 10 ~ 15MPa, and extraction temperature is 45 ~ 60 DEG C, extraction time is 3 ~ 5h, and decompression separation obtains described mixed extract.
9. the preparation method of whitening skin and preserving moisture facial milk cleanser as claimed in claim 1, is characterized in that, comprise the following steps:
S1: the preparation of oil phase: add thickening agent 0.5 ~ 1.5 part in oil phase pot, be heated with stirring to 70 ~ 75 DEG C, be stirred to material and dissolve completely, obtain material A, stand-by;
S2: the preparation of aqueous phase: add wetting agent 15 ~ 35 parts, 30 ~ 40 parts, water in aqueous phase pot, be heated with stirring to 90 ~ 100 DEG C, be stirred to material and dissolve completely, maintains sterilizing in 20 minutes, is then cooled to 70 ~ 80 DEG C, obtains material B, stand-by;
S3: emulsifying: above-mentioned material A and material B are added in emulsifying pot according to the order of water after first oil, carries out high-speed stirred under the condition of 75 ~ 85 DEG C, treat material A and material B mix homogeneously, obtain material C;
S4: cooling: material C above-mentioned steps obtained is cooled to 50 ~ 60 DEG C, adds 5 ~ 25 parts, surfactant, stirs;
S5: when system being cooled to 45 DEG C, adds Chinese medicine extract, 0 ~ 1 part, essence, vitamin E 0 ~ 1 part and propolis 1 ~ 3 part, is stirred to evenly; Be cooled to 35 ~ 40 DEG C, discharging;
S6: homogenizing process: make material particular diameter between 100 ~ 200nm through the process of extra-high-pressure nano homogenizer homogenizing after discharging, through carrying out fill after the assay was approved, obtains whitening skin and preserving moisture facial milk cleanser of the present invention.
10. the preparation method of whitening skin and preserving moisture facial milk cleanser as claimed in claim 9, it is characterized in that, described Chinese medicine extract is obtained by following steps:
S1: get the Cortex Eucommiae, pulverizes mixing after cleaning, drying, and add the water soaking 30 ~ 60 minutes of medical material gross weight 5 ~ 8 times amount, reflux, extract, 1 ~ 2 time, each 3 ~ 6h, filters and retain filtering residue, merging filtrate, obtaining Aqueous extracts; In filtering residue, add medical material gross weight 5 ~ 8 times amount volume fraction is the ethanol of 65 ~ 90%, reflux, extract, 1 ~ 2 time, each 3 ~ 6h, and filter, merging filtrate, obtains alcohol extract; Merge Aqueous extracts and alcohol extract, after stirring, leave standstill 12 ~ 24h, centrifugal 10 ~ 25 minutes of 2000g, gets supernatant, carries out hyperfiltration treatment, temperature is 30 ~ 45 DEG C, and material liquid pH is 6 ~ 8, and inlet pressure is 0.3MPa, the low 0.35kPa of liquid outlet pressure ratio inlet pressure, the pressure wave moment of periodic pressure fluctuation is 0.1 ~ 0.2MPa, when feed liquid stock solution reduces 1/10 ~ 1/4, then the ultrafiltration 2 ~ 3 times that adds water, merge ultrafiltrate, obtain Cortex Eucommiae extract;
S2: Semen Coicis and 2 ~ 5 parts by weight Radix Asparagi of getting 2 ~ 5 parts by weight, coarse powder is ground into after mixing, be placed in supercritical carbon dioxide extraction apparatus, the volume fraction adding 10 ~ 25 parts by weight is the alcoholic solution of 70 ~ 85%, regulation and control carbon dioxide flow is 10 ~ 15L/h, and extracting pressure is 10 ~ 15MPa, and extraction temperature is 45 ~ 60 DEG C, extraction time is 3 ~ 5h, and decompression separation obtains described mixed extract;
S3: get Aloe, cleans, and after drying, is squeezed obtain Aloe mixing juice with squeezer; The Aloe obtained mixing juice is put in filtering tank, removes impurity, obtain Aloe original juice; Put in vacuum-concentrcted device by Aloe original juice liquid and concentrate, concentrated 1 ~ 3 time of circulation, obtains Aloe extract;
S4: Cortex Eucommiae extract, mixed extract and Aloe extract are merged and obtains described Chinese medicine extract.
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Application publication date: 20160127 |